LA400 User`s Manual - Advanced Thermoelectric
Contents
1. Install ElectraCOOL LA400 Chiller on a relatively leveled surface capable of supporting the 26 Lbs 11 7Kg weight of the Unit Allow for 12 clearance around the air inlet and outlet areas to insure proper air circulation and ventilation If obstacles are blocking airflow the Unit may overheat This reduces performance and may lead to early module failure Fill Reservoir 2 3 full with fluid Plug the chiller into a grounded electrical outlet Connect the chiller to the System which you intend to cool control Turn the Unit Power Switch ON Purge air from the System as described in Section 6 of this manual and add fluid if necessary 6 Set Digital Controller to the Temperature desired as instructed in Section 7 7 Run the Unit check for possible leaks 8 Unit is ready for continuous operation UE B oda Note 1 When operating the unit with outlet fluid temperature above 35 F 2 C 100 pure distilled water is recommended Note 2 If operating the unit with outlet fluid temperature below 35 F 2 C a solution of 75 distilled water and 25 glycol alcohol or other appropriate brand of antifreeze is recommended 6 PURGI NG THE FLUID SYSTEM Connect system tubing to the Chiller quick connect input and output valves Fill reservoir 2 3 full with appropriate coolant solution Plug unit to electrical outlet with appropriate voltage Turn power switch ON for 2 3 seconds and then turn OFF Repeat two to four times Che2. Packages should be opened promptly and units inspected for concealed damage An immediate claim must be filed with the freight carrier and an inspection requested Retain all packing materials Advanced Thermoelectric cannot be responsible for Consignee s failure to file a timely freight claim If possible save the box and shipping materials your chiller arrives in should service be required in the future ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL 3 PRODUCT HANDLING DO NOT OPERATE YOUR CHILLER BEFORE READING THIS MANUAL Read MSDS for the coolant used in your system and follow all safety precautions listed in the MSDS prior to connecting the LA400 with coolant tubing or opening the fill cap as this could result in contact with the coolant inside Before operating your new Chiller be certain that Unit is placed in the proper upright vertical position Liquid reservoir and line to object cooled is are filled with coolant The chiller should have at least 12 free air space for air intake and exhaust Make sure that proper input voltage is supplied to the unit In general US line voltage is 115 VAC and Europe is 230 VAC but check with your facilities manger DUN WARNI NG Electrical Shock Hazard PLUG UNIT I NTO GROUNDED ELECTRI CAL OUTLET ONLY DO NOT OPERATE UNIT WITHOUT COOLA
3. ignition sources and incompatibles 11 Toxicological Information Toxicological Data Ethyl alcohol oral rat LD50 7060 mg kg inhalation rat LC50 20 000 ppm 10H Irritation data eye rabbit 500 mg 24H moderate Investigated as a tumorigen mutagen reproductive effector Methyl alcohol oral rat LD50 5628 mg kg inhalation rat LC50 64000 ppm 4H skin rabbit LD50 15800 mg kg Irritation data skin rabbit 20 mg 24H Moderate Investigated as a tumorigen mutagen reproductive effector Isopropyl alcohol oral rat LD50 5045 mg kg skin rabbit LD50 12 8 gm kg inhalation rat 16 000 ppm 8 hr Investigated as a mutagen tumorigen reproductive effector Reproductive Toxicity Ethanol has been linked to birth defects in humans Carcinogenicity Ethanol has been linked to cancer in humans Chronic ethanol ingestion is associated with liver cancer Most industrial ethanol contains denaturants that render it undesirable to drink NTP Carcinogen Ingredient Known Anticipated IARC Category Ethyl Alcohol 64 17 5 No No None Methyl Alcohol 67 56 1 No No None Isopropyl Alcohol 67 63 0 No No 3 12 Ecological Information Environmental Fate Following data for ethanol When released into the soil this material is expected to readily biodegrade When released into the soil this material is expected to leach into groundwater When released into the soil this material is expected to quickly evaporate When released into water this materi
4. Date 05 07 03 Supercedes 01 14 02 24 Hour Emergency Telephone 908 659 2151 CHEMTREC 1 800 424 9300 MSDS Material Safety Data Sheet CANTEccenaneetee Outside U S and Canada Chemtrec 703 527 3887 VI Mallinckrodt i um lt a NOTE CHEMTREC CANUTEC and Nationa CHEMICALS JT Baker Response Cemer emergency numbers to be used only n the event of chemical emergencies involving a spill leak fre exposure of accident involving chemicals From Mallinckrodt Baker Inc 222 Red School Lane Phillipsburg NJ 08865 All non emergency questions should be directed to Customer Service 1 800 582 2537 for assistance REAGENT ALCOHOL 1 Product Identification Synonyms Doubly denatured ethanol modified 3A alcohol alcohol anhydrous CAS No Not applicable to mixtures Molecular Weight Not applicable to mixtures Chemical Formula Mixture CH3CH20OH CH30H CH3CHOHCH3 Product Codes J T Baker 2986 9229 9400 9401 9404 A478 Mallinckrodt 5911 6183 7006 7019 2 Composition Information on Ingredients Ingredient CAS No Percent Hazardous Ethyl Alcohol 64 17 5 90 95 Yes Methyl Alcohol 67 56 1 1 5 Yes Isopropyl Alcohol 67 63 0 1 5 Yes 3 Hazards Identification Emergency Overview POISON DANGER MAY BE FATAL IF SWALLOWED HARMFUL IF INHALED OR ABSORBED THROUGH SKIN VAPOR HARMFUL FLAMMABLE AFFECTS CENTRAL NERVOUS SYSTEM MAY CAUSE BLINDNESS CANNOT BE MADE NONPOISONOUS CAU
5. anything by mouth to an unconscious person Get medical attention Skin Contact Remove any contaminated clothing Wash skin with soap and water for at least 15 minutes Get medical attention if irritation develops or persists Eye Contact Immediately flush eyes with plenty of water for at least 15 minutes lifting lower and upper eyelids occasionally Get medical attention immediately Note to Physician Give sodium bicarbonate intravenously to treat acidosis Urinalysis may show low specific gravity proteinuria pyuria cylindruria hematuria calcium oxide and hippuric acid crystals Ethanol can be used in antidotal treatment but monitor blood glucose when administering ethanol because it can cause hypoglycemia Consider infusion of a diuretic such as mannitol to help prevent or control brain edema and hemodialysis to remove ethylene glycol from circulation 5 Fire Fighting Measures Fire Flash point 111C 232F CC Autoignition temperature 398C 748F Flammable limits in air by volume lel 3 2 uel 15 3 Slight to moderate fire hazard when exposed to heat or flame Explosion ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 10 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL Above flash point vapor air mixtures are explosive within flammable limits noted above Containers may explode when involved in a fire Fire Extinguishing Medi
6. from 150 to 800 watts sufficient to meet a variety of cooling requirements Each is designed to work in close loop systems which separate the coolant within the loop from ambient influences so that the object or item s that are cooled heated or stabilized quite precisely are done so by a clean pure liquid coolant All ElectraCOOL brand chillers are compact and quiet This Operations and Maintenance Manual OMM provides the necessary information for the proper installation operation and maintenance of your new ElectraCOOL LA400 chiller We also make recommendations on how to operate your chiller most efficiently Failure to comply with any part of this Manual could result in voiding the warranty see section 9 Symbols Used on the ElectraCOOL L A 400 Attention See accompanying Documents A WARNING Electrical Shock Hazard t Type B Applied Part Protection by Ground 2 INCOMING INSPECTION Our chillers are designed built and packaged to withstand the shock and vibration normally associated with shipment by common carrier Occasionally improper handling during shipment causes damage to the contents This can include anything from excessive vibration crushing puncturing the box etc so a thorough inspection should be conducted upon receipt of every shipment Any packaging tears dents scratches and loose articles are signs of damage and should be noted on carrier s shipping documents accompanying the shipment
7. involving a spill leak fre exposure or acoxent involving chemicals All non emergency questions should be directed to Customer Service 1 800 582 2537 for assistance ETHYLENE GLYCOL 1 Product Identification Synonyms 1 2 Ethanediol glycol 1 2 Dihydroxyethane Ethylene Alcohol Ethulene Dihydrate CAS No 107 21 1 Molecular Weight 62 07 Chemical Formula CH2OHCH20H Product Codes J T Baker 5387 5845 9140 9298 9300 9346 9356 L715 Mallinckrodt 5001 5037 2 Composition Information on Ingredients Ingredient CAS No Percent Hazardous Ethylene Glycol 107 21 1 99 100 Yes 3 Hazards Identification Emergency Overview WARNING HARMFUL OR FATAL IF SWALLOWED HARMFUL IF INHALED OR ABSORBED THROUGH SKIN MAY CAUSE ALLERGIC SKIN REACTION MAY CAUSE IRRITATION TO SKIN EYES AND RESPIRATORY TRACT AFFECTS CENTRAL NERVOUS SYSTEM SAF T DATA Ratings Provided here for your convenience Health Rating 2 Moderate Life Flammability Rating 1 Slight Reactivity Rating 1 Slight Contact Rating 3 Severe Life Lab Protective Equip GOGGLES amp SHIELD LAB COAT amp APRON VENT HOOD PROPER GLOVES ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL Storage Color Code Green General Storage Inhalation Vapor
8. or advise customers to change any operational mode or to access the controllers Programming Mode We are happy to make any modifications for you prior to shipment C Programming Mode Warning All programmable parameters are Factory set with respect to safe and efficient Chiller operation Any changes to Factory settings are done so at the Customer s risk and may void the warrantee To reprogram Controller follow the Controller Manual included with every chiller Note Default Temperatures see rou in the User s Manual Parameter Table are factory set in degrees Centigrade C If it is desired to have temperature units in F please inform factory when entering the order 8 SERVICE GUIDE No special maintenance is required for day to day use of ElectraCOOL brand Thermoelectric Recirculating Liquid Chillers Your chiller utilizes a state of the art efficient seal less centrifugal magnetic drive pump with 45 000 hours MTBF and a brushless DC motor If your pump fails contact us to arrange replacement The thermoelectric assembly uses high quality fans with 75 000 hours MTBF If you have a fan failure contact us to arrange replacement Attempting to repair or replace these parts will void the warrantee For the most efficient performance and to maximize the life of the chiller and components within it is recommended to clean heat sinks periodically using compressed air If unit doesn t perform properly use the follo
9. storage is preferred Separate from incompatibles Containers should be bonded and grounded for transfers to avoid static sparks Storage and use areas should be No Smoking areas Use non sparking type tools and equipment including explosion proof ventilation Containers of this material may be hazardous when empty since they retain product residues vapors liquid observe all warnings and precautions listed for the product 8 Exposure Controls Personal Protection Airborne Exposure Limits OSHA Permissible Exposure Limit PEL 1000 ppm TWA for ethyl alcohol 400 ppm TWA for isopropyl alcohol 200 ppm TWA for methyl alcohol ACGIH Threshold Limit Value TLV 1000 ppm TWA A4 not classifiable as a human carcinogen for ethyl alcohol 200 ppm TWA 400 ppm STEL A4 not classifiable as a human carcinogen for isopropyl alcohol 200 ppm TWA 250 ppm STEL skin for methyl alcohol Ventilation System A system of local and or general exhaust is recommended to keep employee exposures below the Airborne Exposure Limits Local exhaust ventilation is generally preferred because it can control the emissions of the contaminant at its source preventing dispersion of it into the general work area Please refer to the ACGIH document Industrial Ventilation A Manual of Recommended Practices most recent edition for details Personal Respirators NIOSH Approved If the exposure limit is exceeded wear a supplied air full facepiece respirator
10. 200 300 400 500 600 Cooling Capacity Watts ElectraCOOL L A 400 Flow Rate vs Pressure Drop Curve Figure 2 18 aee 1 6 Pressure Psi a om s ONBKRODOWOOON A 18115 225 3 35 4 45 5 55 6 Flow Rate Lpm Overall Dimensions Weight Height inches mm 13 5 330 26 Lbs 11 7Kg Width inches mm 7 75 196 8 Depth inches mm 11 0 279 Standard Features Programmable digital PID system controller Temperature control accuracy 0 10 C 0 18 F Leak proof fluid inlet and outlet with quick disconnect valves Highly reliable environmentally safe thermoelectric cooling elements Efficient seal less centrifugal magnetic drive pump 45 000 hours MTBF with brushless DC motor ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL Quiet high performance fans 50 dBA CustomChill300 Approved for medical use UL 2601 1 and Canadian CSA C22 2 No 601 1 Optional features include PID with RS232 RS485 communications port Heating option to 500 or 600 Watts Low fluid level indicator or dry contact closure Low Flow Alarm light or sound or Low Flow Alarm with specific set point Temperature alarm light or sound Super Quiet Fan lt 45 dBA Class Type B equipment 5 INSTALLATION AND OPERATION INSTRUCTION 1
11. ElectraCOOL L A 400 ADVANCED THERMOELECTRIC 400 Watt Liquid to Air Thermoelectric Chillers ElectraCOOL LA400 User s Manual November 2005 Index 1 INTRODUCTION Page 1 Symbols Used on the ElectraCOOL L A 400 Page 1 2 INCOMING INSPECTION Page 1 3 PRODUCT HANDLING Page 1 4 TECHNICAL DATA Page 2 Cooling Capacity Curve Figure 1 Page 3 Flow Rate vs Pressure Drop Curve Figure 2 Page 3 5 INSTALLATION AND OPERATION INSTRUCTION Page 4 6 PURGING THE FLUID SYSTEM Page 4 7 DIGITAL CONTROLLER Page 5 8 SERVICE GUIDE Page 5 TROUBLESHOOTING GUI DE Page 6 9 WARRANTY Page 7 10 RETURN POLICY Page 8 11 MSDS for Coolants Page 9 ETHYLENE GLYCOL Page 9 First Aid Measures Section 4 Page 10 REAGENT ALCOHOL Page 15 First Aid Measures Section 4 Page 16 Toll Free Technical Assistance 1 866 665 5434 ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 USA Telephone 603 888 2467 Fax 603 724 6740 www electracool com ElectraCOOL LA400 USER S MANUAL 1 INTRODUCTION ElectraCOOL brand recirculating liquid chillers are designed to provide liquid cooling heating or temperature stabilization for a wide range of applications such as Medical Equipment Laser Electro Optics Semiconductor Laboratory Aquariums and any other use that requires the efficient movement of heat to or from something greater than forced convection or other methods can provide The cooling capacity of our line of chillers ranges
12. For emergencies or instances where the exposure levels are not known use a full face piece positive pressure air supplied respirator WARNING Air purifying respirators do not protect workers in oxygen deficient atmospheres Skin Protection Wear protective gloves and clean body covering clothing Eye Protection Use chemical safety goggles Maintain eye wash fountain and quick drench facilities in work area ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 11 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL 9 Physical and Chemical Properties Appearance Clear oily liquid Odor Odorless Solubility Miscible in water Specific Gravity 1 1 20C 4C pH No information found Volatiles by volume 21C 70F 100 Boiling Point 197 6C 388F Melting Point 13C 9F Vapor Density Air 1 2 14 Vapor Pressure mm Hg 0 06 20C 68F Evaporation Rate BuAc 1 No information found 10 Stability and Reactivity Stability Stable under ordinary conditions of use and storage Hazardous Decomposition Products Carbon dioxide and carbon monoxide may form when heated to decomposition May produce acrid smoke and irritating fumes when heated to decomposition Hazardous Polymerization Will not occur Incompatibilities Strong oxidizing agents Reacts violently with chlorosulfonic acid oleum sulfuric acid perchloric acid Causes ig
13. NT IN THE SYSTEM MAKE SURE THAT LINE CIRCUIT BREAKER COINCIDES WITH NAMEPLATE MAXI MUM FUSE RATI NG Failure to follow the above precautions could result in electrical shock fire personal injury or damage to the unit and will void warranty 4 TECHNI CAL DATA 115V amp 230V I nput Versions Model LA400 115 LA400 230 Input Voltage VAC 115 230 Running Current Amps 7 0 3 5 Frequency Hz 50 60 50 60 Min Ambient F C 14 10 14 10 Max Ambient F C 122 50 122 50 Cooling Capacity BTUH Watt 1023 300 1354 400 Max flow rate GPM LPM 1 6 6 0 1 6 6 0 Max pressure PSI 14 7 14 7 Chiller fluid capacity Gallons ml 0 197 750 0 197 750 Control Temperature Range 14 to 113 F 10 to 45 C 14 to 113 F 10 to 45 C Control Accuracy F or C 0 1 0 1 Reservoir Capacity Gallons ml 0 132 500 0 132 500 Heating Capacity Max Watts Btuh 500 1705 500 1705 For Higher or Lower Ambient or Control Temperatures consult Advanced Thermoelectric Capacity rating at 77 F 25 C for both ambient and outlet fluid temperature For more information see Pumping Capacity chart on the respective chiller Technical Data Sheet ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL ElectraCOOL L A 400 Cooling Capacity Curve Figure 1 Process Fluid Temp in C 0 100
14. Policy outlined in our Operations and Maintenance O amp M Manual Unauthorized returns are not accepted for repair under warrantee Product must then be received inspected and if necessary tested by Advanced Thermoelectric and a product is deemed covered by our warrantee only when Advanced Thermoelectric or it s authorized representative is reasonably satisfied that all conditions in the warranty have been met SHIPPING DAMAGES both concealed and unconcealed are not covered under warrantee All shipping claims are the responsibility of the Buyer and we recommend they be made immediately with the carrier Where possible returns should be sent back in their original carton and packing to avoid subsequent shipping damages SPECIFICALLY NOT COVERED by this warrantee is any damage caused to the product occurring during but not limited to such events as improper installation storage or usage occurring during a situation specifically cautioned against or noted in the product manual Specific situations which invalidate the warranty include but are not limited to Removing the serial number label Any disassembly partial or complete of a heat exchanger loosening or removing the bolts or separating the heat sinks Subjecting a heat exchanger to temperatures below the freezing point of the heat transfer fluid contained inside the unit Subjecting a heat exchanger to unfiltered water Subjecting any product to temperature voltage curre
15. RCRA TSCA Ingredient CERCLA 261 33 8 d Ethylene Glycol 107 21 1 5000 No No Chemical Weapons Convention No TSCA 12 b No CDTA No SARA 311 312 Acute Yes Chronic Yes Fire No Pressure No Reactivity No Pure Liquid Australian Hazchem Code None allocated Poison Schedule None allocated ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 13 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL WHMIS This MSDS has been prepared according to the hazard criteria of the Controlled Products Regulations CPR and the MSDS contains all of the information required by the CPR 16 Other Information NFPA Ratings Health 1 Flammability 1 Reactivity 0 Label Hazard Warning WARNING HARMFUL OR FATAL IF SWALLOWED HARMFUL IF INHALED OR ABSORBED THROUGH SKIN MAY CAUSE ALLERGIC SKIN REACTION MAY CAUSE IRRITATION TO SKIN EYES AND RESPIRATORY TRACT AFFECTS CENTRAL NERVOUS SYSTEM Label Precautions Do not breathe vapor or mist Use only with adequate ventilation Keep container closed Avoid contact with eyes skin and clothing Wash thoroughly after handling Label First Aid If inhaled remove to fresh air If not breathing give artificial respiration If breathing is difficult give oxygen In case of contact immediately flush skin or eyes with plenty of water for at least 15 minutes Call a physician if irritation develops or persists If sw
16. SCA 12 b No CDTA Yes SARA 311 312 Acute Yes Chronic Yes Fire Yes Pressure No Reactivity No Mixture Liquid Australian Hazchem Code 2 S E Poison Schedule S5 WHMIS This MSDS has been prepared according to the hazard criteria of the Controlled Products Regulations CPR and the MSDS contains all of the information required by the CPR 16 Other Information NFPA Ratings Health 1 Flammability 3 Reactivity 0 Label Hazard Warning POISON DANGER MAY BE FATAL IF SWALLOWED HARMFUL IF INHALED OR ABSORBED THROUGH SKIN VAPOR HARMFUL FLAMMABLE AFFECTS CENTRAL NERVOUS SYSTEM MAY CAUSE BLINDNESS CANNOT BE MADE NONPOISONOUS CAUSES IRRITATION TO SKIN EYES AND RESPIRATORY TRACT MAY AFFECT LIVER BLOOD REPRODUCTIVE SYSTEM Label Precautions Keep away from heat sparks and flame Do not breathe vapor Avoid contact with eyes skin and clothing Keep container closed Use only with adequate ventilation Wash thoroughly after handling Label First Aid If swallowed induce vomiting immediately as directed by medical personnel Never give anything by mouth to an unconscious person If inhaled remove to fresh air If not breathing give artificial respiration If breathing is difficult give oxygen In case of contact immediately flush eyes or skin with plenty of water for at least 15 minutes In all cases call a physician Product Use Laboratory Reagent Revision Information MSDS Section s changed since last revision of docume
17. SES IRRITATION TO SKIN EYES AND RESPIRATORY TRACT MAY AFFECT LIVER BLOOD REPRODUCTIVE SYSTEM SAF T DATA Ratings Provided here for your convenience Health Rating 3 Severe Poison Flammability Rating 3 Severe Flammable Reactivity Rating 1 Slight Contact Rating 3 Severe Life Lab Protective Equip GOGGLES amp SHIELD LAB COAT amp APRON VENT HOOD PROPER GLOVES ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 15 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL CLASS B EXTINGUISHER Storage Color Code Red Flammable Inhalation Exposure may cause irritation to the mucous membranes of the upper respiratory tract Prolonged exposures to high concentrations may cause drowsiness loss of appetite and inability to concentrate Ingestion Cause headaches gastritis intoxication blindness and in acute cases death Skin Contact Causes skin irritation cracking or flaking due to dehydration and defatting action Eye Contact Can cause eye irritation Splashes may cause temporary pain and blurred vision Chronic Exposure Prolonged skin contact causes drying and cracking of skin May affect the nervous system May affect liver blood reproductive system Continued ingestion of small amounts could result in blindness Aggravation of Pre existing Conditions Persons with pre existing skin disorders or eye probl
18. a Dry chemical foam or carbon dioxide Water or foam may cause frothing Water spray may be used to extinguish surrounding fire and cool exposed containers Water spray will also reduce fume and irritant gases Special Information In the event of a fire wear full protective clothing and NIOSH approved self contained breathing apparatus with full facepiece operated in the pressure demand or other positive pressure mode Toxic gases and vapors may be released if involved in a fire 6 Accidental Release Measures Ventilate area of leak or spill Remove all sources of ignition Wear appropriate personal protective equipment as specified in Section 8 Isolate hazard area Keep unnecessary and unprotected personnel from entering Contain and recover liquid when possible Use non sparking tools and equipment Collect liquid in an appropriate container or absorb with an inert material e g vermiculite dry sand earth and place ina chemical waste container Do not use combustible materials such as saw dust Do not flush to sewer US Regulations CERCLA require reporting spills and releases to soil water and air in excess of reportable quantities The toll free number for the US Coast Guard National Response Center is 800 424 8802 7 Handling and Storage Keep in a tightly closed container stored in a cool dry ventilated area Protect against physical damage Separate from acids and oxidizing materials Containers of this material may be hazar
19. airlined hood or full facepiece self contained breathing apparatus Skin Protection Wear impervious protective clothing including boots gloves lab coat apron or coveralls as appropriate to prevent skin contact Eye Protection Use chemical safety goggles and or a full face shield where splashing is possible Maintain eye wash fountain and quick drench facilities in work area 9 Physical and Chemical Properties Appearance Clear colorless liquid Odor Mild pleasant whiskey like odor Solubility Miscible in water Density 0 79 20C 4C pH ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 17 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL No information found Volatiles by volume 21C 70F 100 Boiling Point 78C 172F ethanol Melting Point 114C 173F ethanol Vapor Density Air 1 1 6 ethanol Vapor Pressure mm Hg 40 19C 66F ethanol Evaporation Rate BuAc 1 ca 1 4 CCl4 1 ethanol 10 Stability and Reactivity Stability Stable under ordinary conditions of use and storage Hazardous Decomposition Products Carbon dioxide and carbon monoxide may form when heated to decomposition Hazardous Polymerization Will not occur Incompatibilities Strong oxidants silver salts acid chlorides alkali metals metal hydrides hydrazine and many other substances Conditions to Avoid Heat flames
20. al is expected to readily biodegrade When released into water this material may evaporate to a moderate extent This material is not expected to significantly bioaccumulate When released into the air this material is expected to be readily degraded by reaction with photochemically produced hydroxyl radicals When released into the air this ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 18 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL material is expected to be readily removed from the atmosphere by dry and wet deposition When released into the air this material is expected to have a half life between 1 and 10 days Environmental Toxicity This material is not expected to be toxic to aquatic life The LC50 96 hour values for fish are over 100 mg l 13 Disposal Considerations Whatever cannot be saved for recovery or recycling should be handled as hazardous waste and sent to a RCRA approved incinerator or disposed in a RCRA approved waste facility Processing use or contamination of this product may change the waste management options State and local disposal regulations may differ from federal disposal regulations Dispose of container and unused contents in accordance with federal state and local requirements 14 Transport Information Domestic Land D O T Proper Shipping Name ALCOHOLS N O S ETHANOL METHANOL ISOPROPANOL Hazard C
21. allowed give water or milk to drink and induce vomiting Never give anything by mouth to an unconscious person In all cases call a physician Product Use Laboratory Reagent Revision Information MSDS Section s changed since last revision of document include 3 Disclaimer Mallinckrodt Baker Inc provides the information contained herein in good faith but makes no representation as to its comprehensiveness or accuracy This document is intended only as a guide to the appropriate precautionary handling of the material by a properly trained person using this product Individuals receiving the information must exercise their independent judgment in determining its appropriateness for a particular purpose MALLINCKRODT BAKER INC MAKES NO REPRESENTATIONS OR WARRANTIES EITHER EXPRESS OR IMPLIED INCLUDING WITHOUT LIMITATION ANY WARRANTIES OF MERCHANTABILITY FITNESS FOR A PARTICULAR PURPOSE WITH RESPECT TO THE INFORMATION SET FORTH HEREIN OR THE PRODUCT TO WHICH THE INFORMATION REFERS ACCORDINGLY MALLINCKRODT BAKER INC WILL NOT BE RESPONSIBLE FOR DAMAGES RESULTING FROM USE OF OR RELIANCE UPON THIS INFORMATION Prepared by Environmental Health amp Safety Phone Number 314 654 1600 U S A ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 14 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL REAGENT ALCOHOL MSDS Number A2028 Effective
22. ck fluid level in the reservoir and add more fluid if necessary to 2 3 level Turn power switch ON and run the Chiller If possible raise the system above the chiller reservoir level for a few seconds to enable air to gather at the highest point Then lower system below chiller fluid inlet and outlet connections for a few seconds to allow air to travel to chiller reservoir SEO UT An OU NO ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 4 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL 8 If it is not possible to raise system then lower and raise chiller as instructed above for the system 9 Repeat this operation if there is any doubt that air still remains in the system When purging is complete check fluid level and fill reservoir to the top 7 DIGITAL CONTROLLER A The Factory Set Point fluid outlet temperature default is 5 C 41 F or at the value requested by customer when ordering 1 To display Set point Press P button for one second and release The display will now show the Set point value 2 To enter new Set point Press and release P button When Set point value appears on display press UP button to increase or DOWN button to decrease the value you want Push the P button once again to secure that setting B Operation Mode Because of complexity of programming the controller we do not recommend
23. dous when empty since they retain product residues vapors liquid observe all warnings and precautions listed for the product 8 Exposure Controls Personal Protection Airborne Exposure Limits OSHA Permissible Exposure Limit PEL 50 ppm Ceiling ACGIH Threshold Limit Value TLV 50 ppm Ceiling vapor Ventilation System A system of local and or general exhaust is recommended to keep employee exposures below the Airborne Exposure Limits Local exhaust ventilation is generally preferred because it can control the emissions of the contaminant at its source preventing dispersion of it into the general work area Please refer to the ACGIH document ndustrial Ventilation A Manual of Recommended Practices most recent edition for details Personal Respirators NIOSH Approved If the exposure limit is exceeded a half face respirator with an organic vapor cartridge and particulate filter NIOSH type P95 or R95 filter may be worn for up to ten times the exposure limit or the maximum use concentration specified by the appropriate regulatory agency or respirator supplier whichever is lowest A full face piece respirator with an organic vapor cartridge and particulate filter NIOSH P100 or R100 filter may be worn up to 50 times the exposure limit or the maximum use concentration specified by the appropriate regulatory agency or respirator supplier whichever is lowest Please note that N series filters are not recommended for this material
24. ece operated in the pressure demand or other positive pressure mode Water spray can be used to extinguish fires and cool fire exposed containers Water may be used to flush spills away from exposures and to dilute spills to non flammable mixtures ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 16 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL 6 Accidental Release Measures Ventilate area of leak or spill Remove all sources of ignition Wear appropriate personal protective equipment as specified in Section 8 Isolate hazard area Keep unnecessary and unprotected personnel from entering Contain and recover liquid when possible Use non sparking tools and equipment Collect liquid in an appropriate container or absorb with an inert material e g vermiculite dry sand earth and place ina chemical waste container Do not use combustible materials such as saw dust Do not flush to sewer US Regulations CERCLA require reporting spills and releases to soil water and air in excess of reportable quantities The toll free number for the US Coast Guard National Response Center is 800 424 8802 J T Baker SOLUSORB solvent adsorbent is recommended for spills of this product 7 Handling and Storage Protect against physical damage Store in a cool dry well ventilated location away from any area where the fire hazard may be acute Outside or detached
25. ems or impaired liver or kidney function may be more susceptible to the effects of the substance 4 First Aid Measures Inhalation Remove to fresh air If not breathing give artificial respiration If breathing is difficult give oxygen Call a physician Ingestion Induce vomiting immediately as directed by medical personnel Never give anything by mouth to an unconscious person Skin Contact Remove any contaminated clothing Wash skin with soap or mild detergent and water for at least 15 minutes Get medical attention if irritation develops or persists Eye Contact Immediately flush eyes with plenty of water for at least 15 minutes lifting lower and upper eyelids occasionally Get medical attention immediately 5 Fire Fighting Measures Fire Flash point 13C 55F CC Autoignition temperature 422C 792F Flammable limits in air by volume lel 3 3 uel 19 Flammable liquid and vapor Dangerous fire hazard when exposed to heat or flame Explosion Above flash point vapor air mixtures are explosive within flammable limits noted above Vapors can flow along surfaces to distant ignition source and flash back Sealed containers may rupture when heated Sensitive to static discharge Fire Extinguishing Media Water spray dry chemical alcohol foam or carbon dioxide Water may be ineffective Special Information In the event of a fire wear full protective clothing and NIOSH approved self contained breathing apparatus with full facepi
26. inhalation is generally not a problem unless heated or misted Exposure to vapors over an extended time period has caused throat irritation and headache May cause nausea vomiting dizziness and drowsiness Pulmonary edema and central nervous system depression may also develop When heated or misted has produced rapid involuntary eye movement and coma Ingestion Initial symptoms in massive dosage parallel alcohol intoxication progressing to CNS depression vomiting headache rapid respiratory and heart rate lowered blood pressure stupor collapse and unconsciousness with convulsions Death from respiratory arrest or cardiovascular collapse may follow Lethal dose in humans 100 ml 3 4 ounces Skin Contact Minor skin irritation and penetration may occur Eye Contact Splashes may cause irritation pain eye damage Chronic Exposure Repeated small exposures by any route can cause severe kidney problems Brain damage may also occur Skin allergy can develop May damage the developing fetus Aggravation of Pre existing Conditions Persons with pre existing skin disorders eye problems or impaired liver kidney or respiratory function may be more susceptible to the effects of this substance 4 First Aid Measures Inhalation Remove to fresh air If not breathing give artificial respiration If breathing is difficult give oxygen Call a physician Ingestion Induce vomiting immediately as directed by medical personnel Never give
27. lass 3 UN NA UN1987 Packing Group II Information reported for product size 350LB International Water I M O Proper Shipping Name ALCOHOLS N O S ETHANOL METHANOL ISOPROPANOL Hazard Class 3 UN NA UN1987 Packing Group II Information reported for product size 350LB 15 Regulatory Information Ingredient TSCA EC Japan Australia Ethyl Alcohol 64 17 5 Yes Yes Yes Yes Methyl Alcohol 67 56 1 Yes Yes Yes Yes Isopropyl Alcohol 67 63 0 Yes Yes Yes Yes Chemical Inventory Status Part 2 Canada Ingredient Korea DSL NDSL Phil Ethyl Alcohol 64 17 5 Yes Yes No Yes Methyl Alcohol 67 56 1 Yes Yes No Yes Isopropyl Alcohol 67 63 0 Yes Yes No Yes Federal State amp International Regulations Part 1 SARA 302 SARA 313 Ingredient RQ TPQ List Chemical Catg Ethyl Alcohol 64 17 5 No No No No Methyl Alcohol 67 56 1 No No Yes No Isopropyl Alcohol 67 63 0 No No Yes No Federal State amp International Regulations Part 2 RCRA TSCA ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 19 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL Ingredient CERCLA 261 33 8 d Ethyl Alcohol 64 17 5 No No No Methyl Alcohol 67 56 1 5000 U154 No Isopropyl Alcohol 67 63 0 No No No Chemical Weapons Convention No T
28. log octanol water partition coefficient of less than 3 0 When released into water this material is not expected to evaporate significantly When released into the air this material is expected to be readily degraded by reaction with photochemically produced hydroxyl radicals When released into the air this material is expected to have a half life between 1 and 10 days Environmental Toxicity The LC50 96 hour values for fish are over 100 mg l 13 Disposal Considerations Whatever cannot be saved for recovery or recycling should be managed in an appropriate and approved waste disposal facility Processing use or contamination of this product may change the waste management options State and local disposal regulations may differ from federal disposal regulations Dispose of container and unused contents in accordance with federal state and local requirements 14 Transport Information Not regulated 15 Regulatory Information Ingredient TSCA EC Japan Australia Ethylene Glycol 107 21 1 Yes Yes Yes Yes patrscns Chemical Inventory Status Part 2 Canada Ingredient Korea DSL NDSL Phil Ethylene Glycol 107 21 1 Yes Yes No Yes Federal State amp International Regulations Part 1 SARA 302 SARA 313 Ingredient RQ TPQ List Chemical Catg Ethylene Glycol 107 21 1 No No Yes No Federal State amp International Regulations Part 2
29. n t operate properly Contact Advanced Thermoelectric Unit is running Low Fluid indicator Red light lights up Insufficient fluid level in reservoir Fill up reservoir following air purge instructions detailed in section 6 of this Manual Unit runs but liquid level in reservoir decreases Liquid spots visible under or around the Unit Unit or System has a Leak Check the System for leaks Fix if possible If leak found within the Unit shut the Unit OFF and disconnect from Electrical line Contact Advanced Thermoelectric for possible replacement Unit runs but there is no coolant flow Red Light on the front of the Unit does not light up Actual Temperature displayed is high equal or slightly below ambient temperature System coolant line is clogged Check your System for valves turned OFF or kinks in tubing to resolve the problem Fluid froze in heat exchanger This situation is very serious and may indicate that the liquid in the thermoelectric assembly is frozen This can cause permanent damage Turn the chiller off and allow it to sit for an hour or so then take the corrective action in the column to the right Change Temperature Set Point to the highest available on the Temperature Controller Let Unit run until it is a visual coolant flow in reservoir Reset Set point several degrees higher than coolant freezing point Check fluid concentration correct if possible Unit pum
30. n For warranty claims a detailed failure analysis is required 4 Contact name phone and fax numbers and or email address All returns should be packed securely in original shipping carton and packing when possible to prevent shipping damage All shipping cartons must have the RMA clearly marked in large bold numerals on the outside of the box All returns must be sent in freight prepaid Collect shipments will be refused In some causes such as warranty consideration it may be necessary to have someone qualified discuss the failure in detail with our technical staff before we can issue and RMA After and RMA is assigned we ask that the Customer give us an approximate arrival date of the return to our factory ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL 11 MSDS for Coolants ETHYLENE GLYCOL MSDS Number E5125 Effective Date 03 15 04 Supercedes 11 02 01 24 Hour Emergency Telephone 908 659 2151 CHEMTREC 1 300 424 9300 MSDS Material Safety Data Sheet Nationa Response in Canada Outside U S and Canada IN Chemtrec 703 527 3887 From Mallinckrodt Baker Inc y Mallinckrodt ae A 222 Red School Lane CHEMICALS Response Camer emergency numbers to be Phillipsburg NJ 08865 amp used only n the event of chemical emergencies
31. nition at room temperature with chromium trioxide potassium permanganate and sodium peroxide causes ignition at 212F 100C with ammonium dichromate silver chlorate sodium chloride and uranyl nitrate Conditions to Avoid Heat flames ignition sources water absorbs readily and incompatibles 11 Toxicological Information Toxicological Data Oral rat LD50 4700 mg kg skin rabbit LD50 9530 mg kg Irritation skin rabbit 555mg open mild eye rabbit 500mg 24H mild Investigated as a tumorigen mutagen reproductive effector Reproductive Toxicity Has shown teratogenic effects in laboratory animals NTP Carcinogen Ingredient Known Anticipated IARC Category Ethylene Glycol 107 21 1 No No None ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 12 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL 12 Ecological Information Environmental Fate When released into the soil this material is expected to readily biodegrade When released into the soil this material is expected to leach into groundwater When released into the soil this material is not expected to evaporate significantly When released into water this material is expected to readily biodegrade When released into the water this material is expected to have a half life between 1 and 10 days This material is not expected to significantly bioaccumulate This material has a
32. nt or pressure internal or external greater than that specified in the product manual Operation with any replacement components As well as voiding the warranty this will also void the CE Mark Any actions prohibited in the Caution section of the product manual ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 7 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL Advanced Thermoelectric or it s authorized agents shall not be liable for any incidental or consequential damages for breach or any express or implied warranty on this product except to the extent prohibitive by applicable law and implied warranty of merchantability of fitness for a particular purpose on this product is limited in duration to the duration of this warranty 10 RETURN POLICY All products or parts returning to Advanced Thermoelectric or an authorized agent whether for warranty consideration repair restocking etc requires a Return Material Authorization number RMA Customer must first contact Advanced Thermoelectric Customer Service Department at 866 665 5434 Phone or 603 724 6740 Fax and have the following information available 1 Advanced Thermoelectric model part and serial numbers along with product description 2 Advanced Thermoelectric s Invoice number Customer s PO number and shipment date of original order 3 Reason for Retur
33. nt include 8 Disclaimer Mallinckrodt Baker Inc provides the information contained herein in good faith but makes no representation as to its comprehensiveness or accuracy This document is intended only as a guide to the appropriate precautionary handling of the material by a properly trained person using this product Individuals receiving the information must exercise their independent judgment in determining its appropriateness for a particular purpose MALLINCKRODT BAKER INC MAKES NO REPRESENTATIONS OR WARRANTIES EITHER EXPRESS OR IMPLIED INCLUDING WITHOUT LIMITATION ANY WARRANTIES OF MERCHANTABILITY FITNESS FOR A PARTICULAR PURPOSE WITH RESPECT TO THE INFORMATION SET FORTH HEREIN OR THE PRODUCT TO WHICH THE INFORMATION REFERS ACCORDINGLY MALLINCKRODT BAKER INC WILL NOT BE RESPONSIBLE FOR DAMAGES RESULTING FROM USE OF OR RELIANCE UPON THIS INFORMATION Prepared by Environmental Health amp Safety Phone Number 314 654 1600 U S A PIES FOR INTERNAL USE ONLY ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 20 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com
34. p is not running Contact Advanced Thermoelectric ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 USER S MANUAL Caution It is Customer s responsibility to advise Advanced Thermoelectric if the chiller needs to be set for 230V AC The wrong voltage selection can cause permanent Chiller damage and will void the Warranty WARRANTY Your satisfaction is important to us ADVANCED THERMOELECTRIC provides a one year full parts and labor warranty on ElectraCOOL and CustomChill brand chillers At our discretion we will REPAIR OR REPLACE defective products at no charge including parts and labor if necessary provided that work is performed by Advanced Thermoelectric or an authorized service center for Advanced Thermoelectric Contact us to determine who should repair your chiller when seeking and RMA see section 11 Buyer may also return PARTS that are defective with the prior consent of Advanced Thermoelectric We will replace defective parts at no charge Labor charges incurred by others during the inspection removal and replacement of parts are not covered by this warranty FREIGHT CHARGES for shipment to and from Advanced Thermoelectric or it s authorized representative is the responsibility of the Buyer WARRANTY CLAIMES must be made directly by the Buyer and in accordance with our Return
35. wing troubleshooting guide to find the problem or consult the factory If using any kind of coolant solution or antifreeze it is recommended to periodically check the concentration This can be relatively easily checked by measuring specific gravity of a coolant sample using a Hydrometer From time to time you may want to flush the system ADVANCED THERMOELECTRIC PO Box 7091 Nashua NH 03060 5 Toll free 1 866 665 5434 603 888 2467 fax 603 724 6740 e mail sales americool com ElectraCOOL LA400 TROUBLESHOOTING GUI DE USER S MANUAL PROBLEM POSSIBLE CAUSE CORRECTIVE ACTION Unit will not start when power switch is turned ON Controller s display doesn t light up No power supplied to the Unit Check unit is plugged in Confirm power supply is correct for your line voltage Unit runs for a period of time and then shuts OFF Controller display shuts OFF Line circuit breaker tripped due to overload Ensure line circuit breaker matches maximum fuse size on nameplate Check that there are no other electrical components on this line Unit is running but does not maintain desired coolant temperature 1 Heat load is too high Check and correct heat load if possible 2 Controller has incorrect temperature setting Enter correct Set point value according to Digital Controller Programming Instruction included in this Manual 3 Digital Temperature Controller does
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