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MANUAL JEROME J405

1. Jerome Model J405 0007 Serial Number 405 00003 Date 21 MAY 2006 05 21 37 Gas Hg dd MMM yyyy hh mm ss Reading Units Temp C Type Location 20 MAY 2000 20 D0 17 2 LZ2 UG M3 22512 Ny Lab ZO WMAY 20067 20379033035 28 g Mor 29 18 N Lab ZO WAY 20 007207502595 897 UG M3 20 3 lr N Lab ZO MAY 200620 3 51 47 08 ug m3 26 00 N Lab ZU WAY 2000920 752219 445 1 M7 2031 N Lab 20 MAY 2 0060 20252237 DL 19 M37 204907 N Lab Z20O WMAY 20 00720 555701 e977 UG M3 20 8 71 N Lab 2Z2O MAY 20067 20753229 26 ug m3 27 18 N Lab Bo BO Qu Bo Bo Bo INO e The Temp field lists the internal temperature of the instrument in degrees Celsius at the time of sampling e The Type field lists a single letter code that indicates the type of sample taken as follows N Normal Reading S Survey Mode Reading e The Location field lists the location where the sample was taken as set using SET LOCATION NAME in the SAMPLE menu See the SAMPLE menu section on page 15 for more details If Location Names are used and the data 1s output to a printer from the J405 consecutive samples at the same location will be grouped together AZI Customer Service 800 528 7411 or 602 470 1414 Page 29 of 63 The J405 I O port is a DB 25F connector on the back of the instrument that provides numerous specialized functions for specific industrial applications and for factory use System integration utilizing the 4 20mA output feature is the most commo
2. Press the ENTER START button on the keypad to select Regen Now from the Regen menu gt The instrument will respond with Perform Regen Using EXTERNAL POWER gt Press ENTER START to proceed or ESC to exit gt The instrument display will warn Do Not Disconnect External Power while Heating gt Press ENTER START to proceed or ESC to exit gt The instrument will begin a 45 minute regeneration cycle indicated by Regeneration gt in Progress on the display Do not interrupt this cycle If any error message appears on the display see the J405 TROUBLESHOOTING section beginning on page 38 e The LCD screen displays Regeneration in Progress for the duration of the 45 minute cycle and displays a countdown timer as well once the instrument enters the cooling process of the regeneration When the cycle is completed the instrument returns to the main screen e The instrument can be used immediately following the sensor regeneration if necessary e The Jerome J405 is ready for sampling CAUTION The Jerome J405 is intended for gaseous vapor use only DO NOT allow the probe or the instrument s intake to be exposed to liquids dust or other foreign material Moisture or liquids drawn into the instrument can damage the sensor and flow system AZI Customer Service 800 528 7411 or 602 470 1414 Page 23 of 63 Sample Mode This mode used for standard operation produces optimum accuracy with the Jerome J405
3. tubing Refer to page 33 High or erratic results Intake and internal filters may become clogged and need replacement when sampling in a dusty area 1 Open instrument and check for pinched crimped or disconnected internal tubing 2 In extreme conditions an additional particle filter may be installed on the intake AZI Customer Service 800 528 7411 or 602 470 1414 Page 38 of 63 Possible Cause Solution Low response or erratic readings May need a second regeneration 1 Wait 30 minutes and perform after a long period of non use cycle another sensor regeneration 2 Test with FTK Refer to page 56 3 If still unresponsive call AZI Customer Service at 800 528 7411 or 602 470 1414 for assistance False readings Extremely cold or extremely If sampling under these conditions warm air sampled into unit install Zero Air Filter in intake Sample every 15 seconds until the display reads 2 g m or less to equilibrate sensor temperature with the temperature of the sample air stream Remove filter and take samples Or Run the Warm up as described in the REGEN menu Display Warnings and Error Messages Low Battery Battery low Charge Battery See Page 28 Sensor Failure Call AZI Customer Service at 800 528 7411 or 602 470 1414 Data Memory Full Data memory full Save and then delete data See Retrieving Data on page 29 Incomplete Regen Regeneration interrupted Restart Regeneratio
4. 12 30 12 40 12 50 1 00 etc 15 minutes Quarter hour 12 00 12 15 12 30 12 45 1 00 1 15 1 30 etc 30 minutes Half hour 12 00 12 30 1 00 1 30 2 00 2 30 3 00 etc Times that are an even 45 minutes 45 minutes from midnight or noon 12 00 12 45 1 30 2 15 3 00 3 45 4 30 5 15 6 00 6 45 7 30 8 15 9 00 9 45 10 30 11 15 etc es 12 00 1 00 2 00 3 00 4 00 5 00 6 00 etc Times that are an even 90 minutes 90 minutes from 12 00 1 30 3 00 4 30 6 00 7 30 9 00 10 30 etc midnight or noon Times that are an even 120 minutes 120 minutes from 12 00 2 00 4 00 6 00 8 00 10 00 etc midnight or noon SET LOCATION NAME Up to 80 unique location presets are available using the J405 This feature is useful if sampling is done in multiple locations and there is a need to record which readings came from which locations Use the Aand Warrows to scroll through the list of 80 presets until the location to be edited is highlighted Press ENTER START to begin editing the name of the selected location Use the Aand Y arrows to scroll through the available alphanumeric characters and punctuation When the desired character is displayed use the arrow to move to the next character field Ifa mistake is made the arrow can be used to return to the previous character When the location has been named as desired press ENTER START to save the location name and return to the list of locations To select an existing locat
5. See JEROME J405 TECHNICAL SPECIFICATIONS on page 9 for the accuracy specifications e Press the power I O button The display will light up and briefly show the instrument serial number and software revision If necessary press ESC to clear any calibration reminders gt Next the digital meter displays 0 00 u g m If the battery meter is empty and flashing recharge the battery See the section Charging Internal Battery on page 28 e To ensure the instrument s electronics have stabilized allow a 5 minute warm up before beginning the next step e Press the SAMPLE button located at the end of the handle e At the end of the 12 second cycle read the digital meter gt The number shown on the digital meter is the mercury concentration in ug m This value remains displayed until the next sample is taken The digital meter automatically re zeroes at the start of each sample e When the sensor is completely saturated the digital meter displays Sensor Regeneration Required when sampling is attempted No further operation is possible until a sensor regeneration 1s performed Refer to the Sensor Regeneration procedure on page 23 e Press the I O button to turn the power OFF when not in use SAMPLE BUTTON Sampling Notes e The Jerome J405 is intended for vapor use only DO NOT allow the probe or the instrument s intake to come in contact with liquids dust or other foreign material Moisture or liquids drawn into the instru
6. Thermos Septa 20 Septum Holder J405 Maintenance Kit See pictures beginning on page 42 345 0050 2 of 1 8 Tygon tubing 25 inch fritware 3 packs of 20 fritware filters Zero Air Filter AG Filter Scrubber Filter Scrubber Filter with 2 elbows AZI Customer Service 800 528 7411 or 602 470 1414 Hard Side Carry Case Includes a molded case with die 990 0217 cut foam rubber inserts to hold the Jerome J405 and accessories Soft Side Carry Case Includes a shoulder strap for easy carrying a clear plastic window over the instrument display and pockets to hold supplies or accessories 990 0220 A2600 0902 Stopper Assembly Z2600 3914 Septum Holder AZI Customer Service 800 528 7411 or 602 470 1414 Page 42 of 63 3200 0011 Septa A2600 0903 Syringe Assembly 2600 0022 Syringe Needles 22 Ga 1400 2002 Probe 200 0143 Battery Pack Assembly 7 2600 3905 Zero Air Filter 600 0293 AG filter 7 2600 3930 Scrubber filter Aruona instrument LLC SCRUBBER FILTER ff 600 026 q A 600 0262 Scrubber Filter with 2 elbows Z2600 3940 Chlorine Filter AZI Customer Service 800 528 7411 or 602 470 1414 Page 43 of 63 vEROME AMMONIA FILTER FOR MERCURY SAMPLING EPERE ie LA 4 IPP 990 0193 Ammonia Filter 1400 3010 Tubing adapter 2600 3039 25 inch fritware pack of 20 Tygon tubing 1 8 LD 1 345 0050 foot 100 120 VAC Line Cord 6000 4008 959 VAC Line Cord
7. UK i 220 VAC Line Cord 200 0008 Europe AC Adapter Power Supply OS supply charger 990 0225 10 to 1 Dilution Module 371 LNSWNYLSNI VNOZIAV AZI Customer Service 800 528 7411 or 602 470 1414 Page 44 of 63 200 0165 USB Communication Cable Type A to Type B 200 0170 Car Accessory Cable 990 0214 External Battery Pack gt y N Q Z gt 311 LNaWNYLSNI For current prices and delivery information call AZI Customer Service at 800 528 7411 or 602 470 1414 AZI Customer Service 800 528 7411 or 602 470 1414 Page 45 of 63 Installing the J405 USB Driver Note The AZI USB Driver is compatible with Windows XP 32 bit Windows Vista 64 bit and Windows 7 32 and 64 bit However the Hyperterminal program is only included in Windows XP If the Jerome J405 CD is available e Insert the CD in the PC s CD ROM drive e Use Windows to browse to the CD locate the driver file AZI_USB_Driver zip and copy it to your desktop If the CD is not available e Download the driver file from the Drivers tab at http www azic com downloads aspx and save it to your desktop If you received these instructions and the driver in an email save the attached file AZI_USB_Driver zip to your desktop Once the driver file AZI_USB_Driver zip is on your desktop 1 Launch the AZI Driver Installer wizard e Double click the file to open it e Drag the Driver Install directory from the
8. 15 JUN 2606 15 JUN 2006 15 JUN 2006 15 JUN 2006 15 JUN 2006 DATA 2352 ug ma ug ms ug m3 ug m3 a ug md ug m3 ug m3 ug m3 06 5 ug m3 00 5 ug ms ug ms 5 ug ms ug ma ug ms ug m3 ug m3 ug m3 ug m3 k k fk fk App pd pd D Stop capturing 12 If you did not receive any text from the J405 e Goto the Call menu click Disconnect e Goto the File menu click Properties e You will see the same window as in step 4 above Try selecting a different COM port and continue from step 4 Keep trying each COM port in the list If you have tried all of them and still cannot receive data from the J405 try re installing the J405 USB driver If that does not solve the problem call AZI Customer Service at 800 528 7411 or 602 470 1414 or email support azic com See Retrieving Data on page 29 for an explanation of the fields in the data file AZI Customer Service 800 528 7411 or 602 470 1414 Page 55 of 63 11 APPENDIX B J405 FUNCTIONAL TEST KIT If your application requires frequent verification of instrument functionality this test will benefit you If the test results fall within the expected range you may assume the instrument is functioning properly THIS IS A FIELD CHECK OF THE FUNCTIONALITY OF THE INSTRUMENT THIS TEST DOES NOT CALIBRATE THE INSTRUMENT Testing with the Functional Test Kit F
9. FREE OF LIQUID MERCURY e Replace the oxidized mercury with approximately Y2 cc fresh mercury AZI P N A2600 0904 gt Do NOT use the syringe for measuring liquid mercury Dispose of oxidized mercury properly e Reinstall the stopper assembly AZI Customer Service 800 528 7411 or 602 470 1414 Page 57 of 63 Pull and hold the syringe plunger against the bar stop Verify that the black mark on the syringe plunger aligns with the Icc mark on the syringe barrel gt If it does not the holder assembly must be adjusted Call AZI customer service at 602 470 1414 or 800 528 7411 for assistance Insert the needle into the needle guide of the bottle stopper Operate the plunger two or three times to pump mercury vapor into the syringe On the final stroke pull and hold the plunger against the bar stop Holding the plunger against the bar stop remove the syringe from the bottle and move it to the septum attached to the instrument intake Continue to hold the plunger against the bar stop and insert the syringe needle into the septum Press the SAMPLE button on the instrument and Sampling and Purging will appear on the J405 display AZI Customer Service 800 528 7411 or 602 470 1414 Page 58 of 63 When Purging disappears from the display release the plunger and allow gravity to feed the mercury vapor into the airstream If the plunger stops gently press 1t completely closed Remove the syrin
10. Transfer e CAREFULLY pour the mercury into the center of the functional test kit vessel s opening gt ENSURE that no mercury residue is on the outside of the vessel See the supplier s Material Safety Data Sheets MSDS or call AZI Customer Service at 1 800 528 7411 or 1 602 470 1414 for clean up instructions e INSTALL the stopper assembly into the functional test kit vessel carefully to prevent breakage of the thermometer gt PRESS the stopper assembly into the vessel to achieve a good seal e USE the J405 instrument to verify that the outside of the vessel is not contaminated and the mercury vapor emission level if any is below the OSHA TLV for mercury e ALLOW the kit to adjust to room temperature for at least two 2 hours before using gt The temperature range for the test is 16 24 C Avoid temperature fluctuations CAUTION Do not use the FTK vessel as a portable container If the vessel is upset or greatly agitated mercury droplets will cling to the thermometer stem the rubber stopper the mouth of the vessel and the needle guide Replacing Mercury An oxide coating will form on the drop of mercury and will cause lower readings in your testing Gently swirl the vessel to disturb the outer oxidized surface of the droplet If this does not restore higher readings it may be necessary to replace the mercury e Carefully remove the stopper assembly from the FTK vessel A A CAUTION BE SURE NEEDLE GUIDE IS
11. and 48 hours and Saturation and press ENTER START to save the selected interval The J405 will now automatically perform a sample followed by a regen every 6 12 24 or 48 hours starting at the time set in SET HOUR below or when the sensor is saturated as selected Use ESC to exit without saving SET HOUR Use the Aand W arrow keys to select the hour of the day using a 24 hr clock to start regeneration Press ENTER START to save the setting At the time set 1f auto sampling 1s being used the J405 will automatically take one sample and then perform a sensor regeneration This process will repeat at the interval indicated in SET INTERVAL above Use ESC to exit without saving NOTE If the sensor is saturated and a regeneration cycle is performed and completed before the set hour the instrument will perform another regeneration at the set hour However 1f the regeneration cycle does not complete prior to the set hour the regeneration at the set hour will be skipped DATA menu Sample data can be stored within the instrument up to a maximum of twenty thousand 20 000 data points On instruments that have the USB Communications option data can be retrieved from the instrument in one of three ways 1 SEND TO PC 2 SAVE TO USB MEMORY DRIVE 3 PRINT DIRECTLY TO AN AZI APPROVED PRINTER AZI P N Y990 0098 The presence of the USB icon on the main screen indicates that the Communications option has been purchased and that the USB ports ar
12. atic acon ouctein ested 37 Vermicatiomob Funcionalidad ET 37 9 J405 LROUBEESHOO EIN Gotico iii dianas 38 Potential Inte rterence sa a 40 9 ACCESSORIES amp MAINTENANCE PARTS 1 ccssssssssscsccccccccsssssscssesesssees 41 Spare Par tdi oe 42 10 APPENDIX A USB HYPERTERMINAL SETUP o oocccccccccccccccccccccccccncccnccccncncccnos 46 11 APPENDIX B J405 FUNCTIONAL TEST KIT oocccccccccccccccocccccccccccccccccccccncccnss 56 Prepara olor asa 56 Mercury ran oia 57 Replacine Mercu Vereen dada T a 57 Syinse Techniques a a as 58 AZI Customer Service 800 528 7411 or 602 470 1414 Page 3 of 63 Functional Test Procedure cccccececoscsccececsccecsccscaccsceccececsececsccscascscencececsecesccscess 59 J405 FTK Instrument Response Chait uscar 60 Functional Test TroubleshootINg ccoooooonnncncnnncnonononocnnnnnnnnonnnnnonnnncnnnnnnnnnnnnnnnnnnnnnnnnnnos 61 y WARRANEX rana acia 62 All section numbers titles and page numbers in BOLD in this manual are hyperlinks and can be clicked to simplify navigation within the PDF version of the manual The BACK button found in most PDF software programs is also very helpful when navigating using the hyperlinks An up to date electronic copy of this manual can be found at http www azic com downloads aspx AZI Customer Service 800 528 7411 or 602 470 1414 Page 4 of 63 UNPACKING THE INSTRUMENT This manual contains details that will optimize the result
13. crucial link between the sensor and the sample For the instrument to perform correctly the flow system must be properly maintained The user maintainable components of this system are the intake filter 25 inch fritware an AG Filter two scrubber filters and connecting tubing Check the Preventive Maintenance on page 32 for a suggested schedule for changing fritware and internal filters The Tygon tubing in the system must be free of crimps for proper flow Flow System Parts Scrubber Filter 1 1 Elbow 1 Straight Barb 2 2600 3930 Scrubber Filter 2 2 Elbow Barbs 600 0262 AG Filter 600 0293 25 inch Fritware Filter 2600 3039 Tygon Tubing 1 8 LD 2 345 0050 25 inch Fritware Filter Replace the 25 inch fritware filter once each week or as needed In dusty environments the fritware filter may need to be replaced as often as once a day Replacement 25 inch fritware filters are available from AZI Consumable Sales at 800 528 7411 or 602 470 1414 e Remove the two 2 side screws from the intake end of the instrument and open the case e Gently pull the inner portion of the intake out of the intake port in the direction of the arrow as shown in Figure 1 below e Gently push the old fritware filter disc out of the intake with a small blunt instrument as shown in Figure 2 below e Place the new fritware onto the inside end of the intake port as shown in Figure 3 below e Gently press the inner portion of the intake in the
14. direction of the arrow in Figure 4 to seat the fritware disc firmly against the inner ledge of the intake e Once the fritware has been replaced and the inner portion of the intake reinserted close the case and replace the two 2 side screws removed above a Figure 1 Figure 2 Figure 3 Figure 4 AZI Customer Service 800 528 7411 or 602 470 1414 Page 33 of 63 AG Filter Check The increased sensitivity of the J erome J405 requires the replacement of the AG filter 600 0293 every 500 samples to ensure the accuracy of the readings If your application will require in excess of six 6 months to reach 500 samples the AG filter should still be changed every six months along with the other internal filters To check the AG filter e Take 5 samples with Zero Air Filter 2600 3905 connected to front of instrument Readings should decrease with at least 3 of the 5 readings at 0 00 u g m For maximum accuracy wait 15 seconds between samples to allow the sensor to restabilize e If readings are not 0 00 ug m then the internal AG filter 600 0293 needs to be replaced After replacement the new AG filter will need to be acclimated to the system by performing a sensor regeneration followed by twenty 20 manual samples See page 35 for filter change instructions e The number of samples can be monitored by viewing the Sensor Stats within the instrument From the MAIN Screen Press the RIGHT arrow button P to enter the main me
15. mail support azic com to schedule instrument calibration e The digital meter displays 0 00 g m e Look at the battery icon in the top center of the display to determine the current battery level gt If the battery icon is empty and flashing recharge the battery See page 28 AAC DOS IDpYy WA DAD ANAI Y7ED MERK CUR i Al OR ANALYZER e The included AC power supply charger can utilize 110V or 220V AC power and it is not necessary to manually select the input voltage e The J405 contains an auto resetting fuse that does not require care maintenance or replacement by the user AZI Customer Service 800 528 7411 or 602 470 1414 Page 5 of 63 e Perform a sensor regeneration by following these steps Connect the AC power supply charger between the connector on the back of the J405 and an AC power outlet or connect the external battery pack to the back of the J405 If the J405 is turned off press the I O power button to turn the instrument on Press the RIGHT arrow button to enter the main menu Press the DOWN arrow button Y to move the cursor to Regen Press the RIGHT arrow button to select Regen from the menu Press the ENTER START button on the keypad to select Regen Now from the Regen menu The instrument will respond with Perform Regen Using EXTERNAL POWER Press ENTER START to proceed or ESC to exit The instrument display will warn Do Not Disconnect External Power while Heating Pr
16. to select Survey Mode and begin sampling gt The instrument performs a 2 second purge of the flow system and then begins survey mode sampling gt The display updates the measured concentrations at the end of each 2 second sample gt The pump will continue to run and the display will update with a new mercury concentration reading every 2 seconds gt Press any button to stop survey mode sampling and perform a final purge of the flow system gt The instrument remains in the survey mode until one of the following occurs A button is pressed on the keypad The sensor is saturated A low battery signal is encountered The instrument is turned OFF gt The final survey value remains displayed on the main screen until the next sample is taken Press the power I O button to turn the instrument off when not in use AZI Customer Service 800 528 7411 or 602 470 1414 Page 25 of 63 Operating on AC Power or Generator e For stationary use the J405 may be operated on AC power gt Operating the instrument on AC power at all times eliminates the need for the battery pack and its necessary maintenance gt The battery may be disconnected internally or removed completely whenever the instrument is operating on AC power Operating on Internal Battery Power For portable use the J405 may be operated on battery power e When you operate the instrument on battery power please be aware of the following gt A fully charged battery p
17. 0 1414 AZI Customer Service 800 528 7411 or 602 470 1414 Page 37 of 63 8 J405 TROUBLESHOOTING Symptom Possible Cause Solution OOOO Power Problems Instrument does not turn ON Battery will not hold a charge Instrument does not turn on when connected to AC power supply charger Discharged battery or Dead battery Open fuse Insufficient power Internal component failure Recharge battery for a minimum of 3 hours Refer to page 28 Replace battery Refer to page 36 Wait for fuse to automatically reset itself Use a voltmeter to verify there is power to the AC outlet Call AZI Customer Service for information at 800 528 7411 or 602 470 1414 Sampling Problems Airflow is restricted during the sensor regeneration cycle causing possible permanent damage Kinks and crimps in the Tygon tubing Obstructed intake or exhaust Clogged intake filter Periodically check the Tygon tubing in the instrument Refer to page 35 Verify ports are not obstructed Change intake fritware filter Refer to page 33 High erratic results Internal mercury vapor contamination 1 Install Zero Air Filter in intake Press SAMPLE button After three samples 1f readings are over 2 g m replace fritware filter and Tygon tubing Refer to page 33 2 Perform sensor regeneration with the Zero Air Filter in intake Refer to page 23 Retest if necessary Replace scrubber filters and Tygon
18. 1414 Page 8 of 63 Range Resolution Response time sample mode Response time survey mode Flow rate Power requirements Fuse Internal battery pack Operating environment Case construction Dimensions Weight Digital meter display Data storage capacity Output Certifications Accuracy and Precision Calibration Point 1 0 ug m 25 ug m 100 ug m 0 5 g m to 999 g m 0 0005 to 0 999 mg m 0 01 ug m He 12 seconds 2 seconds 750 50 cc min 0 75 0 05 liters min 12 VDC for the instrument provided by the internal battery AC power supply charger external battery pack or car accessory adapter 100 240V AC 47 63Hz 3 2A for the AC power supply charger Auto resetting fuse Rechargeable nickel metal hydride NiMH 0 C to 45 C non condensing non explosive Aluminum powder coated llinLx6inW x 6 5 in H 28 cm Lx 16cm W x 17 cm H 5 3 pounds 2 4 kilograms 3 Y inch 9 cm liquid crystal display LCD 20 000 samples Digital USB serial data to PC printer or USB flash drive Analog 4 20mA current loop requires external power source Accurate to 0 3 of output TUV 61010 CE Accuracy Precision RSD 15 3 3 Sample values below 0 5 g m will be recorded and displayed as 0 00 g m by the J405 Sample values above 999 ug m will be recorded but the display will indicate High Concentration After changing the AG filter accuracy at 1 0 u g m may change from 10 to 20 a
19. 602 470 1414 or e mail support azic com to schedule instrument calibration gt The digital meter displays 0 00 g m gt Check the battery level as indicated by the battery icon at the top center of the instrument display If the battery meter is empty and flashing refer to Charging Internal Battery on page 28 If the battery meter is not empty but is flashing then the instrument is currently charging the battery gt To ensure the instrument s electronics have stabilized allow a 5 minute warm up before beginning the next step e Perform sensor regeneration Refer to Sensor Regeneration on page 23 for the procedure e Ensure the instrument has been powered on for at least five 5 minutes prior to sampling e Use the Zero Air Filter to equilibrate the instrument to ambient air temperature gt Install the Zero Air Filter in the instrument s intake gt Sample repeatedly every 15 seconds until the readings stabilize then remove the Zero Air Filter NOTE For EPA clean up levels less than 3 g m it is necessary to run a warm up routine before sampling To initiate the automatic five minute warm up install a Zero Air Filter AZI P N Z2600 3905 in the intake and select Warmup from the REGEN menu For levels of 3 ug m and above the warm up routine is not necessary e Press the SAMPLE button at the end of the handle e At the end of the sampling cycle read the digital meter gt The number shown on the digital mete
20. Arizona Instrument and may be ordered as Chlorine Filter AZI P N 22600 3940 Ammonia in very high concentrations can cause an off gassing of accumulated acidic fumes from the internal acidic gas filter resulting in positive readings on the instrument In these cases the ammonia odors are very strong A special filter designed to remove ammonia gas from the sample stream is available from Arizona Instrument and may be ordered as Ammonia Filter AZI P N 990 0193 Again either allow the vapors to dissipate or use the ammonia filter Filter replacement at regular intervals or when unexpectedly high readings are encountered in areas of these potential interferences may resolve these problems Visit the Tech Notes section at www azic com for more information concerning the chlorine and ammonia filters Volatile mercury compounds in general will cause the gold film to respond Alkyl organic mercuries such as methyl mercury and other straight chained compounds are typically extremely volatile and change the electrical resistance of the gold film sensor Any such responses should be considered qualitative not quantitative The instruments are designed and calibrated to elemental mercury vapor only Inorganic mercury salts such as mercuric chloride are not very volatile However they may generate some minute level of elemental mercury vapor to which the instruments will respond This response again should be considered a qualita
21. Instrument LLC USER MANUAL JEROME J 405 MERCURY VAPOR ANALYZER OPERATION MANUAL June 2010 ARIZONA INSTRUMENT LLC 3375 N Delaware Street Chandler AZ 85225 USA 800 528 7411 602 470 1414 f 602 281 1745 WWW azic com Email General azi azic com International intl azic com Customer Service support azic com e n AZI P N 700 0099 H Last update J une 2010 JEROME J405 Mercury Vapor Analyzer Operation Manual PROPRIETARY RIGHTS NOTICE This manual contains valuable information and material developed by Arizona Instrument LLC for use with the Jerome J405 Mercury Vapor Analyzer No part of this manual can be reproduced or transmitted in any form or by any means electronic mechanical or otherwise This includes photocopying and recording or in connection with any information storage or retrieval system without the express written permission of Arizona Instrument LLC ALL RIGHTS RESERVED Copyright 2006 2010 Arizona Instrument LLC Resisorb is a registered trademark of Mallinckrodt Baker Inc Tygon is a registered trademark of Saint Gobain Performance Plastics Corporation Sofnolime is a trademark of Molecular Products Limited Windows is a registered trademark of Microsoft Corporation in the United States and other countries AZI Customer Service 800 528 7411 or 602 470 1414 Page 2 of 63 Table of Contents Ll UNPACKING THE INSTRUMEN Lo ooiisi oninnsocacinoiodonoconoco conocido condiac
22. J405 HyperTerminal 13 a Ed Send File Receive File Capture Text Send Text File Capture Eo Printer Creates a file of all incoming text AZI Customer Service 800 528 7411 or 602 470 1414 Page 53 of 63 8 HyperTerminal will prompt for a file to save the data to It is recommended that the data be saved to either the Desktop or My Documents J405 HyperTerminal E ax File Edit View Call Transfer Help Capture Text Folder C Documents and File Settings username Desktops 4050 ata tut Connected 0 02 22 Auto detect Auto detect SCROLL CAPS NUM Capture Print echo 9 Go to the J405 and navigate to the DATA menu then highlight Send to PC and press ENTER START 10 You should see your data scrolling in the HyperTerminal window If you do not see anything in the HyperTerminal window go to step 12 AZI Customer Service 800 528 7411 or 602 470 1414 Page 54 of 63 11 When the J405 stops sending data Click HyperTerminal s Transfer menu again and click Capture Text then Stop 3405 HyperTerminal File Edit View Call BAGEA Help Send File Receive File Capture Text Stop E oa Send Text File Pause As 1 fe a z i mo Y 15 JUN 200L Luco Prae Ug m3 36 00 S AE 1 99 ug m3 36 00 5 15 JUN 2606 15 JUN 2606 15 JUN 2006 1o JUN 2006 15 JUN 2006 15 JUN 2006 15 JUN 2006 15 JUN 2006 15 JUN 2606 19 JUN 2606 15 JUN 2606 13 JUN 2006
23. TK should always be done with the instrument set to display in micrograms per cubic meter u g m If your instrument is displaying results in milligrams per cubic meter mg m switch to u g m by selecting Units from the SAMPLE menu before doing any testing with the FTK See SAMPLE menu on page 15 for more information on changing the display units NOTE Perform the functional test ONLY after a sensor regeneration The J405 Functional Test Kit contains all accessories necessary to perform the functional test See the complete list on page 41 and verify that all the parts to the kit are present CAUTION The vial and thermometer contain liquid mercury and are possible sources of mercury contamination Follow the instructions for handling or transferring the mercury into the Functional Test Kit Vessel carefully For safety information see the supplier s Material Safety Data Sheets MSDS or call AZI Customer Service at 1 800 528 7411 or 1 602 470 1414 for assistance in obtaining the MSDS Preparation e Carefully unpack and inspect the parts of the kit e ENSURE that the mercury shipping container and mercury filled thermometer are not broken e Ina ventilated area preferably under a fume hood remove the mercury vial from its shipping container e Place the functional test kit vessel and the mercury vial close to each other and open the mercury vial AZI Customer Service 800 528 7411 or 602 470 1414 Page 56 of 63 Mercury
24. When the battery fails to hold a charge the battery pack should be replaced gt Battery life under normal usage is approximately 1 year depending on the number of charge and discharge cycles See Replacing the Battery Pack on page 36 AZI Customer Service 800 528 7411 or 602 470 1414 Page 28 of 63 Retrieving Data On instruments that have the USB Communications option sample data can be transmitted from the J405 for analysis using the USB connections on the back panel of the J405 Data may be transmitted directly to a PC saved to a USB drive plugged into the J405 or printed to an AZI printer connected to the J405 See the DATA menu section on page 18 for the specific data transmission options available If the USB Communications option has not been purchased the USB ports will not be present Contact your AZI Sales Representative for information on the USB option The data is transmitted in a comma delimited text file named serialnumber txt for example 40500003 txt with a four line header indicating the model and serial number of the instrument the date and time of the report and the gas being detected The first line of the data indicates the contents of each data field as shown below The USB icon on the main screen will flash during data transmission If an instrument data file with the same filename already exists on the USB drive the current data will be appended to the existing file The data file will look like this example
25. ack AZI P N 200 0143 provides power for a minimum of twenty four 24 hours of operation gt For operating more than twenty four 24 hours an extra fully charged battery pack is needed gt Complete battery recharging takes 3 hours Refer to Charging Internal Battery on page 28 gt The J405 uses a rechargeable Nickel Metal Hydride battery Dispose of worn out batteries properly when you are replacing the battery pack When operating on battery power the J405 will shut down after twenty 20 minutes of non usage However if the instrument is running in Survey Mode or Auto Sampling mode the instrument will not shut off after twenty minutes If the J405 1s reading low levels of mercury in Survey or Auto Sampling mode it will continue to sample until the battery runs out However if the J405 is reading high levels of mercury in Survey mode when the sensor reaches saturation a message will appear indicating that sensor regeneration 1s required and twenty minutes later the instrument will automatically power off In Auto Sampling mode the instrument will regen automatically when the sensor is saturated provided external power is connected If external power is not connected the instrument will indicate Regen Required and the regeneration will not be performed Battery Management With all handheld and battery powered instruments there is a need to keep the battery properly charged and ready for use Proper battery management will
26. acocnaccanadaccdacacacacas 5 2 INTRODUCTION cerea a 7 3 JEROME J405 TECHNICAL SPECIFICATIONS cccccsssssscscssssssssessssesssssseseees 9 4 PRINCIPLE OF OPERATION ciisssssicecccdscstccesidcaccddnceaceesscddeccheatseedsedassedsesaceedsadeddacseres 10 Zero Air Filter CAZL P N Z2000 3905 Jeren a a iia 11 Sy INSTRUMENT OPERATION sccccccececseidescctelenccsstslcactsciencscaciecssciclesectstslenstendencscatianesss 12 JA0S Mam serech DISD LAY ias 12 JOS Back Panc C One CIO iia 13 J405 User Interface Mam Menu Str ae aa ieu te ties cece at saalen tees tbe sire A 14 SAMPLE ICO rss estes a 15 RECEN Menta 17 DATA MOOD ndice ceo ici 18 SIS EE IMU Ci sad da 19 Daly Operas si iii 22 DE MSOR INC CNET O A ida 23 Sample a e E E E EA E EE EE E T A A E ET ET 24 SUVE V MOUE o 25 Op ratine on AC Power or Generada cd 26 Operatine on Internal Battery POW er isaac 26 Battery Mana MM a hoe nies 26 External Battery LO Webstats 27 Chareimo Imtemal Batteries 28 Retenes 29 Instrument VOM AC seca ia as o 30 O 101 0 eee nea nna E eee kT ee ne eee ae ee eee Ce eee eae 30 07 MAINTENANCE cceassieceriescesdecessescceadiedi ila ceteccastus hice a aea aE ai 32 Preventive Maintenance SCHEGUIC msi ata 32 Fow oy eia On mR penn RN ere Me a AE en 33 2S ETW goal mill cs ee rere ere O eine ee eames eee mere 33 AGTE AA A 34 Tite ral Piles os 35 Replace he Batey Pack insisti 36 Le CALIBRATION cnrs aie a a a a a E A RE E E 37 Factory CalbrationS erica a ati acon aetna
27. charger or the external battery pack must be plugged into the back of the instrument before a regen can be performed The following options are available from the REGEN menu REGEN NOW Connect external power to the instrument before performing a regen Highlighting REGEN NOW and pressing ENTER START will start the sensor regeneration process Press ENTER START again on the next screen to confirm your choice and press ENTER START again after reading the warning that appears The regeneration will now begin Do not disconnect external power during the regeneration WARMUP To ensure maximum accuracy when sampling at cleanup levels less than 3 u g m the J405 must be warmed up with the Zero Air Filter in the intake at the location to be sampled To run the warm up insert the Zero Air Filter in the intake highlight WARMUP and press ENTER START While warming up the pump will run and the J405 will display a 5 minute countdown When the warm up finishes remove the Zero Air Filter and begin normal sampling If the J405 is idle for more than 20 minutes another warm up is required to maintain maximum accuracy at these low levels AZI Customer Service 800 528 7411 or 602 470 1414 Page 17 of 63 SET INTERVAL If auto sampling 1s being used as set in SAMPLE MODE above the J405 can be configured to automatically perform sensor regenerations at a predetermined interval Use the Aand VWarrows to scroll through the available intervals of 6 12 24
28. cked with foreign matter Check flow with a flow meter If you find the above does not solve your problem please call AZI Customer Service at 800 528 7411 or 602 470 1414 AZI Customer Service 800 528 7411 or 602 470 1414 Page 61 of 63 12 WARRANTY Arizona Instrument LLC seller warrants to buyer that J erome products delivered pursuant to this agreement shall at the time of delivery and for a period of one 1 year thereafter the Internal Battery Pack where applicable 1s warranted for a period of ninety 90 days only to be free from defects in material or workmanship and shall conform to seller s specifications or such other specifications as seller has agreed to in writing Seller s obligations with respect to claims under this warranty shall be limited at seller s option either to the replacement of defective or non conforming product or to an appropriate credit for the purchase price thereof subject to the provisions of seller s Warranty Policy as amended from time to time said Policy being incorporated herein by reference Returned products under warranty claims will be shipped to seller s plant by buyer at buyer s expense and shall be accompanied by a statement of the reason for the return and an approved Return Material Authorization Number issued by seller Buyer remains responsible for payment for products not accepted for warranty adjustment handling costs and freight costs associated therewith Notwithstanding th
29. d instrument calibration to NIST traceable standards A certificate of calibration is issued from AZI when your instrument 1s factory calibrated For scheduling and shipping authorization call AZI Customer Service at 800 528 7411 or 602 470 1414 or visit our website at www azic com Verification of Functionality The Functional Test Kit FTK AZI P N Y431 0902 is used to verify that your instrument is functioning correctly between recommended annual factory calibrations It allows you to have complete confidence in the sample results This test verifies proper instrument operation through the introduction of a known concentration of mercury vapor into the J erome analyzer THIS IS A FIELD CHECK OF THE FUNCTIONALTTY OF THE INSTRUMENT THIS TEST DOES NOT CALIBRATE THE INSTRUMENT If your application requires frequent verification of instrument function this test demonstrates the instrument s proper operation and function Recording FTK results in an instrument log provides a quality control quality assurance record of instrument function between regular calibrations If test results fall within the expected range you may assume the instrument is functioning correctly See APPENDIX B J405 FUNCTIONAL TEST KIT on page 56 for more information about the FTK procedures Complete instructions for use are supplied with the test kit AZI P N Y431 0902 To order the FTK contact your AZI Sales Representative at 800 528 7411 or 602 47
30. d operation PART COMPONENT MAINTENANCE CYCLE ee Clare batten Depends on usage See Battery Management Page 28 section for guidelines Change 25 inch fritware Weekly or as needed Page 33 Change AG Filter Every 500 samples Page 34 35 se ae ees aid After 6 months of use or as needed Page 35 Replace Zero Air Filter Annually Factory calibration Annually Page 37 Functional check Monthly or as needed Appendix B Page 56 Annually or as needed Replace battery The battery pack contains NIMH batteries Page 36 Please dispose of properly FUSE The J405 utilizes an auto resetting fuse that does not require care maintenance or replacement by the user If the fuse is tripped by electrical power anomalies it will automatically reset itself once it detects that electrical power conditions have returned to normal AG filters contain Sofnolime For safety information see the supplier s Material Safety Data Sheet MSDS or call AZI Customer Service at 800 528 7411 or 602 470 1414 or e mail support azic com for a copy Dispose of all filters properly Zero Air Filters and scrubber filters contain Resisorb For safety information see the supplier s Material Safety Data Sheet MSDS or call AZI Customer Service at 800 528 7411 or 602 470 1414 or e mail support azic com for a copy Dispose of all filters properly AZI Customer Service 800 528 7411 or 602 470 1414 Page 32 of 63 The Jerome J405 s flow system is the
31. e Print echo 3 If HyperTerminal has not been run previously on the target PC it will ask for an area code etc Enter that information as appropriate and click OK AZI Customer Service 800 528 7411 or 602 470 1414 Page 51 of 63 4 Next a window labeled Connect To will be displayed Find the last dropdown list in the dialog box labeled Connect using Select the last COM port from the list and click OK J405 HyperTerminal Sele Connect To Enter details for the phone number that you want to dial Country region United Y Area code 602 Connect using COM e COM COM TCP IP ingack Auto detect Auto detect SCROLL CAPS NUM Capture Print echo 5 Next HyperTerminal will prompt for Port Settings These settings do not apply to USB ports so the default values do not need to be changed Continue by clicking OK 4405 HyperTerminal Sele Da ss 28 COM3 Properties Port Settings Bits per second bli 1 Flow control Hardware yr yr A Restore Defaults k Apply Auto detect Auto detect SCROLL CAPS NUM Capture Print echo AZI Customer Service 800 528 7411 or 602 470 1414 Page 52 of 63 6 A blank HyperTerminal screen will be displayed On the status bar in the lower left hand corner it should say Connected J405 HyperTerminal File Edit View Call Transfer Help De pg 2 Auto detect Auto detect SCROLL CAPS NUM Capture Printecho
32. e and must be powered by an external 12 V DC power supply An example setup 1s shown below pin19 pin20 e CIO gt co 8 o O GROUND 1 8th Amp fuse 4 20mA Readout a e SCADA Port 12 Volts DC POWER SUPPLY In this example the 5 522mA current level displayed above would correspond to a Hg concentration of 47 56 ug m After configuring your system the J405 Diagnostics feature can be used to test your setup When the 4 20mA test portion of the diagnostics is reached the instrument will output current levels of 4 8 12 16 and 20mA and the current level displayed on the J405 should match the readout of your 4 20mA system See SYSTEM menu for additional info on running the diagnostics feature After confirming that the system is configured correctly use the instrument as normal and the 4 20mA signal will be output automatically by the J405 The 4 20mA output is accurate to within 0 3 of the output AZI Customer Service 800 528 7411 or 602 470 1414 Page 31 of 63 6 MAINTENANCE Preventive Maintenance Schedule To keep the Jerome J405 operating at peak performance follow the maintenance schedule below as a guide Since maintenance 1s more a function of application and amount of use rather than time your requirements may be different from the listed schedule Call AZI Customer Service at 800 528 7411 or 602 470 1414 or e mail support azic com for additional guidance for your environment an
33. e foregoing no warranty shall be enforceable in the event that product has been subjected to environmental or stress testing by buyer or any third party without written approval of seller prior to such testing Further no warranty shall be enforceable if the alleged defect is found to have occurred because of misuse neglect improper installation repair alteration accident or improper return handling procedure by buyer Discontinued product is warranted only for a credit or replacement at seller s option THE EXPRESS WARRANTIES GRANTED ABOVE SHALL EXTEND DIRECTLY TO BUYER AND NOT TO BUYER S CUSTOMERS AGENTS OR REPRESENTATIVES AND EXCEPT FOR WARRANTY OF TITLE IS IN LIEU OF ALL OTHER WARRANTIES WHETHER EXPRESSED OR IMPLIED INCLUDING ANY IMPLIED WARRANTIES OF FITNESS FOR A PARTICULAR PURPOSE AND MERCHANTABILITY SUCH OTHER WARRANTIES BEING SPECIFICALLY DISCLAIMED BY SELLER IN NO EVENT SHALL EITHER PARTY S LIABILITY FOR ANY BREACH OR ALLEGED BREACH OF THIS AGREEMENT EXCEED THE TOTAL EXTENDED PRICE OR PRICES SHOWN ON UNFILLED ORDERS NOR SHALL EITHER PARTY BE LIABLE FOR ANY SPECIAL INCIDENTAL OR CONSEQUENTIAL DAMAGES RESULTING FROM BREACH OR ALLEGED BREACH Notwithstanding the foregoing if any product covered by order s placed hereunder is designated as developmental prototype or experimental no warranty whatsoever except a warranty of title to component materials will be applicable thereto and buyer shall indemnify se
34. e functioning properly The USB icon will flash during data transmission See J405 Main Screen Display on page 12 for the location of the USB icon The data is stored in non volatile memory and will not be affected if the battery is changed or disconnected SEND TO PC Before using SEND TO PC the USB driver must be installed on the target PC and HyperTerminal must be configured on the target PC The USB driver is on the CD with this operations manual and on the AZI website at www azic com See APPENDIX A USB HYPERTERMINAL SETUP on page 46 for detailed instructions on installing the USB driver configuring HyperTerminal and downloading data from the J405 Once the target PC has been configured connect the included USB A to B cable AZI P N 200 0165 between the USB TYPE B PORT on the back panel of the J405 and the USB PORT of the target computer and launch HyperTerminal On the J405 with SEND TO PC highlighted press ENTER START and all of the stored data on the J405 will be transmitted to the target computer as a comma delimited text file See Retrieving Data on page 29 for more information AZI Customer Service 800 528 7411 or 602 470 1414 Page 18 of 63 SAVE TO USB DRIVE Before selecting SAVE TO USB DRIVE connect the target USB memory drive to either USB TYPE A PORT on the back panel of the J405 When ENTER START is pressed all of the stored data on the J405 will be transmitted to the target drive as a comma delimited te
35. e used The time and date will need to be reset when the battery is reconnected for instrument use See SYSTEM menu on page 19 for instructions If the instrument will be in storage for more than 4 months it will need to be taken out of storage and fully charged every 4 months before being placed back in storage To do so reconnect the battery and connect the AC power supply charger to charge the instrument for a minimum of 3 hours See Charging Internal Battery on page 28 for charging instructions After charging disconnect the battery before returning the instrument to storage Again the time and date will need to be reset if the battery is reconnected so the instrument can be put into service Sample data is stored in non volatile memory and will not be lost or affected when the battery is disconnected or replaced An optional external battery pack AZI P N 990 0214 is available to power the J405 but it is not recommended for routine use The external battery pack should be reserved for sensor regenerations or sampling when the internal battery is nearly discharged and AC current for recharging the internal battery pack is unavailable The external battery pack will not recharge the J405 s internal battery pack The external battery pack 1s recharged by connecting the J405 s AC power supply charger between an AC outlet and the female DIN connector on the external battery pack The green LED on the external battery pack will
36. er u g m or milligrams per cubic meter mg m of mercury AZI Customer Service 800 528 7411 or 602 470 1414 Page 10 of 63 The instrument s microprocessor automatically re zeroes the digital meter at the start of each sample cycle and holds the meter reading until the next sample cycle is activated thus eliminating drift between samples During the sample mode cycle a sensor saturation meter on the LCD represents the percentage of sensor saturation or adsorbed mercury collected on the gold film With use the sensor becomes saturated and needs to be cleaned This is accomplished by a manually activated 45 minute sensor regeneration cycle which removes the mercury from the sensor The solenoid bypass closes during the sensor regeneration cycle causing the air to pass through the scrubber filter providing clean air for the regeneration process The closed loop film heat cycle ensures the sensor is cleaned to original values The mercury released during regeneration is absorbed by the flow system s final scrubber filter AZI P N Z2600 3930 to prevent any external contamination from the desorbed mercury The 45 minute regeneration process includes a cool down phase so the instrument is ready for use as soon as the regeneration process finishes Zero Air Filter AZI P N Z2600 3905 The Zero Air Filter AZI P N Z2600 3905 removes mercury vapor mercaptans and hydrogen sulfide from the air sample Readings with the filter installed shou
37. ess ENTER START to proceed or ESC to exit The instrument will now begin a 45 minute regeneration cycle indicated by Regeneration in Progress on the display Do not interrupt this cycle For a complete description of this process see page 23 If any error message appears on the display see the Troubleshooting section beginning on page 38 e Ensure the instrument has been powered on for at least five 5 minutes prior to sampling e The instrument is now ready to sample SAMPLE bp BUTTON gt gt gt gt gt gt e Press the SAMPLE BUTTON at the end of the handle of the J405 to start a 12 second sampling cycle e When the instrument measures mercury vapor the 0 00 1g m display will be replaced with a value e To ensure the input to the instrument contains no mercury vapor or mercaptans use a Zero Air Filter AZI P N Z2600 3905 The Zero Air Filter cleans the air sample and should produce sample readings of 0 00 g m Therefore use the filter to gt Equilibrate the instrument to temperatures that are higher or lower than the instrument Sample every 15 seconds with the filter installed until the reading is 0 00 g m gt Identify contamination within the unit gt Confirm the presence of mercury vapor when readings are elevated Install the filter and verify that the readings decrease with the filter installed The instrument is designed for ambient air monitoring WARNING DO NOT allow the probe or
38. for the last three 1cc injections should be within 5 of each other e Refer to the J405 FTK Instrument Response Chart below for the acceptable range gt The average of the last three readings should fall within the range shown on the chart If the average is within range the JEROME J405 is functioning properly e If the last three readings are not within 5 of each other gt Perform sensor regeneration Refer to page 23 for the complete sensor regeneration procedure Wait 1 hour before proceeding to the next step Repeat the mercury injection test procedure If the average of the last three readings is still not within range refer to the section on Functional Test Troubleshooting below J405 FTK Instrument Response Chart VV V AZI Customer Service 800 528 7411 or 602 470 1414 Page 60 of 63 Functional Test Troubleshooting If you do not achieve good results with the functional test procedure check the following Typically too high Ensure the FTK vessel temperature is stable Ensure syringe is calibrated to Icc Use a new syringe needle Straighten or replace crimped or blocked internal tubing Be sure to inject the Hg vapor ONLY after Purging disappears from the display approximately 2 seconds after SAMPLE is pressed Ensure there is no oxidation on the mercury drop in the vessel Too Low Gently swirl the mercury drop in the vessel Replace if necessary Ensure the instrument s intake 1s not blo
39. ge needle from the septum NOTE Perform the functional test ONLY after sensor regeneration A Allow the FTK vessel to remain stable at room temperature for at least 2 hours gt The temperature range for the test is 16 C 24 C gt Temperature fluctuations during the test procedure will produce erratic results Replace the 25 fritware gt Refer to page 33 for instructions Replace the septum on the septum holder assembly Plug the tubing adapter end of the septum assembly firmly into the instrument s intake Attach a Zero Air Filter to the septum assembly Press power ON Take 3 samples gt Ifthe average meter reading is greater than 2 ug m stop here The instrument may be contaminated See J405 TROUBLESHOOTING on page 38 gt Ifthe average meter reading is less than 2 g m continue to the next step Note the temperature of the vessel Press the SAMPLE button and Sampling and Purging will appear on the instrument display Wait 2 seconds and when Purging disappears from the display inject 1 cc of mercury vapor according to the syringe technique described on page 58 Be sure all mercury vapor has been injected before the solenoid closes CAUTION Carefully follow these instructions to minimize error Record the meter reading AZI Customer Service 800 528 7411 or 602 470 1414 Page 59 of 63 e Repeat the instructions for mercury injection three more times gt The readings obtained
40. gnostic check I O should not be used during the diagnostics because I O will power off the instrument and ESC should only be used when specifically indicated by the instrument e When testing the keypad follow the on screen prompts to press each of the keys in turn The J405 will not indicate a pass fail for this test Instead if all of the keys work and the instrument proceeds to the next diagnostic test the keypad diagnostic has passed e When testing 80V power press ENTER START to pass the test and proceed to the next test Pressing ESC will stop the test and return a Fail e If the 4 20mA output function of the J405 is not in use press ENTER START to cycle through the 4 8 12 16 and 20mA checks in the diagnostic routine If the 4 20mA output is in use the diagnostics can be used to verify proper operation Refer to 4 20mA Output on page 30 for more information After the last diagnostic result has been displayed the instrument will display Done and pressing any key will return to the main screen of the J405 AZI Customer Service 800 528 7411 or 602 470 1414 Page 21 of 63 Daily Operations Before each day s use of the Jerome J405 perform the following steps to verify proper instrument operation e Press the power I O button gt The display will light up and show instrument serial number and software revision gt If necessary press ESC to clear any calibration reminders Call AZI Customer Service at 800 528 7411 or
41. he alarm level has been set press ENTER START to select the highlighted alarm level as the current alarm level to be used Upon returning to the SET ALARM LEVELS screen there will be asterisk next to the currently selected alarm level either high or low It is recommended to set the alarm level higher than 0 5 ug m The alarm can be muted using AUDIBLE ALARM ON OFF in the SYSTEM menu AUDIBLE ALARM ON OFF Use the Aand Y arrow keys to toggle the audible alarm on or off and use ENTER START to save the desired setting Press ESC to exit without saving changes The main screen display has a sound icon that indicates if the alarm is currently turned on or muted The action lines in front of the sound icon will disappear when the audible alarm is muted See J405 Main Screen Display on page 12 to locate the sound icon DISPLAY MODE From the DISPLAY MODE screen use the Aand Y arrow keys to toggle between Threshold and Scientific display modes and press ENTER START to save the setting In Scientific display mode the J405 displays the sample reading for every sample taken In Threshold display mode the sample reading must be within 85 of the set alarm level to be displayed Results below 85 of the alarm level value will be displayed as 0 00 g m instead Use ESC to exit without saving See SET ALARM LEVELS above to set Threshold limits VIEW SENSOR STATS Use VIEW SENSOR STATS to display the current saturation level of the sensor the number
42. he labeled items SOUND ICON SYSTEM TIME BATTERY SYSTEM DATE AUTO SENSOR E SAMPLING SATURATION gt INDICATOR METER tence aan USB ICON MERCURY y E aE E boa READING PE Pe E 88 886 8 4ean UNITS in a FM E LL w EA ARDE PENITA wel en PATEAR eo le g eel ve Pick ASE pede b Ese e ak AVAILABLE KEYPAD COMMANDS SYSTEM TIME As set in the SYSTEM menu See SYSTEM menu on page 19 BATTERY Indicates current charge level and charging status See Charging Internal Battery on page 28 SOUND ICON Indicates if the audible alarm is turned on or muted as set in the SYSTEM menu See SYSTEM menu on page 19 SYSTEM DATE As set in the SYSTEM menu See SYSTEM menu on page 19 SENSOR SATURATION METER Graphically indicates mercury saturation level of J405 sensor See REGEN menu on page 17 USB ICON Indicates proper functioning of USB ports and flashes during USB transmission of data See Retrieving Data on page 29 If the USB icon is not present this option is not activated Contact your AZI Sales Representative for details on the USB option AUTO SAMPLING INDICATOR Indicates if the J405 is set to sample automatically at regular intervals as set in Sample Mode in the SAMPLE menu See SAMPLE menu on page 15 MERCURY READING The mercury concentration detected by the J405 in the units indicated UNITS Units of mercury concentration reading either micrograms per cubic meter 1g m or milligrams per cubic
43. he new battery by connecting it to the battery connector and sliding it into the J405 Tuck any excess cabling into the gap between the battery and the case Replace the battery panel and secure with the four 4 screws removed above Dispose of the old nickel metal hydride NiMH battery in accordance with state and federal regulations After battery replacement the date and time will need to be updated See the SYSTEM menu on page 19 for directions Sample data is stored in non volatile memory and will not be lost or affected when the battery is disconnected or replaced WM MU ad E y i ae E BATTERY Page 36 of 63 we CALIBRATION Factory Calibration Service The Jerome J405 s gold film sensor is inherently stable and does not require frequent calibration The interval between calibrations depends upon the application and frequency of use however the recommended interval is every 12 months The Jerome J405 has been factory calibrated using laboratory equipment containing NIST traceable permeation tubes In order to calibrate the Jerome J405 a sophisticated calibration system is required that ensures stability of the calibration gas source eliminates any pressure in the calibration gas stream and controls the temperature of the calibration environment We strongly recommend you take advantage of our calibration and maintenance service at Arizona Instrument Service includes filter replacement component testing an
44. impair or destabilize the correct operation of your system either immediately or in the future Microsoft strongly recommends that you stop this installation now and contact the hardware vendor for software that haz passed Windows Logo testing Continue Anyway STOF Installation AZI Customer Service 800 528 7411 or 602 470 1414 Page 49 of 63 9 Windows will copy a file and finish the wizard Click Finish Found Hew Hardware Wizard Completing the Found New Hardware Wizard The wizard has finished installing the software hor F Communications Port Click Finish to close the wizard 10 Windows will then indicate that the driver has been successfully installed w i Found New Hardware Your new hardware is installed and ready to use 4 04 A Thursday 7i 200E AZI Customer Service 800 528 7411 or 602 470 1414 Page 50 of 63 Using HyperTerminal to receive data from the J405 1 Start HyperTerminal Start gt All Programs gt Accessories gt Communications gt HyperTerminal If prompted to make HyperTerminal the default telnet application click No 2 When prompted for a name for this connection enter J405 and click OK El New Connection HyperTerminal File Edit View Call Transfer Help Connection Description New Connection Enter a name and choose an icon for the connection Mame J405 cor Disconnected Auto detect Auto detect SCROLL CAPS NUM Captur
45. ion from the list for the samples to be taken use the Aand VW arrows to scroll to the desired location and press ENTER START twice Note the asterisk located to the left of the currently selected location The selected location name will be stored with the sample data for all samples taken until a different location 1s selected instead After deleting data it is necessary to re select the Location Name before taking any samples otherwise the location will not be recorded Use ESC to return to the sample menu See Retrieving Data on page 29 for more info SURVEY MODE Highlight SURVEY MODE in the SAMPLE menu and press ENTER START to begin immediate sampling in survey mode In survey mode after an initial two second pause to purge the flow system the J405 will sample continuously For complete information on survey mode see Survey Mode on page 25 AZI Customer Service 800 528 7411 or 602 470 1414 Page 16 of 63 The sensor saturation meter on the main screen to the right of s sat indicates the current level of saturation of the sensor with mercury Clean Regenerated Sensor Saturated Sensor Regen Required When the sensor becomes saturated with mercury as indicated by the sensor saturation meter a regeneration regen must be performed on the sensor to release the accumulated mercury before additional samples can be taken See Sensor Regeneration on page 23 for more information on the regen procedure The AC power supply
46. jack cigarette lighter and draw power directly from the battery of a vehicle The Car Accessory Cable can be used for sensor regeneration or sampling when the internal battery pack 1s nearly discharged and AC current for recharging the internal battery pack 1s unavailable The Car Accessory Cable will not recharge the J405 s internal battery pack In order to use the external battery pack or the Car Accessory Cable the J405 s internal battery pack must be installed in the instrument If the internal battery pack 1s disconnected or removed neither of these accessories will be able to provide power to the instrument To order either of these accessories or for additional information call AZI Customer Service at 800 528 7411 602 470 1414 or e mail supportO azic com _Charging Internal Battery e The internal battery needs to be charged if the battery indicator icon on the main screen is empty and flashing e Connect the AC power supply charger between the J405 power receptacle and an AC power source e The battery icon will flash during charging and show as half full until fully charged gt Complete battery recharging takes 3 hours gt The J405 contains a trickle charger so it may be continually plugged into an AC power source without damaging the battery pack CH mI Flashing Icon Battery Partially Full Battery Fully Charged Battery Needs to be Charged if Flashing Battery is Charging if Flashing Battery is Charging
47. ld be near 0 00 g m For maximum accuracy wait 15 seconds between samples to allow the sensor to restabilize Because air that is cooler than the instrument will cause low readings and warmer air will cause higher readings the Zero Air Filter should be used to equilibrate the instrument to ambient air Repeated sampling with clean air will not cause saturation of the gold film sensor but will equalize temperatures faster to allow accurate analysis to begin sooner For maximum accuracy wait 15 seconds between samples to allow the sensor to restabilize The Zero Air Filter can also be used to identify contamination within the instrument If the readings do not reduce to near 0 00 ug m with the filter installed contamination should be suspected Ifthe readings do drop to near 0 00 ug m with the filter installed but elevate with the filter removed the presence of mercury vapor at the sampled location is confirmed Again for maximum accuracy wait 15 seconds between samples to allow the sensor to restabilize The Zero Air Filter should be inserted into the intake of the instrument when running the instrument Warm up See Warm up in the section REGEN menu on page 17 for more information For more information on the use of the Zero Air Filter contact customer service at 1 800 528 7411 or 602 470 1414 AZI Customer Service 800 528 7411 or 602 470 1414 Page 11 of 63 The J405 Main Screen is depicted below followed by explanations of t
48. light up during charging of the external battery pack and then go out once the external battery pack is fully charged this takes approximately 4 hours The red LED on the external battery pack will only light up if there is a battery fault or error Should this occur call AZI Customer Service at 800 528 7411 602 470 1414 or e mail support azic com for additional information If the AC power supply charger is connected to the external battery pack while the external battery pack 1s connected to the J405 both the J405 and the external battery pack will be recharged AZI Customer Service 800 528 7411 or 602 470 1414 Page 27 of 63 When operating using the external battery pack the J405 will shut down after twenty 20 minutes of non usage However if the instrument is running in Survey Mode or Auto Sampling mode the instrument will not shut off after twenty minutes If the J405 is reading low levels of mercury in Survey or Auto Sampling mode it will continue to sample until the battery runs out However if the J405 is reading high levels of mercury in Survey mode when the sensor reaches saturation a message will appear indicating that sensor regeneration 1s required and twenty minutes later the instrument will automatically power off In Auto Sampling mode the instrument will regen automatically when the sensor is saturated Additionally using the optional Car Accessory Cable AZI P N 200 0170 the J405 may be powered from a car accessory
49. ller for any claims for liability asserted seller in connection therewith The foregoing state the entire liability of seller in connection with products supplied hereunder AZI Customer Service 800 528 7411 or 602 470 1414 Page 62 of 63 TRADEMARK AND COPYRIGHT PROTECTION Jerome Arizona Instrument AZI and the stylized AZI are all registered trademarks of Arizona Instrument LLC Instrument firmware is copyright protected All specifications subject to change without notice Copyright 2006 2010 Arizona Instrument LLC All Rights Reserved Sofnolime is a trademark of Molecular Products Limited Resisorb is a registered trademark of Mallinckrodt Baker Inc Tygon is a registered trademark of Saint Gobain Performance Plastics Corporation Arizona Instrument LLC Jerome J405 Mercury Vapor Analyzer Operation Manual Part Number 700 0099 H June 2010 If you have any questions regarding the operation of this instrument please call our toll free number 800 528 7411 Internationally call 602 470 1414 or fax 480 804 0656 Arizona Instrument LLC 3375 N Delaware Street Chandler AZ 85225 800 528 7411 602 470 1414 Fax 480 804 0656 http www azic com email az1O azic com General intl azic com International support azic com Customer Support AZI Customer Service 800 528 7411 or 602 470 1414 Page 63 of 63
50. lt selection is u g m and u g m is used throughout this manual for consistency The relationship between u g m and mg m 1s as follows 1000 ug m mg m and 1 ug m 0 001 mg m SET SAMPLE INTERVAL If auto sampling 1s being used as set in SAMPLE MODE above the sample interval determines how often the J405 will automatically take samples Use the Aand Y arrow keys to scroll through the available sample intervals of 1 2 5 10 15 30 45 60 90 and 120 minutes and use ENTER START to save the selected interval Use the ESC key to exit without saving changes The sample intervals refer to specific times on the instrument clock as measured in whole multiples of the selected interval For example selecting a 10 minute sample interval will result in samples being taken on the hour 10 minutes after the hour 20 minutes after the hour etc not every ten minutes from when auto sampling is initiated Refer to the chart on the next page for examples of how these intervals work When the clock reads 00 seconds at the appropriate time the sample will be taken AZI Customer Service 800 528 7411 or 602 470 1414 Page 15 of 63 Interval Samples on the Examples 1 minute 1 minute marks 12 00 12 01 12 02 12 03 12 04 12 05 12 06 etc 2 minutes 2 minute marks 12 00 12 02 12 04 12 06 12 08 12 10 12 12 etc 5 minutes 5 minute marks 12 00 12 05 12 10 12 15 12 20 12 25 12 30 etc 10 minutes 10 minute marks 12 00 12 10 12 20
51. ment can damage the sensor and flow system Ensure the instrument has been powered on for at least five 5 minutes prior to sampling For maximum accuracy wait 15 seconds between samples to allow the sensor to restabilize The Jerome J405 operates a minimum of 24 hours on a fully charged battery Use the probe AZI P N 1400 2002 to locate mercury vapor in hard to reach places Plug the probe directly into the instrument s intake e Accessing the menus during sampling can corrupt current sample data and should be avoided AZI Customer Service 800 528 7411 or 602 470 1414 Page 24 of 63 Survey Mode The survey mode takes samples and displays the result every 2 seconds automatically Use this mode to locate mercury spills or to assess areas of potentially high mercury concentrations Sampling in the survey mode is not as accurate e Press the power I O button The display will light up and show the instrument serial number and software revision gt If necessary press ESC to clear any calibration reminders gt Next the digital meter displays 0 00 g m If the battery meter is empty and flashing recharge the battery See Charging Internal Battery on page 28 gt Toensure the instrument s electronics have stabilized allow a 5 minute warm up before beginning the next step From the Main Screen press to enter the Main Menu From the Main Menu select the Sample menu Scroll through the Sample menu to Survey Mode Press ENTER START
52. meter mg m as set in the SAMPLE menu AVAILABLE KEYPAD COMMANDS The bottom line of the screen indicates the currently available keypad commands From the main screen as shown here the Main Menu can be accessed using the gt key AZI Customer Service 800 528 7411 or 602 470 1414 Page 12 of 63 DB25 CONNECTOR POWER CONNECTOR USB TYPE A PORTS EXHAUST PORT USB TYPE B PORT The above labeled connections are available from the back panel of the J405 If the USB option has not been activated the USB ports will not be present Contact your AZI Sales Representative for information on the USB option POWER CONNECTOR Connect the supplied AC power supply charger the optional external battery pack AZI P N 990 0214 or the optional car accessory jack AZI P N 200 0170 here to provide power to the instrument or to recharge the battery USB TYPE A PORTS The USB Type A ports are used to connect a USB printer or USB memory drive for printing or saving sample data The two ports are identical and either can be used For more information see DATA menu on page 18 USB TYPE B PORT The USB Type B port is used to connect the J405 directly to the USB port of a computer using the included USB A to B cable AZI P N 200 0165 For more information see DATA menu on page 18 DB25 CONNECTOR There are multiple specialized uses for the DB25 connector See Instrument I O Interface on page 30 f
53. models e 3 inch 9 cm backlit display showing everything you need to be confident in the instrument including 5 8 inch 1 6 cm tall character readout battery life indicator and sensor saturation percentage e Choice of units for results micrograms per cubic meter u g m default or milligrams per cubic meter mg m Easy to understand diagnostic and error detection Auto zero bridge adjustment Updated electronics including 24 bit a d conversion and 512 MB on board memory Controlled temperature film heat ensures the sensor removes all mercury and returns to its original state e The Jerome J405 can be operated for 24 hours from the internal 12V battery source or it can be operated using the external AC power supply charger Accessories and Maintenance Parts The Accessories and optional items available to support the J405 are listed and pictured beginning on page 41 AZI Customer Service 800 528 7411 or 602 470 1414 Page 7 of 63 Applications Regulatory detection compliance Regulatory clean up compliance Ambient air analysis Quality control Scrubber efficiency testing Accuracy check for other mercury vapor monitors and control systems Mercury vapor source detection Leak detection Portable mercury vapor detection The J erome J405 is operated from an internal 12V battery source For charging the batteries an external AC power supply charger 1s included AZI Customer Service 800 528 7411 or 602 470
54. n Battery Fault Disconnect and re connect the AC power supply charger to the J405 Sensor Regeneration Sensor is saturated with Perform Sensor Regeneration See Required mercury page 23 AZI Customer Service 800 528 7411 or 602 470 1414 Page 39 of 63 Potential Interferences a Potential interferences to the Jerome mercury vapor analyzers are rare and most of these can be eliminated with proper maintenance procedures However erroneously high readings can sometimes occur Here are a few things to be aware of when using the instrument The gold film sensors used in the J erome mercury vapor analyzers do not respond to the following compounds e Hydrocarbons e CO COs and SO e Water vapor Note that water vapor condensation on the gold film can cause irreparable harm to the sensor and must be avoided The AG filter AZI P N 600 0293 an acidic gas filter contained in the internal filter system removes the following compounds that cause the gold film sensor to respond Chlorine NO Hydrogen Sulfide H2S Most mercaptans organic sulfur compounds or thiols In areas containing these highly volatile compounds the filter can quickly become saturated In such situations it is recommended that these gases be allowed to dissipate before sampling for the less volatile more persistent mercury vapor In addition a special filter designed to remove chlorine gas from the sample stream is available from
55. n use of the I O port The 4 20 mA output can be used to indicate the Hg reading level on a proportional scale from 4 20 milliamps for connection to certain industrial systems such as SCADA A 4 mA current level always corresponds to a Hg reading of 0 5 u g m or less while a 20 mA current level always corresponds to a Hg reading of 500 u g m Current levels between 4 and 20 mA correspond to Hg readings between 0 5 and 500 u g m on a proportional scale as determined by this equation current in mA 4 X 500 Hg concentration detected Ol gt gt Mercury levels above 500 g m will also result in 20mA current readings The relationship between the Hg concentration detected and the current level present can be represented graphically as follows 4 20mA Output Level Response in mA Hg concentration detected ug m If the J405 is operating with the internal battery disconnected and loses AC power the J405 s 4 20mA circuit will continue to output the last current value as long as power to the external current loop is maintained AZI Customer Service 800 528 7411 or 602 470 1414 Page 30 of 63 To utilize the 4 20mA output connect the positive wire of your 4 20mA system to pin 19 of the VO port on the J405 and the negative wire to pin 20 The number of each pin of the I O port is labeled on the port itself and the locations of pins 19 and 20 can also be seen in the diagram below The 4 20 mA connection is passiv
56. nd accuracy at 25 u g m and 100u g m may change from 5 to 7 RSD is unchanged AZI Customer Service 800 528 7411 or 602 470 1414 Page 9 of 63 The heart of the J405 is the well proven gold film sensing technology A thin gold film in the presence of mercury vapor undergoes an increase in electrical resistance proportional to the mass of mercury vapor in the sample When the SAMPLE button is pressed an internal pump pulls ambient air through a scrubber filter AZI P N 600 0262 and into the flow system Intake gt lt f Scrubber Scrubber Gold Film Sensor Acidic f Pump Gas Sample Filter Solenoid Closed After 2 seconds the sample solenoid bypass opens closing off the scrubber filter from the flow system Intake Scrubber f N J A Scrubber Gold Film Sensor Acidic Pump Gas Filter Solenoid Open The sample air passes through the AG filter AZI P N 600 0293 an acidic gas filter that removes any acidic gases that interfere with the sensor s response to mercury Then the sample air is drawn over the gold film sensor The sensor adsorbs the mercury vapor Nine seconds after starting the sample solenoid bypass closes and the remainder of the sample is drawn through the scrubber filter and the flow system The instrument determines the amount of mercury adsorbed and displays the measured mercury concentration on the digital meter in micrograms per cubic met
57. not only ensure the instrument is ready when needed but will also extend the life of the battery There are 3 different battery management methods recommended based on the frequency of instrument use An additional option to ensure the instrument is ready to go at a moment s notice 1s to purchase an AZI external battery pack AZI P N 990 0214 See External Battery Power on page 27 for more information on the External Battery Pack High Frequency user Daily and weekly usage For this type of user the instrument should be plugged in anytime the instrument is not being used AZI Customer Service 800 528 7411 or 602 470 1414 Page 26 of 63 Medium Frequency user Once per month usage For this type of user the instrument should be plugged in for a minimum of three 3 hours prior to use Otherwise the instrument can be left unplugged Infrequent user Greater than one month between uses or long term storage For this type of user the instrument should be fully charged and the battery should be disconnected Discomnect the battery by removing the front 2 screws near the intake and opening the instrument On the front most part of the main circuit board there 1s a black 4 pin connector as shown here Depress the safety latch on the connector and pull it out to disconnect the battery Close the instrument and replace the 2 screws in the front of the instrument Reverse these steps to reconnect the battery if the instrument is going to b
58. nu Press the DOWN arrow button V to move the cursor to System Press the RIGHT arrow button P to select System Press the DOWN arrow button V to move the cursor to View Sensor Stats Press ENTER START to select View Sensor Stats on the System menu The screen will display Sensor samples on the last line After changing the AG filter accuracy at 1 0 u g m may change from 10 to 20 and accuracy at 25 u g m and 100 u g m may change from 5 to 7 RSD is unchanged CAUTION Internal filters contain either Sofnolime or Resisorb Used filters will contain trace amounts of Mercury also Use proper methods when disposing of used filters Call AZI Customer Service at 800 528 7411 602 470 1414 or e mail support azic com for a copy of the Sofnolime or Resisorb MSDS or for other questions AZI Customer Service 800 528 7411 or 602 470 1414 Page 34 of 63 Internal Filters Part Number 1 Scrubber Filter 1 elbow 1 straight barb Z2600 3930 2 Scrubber Filter 2 elbow barbs 600 0262 3 AG Filter 600 0293 Internal Filters Replace the internal filters after six 6 months of use or as needed gt The AG filter should be replaced every six 6 months or every 500 samples whichever comes first based on your instrument usage schedule Press the I O button to turn the power OFF and unplug the power cord Remove the two 2 side screws from the intake end of the instrument and open the case Carefully disconnect
59. of regenerations performed on the sensor and the total number of samples read by the sensor Press any key to exit the screen when finished SET SYSTEM TIME The J405 maintains the system time using a 24 hr clock format Use the Aand V arrow keys to change the value in the field where the cursor is flashing Use the and gt arrow keys to move between the two digits within the hour or minute fields and use the A and B keys to switch between the hour and minute fields Use ENTER START to save the indicated time as the system time or ESC to exit without saving AZI Customer Service 800 528 7411 or 602 470 1414 Page 20 of 63 SET SYSTEM DATE Use the Aand W arrow keys to change the highlighted field and the lt and gt arrow keys to move between characters within the day or year fields Use the A and B keys to move between the day month and year fields Press ENTER START to save the system date or ESC to exit without saving RUN DIAGNOSTICS Selecting RUN DIAGNOSTICS will start the J405 s self diagnostic procedure As the instrument proceeds through each diagnostic check follow the on screen prompts and the instrument will display the specific check being performed and the pass fail result of the check If the check is not applicable to the current configuration of the instrument the result field will be blank instead of indicating pass or fail e After viewing each result press any key except I O or ESC to move to the next dia
60. or more information NOTE This is not a printer port EXHAUST PORT After sampling the sampled air is cleaned of any mercury and expelled from the exhaust port on the back of the J405 AZI Customer Service 800 528 7411 or 602 470 1414 Page 13 of 63 J405 User Interface Main Menu Structure NOTE The main menu also contains a selection labeled Factory This option 1s for AZI factory use only and is not accessible by the end user AZI Customer Service 800 528 7411 or 602 470 1414 Page 14 of 63 SAMPLE menu SAMPLE MODE The Sample Mode setting provides the choice between auto sampling and manual sampling For normal use use manual sampling which is the instrument default setting If auto sampling 1s selected the instrument will automatically sample at the interval set in SET SAMPLE INTERVAL below without monitoring or attendance by the user Use the Aand Y arrows to toggle between Manual and Auto and use ENTER START to save the selection Use the ESC key to ex1t without saving changes If auto sampling 1s selected the word Auto will appear below the system date on the instrument s main screen UNITS Sample results can be displayed in micrograms per cubic meter ug m or milligrams per cubic meter mg m To change the displayed units select UNITS from the SAMPLE menu Use the Aand Y arrows to toggle the selection and press ENTER START to save the selection Use the ESC key to exit without saving changes The defau
61. r is the mercury vapor concentration in g m gt This sampled mercury value remains on the display until the next sample is taken gt The digital meter automatically re zeroes at the start of each sample e At the end of each day s use perform sensor regeneration as described in the next section DO NOT ALLOW MERCURY VAPOR TO STAY ON THE GOLD FILM SENSOR OVERNIGHT AZI Customer Service 800 528 7411 or 602 470 1414 Page 22 of 63 Sensor Regeneration Sensor regeneration is needed to clean the J405 sensor of any accumulated mercury vapor and to prolong the life of the sensor This simple procedure should be done e At the beginning of the day on which the instrument is to be used e During the day when the sensor becomes saturated e At the end of the day before storing the instrument e Ata minimum of 30 day intervals while the instrument is in storage To perform sensor regeneration e Plug the AC power supply charger or the external battery pack into the back of the instrument e Press the power I O button to power on the instrument e If necessary press ESC to clear any calibration reminders Call AZI Customer Service at 800 528 7411 or 602 470 1414 or e mail support azic com to schedule instrument calibration From the Main Screen press the RIGHT arrow button gt to enter the main menu Press the DOWN arrow button Y to move the cursor to Regen Press the RIGHT arrow button to select Regen from the menu
62. s and the life of your instrument Read and refer to the manual for complete details on operation maintenance and troubleshooting special voltage inputs and data output The Jerome J405 is easy to operate and ready for use upon receipt from the factory e Remove the instrument from the packing material Retain all packaging materials for any future shipment of the instrument If the instrument is returned to AZI for any reason it must be placed in the original packaging materials that have been tested and proven to be effective protection during shipment e Call AZI Customer Service at 800 528 7411 or 602 470 1414 or go to the AZI website www azic com for Return Material Authorization RMA information prior to returning a unit Boxes and packing materials for all shipments are available from AZI Pack the Jerome instrument only in a Jerome shipping container AZI WILL NOT BE RESPONSIBLE FOR SHIPPING DAMAGE IF YOU RETURN THE INSTRUMENT IMPROPERLY PACKAGED OR SHIPPED YOU SHOULD INSURE IT FOR FULL VALUE e Check for any damage and confirm receipt of all parts on your packing list Contact Arizona Instrument Customer Service at 800 528 7411 or 602 470 1414 if you have any questions e Press the I O button The display will light up and show instrument serial number and software revision gt If necessary press ESC to clear any calibration reminders Call AZI Customer Service at 800 528 7411 or 602 470 1414 or e
63. ter on the hardware installation CD or on the Windows Update Web site with your permission Read our privacy policy Can Windows connect to Windows Update to search for sofware Yes this time only Yes now and every time connect a device No not this time Click Next to continue AZI Customer Service 800 528 7411 or 602 470 1414 Page 48 of 63 7 Select Install the software automatically and click Next Found Hew Hardware Wizard This wizard helps you install software for Communications Port If your hardware came with an installation CD lt or floppy disk insert it now what do pon want the wizard to do 2 Install the software automatically Recommended Install from a list or specific location Advanced Click Next to continue 8 Windows may display a message indicating that the driver has not passed Windows Logo Testing This driver being installed is a generic Communications Port driver that is part of Windows usbser sys so it is safe to ignore this warning Click Continue Anyway to install the driver Please wait while the wizard installs the software S Hardware Installation A The software you are installing for this hardware Communications Port haz not passed Windows Logo testing to verify its compatibility with Windows lt P Tell me why this testing is important Continuing your installation of this software may
64. the Tygon tubing from both ends of the filters and discard the old filters Replace the old filters with new filters oriented as shown in the diagram above gt Push the Tygon tubing as far as it will go onto the filter fittings gt Note that the marked flow direction on the AG filter goes toward the sensor or to the left in the diagram above Push the filters into the mounting clips Remove any crimps or twists in the tubing and ensure that tubing connections are secure If the tubing is loose readings may not be accurate Replace any tubing that has deteriorated due to heat and or age Close the case and replace the screws If the AG filter 1s replaced the new filter must be acclimated to the system by performing a sensor regeneration followed by twenty 20 manual samples using the sample button See page 23 for sensor regeneration instructions Dispose of all filters in accordance with state and federal environmental regulations AZI Customer Service 800 528 7411 or 602 470 1414 Page 35 of 63 PANEL SCREWS Press the I O button to turn the power OFF Unplug the power cord Use a Phillips screwdriver to remove the four 4 screws securing the battery panel as shown above After removing the screws carefully set the panel to the side Note that it is still connected to the instrument via the power connector Slide the battery pack out of the J405 Disconnect the battery connector to detach the old battery Install t
65. the instrument s intake to be exposed to any liquid DO NOT obstruct the intake or exhaust ports of the J405 as this could cause errors in readings and damage to the flow control system The instrument is not explosion proof Perform sensor regeneration before each day s use Perform another sensor regeneration after each day s use During periods of storage or inactivity perform sensor regeneration every 30 days Call AZI Customer Service at 800 528 7411 or 602 470 1414 if you have any questions If you prefer you may send e mail to support azic com AZI Customer Service 800 528 7411 or 602 470 1414 Page 6 of 63 2 INTRODUCTION The Jerome J405 Mercury Vapor Analyzer is an ambient air analyzer with a range of 0 5 to 999 micrograms of mercury vapor per cubic meter u g m Hg CAUTION The Jerome J405 is for gaseous vapor use only DO NOT allow the probe or the instrument s intake to be exposed to any liquid dust or other foreign material The J405 is designed to be easy to operate for quick and accurate analysis of mercury vapor levels It has few maintenance requirements However please take a moment to read this manual before attempting operation If you have any questions about your application or operation please call AZI Customer Service at 800 528 7411 or 602 470 1414 or e mail support azic com for assistance J405 Features e Much lower detection levels than the previous J erome
66. tive response only AZI Customer Service 800 528 7411 or 602 470 1414 Page 40 of 63 9 ACCESSORIES amp MAINTENANCE PARTS ITEM DESCRIPTION J405 Accessory Kit Communications Package Instruments See pictures beginning on page 42 1400 2002 Probe 1400 3010 Tubing Adapter 1 4 to 1 8 2600 3039 25 Fritware 1 pack of 20 fritware filters 2600 3905 Zero Air Filter 200 0165 USB Cable Type A to Type B 6 ft 990 0219 USB Memory Stick 4000 1025 AC Adapter Power Supply power supply charger 6000 4003 Line Cord 115 VAC USA and Canada 200 0003 Line Cord 220 240 VAC England 200 0008 Line Cord 220 240 VAC Europe J405 Accessory Kit Non Communications Package Instruments See pictures beginning on page 42 1400 2002 Probe 1400 3010 Tubing Adapter 1 4 to 1 8 2600 3039 25 Fritware 1 pack of 20 fritware filters 2600 3905 Zero Air Filter 4000 1025 AC Adapter Power Supply power supply charger 6000 4003 Line Cord 115 VAC USA and Canada 200 0003 Line Cord 220 240 VAC England 200 0008 Line Cord 220 240 VAC Europe J405 Functional Test Kit See pictures beginning on page 42 PART Y405 0901 alternate alternate Y405 0904 alternate alternate Y 431 0902 A2600 0902 A2600 0903 A2600 0904 2600 0022 2600 0030 3200 0011 Z2600 3914 Y 405 0903 2600 3039 72600 3905 600 0293 2600 3930 600 0262 Stopper Assembly Syringe Assembly Mercury Vial Syringe Needles 22 Ga Reusable FTK Vessel
67. u is password protected to prevent unwanted or accidental changes to operating parameters The default initial password is AZI but should be changed to something unique if restricted access to the SYSTEM menu is desired The password can be up to 10 characters long When the SYSTEM menu is selected from the Main Menu the J405 will prompt for the password Input the password using A and Y to change the alphanumeric character and gt and lt to move between characters Press ENTER START to proceed after entering the password AZI Customer Service 800 528 7411 or 602 470 1414 Page 19 of 63 When the correct password is entered the J405 will offer the option to change the password by pressing the A key or to proceed to the SYSTEM menu by pressing ENTER START The SYSTEM menu will then remain unlocked until the instrument is powered off and back on SET ALARM LEVELS When sampling if the mercury level exceeds the selected alarm level the word ALARM will flash on the J405 display If AUDIBLE ALARM 1s set ON the J405 will also beep three times Two different alarm levels can be set using this menu option Use the Aand VWarrow keys to change the value of the blinking field and the arrow to move to the next character in the alarm level setting Typically the high alarm is used for an industrial alarm level while the low alarm is set to a residential value Use the A and B buttons to switch between the high and low alarm settings Once t
68. vendor for software that has passed Windows Logo testing Continue Anyway STOP Installation 4 Click Finish AZI USB RS 232 Emulation Driver Completing the Device Driver Installation Wizard The drivers were successfully installed on this computer You can now connect your device to this computer If your device came with instructions please read them first Driver Name Status y Arizona Instrument LLC Ready to use AZI Customer Service 800 528 7411 or 602 470 1414 Page 47 of 63 5 Power on the J405 and connect it to the target computer using the included USB cable AZI P N 200 0165 Windows will detect the J405 and its Communications Port and automatically start the New Hardware wizard The following pictures and descriptions correspond to a Windows XP installation If using Windows Vista or Windows 7 this process 1s abbreviated and requires minimal user interaction Watch for the two info balloons to appear and then proceed to page 51 WD Found New Hardware x 1405 7605 9 04 AM Thursday 716 2006 i Found New Hardware Communications Pork 32 04 OM Thursday 716 2006 6 If the following dialog box appears DO NOT connect to Windows Update to get the driver Select No not this time and click Next Found Hew Hardware Wizard Welcome to the Found New Hardware Wizard Windows will search for current and updated software by looking on Your compu
69. xt file See Retrieving Data on page 29 for more information Z NOTE The J405 is NOT compatible with USB memory drives that have the U3 program pre installed Do not use USB memory drives that have the U3 program with the J405 PRINT DATA Before selecting PRINT DATA connect an AZI printer AZI P N Y990 0098 to either USB TYPE A PORT on the back panel of the J405 using the cable supplied with the printer When ENTER START is pressed all of the stored data on the J405 will be printed on the attached printer See Retrieving Data on page 29 for more information VIEW MEMORY USAGE The J405 can store up to 20 000 data points Selecting VIEW MEMORY USAGE will display what percentage of the data storage area is in use Once the data memory is full no additional data can be stored until the data on the instrument is deleted If the memory is full the J405 will continue to perform as expected but it will indicate that the memory is full and no new sample data will be retained The storage area can be cleared using DELETE DATA as described below DELETE DATA Selecting DELETE DATA will delete all sample data stored on the J405 Prior to deletion the J405 will prompt the user for confirmation as a precaution NOTE If you are using Location Names after deleting data it is necessary to re select the location name in the SAMPLE menu before taking any samples otherwise the location will not be recorded SYSTEM menu The SYSTEM men
70. zip file to the desktop e Double click the Driver Install folder to open it e Double click the Install Driver shortcut to launch the AZI Driver Installer wizard 2 Follow the instructions in the AZI Driver Installer wizard Click Next The description and screenshots pictured are for installation in Windows XP Windows Vista and Windows 7 installations will be similar AZIUSB RS 232 Emulation Driver Welcome to the AZI driver installer for WinxPI This wizard walks pon through updating the driver To continue click Next AZI Customer Service 800 528 7411 or 602 470 1414 Page 46 of 63 3 Windows may display one or more messages indicating that the driver has not passed Windows Logo Testing This driver being installed is a generic Communications Port driver that is part of Windows usbser sys so it is safe to ignore this warning Click Continue Anyway to install the driver Please wait while the wizard installs the software S Hardware Installation A The software you are installing for this hardware Communication Port has not passed Windows Logo testing to verify its compatibility with Windows F Tell me why this testing ls important Continuing your installation of this software may impair or destabilize the correct operation of your system either immediately or in the future Microsoft strongly recommends that you stop this installation now and contact the hardware

MANUAL JEROME J405

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