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1. SUPERHEAT KIT Superheat Expansion Tube Pitot Tube Insulation Temperature probe entry gland 3 F ig 4 PONS DRYNESS TEST KIT Pitot Tube Tubing Tube Clamps Rubber Bung and Tube Assembly 1 Litre Flask IAUN T Ct Fig 5 pa 5 a The Coolant Transfer Unit To condense the steam in the non condensable gas testing unit a supply of cold water is needed Due to the difficulty that is often found in finding an accessible supply of water in a sterilizer plant room a coolant transfer unit has been included in this kit The unit is a 110 volt 60 Hz alternating current pump that needs to be totally submerged in water There are two methods of utilizing this pump unit 1 The unit may be placed in the make up tank of the sterilizer or other convenient water reservoir 2 Alternatively place the pump unit in a bucket of water There should be enough water in a standard bucket to enable testing to continue for approximately 10 15 minutes before replacement of the water with cold is required Do not place the pump in a make up tank that re oS circulates its water as the fluctuating temperatures could make obtaining a consistent condensate temperature hard to achieve and damage to the pump may occur In a tank that has silt or other debris present it is recommended that the filter is fitted to the pump Note Do not let the pump unit run dry as damage to the pump may occur Non co2. assembly weigh the flask and record the mass Me 3 Support the flask close to the pitot tube taking care to avoid the issuing steam Ensure that the rubber tube and flask are protected from excess heat and draughts Do not connect it to the pitot tube yet 4 Introduce the second temperature sensor through the shorter of the two pipes into the water in the flask Agitate the flask and note the temperature of the water in the flask To 5 Ensure the sterilizer is empty except for the usual chamber furniture Select and start a porous load equipment cycle 6 When the steam supply valve to the chamber first opens connect the rubber tube to the pitot tube This will require the tester to be in close proximity to the steam issuing from the pitot tube and extreme care is required to avoid scalding and or burning Gloves overalls and eye protection must be worn 13 7 Observe record the steam temperature for the duration of the test and on completion of the test calculate the average temperature Ts 8 When the temperature in the flask is approximately 80 C disconnect the rubber tube from the stainless steel tube taking the same precautions as when fitting Agitate the water in the flask to make sure it is thoroughly mixed Note the temperature of the water Ti 9 Weigh the flask and stopper assembly including pipe and clips and note the mass Ms 10 Calculate the dryness value by using the following formul
3. the geometric center of the steam pipe Insert the appropriate size pitot tube see Table 1 below for the correct size into the steam supply Turn the steam supply back on taking the necessary precautions against burning scalding from the steam that will issue from the pitot tube Steam Pressure Bar Upto3 Upto 4 Up to7 Table 1 Pitot Hole Size mm 0 8 0 6 0 4 1 Insert a temperature sensor through the entry gland of the expansion tube and position it so the sensing point of the thermocouple element is in the geometric center of the expansion tube Cover the expansion tube with the lagging Push the expansion tube onto the pitot tube taking the necessary precautions This will require the tester to be in close proximity to the steam issuing from the pitot tube and extreme care is required to avoid scalding and or burning Gloves overalls and eye protection must be worn PERFORMING THE TEST 1 Ensure the sterilizer chamber is empty except for the usual chamber furniture Select and start a porous load equipment cycle 2 From the measured temperatures note the temperature in the steam service pipe for use in the dryness test and in the expansion tube Te when the team supply to the chamber first opens 3 Calculate the superheat in C from the following equation Superheat Te To Where Tois the boiling point of water at local atmospheric pressure ACCEPTANCE CRITERIA The test should be considered satisfacto
4. Keith Shuttleworth amp Associates Limited STEAM QUALITY TEST KIT SQ1 Set Up And User Guide Distributed by Steam Quality Test Kit SQ1 User Manual Version 1 5 USA Acknowledgments made to HTM2010 amp EN285 Keith Shuttleworth 8 Associates Ltd 2009 Keith Shuttleworth amp Associates Ltd Unit D5 Basepoint Business Centre 110 Butterfield Luton LU2 8DL Telephone 44 0 1582 433723 Fax 44 0 207 1173251 United Kingdom Email info ksapharma com Web www ksapharma com Table ofContents Introduction 4 Additional Equipment Requirements 5 Steam Test Points 6 Assembling 7 The Coolant Transfer Unit 9 Non Condensable Gas Test 10 Superheat Test 12 Dryness Test 13 Health and Safety 15 Care and Maintenance 15 Equipment Specification 15 Appendix 1 Steam Tables Back Cover Introduction Thank you for choosing the KSA Steam Quality Testing Kit SQ1 This kit was developed through extensive practical experience and has been designed to provide reliable and consistent results that conform to the requirements of EN285 HTM 2010 The non condensable gas test has been designed to be more robust than the standard equipment and also less dependent upon the skill of the operator It will be found that it will provide results that are more consistent than the EN285 HTM 2010 method The dryness test equipment is similar to that described in EN285 HTM 2010 but has been modified to make it more robust If the calculation provided with
5. a D T To 4 18 Mw 0 23 _ 4 18 Ts T1 L Where D Dryness value Mw The initial mass of water in the flask is M2 M Mc The mass of condense collected is M3 M2 To Initial temperature of the water in the flask C T Final temperature of the water and condense in the flask Ts Average temperature of the steam delivered to the flask L Latent heat of dry saturated steam at temperature Ts KJ Kg see Appendix 1 for latent heat tables If a computer spread sheet is to be used then this formula can be used in H17 asin this example spread sheet H9 H7 4 18 H3 H1 0 23 H13 H5 H3 4 18 H11 H9 H13 c D E F G H Totalweight of flask pipes etc 0 8148 3 Totalweightofflask and 650ml of water 1 449 Totalweightofflask condense 1 5368 7 Initialtem perature of water in flask 11 2 a Finaltem perature of water and condense 82 4 a Average tem perature of steam delivered to sterilizer 155 5 E Latent heatofaverage temperature of steam delivered to sterilizer 2096 7 15 16 17 Dryness value 0 969 Note The formula has been modified for stainless steel flasks and dip tubes instead of glass as detailed in HTM 2010 ACCEPTANCE CRITERIA The test should be considered satisfactory if the follovving requirements are met 1 The dryness value is not less than 0 90 if metal loads are process
6. ed the dryness value should not be below 0 95 2 Through out the operating cycle the temperature measured in the steam service pipe is within 3 C of that measured during the superheat test Calculations are included on an enclosed CD 14 Health and Safety Care should always be taken when working on or near steam pipes due to the very high temperatures involved Thermal gloves overalls that cover arms and eye protection must be used VVhile every effort has been made to provide protection from the ex treme temperatures care should be taken when testing with this equip ment Do not plug or restrict the Cooling Out flow as this may pressurize the heat exchanger which it has not been designed for Do not look into the condense collection cylinder while the steam valve is open as hot condense and or steam could be ejected The insulation surrounding the steam pipe is made from glass fibre and can cause irritation to the skin in some instances It is therefore recommended that gloves or a good quality barrier cream be applied as a precaution before handling the material The insulation is designed to prevent burns from transient contact with the pipe and is not designed to protect against prolonged contact The submersible pump is electrically powered and care must be taken to prevent hazards arising from the use of electricity in a potentially wet environment Care and maintenance No special care is required
7. for the steam test kit However the 4 mm copper tubing will with bending become work hardened which will lead to difficulty in returning it to the tight radius required for storage In this instance it may be easily replaced Should difficulty be found in obtaining a replacement or any other components please contact your local Distributor in the first instance or Keith Shuttleworth amp Associates Ltd for replacements Equipment specifications Non condensable gas test kit 0 20 N C per 100ml condensed steam Dryness test Full range Superheat test Full range 4mm steam supply tube Max 10 BarG Steam 8mm Coolant supply tube Condensing unit Steam side Condensing unit Water side 15 Appendix 1 Steam Tables 22071 121 96 2197 0 2192 8 2188 7 2184 8 2181 0 2177S 2173 7 2170 1 2166 7 2163 3 2160 1 2156 9 2153 7 2150 7 2147 6 21447 2141 9 2739 0 2136 1 2133 4 2130 7 145 46 2128 1 2125 5 2122 9 2120 3 2117 8 2115 3 2112 9 2110 5 2108 1 2105 7 2103 5 2101 2 2098 9 2096 7 2094 5 2092 3 2090 2 5 9 2088 1 E AO 6 2 160 20 2081 8 QO ee 16965 mes Fe ET 165 04 2066 0 2056 8 eo ma 2047 7 2039 2 0 ma ET
8. in and on the CD is used results identical to EN285 HTM 2010 will be obtained The superheat test equipment is identical to that in EN285 HTM 2010 Warning Before conducting any tests the contents of this manual must be studied in depth and any associated hazards considered It is stressed that the test methods are defined in EN285 and HTM 2010 and not by the authors of this manual and that these documents are the primary references Sterilizer plant rooms are potentially hazardous areas and the tests involve working on live steam It is assumed by the authors of this manual that staff conducting steam quality testing will be trained and understand the potential dangers involved with respect to burning due to contact with either steam or hot surfaces or any other related hazards Warranty The SQ1 Steam Quality Test Kit is designed and manufactured to the highest standards using top quality materials A one year parts only warranty applies from the date of delivery to the customer The warranty does not apply to abuse or misuse of the equipment or its use outside of the operating parameters defined within this manual Additional Equipment Requirements To enable you to complete the steam tests additional equipment is required 1 Two temperature sensors and indicator recorder capable of measuring over a range of ambient water temperature to maximum steam supply temperature Typical 0 150 C The sensor used for the su
9. ndensable Gas Test SETTING UP 1 Assemble equipment together as illustrated in Fig 2 Placeona level surface Check that the Steam Valve on the test equipment is fully closed and that the Cooling Water Valve is fully open 2 Connect the cooling water supply pipe to the pump at one end and the Cooling Water Inlet on the condensing unit at the other Fig 3 Connect another pipe from the Cooling Water Outlet to drain or a bucket Place the pump unit in a suitable water source If desired the pump unit may be omitted and the water feed connected to a more permanent source Please note that the water from the Cooling Water Outlet may be very hot and care should be taken to ensure that it can run to drain unimpeded and without spillage 3 Isolate the steam supply and after checking that no residual pressure is present connect the 4mm copper steam supply tubing to the non condensable gas take of point Fig 1 via a 44 isolation valve Take care as the steam pipe may be hot and residual steam may be present Connect the other end of the 4mm tube to the steam connection of condensing unit see Fig 3 and turn the steam supply back on Carefully open the V4 isolation valve a small amount The copper steam pipe supplied will be hot While it is insulated this is to protect the user against casual contact Even a short contact time will result in a burn unless the necessary precautions have been taken Warning Do not block or impede
10. perheat test should not exceed 4mm diameter 1 thermocouple entry gland for the steam supply pipe work A balance capable of measuring up to 2Kg with 0 1g accuracy 1 or two buckets or other water storage container A permanent water supply may also be used A mains power source optional A supply of cold water Steam Test Points In order to test the steam quality specific test points on the steam line are required Fig 1 Illustrates the location of the three test points on the steam supply pipe and they are fitted between the steam distribution system and the sterilizer It is expected that the pressure at this point would be 2 5BarA It is important the pitot tube entry point is level and parallel with the steam pipe as any deviation towards the edge of the pipe can influence the results detrimentally Non condensable gas Take Off point MF Min 400 mm Steam Temperature Probe entry Poin Fig 1 To Sterilizer Note All entry points are 1 4 NPT female sockets with full size holes drilled through the pipes Assembling the Steam Test Kit NON CONDENSABLE GAS KIT Burette Bulb Burette Cock Burette Burette Guide Condense Collection Cylinder 250 ml Measuring Cylinder Steam Valve Cooling Water Valve Steam Condensing Unit Q i OONODAKON 10 Cooling VVater Inlet 11 Cooling VVater Outlet 12 Steam inlet AWW Fig 2 Rear View of Steam Condensing Unit fe o Fig 3
11. ry if it the superheat measured in the expansion tube does not exceed 25 C and the temperature measured in the steam pipe did not differ by more than 3 C from that measured in the steam pipe during the steam quality Dryness test Calculations are provided on an enclosed CD 12 Dryness Test SETTING UP 1 Assemble the apparatus as per Fig 5 2 Isolate the steam supply and after checking that no residual pressure is present insert a temperature sensor entry gland into the fitting on the steam pipe The steam pipe may be hot and precautions should be taken against both burning and the presence of residual steam The temperature probe should be at the geometric center of the steam pipe Insert the appropriate size pitot tube see Table 1 below for the correct size into the steam supply Turn the steam supply back on taking the necessary precautions against burning scalding from the steam that will issue from the pitot tube PERFORMING THE TEST Important Before performing the test ensure the pitot hole is not restricted as this will lead to false results This is best done prior to fitment for safety reasons A long heat up time for the flask reaching 800C is not normal It should take no more than 5 minutes 1 Weigh the whole assembly including pipe and clips and note the weight M1 2 Remove the stopper and tube assembly and pour 650 50 ml of cold water below 27 C into the flask Replace the stopper and tube
12. tart a run When the steam supply to chamber first opens ensure the measuring cylinder is empty by emptying it Make a note of the water level in the burette Any non condensable gases present in the steam being sampled will rise to the top of the burette The overflow formed by the condensate and the water displaced by the gases will collect in the measuring cylinder When the at least 100ml of condense has been collected in the measuring cylinder note the volume of gas collected in the burette Vb and the volume of water collected in the measuring cylinder Vc Calculate the fraction of non condensable gases as a percentage as follows Percentage of non condensable gas 100 x Vb Vc ACCEPTANCE CRITERIA The test should be considered satisfactory if the level of non condensable gases does not exceed 3 5 The test should be done three times in total to check consistency If the results of the tests differ significantly then the cause should be investigated before proceeding further Calculations are included on an enclosed CD 11 The Superheat Test SETTING UP 1 Assemble the apparatus as per Fig 4 2 Isolate the steam supply and after checking that no residual pressure is present insert a temperature sensor entry gland into the fitting on the steam pipe The steam pipe may be hot and precautions should be taken against both burning and the presence of residual steam The temperature probe should be at
13. the flow of cooling water The cooling water outlet must be kept clear at all times PERFORMING THE TEST 1 Before starting the test ensure the cooling water valve is fully open and the steam valve is closed 2 Turn on the water supply by supplying power to the pump After ensuring that the cooling water is leaving the outlet pipe the main steam valve may be slowly opened Live steam and boiling water could discharge from the condense collecting chamber if insufficient cooling water is available and present a hazard In any event precautions should be taken Do not look into the collecting chamber and wear eye protection 10 10 11 12 Slowly open the steam valve and by reducing or increasing the flow through the steam and water valves obtain a flow of condense that will give a temperature of between 70 C and 90 C as indicated on the dial temperature gauge Fill the condense collection chamber with water either by filling with water from an external source or allowing condense to accumulate Open the burette cock and draw up condense into the burette with the rubber bulb provided to get a water level near the top Remember to isolate the burette from the rubber bulb by shutting the burette cock before testing commences Fill the condense collection chamber with more water until it overflows Ensure that the sterilizer chamber is empty except the normal furniture etc Select a porous load equipment cycle and s
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