AIAS 3000 Xcalibur Setup Rev D
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1. 33 NL 4816 KB Breda 31 076 587 8722 P R China Thermo Finnigan China Suite 912 916 Ping An Mansion No 28 Jin Rong Street Xicheng District Beijing 100032 86 010 6621 0839 Spain Thermo Finnigan SA Acer 30 32 Edificio Sertram Planta 2 Modulo 3 ES 08038 Barcelona e 84 093 223 0918 Spain Thermo Finnigan SA Avenida de Valdelaparra 27 Edificio Alcor Planta 2a ES 28108 Alcobendas Madrid 34 091 657 4930 Sweden Thermo Finnigan AB Pyramidbacken 3 S 141 75 Kungens Kurva Huddinge 46 08 680 0101 United Kingdom Thermo Finnigan Ltd Paradise Hemel Hempstead Herts HP2 4TG 44 01 442 233 555 Notes The country code is enclosed in square brackets The city code or area code is enclosed in parenthesis For countries other than the U S A when you are dialing from within the specified country dial the 0 of the city code For countries other than Italy when you are dialing from outside the country do not dial the 0 of the city code CopyrightO 2002 Thermo Finnigan a member of the Thermo Electron family of companies All rights reserved Printed in Italy X Contents Chapter 1 AVAS 3000 Set UP VIEW sn na issos ossos 5 LH Configuration A A ii 6 Configuration Cent sorea adi te EE EEN et 6 1 2 AVAS 3000 Method Editor miii nerd 7 AVAS 3000 Paga scaricare bate ad ou ccee Was EE EEE 7 Se del T INJEC HON ONO 8 KO 8 AT2. AS3000 Command Menu ccccccccessscssceeeceececeecseeseceeceseeseeeeseeeasecseceeeneeeenes 9 1 3 Setting AI AS 3000 Parameters cccccccsccescessseeeesseecseceseceseeeseeeseesaeceseecsecesecnseseseeeseeeaeseaeenaeeeas 10 Thermo Finnigan AI AS 3000 Autosampler User s Manual iii Al AS 3000 Autosampler User s Manual Thermo Finnigan Chapter 1 AI AS 3000 Set Up View Thermo Finnigan This chapter contains informations to configure and to set the AI AS 3000 Autosampler This chapter contains these topics Configuration 6 AI AS 3000 Method Editor 7 Setting AI AS 3000 Parameters 10 Al AS 3000 Autosampler User s Manual 1 5 AI AS 3000 Set Up View Configuration 1 6 Serial Port 8 Vials 105 Vials Volume X 1 1 Configuration Configuration Screen Items listed under this heading contain definitions to each control you see listed in this Instrument Configuration window AL AS 3000 Configuration x m Connection Serial port y Cancel m Number of vals Help 105 m Syringe type Volume 10 pL gt Figure 1 1 Al AS 3000 Configuration Screen Connection This parameter specifies the communication port to be used for the AI AS 3000 sampler it can be through the GC or alternatively can be any COM Port from to 8 Number of vials Check this box if you are using the AI 3000 autosampler Check this box if you are using the AS 3000 autosampler Syring
3. U S A Thermo Finnigan Corporation 355 River Oaks Parkway San Jose CA 95134 1991 1 408 965 6000 Thermo Finnigan Technical Support 3661 Interstate Park Road North Riviera Beach FL 33404 800 685 9535 561 844 5241 Fax 561 881 8431 Australia Thermo Finnigan P O Box 239 Rydalmere Unit 20 Metro Centre 38 46 South Street Rydalmere N S W 2116 61 02 9898 9000 Austria Thermo Finnigan GmbH Wehlistrasse 27b A 1200 Wein 43 01 333 50 34 0 info quest thermo at Belgium Thermo Finnigan BVBA Groenenbrogerlaan 84 B 2610 Wilrijk Antwerpen 32 03 825 0670 Canada Thermo Finnigan Canada 5716 Coopers Avenue Unit 1 Mississauga Ontario L4Z2E8 1 905 712 2258 France Thermo Finnigan France SA Parc Hightec Sud 12 Avenue des Tropiques Z A de Courtaboeuf BP141 e F 91944 Les Ulis C dex 33 01 69 18 88 10 Germany Thermo Finnigan Analytische Systeme GmbH Boschring 12 D 63329 Egelsbach 49 06103 408 0 Italy Thermo Finnigan Italia S p A Strada Rivoltana 20090 Rodano Milano 39 02 95059 1 Japan Thermo Finnigan K K Nishi Shinjuku Toyokuni Bldg 3F 2 5 8 Hatsudai Shibuya ku Tokyo 151 0061 e 81 03 3372 3001 Japan Thermo Finnigan K K Esaka Grand Building 2 3 1 Esaka cho Suita City 6 Osaka 564 0063 e 81 06 6387 6681 Netherlands Thermo Finnigan BV Druivenstraat
4. uL in step of 0 1 uL The number of times the syringe plunger will be pulled up and down to eliminate any bubbles from the sample Set a value from 0 to 15 It calculates automatically the speed the sample is pulled up withdrawn from the vial to the syringe Set No for no viscous or low viscous sample Set Yes for high viscous sample Al AS 3000 Autosampler User s Manual 1 7 AI AS 3000 Set Up View AI AS 3000 Method Editor Sampling depth in vial Injection depth Pre inj dwell time s Post inj dwell time s 1 8 X Determines the penetration depth of the syringe needle into the vial When Bottom is set default value the syringe needle penetrates up to the bottom of the vial When Center is set the syringe needle penetrates up to the half of the vial Injection Injection Group Box This group box contains the parameters to control the penetration depth of the needle into the injector and the time the syringe needle stays in the injector before or after the sample is injected It determines the penetration depth of the syringe needle into the vial When Standard is set default value the syringe needle penetrates into the injector up the maximum depth limit When Minimum is set the syringe needle penetrates into the injector up to go beyond the septum only Enter the time in seconds the syringe needle is held in the inlet before the injection of sample When you specify a delay of more than a few sec
5. Thermo Finnigan TRACE GC AI AS 3000 Autosampler User s Manual Published by Technical Publications Thermo Finnigan Italia S p A Strada Rivoltana 20090 Rodano Milan Italy Printing History Revision D printed March 2002 Xcalibur and TRACE GC are trademarks and or product names of Finnigan Corporation Microsoft is a registered trademark of Microsoft Corporation Technical information contained in this publication is for reference purposes only and is subject to change without notice Every effort has been made to supply complete and accurate information however Thermo Finnigan Corporation assumes no responsibility and will not be liable for any errors omissions damage or loss that might result from any use of this manual or the information contained therein even if this information is properly followed and problems still arise This publication is not part of the Agreement of Sale between Thermo Finnigan Corporation and the purchaser of a Thermo Finnigan system In the event of any conflict between the provisions of this document and those contained in Thermo Finnigan Corporation s Terms and Conditions the provisions of the Terms and Conditions shall govern Reference to System Configuration and Specifications supersede all previous information and are subject to change without notice The GC MS and LC MS products of the Thermo Finnigan Division are produced under VISION 2000 accredited quality management systems
6. e Type This parameter specifies the volume of the syringe in use Click OK after you are satisfied with your selection Click Cancel if you would like to exit without saving your changes Click Help for this page to display Al AS 3000 Autosampler User s Manual Thermo Finnigan Sample volume ml Plunger strokers Viscous sample Thermo Finnigan AI AS 3000 Set Up View __ AI AS 3000 Method Editor 1 2 Al AS 3000 Method Editor The Method Editor screen has four tabs which contain all of the parameters used to set up injection events Click the links below to find out more about the parameters in the each tab AIAS 3000 Page Alas 3000 Trigger r Sampling esa Sample volume pL Pre Injection Solvent fA y Plunger strokes 1 e Cycles f1 y Viscous sample No w r Sample Sampling depth in vial Bottom y Rinses 1 y r Injection Post Injecti Injection depth Standard e fj DEI Solvent fA be Pre inj dwell time s 0 Cycles 1 e Post inj dwell time s 0 2 Help Get Send Sampling Sampling Group Box This group box contains the parameters to control syringe rinse bubble elimination sample pull up speed from the vial to the syringe and needle penetration depth into the sample vial This is the volume in microliters of sample injected With the 10 uL syringe set a value from 0 to 5 uL in step of 0 1 uL With the 5 uL syringe set a value from 0 to 2 5
7. iscous box specify if the sample is viscous In Sampling depth in vial box specify the penetration depth of the syringe needle into the vial 2 Inthe Injection group box specify values in the Injection fields 3 In the Sample box specify the number of times the sample rinses the syringe 4 Inthe Pre Injection group box select Solvent A B C D A B or C D a b Specify the amount of solvent used to rinse the syringe in the Solvent field Specify the number of times to rinse the syringe in the cycles field 5 In the Post Injection group box select Solvent A B C D A B or C D a b Specify the amount of solvent used to rinse the syringe in the Solvent field Specify the number of times to rinse the syringe in the cycles field Al AS 3000 Autosampler User s Manual Thermo Finnigan
8. ith sample before actually pulling up the sample for injection The number of times the sample rinses the syringe Select a number from 0 to 15 Post Injection Box The parameters used to rinse the syringe after the sample has been injected Select which of the four solvent vials or the combination of two solvent vials will be used as the post rinse solvent choosing between the following options A B C D A B C D Different solvent vials combinations than A B or C D are not possible The number of times the solvent rinses the syringe Select a number from the pull down list box Al AS3000 Command Menu This menu allows to access the following function This function allows transferring method data from autosampler to GC This function transfers the analytical method from the memory of the GC to the autosampler and enables the method This function permits to start a clean cycle This function permits to start an single sample injection This function interrupts any current operation on the sampler putting it in stand by condition AI AS 3000 Autosampler User s Manual 1 9 AI AS 3000 Set Up View Setting Al AS 3000 Parameters X 1 3 Setting Al AS 3000 Parameters 1 In the Sampling group box specify values in Sample fields a b In the Sample volume box specify the volume of sample injected In the Plunger strokes box specify the number of bubble elimination strokes for the syringe plunger In V
9. onds the needle preheats which makes a Hot Needle Injection Set the wait time from 0 to 63 seconds Enter the time in seconds the syringe needle is held in the after the injection of sample A delay of more than a few seconds will heat the needle with the possible effect of driving those heavier analytes that have condensed in the needle out A solvent flush technique may work better Set the wait time from 0 to 63 seconds Washes Washes Group Box These sections control the sample and pre and post rinses used to clean the syringe Controls displayed in this group box are for Pre Injection Sample and Post Injection Pre Injection Group Box The parameters used to pre rinse the syringe before drawing up the sample Al AS 3000 Autosampler User s Manual Thermo Finnigan X Solvent Cycles Rinses Solvent Cycles Get Method from Sampler Send Method to Sampler Start Clean Cycle Inject Single Sample Force Autoinjector to Stand by Thermo Finnigan AI AS 3000 Set Up View _ AI AS 3000 Method Editor Select which of the four solvent vials or the combination of two solvent vials will be used as the pre rinse solvent choosing between the following options A B C D A B C D Different solvent vials combinations than A B or C D are not possible The number of times the solvent rinses the syringe Select a number from the pull down list box Sample Box Use this control to pre rinse the syringe w
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