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GC Columns Accessories

1. GC Columns and Accessories SS 0 l aceGOLD GC Columns 219 TracePLOT GC Columns 238 TRACE GC Columns 244 Applications 264 Gas Management 287 Injection Port Septa 293 Injection Port Liners 294 Capillary Accessories 301 Tools 304 GC Equipment 305 Syringes 307 Thermo Scientific Technical Information 322 GC Columns and Accessories The Thermo Scientific TRACE family of GC Columns offers high temperature stability and exhibits low bleed and long lifetimes From general purpose non polar to polar columns TraceGOLD TRACE and TracePLOT columns provide excellent quality and performance with guaranteed reproducibility Our range of GC accessories includes all the consumables and tools necessary for today s gas chromatographer TraceGOLD GC Columns GC Equipment u TracePLOT GC Columns Offering you a leap forward in Our new GFM Pro flowmeter and The latest innovation in PLOT column column performance delivering GLD Pro leak detector are essential technology providing reproducible low bleed and superior inertness tools for maintaining optimal analyses of permanent gases performance of your GC instrument hydrocarbons and solvents Go to Go to Go to PAGE 219 PAGE 286 PAGE 238 203 www thermoscientific com chromatography GC Column Selection When selecting a GC column for your analysis it can often be difficult to choose the most appropria
2. www thermoscientific com chromatography 221 im TraceGOLD TG SQC GC Columns Ensure the quality of a Thermo Scientific instrument when installed on site Applications NON HOMES Phase Proprietary e System Qualification Tests Max Temps 330 C 350 C Thermo Scientific GCMS gt Optimized for system qualification tests for new GCMS installations or during service maintenance of an existing instrument gt Thermo Scientific recommends reserving this column for benchmark testing only TraceGold TG SQC GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 26070 1300 1 Each 0 25mm 30m 0 25um 26070 1420 1 Each TraceGOLD TG 5MS AMINE GC Columns Analysis of ppm levels of amines without column priming Applications NON POLAR e Amines and other basic i i Phase Modified 5 Phenyl Methylpolysiloxane for Basic Compounds compounds including Max Temps 305 C 315 C alkylamines USP Listing N A diamines triamines ethanolamines Low polarity phase 5 diphenyl 95 dimethyl polysiloxane T Nitrogen containing gt Tubing surface is chemically altered to reduce tailing of active basic heterocyclics compounds gt Also allows analysis of neutral or weakly acidic compounds e g phenols and compounds susceptible to hydrogen bonding gt Low bleed at maximum operating temperature TraceGOLD TG 5MS AMINE GC Columns I D Length Film Thickness Cat No Quantity 0 25m
3. 26 N N Dimethylacetamide 27 Ethylbenzene 28 m Xylene 29 p Xylene 30 o Xylene 31 Ethylene glycol 34 21min 260X010 1200000 1000000 800000 600000 400000 200000 260X013 04 6 8 10 12 8 00 14 10 00 16 12 00 14 00 16 00 18 00 20 00 18 20 22 24 26 28 30 32 34 Separation of Argon Oxygen in Air Column TG BOND MSieve 5A 30m x 0 53mm x 50um Part Number 26003 6100 Temperature 27 C Isothermal Detector Type TCD Carrier Gas He Flow Rate 4 0 mL min i E Injection Volume 1 0 uL i Injection Mode Split 15 1 100 C 1 Argon 2 Oxygen 3 Nitrogen Standard Gas Mix H2 O2 N2 CH4 CO Column TG BOND MSieve 5A 30m x 0 53mm x 50um Part Number 26003 6100 Temperature 120 C Isothermal Detector Type TCD Carrier Gas He Flow Rate 5 0 mL min 3 3 Injection Volume 1 0 uL s Injection Mode Split 12 1 150 C 1 Hydrogen 4 Methane 2 Oxygen 5 Carbon Monoxide 3 Nitrogen Free Fatty Acids Column TG WAXMS A 30m x 0 25mm x 0 25um Part Number 26087 1420 Temperature 145 C Isothermal Detector Type FID Carrier Gas Hydrogen Flow Rate 40 cm sec Injection Volume 1 0 uL Injection Mode Split 50 1 250 C 1 acetic acid 6 n valeric acid 2 propionic acid 7 isocaproic acid 3 isobutyric acid 8 caproic acid 4 n butyric acid 9 heptanoic acid 5 isovaleric acid 283 www thermoscientific com chromatography FOOD
4. C min to 300 C Final Temp 300 C 0 5 min Detector Type MS Detection PolarisQ source 225 C Conditions 35 400 m z EI 70 eV Carrier Gas He Flow Rate 1 5 mL min Injection Temp 250 C Injection Mode Split Split Ratio 20 1 1 Pentabarbital 2 Secobarbital 3 Hexabarbital 4 Phenobarbital Drugs of Abuse Column Part Number Initial Temp Rate 1 Final Temp Detector Type Detection Conditions Carrier Gas Flow Rate Injection Temp Injection Details Split Ratio 1 Caffeine 2 Phencyclidine 3 Methadone 4 Cocaine TR DoA 5MS 15 m x 0 25 mm x 0 25 um 26AF130P 150 C 0 2 min 20 C min to 300 C 300 C 0 5 min MS PolarisQ source 225 C 35 400 m z EI Q 70 ev He 1 5 mL min 250 C Split 50 1 5 Codeine 6 6 acetylmorphine 7 Heroin 15070501 Relative Abundance 11040505 Relative Abundance E 2 amp 100 95 90 85 80 75 70 65 60 55 50 45 40 35 30 2 2 2 4 26 28 3 0 3 2 3 4 2e 20 e o B u e i L 5 0 28258 md ae 3 00 Time min 3 6 Time mn 50 Time min 3 8 5 5 3 05 4 0 310 3 15 Time min 42 4 4 46 45 5 0 Drugs of Abuse Column TR DoA 35MS 30m x 0 25mm x 0 25um Part Number 26AC497P Temperature 230 C 0 1 minute hold to 320 C at 60 C minute 1 8 minute hold Detector Type MS Carrier Gas He
5. quality and performance with guaranteed reproducibility TraceGOLD GC Columns Offering you a leap forward in column performance delivering low bleed and Superior inertness TracePLOT GC Columns The latest innovation in PLOT column technology providing reproducible analyses of permanent gases hydrocarbons and solvents TRACE GC Columns Offering excellent quality and reproducilbity for a wide range of GC applications 217 www thermoscientific com chromatography Thermo Scientific TRACE GC Capillary Columns A leap forward in column performance e Low bleed even at elevated temperatures e Qutstanding robustness for difficult separations e Reliable and reproducible performance e Complete range of GC consumables for all instruments The heart of any gas chromatograph is the column We have used the knowledge gained more than 30 years of HPLC column production and 50 years in GC and GC MS instrument manufacturing to offer a range of columns and consumables that are unsurpassed in the most important aspects of their performance Low Bleed Bleeding phases cause problems including low sensitivity detector contamination lower temperature limits and short lifetimes All manufacturers have at some time claimed their columns have the lowest bleed but use supporting chromatograms that lack reproducible scale information or methodology By quantifying the amount of phase bleeding from the column we can show
6. 0 25mm 30m 0 5um 26089 2230 1 Each 0 25mm 30m Tum 26089 2960 1 Each 0 32mm 15m 0 25um 26089 1310 1 Each 0 32mm 15m 0 5um 26089 2120 1 Each 0 32mm 15m Tum 26089 2850 1 Each 0 32mm 30m 0 25um 26089 1430 1 Each 0 32mm 30m 0 5um 26089 2240 1 Each 0 32mm 30m Tum 26089 2970 1 Each 0 53mm 15m 0 25um 26089 1320 1 Each 0 53mm 15m 0 5um 26089 2130 1 Each 0 53mm 15m Tum 26089 2860 1 Each 0 53mm 15m 1 5um 26089 3340 1 Each 0 53mm 30m 0 25um 26089 1440 1 Each 0 53mm 30m 0 5um 26089 2250 1 Each 0 53mm 30m Tum 26089 2980 1 Each 0 53mm 30m 1 5m 26089 3360 1 Each www thermoscientific com chromatography 231 TraceGOLD TG 225MS GC Columns Offers better thermal stability than comparable columns Applications NON POLAR j FAMES Phase 50 Cyanopropylpheny Polysiloxane e Carbohydrates Max Temps 220 C 240 C USP Listing G7 G19 e Sterols e Flavor compounds gt Polar phase 50 cyano propylmethyl 50 phenylmethyl polysiloxane Innovative deactivation process for siloxane reduces tailing and improves efficiency over comparable columns gt Equivalent to USP G7 G19 phases Similar to Rtx 225 DB 225 HP 225 SPB 225 TraceGOLD TG 225MS GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 26083 1300 1 Each 0 25mm 15m 0 5um 26083 2110 1 Each 0 25mm 30m 0 25um 26083 1420 1 Each 0 25mm 30m 0 5um 26083 2230 1 Each 0 25mm 60m 0 25um 26083 1540 1 Each 0 25mm 60m 0 5um 26083 2350 1 Each 0 32mm 15m 0 25um 26083
7. 25 Pack 5 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 5 Pack 5 Pack 5 Pack 295 Liner Sealing Rings Suited for use with injection liners in instruments from a variety of manufacturers Liner Sealing Rings For Use with For Liner Type Material Cat No Quantity Thermo Scientific Instruments 8mm O D Liners Graphite 29033406 10 Pack Thermo Scientific TRACE 45322052 Liner Graphite 29013417 2 Pack Agilent Instruments 45341335 453A1355 453A2332 453A2352 Liners Graphite 290GA242 10 Pack 453A2265 453A1255 453A1315 453A1285 453A1295 453A2282 Agilent Instruments 453A1305 453A1312 453A2325 453A1345 453A2375 453A1372 Graphite 290GA243 10 Pack 453A1252 453A1262 453A2292 453A2302 453A2342 Liners Agilent Instruments 453A2275 Liners Graphite 290GA244 10 Pack 453A1335 453A1355 453A2332 453A2352 453A2265 453A1255 Agilent Instruments 453A1315 453A1285 453A1295 453A2282 453A1305 453A1312 453A2325 453A1345 453A2375 453A1372 453A1252 453A1262 453A2292 453A2302 453A2342 453A2275 Liners Viton 2900A241 10 Pack Gold Inlet Base Seals for Agilent GCs Gold plating provides a surface with exceptional inertness suitable for analysis of highly active compounds gt Precision machined to provide exceptional sealing properties gt Reduces activity especially useful for analysis of pesticide PCBs phenols etc High grade stainless steel providing reproducible seal Direct equivalent to Agil
8. 2500 Methyl ethyl ketone TG 1MS 26099 2970 220 2505 Furfuryl alcohol TG 1MS 26099 1420 220 2520 Methyl bromide TG 1MS 26099 2970 220 2529 Furfural TG 5MS 26098 2960 221 2536 Valeraldehyde TG 5MS 26098 1310 221 2537 Methyl methacrylate TG 35MS 26094 2980 226 2541 Formaldehyde TG WAXMS 26088 2240 234 2542 Mercaptans TG 1MS 26099 2960 220 2546 Cresols and phenol TG WAXMS 26088 1430 234 2549 Volatile organic CPDS screening TG 1MS 26099 2960 220 2550 Benzothiazole in asphalt fume TG 1MS 26099 2970 220 2551 Nicotine TG 5MS 26098 2970 221 3511 Monomethylaniline TG 5MS 26098 1420 221 3513 Tetranitromethane TG 1MS 26099 1420 220 5020 Dibutyl phthalate and di 2 ethylhexyl phthalate TG 1MS 26099 1300 220 5515 Polynuclear aromatic hydrocarbons TG 1MS 26099 3090 220 5519 Endrin TG 1MS 26099 3090 220 5523 Glycols TG 35MS 26094 2980 226 5600 Organophosphorus pesticides TG 5MS 26098 2970 221 5602 Chlorinated organonitrogen herbicides air sampling TG 17MS 26089 1420 231 5 01 Resorcinol TG 1MS 26099 1420 220 9200 Chlorinated organonitrogen herbicides hand wash TG 17MS 26089 1420 231 9201 Chlorinated organonitrogen herbicides dermal patch TG 17MS 26089 1420 231 GC Columns Thermo Scientific TRACE GC Columns The Thermo Scientific TRACE family of GC Columns offer high temperature stability and exhibit low bleed and long lifetimes From general purpose non polar to polar columns TraceGOLD TRACE amp TracePLOT columns provide excellent
9. 26 Needle Point Cone Cone Cone Cone Cone Cone Cone Cone Cone Bevel Cone Cone Cone Cone Cone Cone Cone Cone Cone Side hole Cone Cone Cone Cone Cone Side hole Side hole Side hole Side hole Cat No 36504045 365C3701 36500505 365A0490 365D3711 36520060 365D3731 365D1856 365D1840 365D2705 365D2971 365D2972 365D2976 365D2977 365D2985 365D3741 365F3700 365F3761 365F3980 365F3988 365H3771 365H5333 365H5700 365H6700 365J7700 365K8130 365K8135 365L8630 365L8635 Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 6 Pack 1 Each 1 Each 6 Pack 6 Pack 6 Pack 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each Manual Syringes Manual Syringes eee Manual Syringes Volume 0 5uL 1 0uL 1 0uL 5 0uL 5 0uL 10uL 10uL 10uL ZOLL 2byL 2byL 2byL BOuL BOuL BOuL Soul 100uL 100uL 100uL 100uL 250uL 250uL 250uL 250uL 500uL 1 0mL 1 0mL Needle Type Plunger in Needle Plunger in Needle Plunger in Needle Fixed Removable Fixed Fixed Removable Fixed Removable Fixed Gas Tight Removable Gas Tight Fixed Removable Fixed Gas Tight Removable Gas Tight Fixed Removable Fixed Gas Tight Removable Gas Tight Fixed Fixed Gas Tight Removable Gas Tight Fixed Gas Tight Removable Gas Tight Removable Gas Tight Fixed Gas Tight Length 50mm 50mm 70mm 50mm 50mm 50mm 50mm 50mm
10. C 220 C 300 C 320 C 260 C 280 C 240 C 260 C 280 C 240 C 320 C 340 C 275 C 260 C 250 C 220 C 340 C 360 C for films lt 1 0um 300 C 320 C for films 1 5 to 3 0um films 280 C 300 C for films gt 3 0um 370 C 380 C 340 C 350 C for films lt 1 5um 280 C 300 C for films gt 1 5um 360 C 370 C for films lt 1 5um 350 C 360 C for films gt 1 5um 380 C 400 C 360 C 370 C 360 C 370 C 280 C 300 C 280 C 300 C 230 C 250 C 250 C 260 C 260 C 280 C for films lt 1 0um 240 C 260 C for films gt 1 0um 280 C 300 C 240 C 250 C 400 C for films lt 1 0um 370 C for 2 65um films 240 C 260 C 340 C 360 C 330 C 350 C 360 C 370 C 330 C 350 C 330 C 350 C 330 C 350 C 300 C 320 C 300 C 320 C 300 C 320 C 280 C 300 C 380 C 400 C 330 C 350 C 330 C 350 C 330 C 350 C 330 C 350 C 200 C 200 C 300 C 280 C 300 C 250 C 250 C 190 C 205 GC Column Selection by Manufacturer Column Manufacturer Recommended Column Manufacturer Recommended Thermo Scientific Thermo Scientific Alternative Alternative Capillary 007 1 MS Quadrex TG 1MS 220 Capillary DB 225ms Agilent TG 225MS 232 Capillary 007 17 MPS 50 Quadrex TG 17MS 231 Capillary DB 23 Agilent TR FAME 259 Capillary 007 1701 Quadrex TG 1701MS 230 Capillary DB 2887 Agilent TR SimDist 2
11. Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary OV 1 OV 17 OV 1701 OV 5 OV 624 Petrocol 2887 Petrocol DH Petrocol EX2887 Rtx 1 Rtx 1301 Rtx 1701 Rtx IMS Rtx 200 Rtx 200MS Rtx 225 Rtx 2330 Rtx 2560 Rtx 2887 Rtx 35 Rtx 35 Amine Rtx 35MS Rtx 5 Rtx 5 Amine Rtx 50 Rtx 5SIIMS Rtx 624 Rtx Volatiles Rtx Wax Rxi 17 Rxi 1ms Rxi bHT Rxi 5MS Rxi 5Sil MS SE 30 SE 52 SE 54 SolGel Wax SP 2100 SP 2250 SP 2330 SP 2380 SPB 1 SPB 1 Sulfur SPB 17 SPB 35 SPB 5 SPB 50 Stabilwax Stabilwax DA Stabilwax DB SUPELCOWAX 10 VF 17ms VF 1ms Manufacturer Ohio Valley Ohio Valley Ohio Valley Ohio Valley Ohio Valley Sigma Aldrich Sigma Aldrich Sigma Aldrich Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Restek Agilent Agilent Agilent SGE Supelco Supelco Supelco Supelco Supelco Supelco Supelco Supelco Supelco Supelco Restek Restek Restek Supelco Varian Varian Recommended Column Thermo Scientific Alternative TR 1 245 Capillary TG 17MS 231 Capillary TG 1701MS 230 Capillary TR 5 247 Capillary TG 624 229 Capillary TR SimDist 257 Capillary TG 1MS 220 Capillary TR SimDist 257 Capillary TR 1 245 Capillary TG 1301MS 228 Capillary TG 1701MS 230 Capillary TG 1MS 220 Capillary TG 200MS 233 Capillary TG 200MS 233 Capillary
12. Carrier Gas He iur m Flow Rate 1 2 mL min Injection Volume 1 0 uL Wi Injection Mode Splitless 250 C LAN MAI I i DIEI II III III EIC 1 1 4 dioxane 30 naphthalene ge Excellent 2 n nitrosodimethylamine 31 4 chloroaniline peak shape 3 pyridine 32 hexachlorobutadiene of pyridine c toluene 33 4 chloro 3 methylphenol 4 2 fluorophenol SS 34 2 methylnaphthalene 5 phenol d6 SS 35 1 methylnaphthalene 6 phenol 36 hexachlorocyclopentadiene 285 3930 3510 19 139 1 Excellent 7 aniline 37 2 4 6 trichlorophenol 4 resolution 8 bis 2 chloroethyl ether 38 2 4 5 trichlorophenol gi PAHs 9 2 chlorophenol 39 2 fluorobiphenyl SS 5 10 1 3 dichlorobenzene 40 2 chloronaphthalene 11 1 4 dichlorobenzene d4 IS 41 2 nitroaniline 12 1 4 dichlorobenzene 42 1 4 dinitrobenzene 13 benzyl alcohol 43 dimethyl phthalate 14 1 2 dichlorobenzene 44 1 3 dinitrobenzene 15 2 methylphenol 45 2 6 dinitrotoluene 16 bis 2 chloroisopropyl ether 46 1 2 dinitrobenzene 17 4 methylphenol 3 methyl 47 acenaphthylene phenol 48 3 nitroaniline PIL N IL 18 n nitroso di n propylamine 49 acenaphthene d10 IS 358 R28 s m ne peo ve N 68 X5 DE 0m 19 hexachloroethane 50 acenaphthene PO 20 nitrobenzene d5 SS 51 2 4 dinitrophenol 21 nitrobenzene 52 4 nitrophenol 61 4 6 dinitro 2 methylphenol 68 phenanthrene d10 IS 77 p terphenyl d14 SS 86 di n octyl phthalate 22 isophorone 53 2 4 dinitrotoluene 62
13. Check the column and connections Check electrometer or amplifier and associated connections Replace if required Replace the recording device Clean FID jet check detector gas flows and re light flame Check the column position Inject a test mixture and evaluate the column Increase the column oven temperature Do not exceed the recommended maximum temperature for the stationary phase Trim first 10 20cm from column and re install in injector Replace with fresh silanized wool and a clean inlet liner Increase the inlet temperature Remake the column inlet connection Replace the column according to the column manufacturer s literature Reinstall the column Reduce the initial oven temperature Check and adjust the septum purge and vent flows Reduce the injection size Reduce the carrier gas flow rate Replace the column Lower the column oven temperature Use a longer column Install a suitable column Choose a correct injection technique Condition or change the column Replace the septum Discard sample Store samples upright in a refrigerator Use Teflon faced septa with the Teflon facing downwards i e towards the sample If you need more assistance or information on specific detection systems please contact us and request our Troubleshooting Guide GC Technical Information Symptom Recommended Solutions Results Related Problems Low Reproducibility of Concentration not compatible with the
14. Siltek I D x 0 D 3 x 8mm 5 x 8mm 5 x 8mm 5 x 8mm 3 x 8mm 3 x 8mm 3 x 8mm 3 x 8mm 5 x 8mm 5 x 8mm 5 x 8mm 5 x 8mm 5 x 8mm 5 x 8mm 5 x 8mm 5 x 8mm Mixed 5 x 8mm 5 x 8mm 1 x 2 5mm 2 x 2 bmm 0 75 x 2 5mm 1 x 2 5mm 1 x 2 5mm 2 x 2 bmm 2 x 2 bmm 2 x 2 5mm 1 x 2 bmm 1 x 2 5mm 2 x 2 bmm 1 x 2 5mm 2 x 2 5mm Length 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm 105mm Mixed 105mm 105mm 120mm 120mm 105mm 125mm 125mm 120mm 120mm 120mm 120mm 120mm 120mm 120mm 120mm Packing No No No No No No No No No No Quartz Wool Quartz Wool Quartz Wool Quartz Wool Quartz Wool Quartz Wool Mixed CarboFrit CarboFrit No No No No No No No No No No No No No Cat No 45372121 45311001 45350030 45354030 45350031 45354031 45350032 45354032 45350033 45354033 45311905 45314905 45312895 45314895 45312999 45314999 453TH001 45312130 45312131 45322052 45322056 45352083 45352054 45354054 45352057 45354057 45352060 45352062 45354062 45322044 45322046 45312120 Quantity 5 Pack 5 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 2 Pack 5 Pack 25 Pack 5 Pack 5 Pack 5 Pack 2 Pack 2
15. gt Specially designed convoluted stainless steel diaphragm provides good regulating performance and maximum purity integrity without the needfor a soft seal gt Capable of withstanding an internal vacuum gt All regulators supplied with in stainless steel output adaptor gt Built in check valve allows for cylinder change without contaminating the gas line High Purity Two Stage Brass Gas Regulators Inlet Filter Cat No Quantity CGA 580 Triple Filter 60180 902 1 Each DIN 6 Triple Filter 60180 904 1 Each CGA 350 Triple Filter 60180 906 1 Each DIN 1 Triple Filter 60180 908 1 Each CGA 320 Triple Filter 60180 910 1 Each CGA 580 Combi Filter 60180 916 1 Each DIN 6 Combi Filter 60180 918 1 Each CGA 350 Combi Filter 60180 920 1 Each DIN 1 Combi Filter 60180 922 1 Each CGA 320 Combi Filter 60180 924 1 Each CGA 590 Combi Filter 60180 926 1 Each DIN 13 Combi Filter 60180 928 1 Each Specifications Maximum Rated Inlet Pressure 3 500 psig Outlet Pressure Ranges 0 to 100 Flow Capacity Cv 0 05 Ambient Operating Temperature 40 F to 165 F Designed Leak Rate 2 x10 ccs helium Weight 5 6 Ibs Ports 5 1 4 FNPT Inlet A FNPT Outlet Compression Decay Inlet Characteristic 0 02 100 psi Materials Body Nickel Plated Brass Bonnet Nickel Plated Brass Seat PCTFE Diaphragm 316 Stainless Steel Gauges 2 Nickel Plated Brass Filter 316 Stainless Steel Outlet Valve Nickel Plated Brass Trim Nickel Plated Brass
16. 0 25 mm 1 290MA194 0 32 mm 1 290MA195 0 53 mm 1 290MA196 0 1 0 25 mm P 290MA215 0 32 mm 1 290MA216 0 53 mm 17 290MA217 0 1 0 25 mm 10 290MA201 0 32 mm 10 290MA202 0 53 mm 10 290MA203 290MA205 5 290MA207 2 290MA227 10 290MA228 GC Accessories Retention Gap Kits Support Thermo Scientific gas chromatography consumables gt Length of deactivated fused silica tubing al Ben gt Mini union gt 5 Ferrules Retention Gap Kits Description Cat No Quantity Retention gap kit I D 0 22 0 32mm 2m includes connectors 260RG497 1 Each Retention gap kit I D 0 53mm 2m includes connectors 260RG499 1 Each Retention gap kit I D 0 53mm 5m includes connectors 260RG500 1 Each Deactivated silica tubing 0 32mm I D 2m Length 260G498P 1 Each Deactivated silica tubing 0 53mm I D 2m Length 260G499P 1 Each Deactivated silica tubing I D 0 2bmm 5m 260G495P 1 Each Deactivated silica tubing I D 0 32mm 5m 260G496P 1 Each Deactivated silica tubing ID 0 53mm 5m 260G500P 1 Each Deactivated silica tubing ID 0 53mm 1m Siltek 260G401P 1 Each gt Kit contains one union and five ferrules Mini Capillary Unions For Use with Cat No Quantity 0 32mm ID capillary GC column 290GU498 1 Each 0 53mm ID capillary GC column 290GU499 10 Pack Capillary Column End Caps Feature a universal fit to all GC capillary columns gt Eliminate column contamination caused by leaving a column unsealed
17. 0 32mm 10m 0 1m 26RF024P 1 Each www thermoscientific com chromatography 261 TRACE GC Columns for Pesticides Specifically designed and tested for analysis of pesticides Applications gt Low bleed decreases MS contamination e rganophosphate pesticides gt Particularly useful for applications requiring a higher temperature e rganochlorine pesticides gt Column inertness results in minimal peak tailing and decreased breakdown e Pyrethroid pesticides of sensitive samples e Herbicides TRACE GC Columns for Pesticides Phase I D Length Film Thickness Guard Cat No Quantity TR Pesticide 0 25mm 30m 0 25um 5m guard column attached 26RF142F 1 Each TR Pesiticide Il 0 25mm 30m 0 25um bm guard column attached 26RD142F 1 Each TR Pesticide Ill 0 25mm 30m 0 25um 5m guard column attached 26RC142F 1 Each TR Pesticide IV 0 25mm 30m 0 25um 26RC142P 1 Each Ultrafast GC Columns Short narrow bore columns for use with the Thermo Scientific TRACE GC UltraFast instrument Applications e Chemical e Petrochemical e Environmental e Flavors and fragrances gt Dramatically shorter analysis times gt Increase sample throughput by a factor of 20 gt Lengthen column lifetimes Ultrafast Packed GC Columns Phase UFC 1 UFMC00001010401 UFC 1 UFC 1 UFC 1 UFMC00001070404 UFC 1 UFC 1 UFMC00001070907 UFC 5 UFC 5 UFC 5 UFMC00200000000 UFC 5 UFC 1701 UFC WAX UFC WAX UF
18. 0 32mm 30m 0 25um 26084 1430 1 Each 0 32mm 30m 0 5um 26084 2240 1 Each 0 32mm 30m Tum 26084 2970 1 Each 233 www thermoscientific com chromatography TraceGOLD TG WaxMS GC Columns Manufactured for better column to column reproducibility Applications NON POLAR eo u Phase Polyethylene Glycol PEG e Flavor compounds and Max Temps 240 260 C USP Listing G14 G15 G20 G39 essential oils e Solvents gt Polar phase polyethylene glycol e Xylene isomers e EPA Method 603 for Acrolein Acrylonitrile gt Polar deactivated surface tightly binds polymer for excellent thermal stability gt Resists oxidative damage damage from strongly acidic or basic volatiles better than silicone solid phases gt Equivalent to USP G14 G15 G16 G20 and G39 phases Similar to DB WAX DB WAXetr HP Wax HP Innowax Supelcowax 10 CP Wax 52 CB Stabilwax Rtx Wax BP20 ZB Wax Optima Wax AT Wax TraceGOLD TG WaxMS GC Columns I D Length Film Thickness Cat No Quantity 0 1mm 10m 0 1um 26088 0200 1 Each 0 25mm 15m 0 25um 26088 1300 1 Each 0 25mm 15m 0 5um 26088 2110 1 Each 0 25mm 30m 0 25um 26088 1420 1 Each 0 25mm 30m 0 5um 26088 2230 1 Each 0 25mm 60m 0 25um 26088 1540 1 Each 0 25mm 60m 0 5um 26088 2350 1 Each 0 32mm 15m 0 25um 26088 1310 1 Each 0 32mm 15m 0 5um 26088 2120 1 Each 0 32mm 15m Tum 26088 2850 1 Each 0 32mm 30m 0 25um 26088 1430 1 Each 0 32mm 30m 0 5um 26088 2240 1 Each 0 32mm 30m Tum 26088
19. 1 1 dichloroethene 2 1 1 1 trichloroethane 3 carbon tetrachloride TG 624 30m x 0 32mm x 1 80um 26085 3390 40 C 20 minute hold to 240 C hold FID He 2 15 mL min 1 0 uL Headspace Split 1 5 140 C 4 benzene 5 1 2 dichloroethane Residual Solvents Class 2 Mix A Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 methanol 2 acetonitrile resolution 1 35 3 dichloromethane 4 trans 1 2 dichloroethene 5 cis 1 2 dichloroethene 6 tetrahydrofuran 7 cyclohexane TG 624 30m x 0 32mm x 1 80um 26085 3390 40 C 20 minute hold to 240 C at 10 C min 20 minute hold FID He 2 15 mL min 1 0 uL Headspace Split 1 5 140 C 8 methylcyclohexane 9 1 4 dioxane 10 toluene 11 chlorobenzene 12 ethyl benzene 13 m xylene p xylene 14 o xylene Residual Solvents Class 2 Mix B Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 hexane 2 nitromethane 3 chloroform 4 1 2 dimethoxyethane TG 624 30m x 0 32mm x 1 8um 26085 3390 40 C 20 minute hold to 240 C at 10 C minute 20 minute hold FID He 2 mL min 1 0 uL Headspace Split 1 5 140 C 5 trichloroethylene 6 pyridine 7 2 hexanone 8 tetralin www thermoscientific com chromatography GC Applications CHEMICAL BIOCHEMICAL 219 CHEMICAL BIOCHEMICAL
20. 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each TRACE TR FAME GC Columns High polarity phase optimized for FAME analysis Applications WI NON POLAR e Fatty Acid Methyl Esters FAMES Phase 70 Cyanopropyl Polysilphenylene siloxane e FAMEs Cis Trans Isomers Mer en an USP Listing N A gt Polar phase 70 Cyanopropyl Polysilphenylene siloxane High operating temperature compared to competitor columns gt Low bleed for mass spectrometry use Similar to DB 23 BPX70 Rtx 2330 SP 2330 CP Sil 88 SP 2380 HP 23 VF 23ms 007 23 AT Silar PE 23 TRACE TR FAME GC Columns I D Length Film Thickness Cat No Quantity 0 10mm 10m 0 20um 260M096P 1 Each 0 22mm 25m 0 25um 260M135P 1 Each 0 22mm 30m 0 25um 260M141P 1 Each 0 22mm 50m 0 25um 260M147P 1 Each 0 22mm 60m 0 25um 260M153P 1 Each 0 25mm 30m 0 25um 260M142P 1 Each 0 25mm 60m 0 25um 260M154P 1 Each 0 25mm 120m 0 25um 260M166L 1 Each 0 32mm 25m 0 25um 260M137P 1 Each 0 32mm 30m 0 25um 260M143P 1 Each 0 32mm 50m 0 25um 260M149P 1 Each 0 32mm 60m 0 25um 260M155P 1 Each 259 www thermoscientific com chromatography TRACE GC Columns for Specific EPA Methods Low bleed and temperature stable performance tailored to specific EPA methodologies Applications gt TRACE TR 524 and TRACE TR 525 US EPA Drinking Water Test Methods 524 or 525 e Volatile Organic Compounds VOC s gt TRACE TR 527 US EPA Drinking Water Test Meth
21. 1310 1 Each 0 32mm 15m 0 5um 26083 2120 1 Each 0 32mm 15m Tum 26083 2850 1 Each 0 32mm 30m 0 25um 26083 1430 1 Each 0 32mm 30m 0 5um 26083 2240 1 Each 0 32mm 30m Tum 26083 2970 1 Each 0 32mm 60m 0 25um 26083 1550 1 Each 0 32mm 60m 0 5um 26083 2360 1 Each 0 32mm 60m Tum 26083 3090 1 Each 0 53mm 15m 0 25um 26083 1320 1 Each 0 53mm 15m 0 5um 26083 2130 1 Each 0 53mm 15m Tum 26083 2860 1 Each 0 53mm 30m 0 25um 26083 1440 1 Each 0 53mm 30m 0 5um 26083 2250 1 Each 0 53mm 30m Tum 26083 2980 1 Each 0 53mm 60m 0 5um 26083 2370 1 Each 0 53mm 60m Tum 26083 3100 1 Each TraceGOLD TG 200MS GC Columns Exceptionally inert mid polarity columns with selectivity and elution order optimized for difficult separations Applications NONE Phase Trifluoropropylmethyl Polisiloxane e Solvents Max Temps 320 C 340 C USP Listing G6 e Fluorocarbons Alcohols and letones gt Polar phase TrifluoropropyImethyl polysiloxane solid phase resolves e Silanes compounds that phenyl and cyano phases cannot e Glycols gt Outstanding thermal stability and low bleed gt Suitable for use with sensitive detectors including ECDs NPDs and MS gt Equivalent to USP G6 phase gt Confirmation column in combination with another GC column Similar to Rtx 200MS DB 200 DB 210 TraceGOLD TG 200MS GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 30m 0 25um 26084 1420 1 Each 0 25mm 30m 0 5um 26084 2230 1 Each 0 25mm 30m Tum 26084 2960 1 Each
22. 1430 226 552 1 Haloacetic acids and dalapon TG 1701MS 26090 1430 230 TG 35MS 26094 1430 226 GC Column Selection GC Column Selection by US EPA Waste Water Test Method selected EPA Waste Water methods are listed below with the appropriate recommended that you consult the original complete method or contact our Thermo Scientific GC column offerings In some cases there is more than technical support team for additional information or help in choosing the one phase or column dimension that can be used When in doubt it is correct column for your application Method Title Recommended Part Number Thermo Scientific Phase 601 Purgable halocarbons TG 624 26085 4080 229 TG 624 26085 3320 229 602 Purgable aromatics TG 624 26085 4080 229 TG 5MS 26098 2960 221 603 Acrolein and acrylonitrile TG 624 26085 4080 229 TG 5MS 26098 2960 221 604 Phenols TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 606 Phthalate ester TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 607 Nitrosamines TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 608 1 Organochlorine pesticides in industrial and municipal water TG 5MS 26098 2240 221 608 2 Organochlorine pesticides in wastewater TG 5MS 26098 2240 221 609 Nitroaromatics and isophorone TG 5MS 26098 1430 221 TG 35MS 26094 1430 226 610 Polynuclear aromatic hydrocarbons TG 5MS 26098 1420 221 611 Haloethers TG 5MS 26098 1430 221 TG 35MS 26094 1430 226 612 Chlorinated hydrocarbons TG 5MS 26098 1430 221 TG 35MS 26094 1430 226 613
23. 26088 2970 1458 Methyl acetate TG WAXMS 26088 2970 1500 Hydrocarbons b p 36 126 C TR 1 260A395P 1501 Aromatic hydrocarbons TG WAXMS 26088 2970 1550 Naphthas TG 1MS 26099 1540 1551 Turpentine TG 1MS 26099 1540 1552 Terpenes TG WAXMS 26088 3100 1601 1 1 Dichloro 1 nitroethane TG 1MS Inquire 1602 Dioxane TG 5MS 26098 2970 1604 Acrylonitrile TG WAXMS 26088 2240 1606 Acetonitrile TG WAXMS 26088 2970 1608 Glycidol TG WAXMS Inquire 1609 Tetrahydrofuran TG WAXMS 26088 2240 1610 Ethyl ether TG 1MS 26099 2970 1611 Methylal TG WAXMS Inquire 1612 Propylene oxide TG 5MS 26098 2970 1613 Pyridine TG 5SiIMS 26096 2970 1614 Ethylene oxide TG WAXMS Inquire 1615 Methyl tert butyl ether TG 1MS 26099 2240 1618 Isopropyl ether TR 1 260A395P 2000 Methanol TG 35MS 26094 2980 2004 Dimethlyacetamide and dimethylformamide TG WAXMS 26088 2240 2005 Nitroaromatics TG 5MS 26098 2250 2007 Aminoethanol compounds 1 TG 5MS Inquire 2010 Aliphatic amines TG 5MS 26098 1420 2012 n Butylamine TG 5MS 26098 1420 www thermoscientific com chromatography 259 220 220 229 220 234 234 234 234 229 234 220 234 234 234 221 234 234 234 234 234 221 221 220 234 234 245 234 220 220 234 220 221 234 234 234 234 220 234 221 221 234 220 245 226 234 221 221 221 221 215 GC Column Selection by NIOSH Method Title Recommended Part Number Thermo Scientific Phase 2017 Aniline o toluidine and nitrobenzene TG 5MS 26098 2970 221
24. 2970 1 Each 0 32mm 60m 0 25um 26088 1550 1 Each 0 32mm 60m 0 5um 26088 2360 1 Each 0 32mm 60m Tum 26088 3090 1 Each 0 53mm 15m 0 25um 26088 1320 1 Each 0 53mm 15m 0 5um 26088 2130 1 Each 0 53mm 15m Tum 26088 2860 1 Each 0 53mm 15m 1 5um 26088 3340 1 Each 0 53mm 30m 0 25um 26088 1440 1 Each 0 53mm 30m 0 5um 26088 2250 1 Each 0 53mm 30m Tum 26088 2980 1 Each 0 53mm 30m 1 5um 26088 3360 1 Each 0 53mm 60m 0 25um 26088 1560 1 Each 0 53mm 60m 0 5um 26088 2370 1 Each 0 53mm 60m Tum 26088 3100 1 Each 0 53mm 60m 1 5um 26088 3370 1 Each TraceGOLD TG WaxMS A GC Columns Acidic functionality in the polymer structure allows analysis ofacidic compounds without derivatization Applications NON OE PP Phase Polyethylene Glycol PEG e Organic acids Max Temps 250 C i USP Listing G25 G35 e Free fatty acids e Alcohols gt Polar phase acid deactivated polyethylene glycol gt Resists oxidative damage and adsorption of acids gt Excellent peak shapes for high MW acids gt Equivalent to USP G25 G35 phases Similar to DB FFAP HP FFAP NUKOL OV 351 CP Wax 58 CB FFAP Stabilwax DA BP 21 Optima FFAP TraceGOLD TG WaxMS A GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 26087 1300 1 Each 0 25mm 15m 0 5um 26087 2110 1 Each 0 25mm 30m 0 25um 26087 1420 1 Each 0 25mm 30m 0 5um 26087 2230 1 Each 0 25mm 60m 0 25um 26087 1540 1 Each 0 25mm 60m 0 5um 26087 2350 1 Each 0 32mm 15m 0 25um 26087 1310 1 Each 0
25. 32mm 15m 0 5um 26087 2120 1 Each 0 32mm 15m Tum 26087 2850 1 Each 0 32mm 30m 0 25um 26087 1430 1 Each 0 32mm 30m 0 5um 26087 2240 1 Each 0 32mm 30m Tum 26087 2970 1 Each 0 32mm 60m 0 25um 26087 1550 1 Each 0 32mm 60m 0 5um 26087 2360 1 Each 0 32mm 60m Tum 26087 3090 1 Each 0 53mm 15m 0 25um 26087 1320 1 Each 0 53mm 15m 0 5um 26087 2130 1 Each 0 53mm 15m Tum 26087 2860 1 Each 0 53mm 15m 1 5um 26087 3340 1 Each 0 53mm 30m 0 25um 26087 1440 1 Each 0 53mm 30m 0 5um 26087 2250 1 Each 0 53mm 30m Tum 26087 2980 1 Each 0 53mm 30m 1 5um 26087 3360 1 Each 0 53mm 60m 0 25um 26087 1560 1 Each 0 53mm 60m 0 5um 26087 2370 1 Each 0 53mm 60m Tum 26087 3100 1 Each 0 53mm 60m 1 5um 26087 3370 1 Each www thermoscientific com chromatography 235 gt TraceGOLD TG WaxMS B GC Columns Base deactivation allows analysis of basic analytes without derivatization or column priming Applications M Phase Modified Polyethylene Glycol PEG for Basic Compounds e Amines Max Temps 200 C 220 C USP Listing N A e Alkylamines e Diamines gt Polar phase base deactivated polyethylene glycol phase e Other basic compounds gt Reduced absorption and improved responsiveness for basic compounds gt Not suitable for use with water or alcohols Similar to CAM Carbowax Amine CP Wax51 Stabilwax DB TraceGOLD TG WaxMS B GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 26086 1300 1 Each 0 25mm 30m 0 25um 2
26. 400 C 360 C 370 C for films lt 1 5um 350 C 360 C for films gt 1 5um 360 C 370 C 360 C 370 C 280 C 300 C 280 C 300 C 230 C 250 C 250 C 260 C 260 C 280 C for films lt 1 0um 240 C 260 C for films gt 1 0um 280 C 300 C 240 C 250 C TR SIMDIST TR 524 TR 525 TR 527 TR 8095 TR 8270 TR Pesticide TR Pesticide II TR Pesticide III TR Pesticide IV TR Biodiesel M TR Biodiesel F TR Biodiesel G TR DoA5 TR DoA35 TR Dioxin 5MS TR PCB 8MS achieved in approximately one hour This duration may be longer in the Maximum Operating Temperature 400 C for films lt 1 0um 370 C for 2 65um films 240 C 260 C 340 C 360 C 330 C 350 C 360 C 370 C 330 C 350 C 330 C 350 C 330 C 350 C 300 C 320 C 300 C 320 C 300 C 320 C 280 C 300 C 380 C 400 C 330 C 350 C 330 C 350 C 330 C 350 C 330 C 350 C GC Technical Information Column Conditioning for the TRACE TR WaxMS and TR MS Columns This procedure will ensure an ultra low bleed for the columns entire lifetime After installing the column according to the instrument manufactures and is only required once Once performed future installation of the column instructions need only be followed by a 30 minute hold at the maximum temperature limit follow the procedure below Steps TR WaxMS TR 1MS 1 Equilibrate the column at 40 C with carrier gas flow
27. 5 mL min 0 2 uL Direct 290 C 9 propachlor 17 Paarlan 10 Tolban 18 Prowl 11 propazine 19 bromacil 12 atrazine 20 oxadiazon 13 simazine 21 GOAL 14 terbacil 22 hexazinone 15 Sencor 16 Dua EPA 1671 Volatile Organic Compounds Column TG WAXMS 30m x 0 32mm x 1 0um Part Number 26088 2970 Temperature 40 C 5 0 minute hold to 180 C at 7 C minute 5 0 minute hold Detector Type FID Carrier Gas He Flow Rate 2 5 mL min Injection Volume 1 0 ul Injection Mode Split 12 1 200 C 1 tetrahydrofuran IS 4 acetonitrile 7 formamide 2 methanol 5 n propanol 8 dimethyl sulfoxide 3 ethanol 6 Methyl Cellosolve 9 ethylene glycol EPA 1671 Volatile Organic Compounds Column TG WAXMS B 30m x 0 32mm x 1 0um Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 dimethylamine 2 methylamine 3 diethylamine 4 triethylamine 5 tetrahydrofuran IS 6 methanol 7 ethanol 8 acetonitrile 26086 2970 40 C 5 0 minute hold to 180 C at 7 C minute 5 0 minute hold FID He 2 5 mL min 1 0 uL Split 12 1 200 C 9 n propanol 10 Methyl Cellosolve 11 formamide 12 dimethyl sulfoxide ethylene glycol no elution Included in sample but does not elute due to base deactivation in the TG WAXMS B phase Tame min Time min GC Applications Polycyclic Aromatic Hydrocarbons Column TG 17MS 30m x 0 2
28. 50mm 50mm 50mm 70mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm Gauge 23 23 23 26 26 26 26 26 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 22 Needle Point Cone Cone Cone Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Bevel Replacement Needles for GC Syringes Replacement Needles for GC Syringes For Syringe Models 365D1611 365D1841 365D1771 365D3731 365H2301 365K3041 365F1931 36562161 365H2381 36512611 365F1901 365G2091 365J2881 36500495 36503015 36500490 36520050 36520051 36520055 365D1811 36500761 365D1171 365D1781 36500510 36500520 36545333 365F3988 365D1791 www thermoscientific com chromatography Cat No 365A0331 365B0511 365B0531 365C0741 365C0761 365D1091 365D1096 365D1171 365F1891 365F1901 365F1921 365F1931 365G2081 365G2091 365G2111 365G2161 365H2291 365H2301 365H2321 365H2381 36512541 36512561 36512611 365J2831 365J2881 365K3041 365K3051 Cat No 365RN252 365RN362 365RN272 365RN372 365RN225 365RN235 36566485 36566480 36550040 365RN351 365RN555 365RN215 365RN282 36550045 36550046 365RN732 365RN749 GC Accessories Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 6 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Eac
29. Columns Non polar columns incorporating particles to the walls ofthe tubing for essentially no particle release Applications gt Non polar 100 divinyl benzene phase e C1 to C3 isomers and alkanes up gt Particles incorporated to the walls of the tubing for essentially to C12 no particle release e Separation of CO methane and O N CO e Analysis of oxygenated compounds and solvents Similar to CP PoraPLOT Q Rt Q BOND CP PoraBond Q Supel Q Plot AT Q TracePLOT TG BOND Q GC Columns I D Length Film Thickness Cat No Quantity 0 32mm 15m 10um 26004 6000 1 Each 0 32mm 30m 10um 26004 6030 1 Each 0 53mm 15m 20um 26004 6060 1 Each 0 53mm 30m 20um 26004 6090 1 Each TracePLOT TG BOND Q GC Columns Intermediate polarity columns incorporating particles to the walls of the tubing for essentially no particle release Applications gt Intermediate polarity porous divinyl benzene homopolymer Separation of ethane ethylene and Particles incorporated to the walls of the tubing for essentially acetylene to baseline no particle release Similar to GS Q Rt OS BOND TracePLOT TG BOND 0 GC Columns I D Length Film Thickness Cat No Quantity 0 32mm 15m 10um 26005 6000 1 Each 0 32mm 30m 10um 26005 6030 1 Each 0 53mm 15m 20um 26005 6060 1 Each 0 53mm 30m 20um 26005 6090 1 Each www thermoscientific com chromatography 241 TracePLOT TG BOND S GC Columns Midpolarity columns incorporating particles to the walls of
30. Derivatized Cholrinated Acetic Acids Alkylated Column TR 5 30m x 0 25mm x 0 25um Part Number 260E142P Temperature 40 C 1 minute hold to 300 C at 10 C min 5 minute hold Detector Type FID Carrier Gas He Flow Rate 1 2 mL min Injection Volume 1 0 uL Injection Mode Split 50 1 240 C 1 Derivatised TCA 2 Derivatised TCA 3 PFB byproduct 4 Derivatised CA 5 Derivatised DCA 9 10 11 12 13 minutes 14 15 16 17 Derivatized Amino Acids Silylated Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 Derivatised L Alanine 2 Derivatised L Leucine INDUSTRIAL Analysis of Tea Tree Oil Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 alpha Pinene 2 beta Phellandrene 3 beta Pinene 4 beta Myrcene 5 alpha Terpinene 6 Cymene 7 Limonene Terpenes Column Part Number Initial Temp Rate 1 Final Temp Detector Type Detection Conditions Carrier Gas Flow Rate Injection Temp Injection Mode Split Ratio 1 a pinene 2 Camphene 3 B pinene 4 d limonene 5 p cymene 6 a terpinene 7 Linalool 8 Fenchone 9 isopulegol TR 5 30m x 0 25mm x 0 25um 260E142P 100 C to 300 C at 15 C min FID He 1 2 mL min 1 0 uL Split 90 1 240 C 3 Derivatised L Lysine TG 5MS 30m x
31. Dioxin TG 5MS 26098 1540 221 614 Organophosphorous pesticides in industrial and municipal water TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 614 1 Organophosphorous pesticides in wastewater TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 615 Chlorinated herbicides in industrial and municipal water TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 616 C H and O compounds TG 1MS 26099 1420 220 TG 5MS 26098 1420 221 617 Organohalide pesticides and PCBs in industrial and municipal water TG 5MS 26098 1420 221 618 Volatile pesticides in industrial and municipal water TG 1MS 26099 2240 220 TG 5MS 26098 2240 221 619 Triazines pesticides and PCBs in industrial and municipal water TG 35MS 26094 1430 226 620 Diphenylamine in industrial and municipal water TG 1MS 26099 1430 220 TG 5MS 26098 1430 221 622 Organophosphorous pesticides in industrial and municipal water TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 622 1 Thiophosphate pesticides TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 624 Purgeables TG 624 26085 4080 229 TG 624 26085 3320 229 625 Base neutrals and acids TG 5MS 26098 1420 221 TG 5MS 26098 1430 221 627 Dinitroaniline pesticides in industrial and municipal water TG 5MS 26098 1430 221 TG 35MS 26094 1430 226 630 1 Dithiocarbamate pesticides as carbon disulfide TG 5MS 26098 1420 221 TG 5MS 26098 1430 221 633 Organonitrogen pesticides TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 633 1 Neutral nitrogen containing pesticides TG 5MS 26098 1420 221 TG 35MS
32. Flow Rate 2 5 mL min Injection Volume 2 0 uL Injection Mode split 10 1 270 C High Throughput Confirmation and Quantitation of a THC Metabolite in Urine using the DSQ II GC MS For the sample preparation procedure and conditions used for the GC MS analysis please request Application Note TN10161 Antidepressant and Anticonvulsant Drugs Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Details TR 50MS 30 m x 0 25 mm x 0 25 um 260R142P 150 C 0 5 min 10 C min to 180 C 1 5 C min to 220 C 30 C min to 260 C hold 5 min MS He 25 7 psi 1 8 1 0 uL Splitless 0 5 min Blood Alchohols Column Part Number Temperature Detector Type Carrier Gas Fow Rate Injection Volume Injection Mode 1 Acetaldehyde 2 Methanol 3 Ethanol TR WAX 30m x 0 53mm x 1 0um 260W298P 55 C Isothermal FID He 4 mL min 1 0 uL Split 20 1 200 C 4 Acetone 5 Isopropanol propan 2 ol 6 n Propanol RT 1 73 MA 1062883 RT 1 73 MA 307106 Relative Abundance RT 1 73 MA 153375 n c PR OG Oo o do o oo 1 75 Time min 24060504 2000000 1600000 www thermoscientific com chromatography GC Applications 271 FORENSIC AND TOXICOLOGY Amines and Phenols Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection M
33. HP 624 SPB 1301 SPB 624 VP 1301 BF 624ms CP 1301 CP Select 624 CB TraceGOLD TG 1301MS GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 26091 1300 1 Each 0 25mm 15m 0 5um 26091 2110 1 Each 0 25mm 15m Tum 26091 2840 1 Each 0 25mm 30m 0 25um 26091 1420 1 Each 0 25mm 30m 0 5um 26091 2230 1 Each 0 25mm 30m Tum 26091 2960 1 Each 0 25mm 60m 0 25um 26091 1540 1 Each 0 25mm 60m 0 5um 26091 2350 1 Each 0 25mm 60m Tum 26091 3080 1 Each 0 25mm 60m 1 4um 26091 3330 1 Each 0 32mm 15m 0 25um 26091 1310 1 Each 0 32mm 15m 0 5um 26091 2120 1 Each 0 32mm 15m Tum 26091 2850 1 Each 0 32mm 15m 1 5um 26091 0680 1 Each 0 32mm 30m 0 25um 26091 1430 1 Each 0 32mm 30m 0 5um 26091 2240 1 Each 0 32mm 30m Tum 26091 2970 1 Each 0 32mm 30m 1 5um 26091 3350 1 Each 0 32mm 30m 1 8um 26091 3390 1 Each 0 32mm 60m 0 25um 26091 1550 1 Each 0 32mm 60m 0 5um 26091 2360 1 Each 0 32mm 60m Tum 26091 3090 1 Each 0 32mm 60m 1 8um 26091 3410 1 Each 0 53mm 15m 0 25um 26091 1320 1 Each 0 53mm 15m 0 5um 26091 2130 1 Each 0 53mm 15m Tum 26091 2860 1 Each 0 53mm 15m 1 5m 26091 3340 1 Each 0 53mm 15m 3um 26091 3840 1 Each 0 53mm 30m 0 25um 26091 1440 1 Each 0 53mm 30m 0 5um 26091 2250 1 Each 0 53mm 30m Tum 26091 2980 1 Each 0 53mm 30m 1 5um 26091 3360 1 Each 0 53mm 30m 3um 26091 3960 1 Each 0 53mm 60m 0 25um 26091 1560 1 Each 0 53mm 60m 0 5um 26091 2370 1 Each 0 53mm 60m Tum 26091 3100 1 Each 0 53mm 60m 1 5um 26091 3370 1 Each 0 53mm 60m 3um 26091 4080
34. Manual On Column and Septum Injection Series N Fixed Needle 90 Volume Length Needle Gauge Needle Point Cat No Quantity 25uL 51mm 22s 90 NS101502 1 Each 50uL 51mm 225 90 NS101602 1 Each 100uL 51mm 225 90 NS101702 1 Each 250uL 51mm 225 90 NS101802 1 Each Syringes for Manual On Column and Septum Injection Series N Removable Needle Bevel Use with JADE or Merlin septumless injectors split and splitless mode gt 26s and 22s Gauge needle National Scientific Target Precision Syringes for Manual On Column and Septum Injection Series N Removable Needle Bevel Volume Length Gauge Needle Point Cat No Quantity SuL 51mm 26s Bevel NS100305 1 Each 10uL 51mm 26s Bevel NS100405 1 Each 25uL 51mm 22s Bevel NS100505 1 Each 50uL 51mm 22s Bevel NS100605 1 Each 100uL 51mm 22s Bevel NS100705 1 Each 250uL 51mm 22s Bevel NS100805 1 Each 500uL 51mm 22s Bevel NS100905 1 Each Syringes for Manual On Column and Septum Injection Replacement Needles Bevel National Scientific Target Precision Syringes for Manual On Column and Septum Injection Replacement Needles Bevel Volume Length Gauge Needle Type Cat No Quantity SuL 51mm 26s Bevel NS832301 3 Pack 10uL 51mm 26s Bevel NS832401 3 Pack 25 100uL 2 51mm 22s Bevel NS832401 3 Pack 250 500uL 2 51mm 22s Bevel NS832601 3 Pack Pe GC Accessories Syringes for Manual On Column and Septum Injection Replacement Needles Blunt National Scientific Target Precision S
35. Nes Where L is the column length The smaller the N s the more efficient the column s performance HETP H Height Equivalent to a Theoretical Plate is a measure of column efficiency where L is the column length and N is the number of theoretical plates H L N HETP is based on actual tg rather than adjusted retention times te Linear Velocity u Mobile phase flow rate expressed in cm s and is expressed as u Lt Where L is the column length and t is the breakthrough time of an unretained peak Phase Ratio The ratio of the volume of mobile phase to the stationary phase An important value when changing the column dimensions in a method B column ID um 4 x film thickness um Resolution A measure of the separation of two peaks taking into account both the difference in elution time and the peak widths tt 0 5 W Wa Where t and t are the two retention times and W and W are baseline peak widths S Selectivity o The relative retention of two adjacent peaks Selectivity can be calculated using capacity factor ko ki Trennzahl Number A value to describe a separation The Trennzahl number is calculated from the resolution between two consecutive homolo gous hydrocarbons The Trennzahl number represents the number of peaks that can be included between the two hydrocarbon peaks tut T R2 R1 f mm wi Where tg equals analyte retention time and W equals peak width at ha
36. No 60180 840 1 Each High Flow Cartridge Pack 2 x H 0 with indicator for LEMS No 60180 841 1 Each Super Clean Cartridge Filter Baseplates One time installation procedure Can be configured to the individual user requirements Needle valves ensure gas line is not contaminated during cartridge change Filters are not included Type For Use with For Gas Single Base Triple Filter Carrier Gas Only Dual Base 2 x Combi Filter Air and Fuel Gas Triple Base Triple and 2 x Combi Filter Carrier Make Up and Fuel Gas Four position Base Moisture Oxygen 2 x Hydrocarbon High capacity carrier fuel make up Two position High flow Base N in LC MS HO in H air generators Carrier make up and fuel Super Clean Cartridge Filter Baseplates Manifolds Type Cat No Quantity Single Base 60180 814 1 Each Dual Base 60180 815 1 Each Triple Base 60180 817 1 Each Two position High flow Base 60180 816 1 Each Four position Base 60180 818 1 Each O rings for base plates 60180 837 1 Each Flush Cap 60180 838 1 Each www thermoscientific com chromatography 289 gt For non corrosive analytical and process applications gt Includes a built in Smart Purifier Base and Cartridge ensuring 99 99999 gas purity gt Specially designed convoluted stainless steel diaphragm provides good regulating performance and maximum purity integrity without the need for a soft seal gt Capable of withstanding an internal vacuum gt All
37. Non polar phase 100 Dimethyl polysiloxane gt Optimized for simulated distillation analysis High temperature limits gt Strongly cross linked Similar to DB HT Sim Dis DB 2887 BPX1 Rtx 2887 HP 1 Petrocol 2887 Petrocol EX2887 TRACE TR SimDist GC Columns I D Length Film Thickness Cat No Quantity 0 10mm 10m 0 10um 260S020P 1 Each 0 53mm 6m 2 65um 26053475 1 Each 0 53mm 10m 0 10um 260S025P 1 Each 0 53mm 10m 0 90um 260S250P 1 Each 0 53mm 10m 2 65um 260S348P 1 Each 25 www thermoscientific com chromatography TRACE TR V1 GC Columns Mid polarity thick film columns Applications e Volatile Organics e Alcohols e EPA 502 2 608 amp 624 NON POLAR Phase Max Temps USP Listing 6 Cyanopropylpheny Polysiloane 280 C 300 C G43 gt Mid polarity phase 6 Cyanopropylphenyl Polysiloxane gt Thick films for the analysis of volatile analytes gt Low bleed suitable for MS detection Similar to DB 624 BPX Volatiles Rtx Volatiles VOCOL 56 0V 624 AT 624 HP VOC CP Select 624CB 007 624 ZM 624 TRACE TR V1 GC Columns I D Length 0 18mm 20m 0 18mm 40m 0 25mm 30m 0 25mm 60m 0 32mm 30m 0 32mm 60m 0 53mm 30m 0 53mm 30m 0 53mm 60m 0 53mm 75m Film Thickness 1 00um 1 00um 1 40um 1 40um 1 80um 1 80um 3 00um 5 00um 3 00um 3 00um Cat No 260V495P 260V496P 260V332P 260V333P 260V339P 260V341P 260V396P 260V470P 260V408P 260V490P Quantity
38. Oc ol 16 2 Amino 4 6 dinitrotoluene 17 Tetryl 18 HMX 1 3 Dichlorobenzene p Isopropyltoluene 1 2 Dichlorobenzene n Butylbenzene 1 4 Dichlorobenzene 1 2 Dibromo 3 chloropropan 1 2 4 Trichlorobenzene Hexachlorobutadiene Naphthalene 1 2 3 Trichlorobenzene 271 PETROCHEMICAL Unleaded Gasoline Column TG 1MS 30m x 0 25mm x 0 25um Part Number 26099 1420 Temperature 50 C 2 0 minute hold to 75 C at 10 C minute to 300 C at 20 C minute 5 minute hold Detector Type FID Carrier Gas He Flow Rate 1 0 mL min Injection Volume 1 0 uL Injection Mode Split 20 1 250 C TT TT T 1 T 1 6 8 10 12 14 GC PCOLO 1 Biodiesel aom Column TR Biodiesel F 30 m x 0 25 mm x 0 25 um Part Number 26AX142P Temp 200 C isothermal Inlet Temp 250 C Detector Type FID Detector Temp 250 C Carrier Gas Helium Flow Rate 1 6 mL minute 2 Split Ratio 50 1 Injection Volume 1 0 uL 1 C12 0 7 C18 1ngcis 2 C14 0 8 C18 2n6cis 3 C16 0 9 C18 3n3 4 C16 1 10 C20 0 5 17 0 Internal standard 11 C24 0 6 C18 0 Minutes Hydrocarbon Standard 24060510 SimDist Column TR SimDist 10 m x 0 53 mm x 0 9 um Part Number 2605250P Temperature 40 C 10 C min to 39 0 C hold 10 min C20 Detector Type FID Detection Conditions 400 C Carrier Gas He Flow Rate 20 mL min Hydrocarbon Standard Mix 10 20 minutes ASTM D2887 Colu
39. Pack 5 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 5 Pack 25 Pack 2 Pack 2 Pack 5 Pack GC Accessories Mega 4000 5000 and 6000 FT Split Straight Liner 2 x 5mm 79 5mm No 45350300 5 Pack Split Straight Liner 3 x 5mm 79 5mm No 45350400 5 Pack a JJ Z Split Splitless Liner With 5 x 5mm 79 5mm Quartz Wool 45312955 5 Pack Recessed Gooseneck Injection Port Liners for Agilent Instruments Injection Port Liners for Agilent Instruments Injection Type Direct Straight Liner Direct Straight Liner oplit Splitless FocusLiner oplit Splitless FocusLiner Split Splitless Fast FocusLiner Split Splitless FAST FocusLiner Split Splitless Liner w Recessed Gooseneck Split Splitless Liner w Recessed Gooseneck Split Straight Liner Split Straight Liner oplit Splitless FocusLiner with Single Taper oplit Splitless FocusLiner with Single Taper Splitless Liner with Single Taper Splitless Straight Liner Splitless Liner with Recessed Gooseneck Split Straight Liner Split Straight Liner Split Splitless Liner with Single Taper Split Splitless Liner with Single Taper Cyclo Single Gooseneck Deactivated Metal Split Splitless Liner with Double Taper Split Splitless Liner with Double Taper Split Splitless FAST FocusLiner with Single Taper Split Splitless FAST FocusLiner with Single Taper single Gooseneck Deactivated Metal Split
40. Part Number 260X224P Temperature Detector Type Detection Carrrier Gas Flow Rate Injection Volume Injection Mode 1 Acetone 2 Ethyl acetate 3 Methyl ethyl ketone 4 Contaminant 9 Butyl acetate 10 iso Butanol 11 Propylene glycol Monomethyl ether 35 C 3 min 15 C min to 230 C hold 4 min FID 270 C He 8 4 psi 30cm s 1 84 mL min 0 1 uL oplit 83 1 purge on vent 150 mL min 17 Butyl Cellosolve acetate 18 Cyclohexanone 19 Butyl Cellosolve 5 iso Propanol 12 n Butanol 20 Butyl glycol acetate 6 Ethanol 13 Ethyl benzene 22 Isophorone 7 Methyl isobutyl 14 p Xylene 23 Butyl Carbitol ketone 15 m Xylene 24 Benzyl alcohol 8 Toluene 16 o Xylene Solvent Mixture Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode Methanol Ethanol Acetonitrile Acetone Dichloromethane 1 1 1 Trichloroethene Nitromethane Trans 1 2 Dichloroethene 9 Cis 1 2 Dichloroethene 10 Tetrahydrofuran 11 Ethyl acetate 12 1 2 Dichloroethane 13 n Hexane 14 1 1 1 trichloroethane 15 Benzene Trichloroethylene CO TON GL I c TG BOND Q 30m x 0 32mm x 10um 26004 6030 100 C to 240 C at 5 C minute 10 minute hold FID He 1 5 mL min 1 0 uL Split 220 C 17 1 4 Dioxane 18 2 Hexanone 19 Pyridine 20 N N Dimethylformamide 21 n Heptane 22 Methycyclohexane 23 Toluene 24 DMSO 25 Chlorobenzene
41. Peak Fronting Ghost Peaks Broad Ghost Peaks Irregular Chair shaped Peaks No Peaks After Solvent Peak No Peaks at All Sample Peak Tailing Solvent Peak Tailing Unresolved Peaks Discrete High intensity Contaminant Peaks Cause Injection speed too low Wrong autosampler injection speed or mode Column or detector overloaded Column temperature too low Stationary phase too thin Poor injection technique Contaminated carrier gas Contamination from laboratory glassware Decomposition of injected sample Dirty injection solution Contaminated inlet or pneumatics Incomplete elution of previous sample Solvent flooding of column Carrier gas flow too high Combustion gas flow incorrect Detector contaminated FID flame extinguished by solvent peak Too much sample injected Incorrect column position in S SL injector too high Clogged syringe needle Column broken or disconnected Defective electrometer or amplifier Defective recording device FID flame is out Incorrect column position in S SL injector too high Column degradation causing activity Column oven temperature too low Column contaminated at inlet Glass wool or inlet liner causing activity Inlet temperature too low Poor or obstructed column connections Wrong stationary phase Incorrect column position in inlet Initial oven temperature too high On Column Septum purge flow too low and or split splitless ve
42. Phthalate esters TG 5MS 26098 1420 221 8070 Nitrosamines TG 5MS 26098 1430 221 8081 Organochlorine pesticides and PCBs TG 5MS 26098 2230 221 TG 17MS 26089 1420 231 8090 Nitroaromatics and cyclic ketones TG 5MS 26098 1430 221 8095 Explosives TR 8095 260P123P 260 8100 Polynuclear aromatic hydrocarbons TG 5MS 26098 1420 221 8110 Haloethers TG 5MS 26098 1420 221 8120A Chlorinated hydrocarbons TG 5MS 26098 1430 221 8121 Chlorinated hydrocarbons TG 5MS 26098 1430 221 8140 Organophosphorous pesticides TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 8141A Organophosphorous pesticides TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 8150B Chlorinated herbicides TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 8151 Chlorinated herbicides TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 8240B Volatile organic compounds TG 624 26085 4080 229 TG 624 26085 3320 229 8250A Semi volatile organic compounds TG 5MS 26098 1420 221 TG 5MS 26098 1430 221 8260A Volatile organic compounds TG 624 26085 4080 229 TG 624 26085 3320 229 8270B Semi volatile organic compounds TG 5MS 26098 1420 221 TG 5MS 26098 1430 221 8270C Semi volatile organic compounds TR 8270 26RF296P 260 8280 Polychlorinated dioxins and furans TG 5MS 26098 1540 221 8290 Polychlorinated dioxins and furans TG 5MS 26098 1540 221 GC Column Selection GC Column Selection by NIOSH Method selected NIOSH methods are listed below with the recommended Thermo doubt it is recommended that you consult the original co
43. Replacement Indicating Cartridge Filters Indicating cartridge filters for inert carrier gases Replacement Indicating Cartridge Filters For High Purity Regulators Description Indicator Change Cat No Quantity Combi Indicating Filter H20 HC Purple to Green 60180 941 1 Each Triple Indicating Filter H20 O HCs Orange to Gray 60180 940 1 Each Purple to Green www thermoscientific com chromatography 291 Valve with SMART Indicating Purifier VIP Provide either flow control or positive shut off while maintaining gas purity for gasses 99 9999 pure or better gt Provides a visual indication of contaminants in the gas stream while it is removing them ensuring consistent performance of analytical processes gt Safeguards the gas stream and process gt Specially cleaned for all analytical applications and will not generate contaminates that consume the purifier Patented Quick Change Base to allow for easy change out of spent purifiers gt Available in both a multiturn and quarter turn models gt All valves supplied with a in stainless steel output adaptor VIP Valves with SMART Filter Description Filter Cat No Quantity Multi Turn Triple Filter 60180 950 1 Each Multi Turn Combi Filter 60180 951 1 Each Quarter Turn Triple Filter 60180 952 1 Each Quarter Turn Combi Filter 60180 953 1 Each Specifications Weight 1 Ib Maximum Rated Inlet Pressure 165 PSIG Flow Capacity 12 L min Ambient Op
44. Replacement Needle National Scientific Target Precision Syringes for On Column Fused Silica Replacement Needle Volume Needle Length 0 D Cat No Quantity SuL 100mm 0 23mm NS822031 3 Pack 10uL 100mm 0 23mm NS822042 3 Pack www thermoscientific com chromatography 321 GC Method Selection and Optimization The following flow chart briefly describes the common steps in GC method development and optimization Start Identify analytes Improve sensitivity Increase injection volume Reduce film thickness Produces sharper peaks Reduce column diameter reduces HETP Increase pressure to maintain linear flow rate I Review applications library applications Index application found Suitable Yes Increase retention Reduce temperature ramp rate Increases the distribution co efficient and increases analyte dwell time in the stationary phase Reduce carrier linear flow rate Increases interaction with the stationary phase Increases retention and resolution but also peak broadening Increase film thickness More interaction with the sample Change the phase More polar columns retain polar compounds better and vice versa Increase column length Maintain linear velocity Improve resolution Reduce temperature ramp rate Increases the distribution co efficient and increases analyte dwell time in the stationary phase Reduce carrier linear flow rate Increases interaction wi
45. Splitless Mixed Liner Sample Pack Cyclosplitter Liner Deactivated Metal Split Splitless Liner with Wool Deactivated Metal www thermoscientific com chromatography I D x 0 D 1 2x 6 3mm 1 2x 6 3mm 4 x 6 3mm 4 x 6 3mm 2 3 x 6 3mm 2 3 x 6 3mm 4 x 6 3mm 4 x 6 3mm 4 x 6 3mm 4 x 6 3mm 4 x 6 3mm 4 x 6 3mm 4 x 6 3mm 2 0 x 6 1mm 2 0 x 6 3mm 4 x 6 3mm 4 x 6 3mm 4 x 6 3mm 4 x 6 3mm 5 2 x 6 3mm 4 x 6 3mm 4 x 6 3mm 2 3 x 7 3mm 2 3 x 6 3mm 5 2 x 6 3mm Mixed 5 2 x 6 3mm 5 2 x 6 3mm Length 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm 78 5mm Mixed 78 5mm 78 5mm Packing None None Quartz Wool Quartz Wool Quartz Wool Quartz Wool Quartz Wool Quartz Wool Quartz Wool Quartz Wool None None Quartz Wool Quartz Wool None None None None None None None None Quartz Wool Quartz Wool None None None Quartz Wool Cat No 453A1335 453A2332 453A1255 453A1252 453A1285 453A2282 453A1305 453A2302 453A2265 453A1262 453A1315 453A1312 453A1925 453A2275 453A2325 453A1295 453A2292 453A1345 453A2342 453A2000 453A1355 453A2352 453A2375 453A1372 453A2001 453AG001 453A2002 453A2003 Quantity 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 25 Pack 5 Pack 5 Pack 5 Pack 5 Pack 25 Pack 5 Pack
46. are sorted by industry GC Applications ENVIRONMENTAL Organochlorine and Organophosphorus Pesticides Column TG 5MS 30m x 0 25mm x 0 25um Part Number 26098 1420 Temperature 100 C 0 5 minute hold to 300 C at 7 C minute 1 minute hold Detector Type MS Carrier Gas He Flow Rate 1 2 mL min Injection Volume 1 0 uL Injection Mode Split 10 1 290 C 1 naphthalene d8 14 heptachlor 27 endrin 2 dichlorvos 15 fenitrothion 28 endosulfan Il 3 acenaphthene d10 16 pirimiphos methyl 29 4 4 DDE bL I 4 methacrifos 17 malathion 30 4 4 DDD 5 a BHC 18 aldrin 31 endosulfan sulfate 6 hexachlorobenzene 19 chlorpyrifos 32 44 DDT l IJ MI 7 y BHC lindane 20 heptachlor epoxide 33 chrysene d12 E M Al LAU JUN MUN MA lL A z 8 B BHC 21 oxychlordane 34 perylene d12 5 00 6 00 7 00 8 00 9 00 10 00 11 00 12 00 13 00 14 00 15 00 16 00 17 00 18 00 aim al 0022 00 23 00 24 00 25 00 26 00 27 00 min 9 phenanthrene d10 22 trans chlordane 10 diazinon 23 endosulfan 11 etrimphos 24 cis chlordane 12 phosphamidon 25 2 4 DDT 13 chlorpyrifos methyl 26 dieldrin EPA 8270 Semivolatile x Organics 14 denropbend RF 0 245 Column TG 5SilMS 30m x 0 25mm x 0 25um EIC 184m z Part Number 26096 1420 Temperature 40 C 1 0 minute hold to 280 C at 25 C minute to 320 C at 5 C minute 1 0 minute hold Detector Type MS 22
47. excellent quality and performance with guaranteed reproducibility 244 TRACE TR GC Columns General purpose nonpolar columns Applications E NON POLAR e Hyd rocarbons Phase 100 Dimethyl Polysiloxane e PO NA Max Temps 340 C 360 C for films lt 1 0um 300 C 320 C for 3 0um films 280 C 300 C for films gt 3 0um e Esters USP Listing G1 G2 G38 e Pesticides e Drugs gt Non polar phase 100 dimethyl polysiloxane e Amines gt Low bleed for increased sensitivity even at high temperatures gt Outstanding robustness for difficult separations gt Reliable and reproducible performance Similar to DB 1 DB Petro BP1 HP 1 HP 1MS Rtx 1 Ultra 1 SPB 1 SPB 1 Sulfur Petrocol DH CP Sil 5CB RSL 150 RSL 160 ZB 1 CB 1 OV 1 PE 1 007 1 MS SP 2100 SE 30 RH 1 CC 1 CP Sil 5CB MS VF 1ms TRACE TR 1 GC Columns I D Length Film Thickness Cat No Quantity 0 10mm 10m 0 1um 260A020P 1 Each 0 10mm 10m 0 5um 260A196P 1 Each 0 15mm 50m 0 50um 260A227P 1 Each 0 25mm 15m 0 1um 260A035P 1 Each 0 25mm 15m 0 25um 260A130P 1 Each 0 25mm 30m 0 1um 260A047P 1 Each 0 25mm 30m 0 25um 260A142P 1 Each 0 25mm 30m 0 5um 260A223P 1 Each 0 25mm 30m Tum 260A296P 1 Each 0 25mm 60m 0 25um 260A154P 1 Each 0 25mm 60m Tum 260A308P 1 Each 0 25mm 100m 0 5um 260A241P 1 Each 0 25mm 100m Tum 260A314P 1 Each 0 32mm 15m 0 1um 260A036P 1 Each 0 32mm 15m 0 25um 260A131P 1 Each 0 32mm 15m 0 5um 260A212P 1 Each 0 32mm 30m 0 1um
48. for 20 minutes purging air content Equilibrate the column at 40 C with carrier gas flow for 20 minutes purging air content 2 Raise the temperature to 100 C at 5 C min Raise the temperature to 100 C at 5 C min 3 Hold for 30 minutes Hold for 30 minutes 4 Raise to 150 C at 5 C min Raise to 150 C at 5 C min 5 Hold for 30 minutes Hold for 30 minutes 6 Raise to 200 C at 5 C Raise to 250 C at 5 C 7 Hold for 40 minutes Hold for 40 minutes 8 Raise to 250 C at 5 C min Raise to 300 C at 5 C min 9 Hold for 40 minutes Hold for 40 minutes 10 Raise to 280 C at 5 C min Raise to 360 C at 5 C min 11 Hold for 30 minutes Hold for 30 minutes Although quite a long procedure it will result in longer lifetimes and lower bleed for your column Performance Recovery The performance of the column may exhibit signs of deterioration over time root of its length the removal of the front end will not lower the separation as a result of many different causes Some of these such as contamination by effectiveness by the same ratio as 50cm column length A last resort in column high boiling or strongly retained compounds can be cleared by repeating the regeneration is column washing Column washing uses a pressurized vessel column conditioning until a stable baseline is achieved to force solvent through the column in a reverse direction The selection of the solvent is dependent on the nature of the samples that have been analyz
49. gasoline TR 1 260A470P 245 D2456 Polyhydric alcohols in alkyd resin TG WAXMS 26088 2980 234 D2580 Phenols in water TG 5MS 26098 2230 221 D2753 Oil and oil acids TR FAME 260M154P 259 D2800 FAME analysis TR FAME 260M154P 259 D2804 Purity of methyl ethyl ketone TG WAXMS 26088 2980 234 D2887 Boiling range distribution of petroleum fractions TR SimDist 2605348P 257 TR SimDist 26053478 257 D2998 Polyhydric alcohols in alkyd resin TG 1MS 26099 2970 220 D2999 Monopentaerythritol in commercial pentaerythritol TG 1MS Inquire 220 D3009 Composition of turpentine TG WAXMS 26088 2240 234 D3054 Cyclohexane TG 1MS Inquire 220 D3168 Polymers in emulsion paints TG 1MS 26099 2970 220 D3257 Aromatics in mineral spirits TG 624 26085 3960 229 D3271 Solvent analysis in paints TG WAXMS 26088 2980 234 D3304 PCBs in environmental materials TG 5MS 26098 1540 221 TR PCB 8MS 26AJ148P 260 D3328 Comparison of waterborne petroleum oils TR 1 260A395P 245 D3329 Purity of methyl isobutyl ketone TG WAXMS 26088 2980 234 TG 624 26085 3960 229 D3432 Unreacted toluene diisocyanates in urethane prepolymers and coating solutions TG 1MS 26099 3090 220 D3447 Purity of halogentated organic solvents TG 624 26085 3960 229 D3452 Identification of rubber TG 1MS 26099 3090 220 D3457 FAME analysis TR FAME 260M154P 259 D3534 PCBs in water TG 5MS 26098 336 221 TR PCB 8MS 26AJ148P 260 D3545 Alcohol content and purity of acetate esters TG 624 26085 3960 229 D3687 Alcohol content and purity of aceta
50. or sealed with a septum gt Color coordinated fittings ensure that the column is reinstalled the same Way it came out gt Reusable Capillary Column End Caps Description Cat No Quantity Capillary Column End Caps Paired 260EC111 10 Pack www thermoscientific com chromatography 301 n Capillary GuardGOLD Columns Providing protection to the analytical column gt Protects against column contamination caused by non volatile materials extending the column lifetime gt Focuses target analytes at the head of the analytical column leading to better chromatographic peak shape gt Highly deactivated to provide superior inertness essential for analysis of active compounds High maximum operating temperature of 360 C EE Capillary Guard Columns ID Length Cat No GuardGOLD Columns 0 25mm 2m 26050 0225 0 32mm 2m 26050 0232 0 53mm 2m 26050 0253 0 25mm 5m 26050 0525 0 32mm 5m 26050 0532 0 53mm 5m 26050 0553 0 25mm 10m 26050 1025 0 32mm 10m 26050 1032 0 53mm 10m 26050 1053 SilTite Capillary Column Connectors For use with capillary GC columns gt For fused silica capillary columns gt Glass lined for inertness gt Low thermal mass Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each SilTite Capillary Column Connectors Column I D 2nd Column I D Pack Contents Cat No 0 1 0 25mm 0 1 0 53mm 1 Connector 2 Nuts and 5 Ferrules 0 1 0 2bmm I D 29
51. regulators supplied with in stainless steel output adaptor gt Built in check valve allows for cylinder change without contaminating the gas line High Purity Single Stage Brass Gas Regulators Inlet Filter Cat No Quantity CGA 580 Triple Filter 60180 901 1 Each DIN 6 Triple Filter 60180 903 1 Each CGA 350 Triple Filter 60180 905 1 Each DIN 1 Triple Filter 60180 907 1 Each CGA 320 Triple Filter 60180 909 1 Each CGA 580 Combi Filter 60180 915 1 Each DIN 6 Combi Filter 60180 917 1 Each CGA 350 Combi Filter 60180 919 1 Each DIN 1 Combi Filter 60180 921 1 Each CGA 320 Combi Filter 60180 923 1 Each CGA 590 Combi Filter 60180 925 1 Each DIN 13 Combi Filter 60180 927 1 Each Specifications Maximum Rated Inlet Pressure 3 500 psig Outlet Pressure Ranges 0 to 100 Flow Capacity Cv 0 095 Ambient Operating Temperature 40 F to 165 F Designed Leak Rate 2 x10 ccs helium Weight 4 6 Ibs Ports 5 1 4 FNPT Inlet 1 4 FNPT Outlet 1 4 Compression Decay Inlet Characteristic 0 78 100 psi Materials Body Nickel Plated Brass Bonnet Nickel Plated Brass Seat PCTFE Diaphragm 316 Stainless Steel Gauges 2 2 Nickel Plated Brass Filter 316 Stainless Steel Outlet Valve Nickel Plated Brass Trim Nickel Plated Brass GC Accessories High Purity Two Stage Brass Gas Regulators gt For non corrosive analytical and process applications gt Includes a built in Smart Purifier Base and Cartridge ensuring 99 99999 gas purity
52. their polarities then a polar column such as the TG WAXMS will be ideal If you know the particular class of your sample please refer to the column Selection by Application for a recommended phase see page 208 Always select the least polar column which will perform the separation B Internal Diameter The selection of the internal diameter is often determined by the instrument or detection method Most modern GC equipment will accommodate most column sizes With a larger internal diameter column sample capacity increases but resolution and sensitivity decrease Conversely a smaller 204 1 B ID column can improve resolution and sensitivity but with the drawback of reduced sample capacity and a greater need for sample preparation It is a good idea to find a similar application which gives separation of the desired components and use this as a guide C Film Thickness Increasing the film thickness increases the sample capacity of the column and slows the elution of the peaks which can help when analyzing volatile compounds A thicker film also reduces the potential of overloading the column thus improving the resolution However a thicker film can be more sensitive to degradation The same component will elute at a higher temperature on a thick film when compared to a thin film Compounds with high boiling points or those with a high molecular weight should be analyzed using a thin film to improve reso
53. vv vvvvvvvvvvvvv vw viviviv vvvvvvvv vvvvvvvv v vv v vvvvvvvvv vvvvv vviviv vv vvv vv vvvvvvvv vv v vv v vvvivvvvvv v vvvvvvVvv vvvvvv GC Column Selection GC Column Selection by U S Pharmacopeia Specifications When in doubt it is recommended that you consult the original complete method or contact our technical support team for additional information or help in choosing the correct column for your application The USP specifications are listed below with the appropriate Thermo scientific GC column offerings included for your convenience In some cases there is more than one phase that matches the phase description USP Code Description Recommended Thermo Scientific Phase G1 Dimethylpolysiloxane oil TG 1MS 220 TR 1 MS 246 TR 1 245 G2 Dimethylpolysiloxane gum TG 1MS 220 TR 1 MS 246 TR 1 245 G3 50 Phenyl 50 methylpolysiloxane TG 17MS 231 TR 50MS 252 G5 3 Cyanopropylpolysiloxane TR FAME 259 G6 Trifluoropropyl Methylpolysiloxane TG 200MS 233 G7 5096 Cyanopropyl Phenylmethyl Polysiloxane TG 225MS 232 G16 Polyethylene glycol compound ave mol wt 15 000 with diepoxide linker TG WAXMS 234 TR WAX MS 255 TR WAX 254 G19 50 Cyanopropyl 50 Phenylmethyl Polysiloxane TG 225MS 232 G20 Polyethylene glycol ave mol wt of 380 420 TG WAXMS 234 TR WAX MS 255 TR WAX 254 G27 5 Phenyl 95 methylpolysiloxane TG 5MS 221 TR 5MS 248 TR 5 247 G36 1 Vinyl 5 phenylmethylpolysiloxane TR 5MS 248 TR 5 247 G38 Phase G1 contai
54. 0 Deca BDE 209 Minnesota Ag List Pesticides Mix A Column Part Number Initial Temp Rate 1 Final Temp Detector Type Detection Conditions Carrier Gas Flow Rate Injection Mode Split Ratio 1 Ethalfluralin 2 Tifluralin 3 Propachlor 4 Atrazine desethyl 5 Atrazine desisopropyl 6 Prometon 7 Propazine 8 Atrazine TR 35MS 30 m x 0 25 mm x 0 25 um 260C142P 100 C 1 min 15 C min to 250 C 250 C 5 min MS TRACE DSO MS source 225 C 50 650 m z EI 70 eV He 1 mL min PTV Split at 250 C 20 1 9 Simazine 10 Acetochlor 11 Dimethenamid 12 Alachlor 13 Metribuzin 14 Metolachlor 15 Pendimethalin 16 Cyanazine AN10147 100 95 80 853 80 75 70 65 60 55 50 45 40 35 30 06040505 1003 8 Time min 110 Time min Minnesota Ag List a Pesticides Mix B s x 0 25 um Part Number 260F130P Initial Temp 100 C 1 min Rate 1 15 C min to 250 C Final Temp 250 C 5 min 5 Detector Type MS Detection PolarisQ source 225 C 3 Conditions 35 500 m z EI 70 eV E Carrier Gas He 203 Flow Rate 1 mL min 4 Injection Mode PTV split 20 C E Split Ratio 90 1 j 1 EPTC 4 Fonofos 2 Phorate 5 Triallate 3 Terbufos 6 Chlorpyrifos Keto nes 260X018 Column TR WaxMS 5000000 30 m x 0 25 mm x 0 25 um Part Number 260X142P Temperature Detector Type Carrrier Gas Flow Rate In
55. 0 25mm 15m 0 25um 260W130P 1 Each 0 25mm 30m 0 25um 260W142P 1 Each 0 25mm 60m 0 25um 260W154P 1 Each 0 25mm 30m 0 50um 260W223P 1 Each 0 25mm 60m 0 50um 260W235P 1 Each 0 25mm 30m 1 00um 260W296P 1 Each 0 32mm 15m 0 25um 260W131P 1 Each 0 32mm 30m 0 25um 260W143P 1 Each 0 32mm 60m 0 25um 260W155P 1 Each 0 32mm 30m 0 50um 260W224P 1 Each 0 32mm 60m 0 50um 260W236P 1 Each 0 32mm 30m 1 00um 260W297P 1 Each 0 32mm 60m 1 00um 260W309P 1 Each 0 53mm 30m 0 50um 260W225P 1 Each 0 53mm 15m Tum 260W286P 1 Each 0 53mm 30m 1 00um 260W298P 1 Each 0 53mm m 1 00um 260W310P 1 Each TRACE TR WaxMS GC Columns Feature a high polarity phase designed for mass spectometry detectors Applications NON PAES ications pp Phase Polyethylene Glycol PEG e Aromatic hydrocarbons Max Temps 280 C 300 C M USP Listing G16 e Food additives e Essential oils gt Polar phase Polyethylene glycol e Alcohols scu gt Proprietary bonding method expands operating temperatures e Aldehydes gt Extremely low bleed improves sensitivity and library matches e Ketones gt High stability with oxygen and water Similar to DB Wax Rtx Wax Stabilwax HP20M BP20 HP Wax HP INNOWax SUPELCOWAX 10 AT Wax Nukol CP Wax 52CB ZB Wax TRACE TR WaxMS GC Columns I D Length Film Thickness Cat No Quantity 0 10mm 20m 0 1m 260X145P 1 Each 0 25mm 30m 0 5um 260X223P 1 Each 0 25mm 30m 0 25um 260X142P 1 Each 0 25mm 60m 0 25um 260X154P 1 Each 0 25mm 30m 1 0um 260X
56. 0 25mm x 0 25um 26098 1420 40 C 1 minute hold to 200 C at 10 C min to 250 C at 30 C min MS He 1 1 mL min 1 0 uL Split 30 1 250 C 8 Cineole 9 gamma Terpinene 10 Terpinoline 11 Terpinen 4 ol 12 alpha Terpineol 13 Sesquiterpine TR 35MS 30 m x 0 25 mm x 0 25 um 260C142P 40 C 0 5 min 10 C min to 200 C 200 C 1 min MS TRAGE DSQ MS source 225 C 35 500 m z EI 70 eV He 1 mL min 200 C Split 50 1 10 dl menthol 11 Borneol 12 l a terpineol 13 Dihydrocarveol 14 Citronellol 15 Geraniol 16 Pulegone 17 2 piperidone GC Applications Relative Abundanca 10 11 Time min 11040501 4 7 12 10 n 13 13 16 M 11 6 g 5 r i m tr i B i i 10 Tire min v www thermoscientific com chromatography 281 INDUSTRIAL Grob Test Column Part Number Temperature Detector Type Carrrier Gas Flow Rate Injection Volume Injection Mode 1 n Decane 2 n Undecane 3 1 Nonanal 4 2 3 Butanediol 5 1 Octanol 6 Methyl decanoate w i TR WaxMS 30 m x 0 25 mm x 0 25 um 260X142P 40 C 1 min 6 C min to 160 C hold 5 min MS He 25 7 psi 35cm s 1 8 mL min 1 uL Split 50 1 250 C 7 Dieyclohexylamine 8 Methyl undecanoate 9 Methyl dodecanoate 10 2 6 Dimethylaniline 11 2 6 Dimethylphenol 12 2 Ethylhexanoic acid Industrial Solvents Column TR WaxMS 30 m x 0 32 mm x 0 5 um
57. 0 32mm ID 0 32mm 60180 860 1 Each PLOT Particle Trap 2 5m x 0 53mm ID 0 53mm 60180 861 1 Each Notes Our interactive online version features access to an expanded range of content to help guide you through any application on any instrument e Find your application method or part number using our robust search tool e Method Development Guides Application Notebooks e Product Technical Guides View the Online Thermo Scientific Chromatography Consumables Catalog today www thermoscientific com catalog Check back often new material added regularly www thermoscientific com chromatography 243 GC Columns TR 1 TR IMS NO gt O1 NO I O gt I on No I I NO I CO TR 5MS TR 5HT TR 35MS TR 1701 TR 50MS TR 225 TR WAX TR WaxMS TR FFAP TR SimDist TR V1 TR FAME TR 524 TR 525 TR 527 TR 8095 TR 8270 TR Dioxin 5MS TR PCB 8MS TR DoA NO BRO BR BRT BO TBR BD RO O1 O1 O1 OT OH OT OT gt MW UI PRIOI INI IOI O NO OT I NO FT RS FT BY JF BOT BY TBO BO BO Od GO Od OG GI GO O11 O1 NO OD oO No O TR Biodiesel 261 TR Pesticide 262 TRACE GC Columns UltraFAST 263 TRACE GC Columns offer high temperature stability and exhibit low bleed and long lifetimes TRACE GC columns provide
58. 0MU498 0 32mm 0 32 0 53mm 1 Connector 2 Nuts and 5 Ferrules 0 32mm I D 290MU499 0 45 0 53 0 45 0 53mm 1 Connector 2 Nuts and 5 Ferrules 0 45 0 53mm I D 290MU500 Replacement SilTite Connector Nuts 5 Nuts 290MN211 t SilTite nuts must be used with Siltite ferrules Quantity 1 Each 1 Each 1 Each 1 Each SilTite Ferrules Column I D Cat No 0 2bmm 290MF229 0 32mm 290MF230 0 53mm 290MF231 u Quantity 10 Pack 10 Pack 10 Pack GC Accessories SWAP IT GC MS Interface System Easy to install for quick column changeovers The SWAP IT GCMS Interface provides a powerful tool for switching capillary columns without the need to vent the MS gt Specially deactivated robust stainless steel transfer capillary provides an interface between the analytical column and the MS detector gt Small ID of transfer capillary ensures exposure to air and water is reduced to a minimum during disconnection of the analytical column gt The system works without the requirement for additional He purge make up gas flow gt Finger tight connections make exchanging the analytical column quick and easy without the need for tools SWAP IT No Vent System Description Cat No Quantity For Thermo Scientific Instruments DSO DSOII Polaris Q ITO only SWAP IT GCMS Interface Kit SWAP IT GCMS Interface Nuts Ferrules Accessories 60180 790 1 Each SWAP IT GCMS Interface SWAP IT only 60180 792 1 Each Tr
59. 0um 260B309P 1 Each TRACE TR 5 GC Columns Excellent starting columns for method development capable of performing most required separations NON POLAR Applications Phase 5 Phenyl Methylpolysiloxane e Alcohols Max Temps 340 C 350 C for films 1 5um 280 C 300 C for films gt 1 5um e Free fatty acids USP Listing G27 G36 Aromatics Non polar phase 5 Phenyl methyl polysiloxane e Flavors High operating temperature and extremely low bleed e Low polarity pesticides Widely used in a variety of applications Similar to DB 5 BP5 Rtx 5 HP 5 Ultra 2 PTE 5 SPB5 MDN 5 CP Sil 8CB SPB 5 AT 5 ZB 5 007 2 MP S 5 SE 52 SE 54 TRACE TR 5 GC Columns I D Length Film Thickness Cat No 0 25mm 7m 0 25um 260E113P 0 25mm 15m 0 25um 260E130P 0 25mm 30m 0 25um 260E142P 0 25mm 30m 0 50um 260E223P 0 25mm 30m 1 00um 260E296P 0 25mm 60m 0 25um 260E154P 0 25mm 60m 1 00um 260E308P 0 32mm 15m 0 25um 260E131P 0 32mm 30m 0 25um 260E143P 0 32mm 30m 0 50um 260E224P 0 32mm 30m 1 00um 260E297P 0 32mm 60m 0 25um 260E155P 0 32mm 60m 1 00um 260E309P 0 32mm 100m 0 50um 260E242P 0 53mm 15m 1 00um 260E286P 0 53mm 15m 1 50um 260E334P 0 53mm 30m 0 50um 260E225P 0 53mm 30m 1 00um 260E298P 0 53mm 30m 1 50um 260E336P 0 53mm 30m 5 00um 260E470P www thermoscientific com chromatography Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Eac
60. 1 Each 0 53mm 75m 3um 26091 4900 1 Each 0 53mm 105m 3um 26091 4090 1 Each 000 s TraceGOLD TG 624 GC Columns Offers 90 resolution of the first six gases in EPA Method 8260 and EPA Method 524 2 for volatile organics analysis Applications NON POLAR Phase 6 Cyanopropylphenyl Polysiloane e Residual Solvents Max Temps 220 C 240 C USP Listing G43 e Volatile Organic Compounds e Alcohols gt Low to mid polarity phase 6 cyanopropylphenyl 94 dimethyl polysiloxane gt Ideal for EPA methods 624 and 608 gt Allows resolution of 2 nitropropane from 1 1 dichloropropanone under EPA Method 524 2 revision IV e xygenates Similar to DB 1301 DB 624 HP 1301 HP 624 SPB 1301 SPB 624 VF 1301 VF 624ms CP 1301 CP Select 624 CB Rtx 624 BP 624 ZB 624 Optima 1301 Optima 624 AT 624 007 1301 TraceGOLD TG 624 GC Columns I D Length Film Thickness Cat No Quantity 0 18mm 20m Tum 26085 4950 1 Each 0 18mm 40m Tum 26085 4960 1 Each 0 25mm 30m 1 4um 26085 3320 1 Each 0 25mm 60m 1 4um 26085 3330 1 Each 0 32mm 30m 1 8um 26085 3390 1 Each 0 32mm 60m 1 8um 26085 3410 1 Each 0 53mm 30m 3um 26085 3960 1 Each 0 53mm 60m 3um 26085 4080 1 Each 0 53mm 75m 3um 26085 4900 1 Each 0 53mm 105m 3um 26085 4090 1 Each 229 www thermoscientific com chromatography TraceGOLD TG 1701MS GC Columns Feature a mix of cyano and phenyl groups for increased polarity and a different elution order relative to les
61. 20 26090 2850 26090 0680 26090 1430 26090 2240 26090 2970 26090 3350 26090 1550 26090 2360 26090 3090 26090 0630 26090 1320 26090 2130 26090 2860 26090 3340 26090 3840 26090 1440 26090 2250 26090 2980 26090 3360 26090 3960 26090 1560 26090 2370 26090 3100 26090 3370 26090 4080 Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each TraceGOLD TG 17MS GC Columns Particularly suited to GCMS applications that require more polarity than a 5 Phenyl phase Applications NONE en D Phase 50 Phenyl Methylpolysiloxane e Pesticides and herbicides Max Temps 300 C 320 C i USP Listing G43 e Rosin acids e Phthalate esters gt Mid polarity phase of 50 diphenyl 50 dimethyl polysiloxane e Triglycerides gt Ideal for confirmational analysis e Sterols gt Excellent inertness for active compounds such as pesticides gt Very low bleed ideal for analysis by GCMS Similar to Rxi 17 DB 17 DB 608 VF 17ms CP Sil 24 CB TraceGOLD TG 17MS GC Columns I D Length Film Thickness Cat No Quantity 0 1mm 10m 0 1um 26089 0200 1 Each 0 25mm 15m 0 25um 26089 1300 1 Each 0 25mm 15m 0 5um 26089 2110 1 Each 0 25mm 15m Tum 26089 2840 1 Each 0 25mm 30m 0 25um 26089 1420 1 Each
62. 23 26s Volume Length Agilent No Cat No Quantity Sul 42mm N A NS604304 1 Each 10uL 42mm 5181 3354 NS604404 1 Each Sul 42mm N A NS604314 6 Pack 10uL 42mm 5181 3361 NS604414 6 Pack Syringes for Agilent Technologies Removable Needle 23 265 23 26s Tapered needle Use with 7673 Series 7683 Series 6850 ALS Feature HP style dual gauge cone shaped blunt tip w wv v v Tapered design combines strength of larger diameter 23s with narrow 26s gauge piercing for minimized evaporation and easy on column injection National Scientific Target Precision GC Syringes for Agilent Technologies Removable Needle 23 26s Volume Length Agilent No Cat No Quantity Sul 42mm 5182 0835 NS104308 1 Each 10uL 42mm 5181 3321 NS104408 1 Each www thermoscientific com chromatography 311 D Syringes for Agilent Technologies Removable Needle PTFE Tip Plunger 23 265 23 26s Tapered needle PTFE tipped plunger Use with 7673 Series 7683 Series 6850 ALS Feature HP style dual gauge cone shaped blunt tip ww cw cw v Tapered design combines strength of larger diameter 23s with narrow 26s gauge piercing for minimized evaporation and easy on column injection National Scientific Target Precision GC Syringes for Agilent Technologies Removable Needle PTFE Tip Plunger 23 26s Volume Length Agilent No Cat No Quantity Sul 42mm 5181 3356 NS604408 1 Each Syringes for Agilent Technologies Replacement Needles 23 265 gt 23 26
63. 25mm 30m 0 5um 26096 2230 1 Each 0 25mm 30m Tum 26096 2960 1 Each 0 25mm 60m 0 25um 26096 1540 1 Each 0 25mm 60m Tum 26096 3080 1 Each 0 32mm 15m 0 25um 26096 1310 1 Each 0 32mm 30m 0 25um 26096 1430 1 Each 0 32mm 30m 0 5um 26096 2240 1 Each 0 32mm 30m Tum 26096 2970 1 Each 0 53mm 30m 1 5um 26096 3360 1 Each TraceGOLD TG 5HT GC Columns Offers extended operation up to 400 C ideal for high temperature extended GC applications Applications NON POLAR Phase 5 Phenyl Methylpolysiloxane e Phenols Max Temps 380 C 400 C USP Listing G27 G36 e Residual solvents e Solvents a Sons Low polarity 5 diphenyl 95 dimethyl polysiloxane Lower bleed and better inertness than comparable high temperature columns e Pesticides e PCBs e Solvent impurities gt Special design of fused silica tubing extends column lifetime by up to 40 Similar to Rxi bHT BP 5HT VF 5HT ZB 5HT TraceGOLD TG 5HT GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 1um 26095 0350 1 Each 0 25mm 30m 0 1um 26095 0470 1 Each 0 25mm 30m 0 25um 26095 1420 1 Each 0 32mm 15m 0 1um 26095 0360 1 Each 0 32mm 30m 0 1um 26095 0480 1 Each 0 32mm 30m 0 25um 26095 1430 1 Each 0 53mm 30m 0 15um 26095 0620 1 Each 225 www thermoscientific com chromatography TraceGOLD TG 35MS GC Columns Higher phenyl content for useful elution order and retention time changes Applications NON ERDE AR Phase 35 Phenyl Me
64. 25um 2600142P 1 Each 0 25mm 60m 0 25um 2600154P 1 Each 0 32mm 15m 0 25um 2600131P 1 Each 0 32mm 30m 0 25um 2600143P 1 Each 0 32mm 60m 1 00um 2600309P 1 Each 0 32mm 30m 0 50um 2600224P 1 Each 0 53mm 30m 1 00um 2600298P 1 Each 251 www thermoscientific com chromatography TRACE TR 50MS GC Columns Mid polarity columns well suited to GC MS applications Applications u NON POLAR E Herbicides Phase 50 Phenyl Polysilphenylene siloxane e Drugs of Abuse Max Temps 360 C 370 C USP Listing G3 e EPA 604 608 8060 8081 e Pharmaceuticals gt Mid polarity phase 50 Phenyl polysilphenylene siloxane gt Low bleed decreases MS contamination gt Particularly useful for applications requiring a higher temperature and more polarity than a 5 phenyl column gt Column inertness results in minimal peak tailing and decreased breakdown of sensitive samples Similar to OV 17 SP 2250 DB 17 DB 17ms DB 17ht BPX50 Rtx 50 SPB 50 HP 50 HP 17 AT50 RSL 300 PE 17 CC 17 007 17 MPS 50 SPB 17 ZB 50 TRACE TR 50MS GC Columns I D Length Film Thickness Cat No Quantity 0 10mm 10m 0 10um 260R020P 1 Each 0 25mm 30m 0 10um 260R047P 1 Each 0 25mm 30m 0 15um 260R050P 1 Each 0 2bmm 15m 0 25um 260R130P 1 Each 0 25mm 30m 0 25um 260R142P 1 Each 0 25mm 60m 0 25um 260R154P 1 Each 0 32mm 15m 0 25um 260R131P 1 Each 0 32mm 30m 0 25um 260R143P 1 Each 0 32mm 60m 0 25um 260R155P 1 Each 0 53mm 15m 0 50um 260R213P 1 Each 0 53mm 30m 0 50
65. 26094 1420 226 634 Thiocarbamate pesticides TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 645 Amine pesticides and lethane in industrial and municipal water TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 646 Dinitro aromatic pesticides TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 www thermoscientific com chromatography 213 GC Column Selection by US EPA Solid Waste Test Method Selected EPA Solid Waste methods are listed below with the doubt it is recommended that you consult the original complete method appropriate Thermo Scientific GC column offerings In some cases there or contact our technical support team for additional information or help in is more than one phase or column dimension that can be used When in choosing the correct column for your application Method Title Recommended Part Number Thermo Scientific Phase 8010B Halogenated volatile organics TG 624 26085 4080 229 TG 624 26085 3320 229 8011 EDB and DBCP TG 5MS 26098 1420 221 8015B Nonhalogenated volatile organics TG 624 26085 4080 229 TG 5MS 26098 2960 221 8020A Aromatic volatile organics TG 624 26085 4080 228 TG 5MS 26098 2960 221 8021A Halogenated and aromatic volatile organics TG 624 26085 4080 229 TG 5MS 26098 2960 221 8030A Acrolein and acrylonitrile TG 624 26085 4080 229 8031 Acrylonitrile TG 624 26085 3390 229 8032 Acrylamide TG 624 26085 3390 229 8040A Phenols TG 5MS 26098 1420 221 TG 35MS 26094 1420 226 8060 Phthalate esters TG 5MS 26098 1420 221 8061
66. 260A048P 1 Each 0 32mm 30m 0 25um 260A143P 1 Each 0 32mm 30m 0 5um 260A224P 1 Each 0 32mm 30m Tum 260A297P 1 Each 0 32mm 30m 3um 260A395P 1 Each 0 32mm 30m Sum 260A469P 1 Each 0 32mm 60m 0 25um 260A155P 1 Each 0 32mm 60m Tum 260A309P 1 Each 0 32mm 60m 5 00um 260A481P 1 Each 0 53mm 15m 0 5um 260A213P 1 Each 0 53mm 30m 0 5um 260A225P 1 Each 0 53mm 30m Tum 260A298P 1 Each 0 53mm 30m 1 5um 260A336P 1 Each 0 53mm 30m 3um 260A396P 1 Each 0 53mm 30m Bum 260A470P 1 Each www thermoscientific com chromatography 245 ie TRACE TR 1MS GC Columns Extremely low bleed nonpolar columns suitable for GC MS applications A NON POLAR Applications Phase 10096 Dimethyl Polysiloxane e Chlorinated and nitroaromatic Max Temps 370 C 380 C compounds USP Listing G1 G2 G38 e GC MS environmental analyses i i Non polar phase 100 dimethyl polysiloxane High operating temperature gt Inert phase suited for environmental analyses Similar to DB 1 DB Petro BP1 HP 1 HP 1MS Rtx 1 Ultra 1 SPB 1 SPB 1 Sulfur Petrocol DH CP Sil 5CB RSL 150 RSL 160 ZB 1 CB 1 OV 1 PE 1 007 1 MS SP 2100 SE 30 RH 1 CC 1 CP Sil 5CB MS VF 1ms TRACE TR 1MS GC Columns ID Length Film Thickness Cat No Quantity 0 25mm 30m 0 10um 260B047P 1 Each 0 25mm 15m 0 25um 260B130P 1 Each 0 25mm 30m 0 25um 260B142P 1 Each 0 25mm 60m 0 25um 260B154P 1 Each 0 32mm 30m 0 25um 260B143P 1 Each 0 32mm 60m 0 25um 260B155P 1 Each 0 32mm 60m 1 0
67. 260F143P 1 Each 0 32mm 30m 0 50um 260F224P 1 Each 0 32mm 30m 1 00um 260F297P 1 Each 0 32mm 60m 1 00um 260F309P 1 Each 0 32mm 100m 0 50um 260F242P 1 Each 0 53mm 15m 0 50um 260F213P 1 Each 0 53mm 15m 3 00um 260F384P 1 Each 0 53mm 30m 0 5um 260F225P 1 Each 0 53mm 30m 1 00um 260F298P 1 Each 0 53mm 30m 1 50um 260F336P 1 Each 0 53mm 30m 3 0um 260F396P 1 Each TRACE TR 5HT GC Columns Feature upper temperature limits as high as 400 C Applications NON POLAR E Hydrocarbons Phase 5 Phenyl Polycarborane Siloxane e Solvents Max Temps 380 C 400 C USP Listing G27 G36 e Pesticides e Herbicides gt Non polar phase 5 Phenyl polycarborane siloxane e Phenols gt Allow the elution of higher boiling hydrocarbons up to Cio e Amines Low bleed even at elevated temperatures Similar to DB 5 BP5 Rtx 5 HP 5 Ultra 2 PTE 5 SPB5 MDN 5 CP Sil 8CB SPB 5 AT 5 ZB 5 007 2 MP S 5 SE 52 SE 54 TRACE TR 5HT GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 1um 260H035P 1 Each 0 25mm 30m 0 1um 260H047P 1 Each 0 25mm 30m 0 25um 260H142P 1 Each 0 32mm 12m 0 1um 260H030P 1 Each 249 www thermoscientific com chromatography TRACE TR 35MS GC Columns Mid polarity columns excellent for many applications Applications NON POLAR Pesticides Phase 35 Phenyl Polysilphenylene siloxane e Herbicides Max Temps 360 C 370 C USP Listing G42 e Drugs of Abuse e Poly Aromatic Hydrocar
68. 26s Gauge needle PTFE tipped plunger gastight e Use with AS100 200 AS3000 Autosystem gt Feature cone shaped 90 blunt tip National Scientific Target Precision GC Syringes for PerkinElmer Fixed Needle Gas Tight Volume Length Needle Gauge PerkinElmer No Cat No Quantity SuL 70mm 26s N6101390 NS608302 1 Each SuL 70mm 23s N6101380 NS608303 1 Each SuL 70mm 26s NS108302 1 Each Syringes for Shimadzu Fixed Needle gt 23s and 26s gauge needle gt Use with AOC 14 AOC 17 AOC 20 gt Feature cone shaped 90 blunt tip National Scientific Target Precision GC Syringes for Shimadzu Fixed Needle Volume Length Needle Gauge For Use with Cat No Quantity SuL 42mm 26s NS105303 1 Each SuL 42mm 23s NS105304 1 Each 10uL 42mm 26s NS105403 1 Each 10uL 42mm 23s 221 34618 00 NS105404 1 Each Syringes for CTC Leap Technologies Fixed Needle gt 26s Gauge needle Use with A200s GC Pal LC Pal HTS Combi Pal National Scientific Target Precision GC Syringes for CTC Leap Technologies Fixed Needle Volume Length Gauge Needle Point Cat No Quantity 10uL o1mm 26s Bevel NS100401 1 Each Syringes for CTC Leap Technologies Fixed Needle PTFE Tip Plunger Gas Tight gt 26s Gauge needle gt PTFE tipped plunger gastight Use with A200s GC Pal LC Pal HTS Combi Pal National Scientific Target Precision GC Syringes for CTC Leap Technologies Fixed Needle PTFE Tip Plunger Volume Length Gauge N
69. 27 G36 e Amines e Residual solvents and solvent Low polarity phase 5 diphenyl 95 dimethyl polysiloxane apuntes gt Low bleed for excellent signal to noise ratio sensitivity and mass e Drugs of abuse spectral integrity e Pesticides gt Exceptional inertness ideal for analysis of active compounds e PCB cogeners gt Equivalent to USP G27 phase e Aroclor mixes Similar to Rxi 5ms DB 5 HP 5 HP 5ms Ultra 2 SPB 5 Equity 5 CP Sil 8 TraceGOLD TG 5MS GC Columns I D Length Film Thickness Cat No Quantity 0 1mm 10m 0 1um 26098 0200 1 Each 0 25mm 15m 0 25um 26098 1300 1 Each 0 25mm 15m 0 5um 26098 2110 1 Each 0 25mm 15m Tum 26098 2840 1 Each 0 25mm 30m 0 25um 26098 1420 1 Each 0 25mm 30m 0 5um 26098 2230 1 Each 0 25mm 30m Tum 26098 2960 1 Each 0 25mm 60m 0 25um 26098 1540 1 Each 0 25mm 60m 0 5um 26098 2350 1 Each 0 25mm 60m tum 26098 3080 1 Each 0 32mm 15m 0 25um 26098 1310 1 Each 0 32mm 15m 0 5um 26098 2120 1 Each 0 32mm 15m Tum 26098 2850 1 Each 0 32mm 30m 0 25um 26098 1430 1 Each 0 32mm 30m 0 5um 26098 2240 1 Each 0 32mm 30m Tum 26098 2970 1 Each 0 32mm 60m 0 25um 26098 1550 1 Each 0 32mm 60m 0 5um 26098 2360 1 Each 0 32mm 60m tum 26098 3090 1 Each 0 53mm 15m 0 25um 26098 1320 1 Each 0 53mm 15m 0 5um 26098 2130 1 Each 0 53mm 15m Tum 26098 2860 1 Each 0 53mm 15m 1 5m 26098 3340 1 Each 0 53mm 30m 0 25um 26098 1440 1 Each 0 53mm 30m 0 5um 26098 2250 1 Each 0 53mm 30m Tum 26098 2980 1 Each 0 53mm 30m 1 5m 26098 3360 1 Each
70. 296P 1 Each 0 32mm 30m 0 25um 260X143P 1 Each 0 32mm 30m 1 0um 260X297P 1 Each 0 32mm 60m 0 25um 260X155P 1 Each 0 32mm 30m 0 5um 260X224P 1 Each 0 32mm 60m 1 0pm 260X309P 1 Each 0 53mm 30m 1 0um 260X298P 1 Each www thermoscientific com chromatography 255 TRACE TR FFAP GC Columns High polarity phase optimized for FFAP analysis Applications NON POLAR e Organic acids Phase TPA Modified Polyethylene Glycol PEG e Free fatty acids Max TE 240 C 250 C ete USP Listing G25 G35 gt Polar phase TPA modified Polyethylene glycol Bonded FFAP phase gt Quality tested for acidic compound analysis Similar to DB FFAP HP FFAP Stabilwax DA CPWax 58CB TRACE TR FFAP Capillary GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 260N130P 1 Each 0 25mm 30m 0 25um 260N142P 1 Each 0 25mm 60m 0 25um 260N154P 1 Each 0 32mm 15m 0 25um 260N131P 1 Each 0 32mm 30m 0 25um 260N143P 1 Each 0 32mm 60m 0 25um 260N155P 1 Each 0 32mm 50m 0 50um 260N230P 1 Each 0 53mm 15m 0 50um 260N213P 1 Each 0 53mm 30m 0 50um 260N225P 1 Each 0 53mm 30m 1 00um 260N298P 1 Each TRACE TR SimDist GC Columns Feature a low polarity phase for high temperature analyses Applications NON POLAR I e High molecular weight Phase 10096 Dimethyl Polysiloxane hydrocarbons Max Temps 400 C for films 1 0um we 370 C for 2 65um films e Simulated distillation USP Listing ASTM D2887 D6532 gt
71. 2S Bevel point 278 Blunt end 22s side hole 22S Bevel point 22S Blunt end Cat No NS600305 NS600306 NS600405 NS600406 NS600505 NS600506 NS600605 NS600606 NS600705 NS600706 NS600805 NS600905 NS600906 NS600908 NS600005 NS600006 NS600007 NS600045 NS600046 NS600047 NS600065 NS600066 Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each GC Accessories Syringes for Accurate Dosing of Liquids Replacement Needles gt Suitable for liquid or gas samples National Scientific Target Precision Syringes for Accurate Dosing of Liquids Replacement Needles Volume Length Gauge Needle Type Cat No Quantity Sul 42mm 26s 90 Blunt End NS834307 3 Pack 10uL 42mm 26s 90 Blunt End NS834407 3 Pack Sul 51mm 26s Bevel NS832301 3 Pack Sul 51mm 26s side Hole NS832304 2 Pack 10uL 51mm 26s Bevel NS832401 3 Pack 10uL 51mm 26s side Hole NS832404 2 Pack 25 to 100uL 51mm 225 90 Blunt End NS831014 3 Pack 25 to 100uL 51mm 22s side Hole NS831015 3 Pack 25 to 100uL 51mm 22s side Hole NS832504 2 Pack 25 to 100uL 51mm 22s Bevel NS831013 3 Pack 250uL to 10mL 51mm 22s 90 Blunt End NS841014 3 Pack 250uL to 10mL 51mm 22s side Hole NS841015 2 Pack 250uL to 10mL 51mm 22s Side hole NS832604 2 Pack 250uL to 10mL 51mm 22s Bevel NS841013 3 Pack Syringes for Accurate Dosing of Liquids PTFE Luer Lok Gas Tight Suit
72. 396P 245 D4864 Traces of methanol in propylene concentrates TG 5MS Inquire 221 D4947 Chlordane and heptachlor in indoor air TG 5MS 26098 3360 221 D5060 Impurities in high purity ethylbenzene TG WAXMS 26088 2360 234 D5075 Nicotine in indoor air TG 5MS 26098 2970 221 D5134 Petroleum naphthas through n nonane TG 1MS Inquire 220 D5135 Styrene TG WAXMS 26088 2360 234 D5399 Boiling point distribution of hydrocarbon solvents TR SimDist 2605348P 257 D5441 Methyl t butyl ether TG 1MS Inquire 220 D5442 Petroleum waxes TG 1MS 26099 1430 220 TG 5MS 26098 1300 27 D5480 Motor oil volatility TG 5MS Inquire 221 D5501 Ethanol content of denatured fuel ethanol TG 1MS Inquire 220 D5580 Benzene toluene ethylbenzene p o m xylene C9 and heavier aromatics in finished gasoline TR 1 260A470P 245 D5599 Oxygenates in gasoline by oxygen selective FID TG 1MS 26099 3080 220 D5623 Sulfur compounds in light petroleum liquids using sulfur selective detection TG 1MS Inquire 220 D5713 High purity benzene for cyclohexane feedstock TG 1MS Inquire 220 D5739 Oil spill source identification using positive ion electron impact low resolution MS TG 5MS 26098 1420 221 D5769 Benzene toluene and total aromatics in finished gasolines TG 1MS 26099 3080 220 TG 624 26085 3330 229 D5790 Purgeable organic compounds in water TG 5MS 26098 1420 221 D5812 Organochlorine pesticides in water TG 1701MS 26090 1420 230 TG 17MS 26089 1420 23 TG WAXMS 26088 1550 234 D5917 Trace impurities in monocyclic arom
73. 42mm 42mm 42mm 42mm 42mm 42mm 42mm 42mm Gauge 26 23 23 to 26 26 26 23 23 23 to 26 23 to 26 26 26 23 to 26 23 23 23 23 26 23 26 Autosampler Syringes for CTC Autosampler Syringes for CTC Needle Point Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cone Cat No 365A0411 365A0421 365A0431 365C0921 365C0926 365C0951 365C0956 365C0971 365C0976 365D 1521 365D 1526 365D 1561 365D 1571 365D 1576 365D 1611 365D 1621 365D 1636 Quantity 1 Each 1 Each 1 Each 1 Each 6 Pack 1 Each 6 Pack 1 Each 6 Pack 1 Each 6 Pack 1 Each 1 Each 1 Each 6 Pack 1 Each 6 Pack Volume 0 5uL Sul Sul 0 5uL 10uL 10uL 10uL 10uL 10uL 10uL 10uL 10uL 10uL 10uL 10uL 10uL 2byL 2byL 2byL 2byL 100uL 100uL 100uL 250uL 500uL 1mL 1mL 2 5mL 2 5mL Gas Tight Needle Type Plunger in Needle Fixed Fixed Removable Fixed Fixed Removable Fixed Removable Fixed Fixed Fixed Fixed Fixed Removable Fixed Fixed Fixed Fixed Removable Fixed Removable Fixed Fixed Fixed Fixed Removable Removable Removable 0000s Length 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm 50mm Gauge 23 23 26 26 26 23 23 26 26 26 23 23 26 26 23 23 26 23 26 26 23 26 26 26 26 23 26 23
74. 50 Pack TR Green Low Coring Silicone 9mm 313G3240 50 Pack TR Green Low Coring Silicone 11mm 313G3230 50 Pack TR Green Low Coring Silicone 12 mm 31363228 50 Pack TR Green Low Coring Silicone 17mm 313G3211 50 Pack www thermoscientific com chromatography 293 Injection Port Liners for Thermo Scientific Instruments Highly deactivated and produced to exacting tolerances to ensure a high degree ofreproducibility TRACE and FOCUS SSL RTS EEE ar TRACE PTV Injection Type Splitless Straight Liner Siltek Baffle Liner Split Straight Liner Split Straight Liner Split Straight Liner Split Straight Liner Splitless Straight Liner Splitless Straight Liner Splitless Straight Liner Splitless Straight Liner Split FocusLiner for 50mm Needle Split FocusLiner for 50mm Needle Splitless FocusLiner for 70mm Needle Splitless FocusLiner for 70mm Needle Splitless FocusLiner for 50mm Needle Splitless FocusLiner for 50mm Needle Mixed Liner Split Splitless Sample Pack Splitless Straight Liner Split Straight Liner PTV Silcosteel Liner for OC PTV Siltek Metal Liner PTV Straight Liner PTV Straight Liner PTV Straight Liner PTV Straight Liner PTV Straight Liner PTV Liner with Sintered Lining PTV Liner with Three Baffles PTV Liner with Three Baffles PTV Siltek Metal Liner PTV Siltek Metal Liner PTV Baffle Liner
75. 57 Capillary 007 2 MP 5 Quadrex TG 5MS 221 Capillary DB 35 Agilent TG 35MS 226 Capillary 007 2 MPS 5 Quadrex TG 5SiIMS 224 Capillary DB 35ms Agilent TG 35MS 226 Capillary 007 23 Quadrex TR FAME 259 Capillary DB 5 Agilent TR 5 247 Capillary 007 5MS Quadrex TG 5MS 221 Capillary DB 5 625 Agilent TG 5MS 221 Capillary 007 624 Quadrex TG 624 229 Capillary DB 5ht Agilent TG 5HT 225 Capillary 007 CW Quadrex TG WAXMS 234 Capillary DB 5ms Agilent TG 5MS 221 Capillary Al 5 Alltech TR 5 247 Capillary DB 624 Agilent TG 624 229 Capillary AT50 Alltech TG 17MS 231 Capillary DB FFAP Agilent TG WAXMS A TR FFAP 235 256 Capillary AT 5MS Alltech TG 5MS 221 Capillary DB HT Sim Dis Agilent TR SimDist 251 Capillary AT 624 Alltech TG 624 229 Capillary DB PETRO Agilent TG 1MS 220 Capillary AT Silar Alltech TR FAME 259 Capillary DB WAX Agilent TG WAXMS 234 Capillary Al Wax Alltech TR WAXMS 255 Capillary DB WAXetr Agilent TR WAXMS ZDD Capillary BP 1 SGE TR 1 245 Capillary Elite 1 PerkinElmer TR 1 245 Capillary BP10 SGE TG 1701MS 230 Capillary Elite 1301 PerkinElmer TG 1301MS 228 Capillary BP20 SGE TG WAXMS 234 Capillary Elite 17 PerkinElmer TG 17MS 231 Capillary BP21 SGE TG WAXMS A TR FFAP 235 256 Capillary Elite 1701 PerkinElmer TG 1701MS 230 Capillary BP225 SGE TG 225MS 232 Capillary Elite 17ms PerkinElmer TG 17MS 231 Capillary BP5 SGE TG 5MS 221 Capillary Elite 200 PerkinElmer TG 200MS 233 Capillary BP624 SGE TG 624 229 Capillary Elite 23 PerkinElmer TR FAME 259 Capillary BP
76. 5mL 51mm 22S Side Hole NS600042 1 Each 10mL 51mm 22s Bevel NS600060 1 Each 10mL 51mm 22s Blunt End NS600061 1 Each 10mL 51mm 22s side Hole NS600062 1 Each www thermoscientific com chromatography 317 Syringes for Accurate Dosing of Liquids Fixed Needle Gas Tight 22s Gauge bevel type fixed needles National Scientific Target Precision Glass Syringes Liquid Dosing FN Volume d0uL 250uL 500uL Syringes for Accurate Dosing of Liquids Removable Needle Gas Tight National Scientific Target Precision Syringes for Accurate Dosing of Liquids Removable Needle Gas Tight Length 51mm 51mm 51mm Gauge Needle Point 26s Bevel 26s Bevel 26s Bevel gt Suitable for liquid or gas samples gt PTFE tipped stainless steel plunger eliminates frozen plungers Cat No NS100601 NS100801 NS100901 Quantity 1 Each 1 Each 1 Each Volume Sul Sul 10uL 10uL 25uL 25uL BOuL 50uL 100uL 100uL 250uL 500uL 500uL 500uL 1 0mL 1 0mL 1 0mL 5 0mL 5 0mL 5 0mL 10 0mL 10 0mL Length 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm 51mm Gauge Needle Type 26s Bevel point 26s Blunt end 26s Bevel point 26s Blunt end 22S Bevel point 22S Blunt end 22S Bevel point 22S Blunt end 278 Bevel point 228 Blunt end 26s Bevel point 22S Bevel point 228 Blunt end 22s side hole 22S Bevel point 22S Blunt end 22s side hole 2
77. 5mm x 0 25um Part Number 26089 1420 Temperature 90 C 1 0 minute hold to 215 C at 25 C minute 0 5 minute hold to 235 C at 4 C minute to 280 C at 15 C minute to 320 C at 4 C minute 20 minute hold Detector Type MS Carrier Gas He Flow Rate 1 2 mL min Injection Volume 1 0 uL Injection Mode Splitless 300 C 1 naphthalene 14 benzolkjfluoranthene 24 26 2 1 methylnaphthalene 15 benzo j fluoranthene 25 3 2 methylnapthalene 16 benzo a pyrene 4 acenaphthylene 17 3 methylcholanthrene 5 acenaphthene 18 dibenzola h acridine er 6 fluorene 19 dibenzo a jJacridine 12 14 16 18 20 2 24 26 28 30 32 34 36 38 40min 7 phenanthrene 20 indeno 1 2 3 cd pyrene 8 anthracene 21 dibenzo a h anthracene 9 fluoranthene 22 benzo ghi perylene 10 pyrene 23 7H dibenzo c g carbazole 11 benzo a anthracene 24 dibenzola e pyrene 12 chrysene 25 dibenzola i pyrene 13 benzo b fluoranthene 26 dibenzola h pyrene EPA 515 4 Methylated Chlorinated Acid Herbicides Column TG 5SiIMS 30m x 0 25mm x 0 25um Part Number 26096 1420 Temperature 70 C 1 minute hold to 210 C at 20 C minute 1 minute hold to 250 C at 5 C minute Detector Type ECD at 310 C base at 300 C Carrier Gas He Flow Rate 1 0 mL min Injection Volume 0 5uL Injection Mode Split 75 1 230 C 1 Dalapon methyl ester 10 2 4 DB methyl ester 2 3 5 dichlorobenzoic acid 11 Dinoseb methy ether methyl ester 12 Bentazo
78. 6086 1420 1 Each 0 25mm 30m 0 50um 26086 2230 1 Each 0 32mm 15m 0 25um 26086 1310 1 Each 0 32mm 30m 0 25um 26086 1430 1 Each 0 32mm 30m 0 50um 26086 2240 1 Each 0 32mm 15m Tum 26086 2850 1 Each 0 32mm 30m Tum 26086 2970 1 Each 0 32mm 60m Tum 26086 3090 1 Each 0 53mm 30m 0 5um 26086 2250 1 Each 0 53mm 15m Tum 26086 2860 1 Each 0 53mm 30m Tum 26086 2980 1 Each 0 53mm 60m Tum 26086 3100 1 Each 0 53mm 30m 1 5um 26086 3360 1 Each TraceGOLD TG POLAR GC Columns Specifically designed polymer and surface treatment overcome traditional problems with high polarity columns T NON POLAR Te Phase 90 Cyanopropylpheny Polysiloxane e Cis Trans FAMES Max Temps 260 C 275 C 2 USP Listing G8 G48 e Dioxins gt Highly polar phase 90 biscyanopropyl 10 phenylcyanopropyl polysiloxane not bonded gt Strong dipole moment and high selectivity for cis trans compounds or compounds with conjugated double bonds gt Equivalent to USP G8 and G48 Similar to DB 23 HP 23 Rtx 2330 SP 2330 SP 2380 SPB 2560 HP 88 Silar 10c CP Sil 88 FAME CP Sil 88 BPX 70 BPX 90 TraceGOLD TG POLAR GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 30m 0 1m 26082 0470 1 Each 0 25mm 30m 0 2um 26082 5010 1 Each 0 25mm 60m 0 1m 26082 0590 1 Each 0 25mm 60m 0 2um 26082 5020 1 Each 0 25mm 105m 0 1m 26082 5000 1 Each 0 25mm 105m 0 2um 26082 5030 1 Each 0 32mm 30m 0 2um 26082 5040 1 Each 0 32mm 60m 0 2um 26082 5050 1 Each 0 32mm 105m 0 2
79. Away Slowly After a High Initial Value Purge valve left closed during acquisition Inadequate purge flow rate Purge valve left closed for too long Solvent tail peak Pre filters are dirty when using a quadrupole MS detector Baseline Rising Accumulation of impurities in the column Contaminated detector There is bleeding from the GC column Air is leaking into the system Baseline Rising Under Column contaminated Temperature Program Control Baseline High Standing Current Carrier gas flow rate too high Column contaminated Contaminated gases Excessive column stationary phase bleeding Loose connections Baseline Irregular Shape Detector contaminated Dip After Solvent Peak Baseline Irregular Shape Excessive column bleed during column S shaped temperature programming Oxygen contamination is decomposing the stationary phase Baseline High Contaminated detector Frequency Noise Combustion gas flow too low or too high Column contaminated Contaminated detector gas supply Detector temperature higher than column maximum temperature Loose column fittings Baseline Spiking Column too close to flame when using an FID Dirty jet or detector FID temperature too low when using an FID Peak Related Problems Peaks Broadening Column flow too high Column flow too low Split flow too low in split injection Column performances degraded Dirty injector Stationary phase accumulated i
80. Bacterial Acid 250M010 Methyl Esters Column TR FAME 30 m x 0 25 mm x 0 25 um Part Number 260M142P Temperature 100 C 1 min 5 C min to 220 C Detector Type FID Injection Mode Split 1 C11 0 15 C17 0 2 C12 0 16 C9 10 methylene 16 0 3 C13 0 17 C14 0 2 0H 4 C10 0 2 OH 18 C18 0 5 C14 0 19 C18 1n9 trans 6 C15 0 i 20 C18 1n9 cis 7 C15 0 a 21 018 1n7 cis 8 C15 0 22 C18 2n6 cis 9 C12 0 2 0H 23 C19 0 10 C16 0 i 24 C16 0 2 0H 11 C16 0 25 C9 10 methylene 18 0 12 C15 1n7 cis 26 C20 0 13 C12 0 3 0H 27 C18 0 2 0H 14 C17 0 a Partially Methylated 260M011 Glucose Column TR FAME 25 mx 0 22 mm x 0 25 um Part Number 260M135P Temperature 185 C 1 min 3 C min to 260 C hold 10 min Detector Type MS Detection 70 eV 100 350 m z Carrrier Gas He 50 kPa Injection Volume 1 ul Injection Mode Split 1 2 3 4 0 methyl rhamnitol 2 2 3 5 0 methyl arabinitol f 3 2 3 4 0 methyl arabinitol p 4 3 5 0 methyl arabinitol 5 2 3 4 6 0 methyl glucitol 6 2 5 0 methyl arabinitol 7 2 3 4 6 0 methyl galactitol 8 2 3 0 methyl arabinitol 9 2 4 6 0 methyl galactitol 10 2 0 methyl arabinitol 11 2 3 6 0 methyl glucitol 12 2 3 4 0 methyl galactitol 13 arabinitol hexa acetate 14 xylitol hexa acetate 15 2 3 4 6 0 methyl galactitol 16 2 0 methyl galactitol 17 4 0 methyl galactitol 18 Galactitol hexa acetate 19 Glucitol hexa acetate 20 Myo inositol hexa acetate
81. C 200 UFC 264 UFMC00002010207 UFC 23 UFC BioDiesel UFC M1 UFMC00001070904 ID 0 1mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 1mm 0 1mm 0 1mm 0 1mm 0 1mm 0 1mm 0 1mm 0 18mm 0 1mm 0 18mm 0 32mm 0 32mm Length 5m 2 5m 5m 5m 5m 10m 2 5m 5m 5m 10m 10m 10m 10m 5m 5m 5m 5m 5m Film Thickness 0 1um 0 1um 0 1um 0 25um 3 0um 0 5um 0 4um 0 4um 0 4um 0 1um 0 1um 0 1um 0 2um 0 4um 0 5um 0 2um 0 5um 0 25um Uses General ASTM D 2887 ASTM D 2887 ISO 9377 2 ASTM D 3710 General General General General General General General Alcohols Ketones Volatiles FAMEs BioDiesel General www thermoscientific com chromatography Cat No UFMC00000070401 UFMC00001070401 UFMC00002070414 UFMC00002010006 UFMC00100000000 UFMC00300000000 UFMC00400000000 UFMC00001010501 UFMC00001010503 UFMC00002030306 UFMC00002030603 UFMC00001070600 Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 263 GC Applications Environmental Petrochemical Forensic amp Toxicology 2 Chemical Biomedical 279 Industrial 281 Food Safety 284 GC and GCMS Applications Compiled from our years of experience in chromatography the Application Compendium contains GC and GCMS applications to help you find the solution you need For your convenience the applications
82. C Column Selection by Application v Recommended v Alternative Acids Acid Neutral Drugs Alcohols Alcohols in Beverages Aldehydes Alditol Acatates sugars Amines Aliphatic Amines Aromatic Antidepressants Benzenes substituted Biodiesel Methanol Biodiesel FAMEs Biodiesel Glycerine Brominated Flame Retardants Butter Fat Carboxylic Acids Cigarette Lighter Fuel Chlorinated Aromatics Dioxins Drugs of Abuse Drugs of Abuse THC Essential Oils Explosives FAMEs Glucose Methylated Herbicides Hydrocarbons Ketones Monomers Nitroaromatics Organic acids Organochlorine Pesticides Organophosphorous Pesticides PAHs Paraffins PCBs Pesticides Petroleum Phenols Phthalates Plant Sterols Polyethylene Polymers Polywax Pyrethroids Sedatives Semivolatiles Silicon Oil Solvents Terpenes Triglycerides TRPH Volatiles Xylenes S SU COS IR SO 393 QD e ESS BESS SSE BLESS BS SS EEE I SESE A EG vwwww vv v viv vvvvvvvv vvvvv v vvvvvvivvivv v vvvvvv vw vvvvvviv vwwww vv v vvv vv vvvvvvvv v vv v vi vv vvvvvvvv v vv v vi vv vvvvvvvv vv v vvvvv v vvvvv vv vwwwv v vv vvvivvvvvvvv vv v v vvv vvvvv vv v vvv vvv vvv v v vv Viv v vvvvvvvvvv vwvwvwvwviviwviwv v vvvv v vvvvvvvvvvvvvvvvv v vv vvvvvvvvvvi vvvvvivvvvv vvvvvvvvvvvvv vv v vvvv vvvvvvvvvvvvv vvvv vvvvvvvvvvvvv vv viv vvvvvvvv vv v vv v vv v vvvv v viv vvvvvvvv vvv vvv v v vvrvvvvvv vvvvvvvvvv viviviv vw vvv vvvvvvvv
83. SAFETY AND TESTING Sugars Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 rhamnitol 2 fucitol 3 ribitol 4 arabinitol TG 225MS 15m x 0 25mm x 0 25um 26083 1300 190 C 5 minute hold to 250 C at 8 C min 5 minute hold FID Hydrogen 45 cm sec 0 5 uL Split 35 1 260 C 5 mannitol 6 galactitol 7 glucitol 8 inositol FAMES PUFA Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 C14 0 2 C16 0 3 C16 1n7 4 C18 1n9 5 C18 1n7 6 018 2n6 7 C18 3n3 8 C20 1n11 9 C20 1n9 TG POLAR 30m x 0 25mm x 0 20um 26082 5010 160 C to 225 C at 2 C min FID Hydrogen 45 cm sec 0 5 uL Split 35 1 225 C 10 C20 1n7 11 C18 4n3 12 C22 1n11 13 22 18 14 C20 4n3 15 C20 5n3 16 C21 5n3 17 C22 5n3 18 C22 6n3 FAMES C8 C24 Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 Methyl octanoate 2 Methyl decanoate 3 Methyl decanoate 4 Methyl myristate 5 Methyl palmitate 6 Methyl palmitoleate 7 Methyl stearate TG WAXMS 30m x 0 25mm x 0 25um 26088 1420 100 C 0 5 minute hold to 220 C at 5 C minute to 250 C at 10 C minute 3 minute hold MS He 1 2 mL min 0 1uL Split 100 1 250 C 8 Methyl oleate 9 Methyl linoleate 10 Methyl linolenate 11 Me
84. TG 225MS 232 Capillary TG POLAR 237 Capillary TR FAME 259 Capillary TR SimDist 257 Capillary TG 35MS 226 Capillary TG 35MS AMINE 227 Capillary TG 35MS 226 PLOT TR 5 247 PLOT TG 5MS AMINE 223 PLOT TG 17MS 231 PLOT TG 5SilMS 224 PLOT TG 624 229 PLOT TG 624 229 PLOT TG WAXMS 234 PLOT TG 17MS 231 PLOT TG 1MS 220 PLOT TG 5HT 225 PLOT TG 5MS 221 PLOT TG 5SilMS 224 PLOT TG 1MS 220 PLOT TG 5MS 221 PLOT TG 5MS 221 PLOT TG WAXMS 234 PLOT TG 1MS 220 PLOT TG 17MS 231 PLOT TR FAME 259 PLOT TR FAME 259 PLOT TR 1 245 PLOT TR 1 245 PLOT TG 17MS 231 PLOT TG 35MS 226 TR 5 247 PLOT TG 17MS 231 PLOT TG WAXMS 234 PLOT TG WAXMS A TR FFAP 235 256 PLOT TG WAXMS B 236 PLOT TG WAXMS 234 PLOT TG 17MS 231 TG 1MS 220 VF 200ms VF 23ms VF 35ms VF 5ht VF 5ms ZB 1 ZB 1701 ZB 1701P ZB 1HT Inferno ZB 1MS ZB 35 ZB 5 ZB 50 ZB 5HT Inferno ZB 5MS ZB 5MS Si ZB 624 ZB FFAP ZB WAX ZB WAXplus Alumina PLOT AT Alumina AT Molsieve AT Q CP AI203 KCI CP AI203 Na2S04 CP Molsieve 5A CP PoraPLOT Q CP PoraPLOT S CP PoraPLOT U GS Alumina GS Alumina KCI GS Molsieve GS 0 HP PLOT M HP PLOT Molsieve HP PLOT S HP UPLOT Molsieve 5A PLOT PLT 5A PoraBond Q PoraBond U Rt Alumina Bond KCI Rt Alumina Bond Na2S04 Rt Msieve 5A Rt 0 BOND Rt OS BOND Rt S BOND Rt U BOND Supel Q PLOT www thermoscientific com chromatography GC Column Selection Manufacturer Varian Varian Varian Varian Varian Phenomenex Phenomenex Pheno
85. TG 5MS 221 Capillary CP Wax 51 Amines Varian TG WAXMS B 236 Capillary HP5 TA Agilent TG 5MS 221 Capillary CP Wax 52CB Varian TG WAXMS 234 Capillary HP 88 Agilent TR FAME 259 Capillary CP Wax 58 CB FFAP Varian TG WAXMS A TR FFAP 235 256 Capillary HP FFAP Agilent TG WAXMS A TR FFAP 235 256 Capillary DB 1 Agilent TR 1 245 Capillary HP INNOWax Agilent TG WAXMS 234 Capillary DB 1301 Agilent TG 1301MS 228 Capillary HP VOC Agilent TG 624 229 Capillary DB 17 Agilent TG 17MS 231 Capillary HP Wax Agilent TG WAXMS 234 Capillary DB 1701 Agilent TG 1701MS 230 Capillary HI5 SGE TG 5HT 229 Capillary DB 17ht Agilent TG 17MS 231 Capillary HI8 SGE TR PCB 8MS 260 Capillary DB 17ms Agilent TG 17MS 231 Capillary MDN 35 Sigma Aldrich TG 35MS 226 Capillary DB 1ms Agilent TG 1MS 220 Capillary MDN 5 Sigma Aldrich TR 5 24 Capillary DB 200 Agilent TG 200MS 233 Capillary MDN 5S Sigma Aldrich TG 5SilMS 224 Capillary DB 225 Agilent TG 225MS 232 Capillary Nukol Sigma Aldrich TG WAXMS 234 Column Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary Capillary
86. Toluene 5 m Xylene 3 Ethyl benzene 6 o Xylene EPA 624 Purgeables Column TR WaxMS 500000 30 m x 0 25 mm x 0 25 um Part Number 260X142P 400000 Temperature 32 C 3 min 8 C min to 90 C 6 C min to 200 C hold 5 min Detector Type MS 300000 Carrrier Gas He 27 2 psi 35cm s Flow Rate 1 8 mL min 200000 Injection Volume 0 5 ul Injection Mode Split 40 1 250 C 100000 1 Chloromethane 14 Benzene 2 Vinyl chloride 15 Trichloroethene TT 3 Trichlorofluoromethane 16 Tetrachloroethene 100 200 300 400 500 6 00 700 800 900 10 00 11 00 12 00 13 00 14 00 4 Chloroethane 17 Toluene 5 Bromomethane 18 1 2 Dichloropropane 27 2 Chloroethylvinyl ether 6 1 1 Dichloroethene 19 1 2 Dichloroethane 28 1 3 Dichlorobenzene 7 Unknown 20 Ethylbenzene 29 Tribromomethane 8 trans 1 2 Dichloroethene 21 1 3 Dichloropropene Z 30 1 4 Dichlorobenzene 9 Carbon tetrachloride 22 Bromodichloromethane 31 1 2 Dichlorobenzene 10 1 1 1 Trichloroethane 23 1 3 Dichloropropene E 32 1 1 2 2 Tetrachloroethane 11 1 1 Dichloroethane 24 Chlorobenzene 12 Chloroform under methanol 25 1 1 2 Trichloroethane 13 Dichloromethane 26 Dibromochloromethane EPA 625 Chloro Nitro 260R010 Phenols Column TR 50MS g 30 m x 0 25 mm x 0 25 um z Part Number 260R142P Temperature 50 C 1 min 8 C min to 300 C hold 10 min Detector Type MS Injection Mode Split 40 1 1 2 Chlorophenol 6 2 4 6 Trichlorophenol 2 2 Nit
87. X1 SGE TG 1MS TR SimDist 220 257 Capillary Elite 35ms PerkinElmer TG 35MS 226 Capillary BPX1 SGE TR SimDist 257 Capillary Elite 5 PerkinElmer TR 5 24 Capillary BPX1 SGE TR SimDist 257 Capillary Elite 5ms Perkin Elmer TG 5MS 221 Capillary BPX5 SGE TG 5MS 221 Capillary Elite 5ht PerkinElmer TG 5HT 225 Capillary BPX50 SGE TG 17MS 231 Capillary Elite 624 PerkinElmer TG 624 229 Capillary BPX608 SGE TG 35MS 226 Capillary Elite FFAP PerkinElmer TG WAXMS A TR FFAP 235 256 Capillary BPX70 SGE TR FAME 259 Capillary Elite WAX PerkinElmer TG WAXMS 234 Capillary BPX90 SGE TG POLAR 237 Capillary Elite WAX ETR PerkinElmer TG WAXMS 234 Capillary BPX Volatiles SGE TG 624 229 Capillary HP 1 Agilent TR 1 245 Capillary CARBOWAX Agilent TR WAXMS 255 Capillary HP 17 Agilent TG 17MS 231 Capillary CP 1301 Varian TG 1301MS 228 Capillary HP 1701 Agilent TG 1701MS 230 Capillary CP FFAP CB Varian TG WAXMS A TR FFAP 235 256 Capillary HP 1MS Agilent TG 1MS 220 Capillary CP Select624CB Varian TG 624 229 Capillary HP20M Agilent TG WAXMS 234 Capillary CP Sil 19CB Varian TG 1701MS 230 Capillary HP 23 Agilent TR FAME 259 Capillary CP Sil 5CB Varian TR 1 245 Capillary HP 35 Agilent TG 35MS 226 Capillary CP Sil 5CB MS Varian TG 1MS 220 Capillary HP 35MS Agilent TG 35MS 226 Capillary CP Sil 88 Varian TR FAME 259 Capillary HP 5 Agilent TR 5 24 Capillary CP Sil 8CB Varian TG 5SiIMS 224 Capillary HP 50 Agilent TG 17MS 231 Capillary CP SimDist Varian TR SimDist 257 Capillary HP 5MS Agilent
88. able for liquid or gas PTFE tipped plunger eliminates frozen plungers National Scientific Target Precision Syringes for Accurate Dosing of Liquids PTFE Luer Lok Gas Tight Volume Cat No Quantity SuL NS600309 1 Each 10uL NS600409 1 Each 25uL NS600509 1 Each 50uL NS600609 1 Each 100uL NS600709 1 Each 250uL NS600809 1 Each 500uL NS600909 1 Each 1mL NS607011 1 Each 2 5mL NS607031 1 Each 5mL NS607051 1 Each 10mL NS607071 1 Each 25mL NS607091 1 Each www thermoscientific com chromatography 319 Metal Luer screw Replacement Needles Feature a precision machined PTFE tipped plunger in 4 Mm National Scientific Target Precision Metal Luer screw Replacement Needles Needle Length 51mm 51mm 51mm 51mm Syringes for Accurate Dosing of Liquids Luer Tip Gas Tight Gauge 26s 26s 22S 22S Needle Type 90 Blunt End Bevel 90 Blunt End Bevel Glass Luer slip tip is compatible with standard Luer profile needles and fittings Sold without needle Cat No NS842047 NS840047 NS842070 NS840070 Quantity 3 Pack 3 Pack 3 Pack 3 Pack National Scientific Target Precision Syringes for Accurate Dosing of Liquids Luer Tip Gas Tight Volume 2byL 50uL 100uL 250uL 500uL 1mL 2 5mL 5mL 10mL Syringes for Headspace Soil Gas Sampling Fixed Needle Gas Tight With PTFE tipped stainless steel plungers National Scientific Target Precision Syringes for Headspace Soil Ga
89. ack 0 8mm 290GA092 2 Pack Siltek Cross Inlet Base Seals for Agilent GCs Siltek coating provides a surface with exceptional inertness suitable for analysis of highly active compounds gt Ideal for high flow split applications on Agilent GCs gt Precision machined to provide exceptional sealing properties gt Reduces activity especially useful for analysis of pesticides PCB s phenols etc High grade stainless steel providing reproducible seal Siltek Treated Cross Inlet Base Seals for Agilent GC Instruments I D Cat No Quantit 0 8mm 290GA094 10 Pack 0 8mm 290GA093 2 Pack www thermoscientific com chromatography 297 om Um Finger Tite Connectors Easier fit reliabililty and leak free connections gt Advantages over conventional graphite polymer ferrules gt Perfect metal to metal seal eliminates contamination and gives lower air water background gt No need to retighten ferrules as they expand and contract with the fitting over GC operating temperatures gt Easy to handle with the nut touchable even with a hot injector detector gt No tools required gt Available for Thermo Scientific and Agilent GC instruments Finger Tite Connectors for Thermo Scientific Instruments Description Cat No Quantity Female Nut 290ST130 5 Pack Split Splitess and MS Starter Kit 290ST131 1 Each Split Splitless amp FID Starter Kit 290ST132 1 Each Finger Tite Connectors for Agile
90. amine 8 diphenhydramine 9 lidocaine 10 phenyltoloxamine 11 tripelennamine 12 phenothiazine 13 dextromethorphan 14 methadone 15 amitriptyline 16 trimipramine 17 tetracaine 18 pyrilamine 19 medazepam TG 35MS 30m x 0 25mm x 0 25um 26094 1420 100 C to 325 C at 4 C minute 10 minute hold FID He 30cm sec 1 0 uL Split 50 1 250 C 20 bupivacaine 21 scopolamine 22 codeine 23 morphine 24 diazepam 25 chlorpromazine 26 temazepam 27 flunitrazepam 28 bromazepam 29 prazepam 30 acetopromazine 31 flurazepam 32 papaverine 33 clonazepam 34 haloperidol 35 alprazolam 36 triazolam 7 thioridazine 38 trazodone I 99 GC Applications www thermoscientific com chromatography 215 FORENSIC AND TOXICOLOGY Performance Enhancing Drugs in Racehorses Column Part Number Temperature Detector Type Carrrier Gas Flow Rate Injection Volume Injection Mode 1 Metronidazole 2 Amylobarbitone 3 Pentobarbitone 4 Caffeine 5 Diphenhydramine TR 5MS 15 m x 0 15 mm x 0 25 um 260F128P 45 C 200 C min to 200 C 30 C min to 350 C MS He 0 8 mL min 1 uL 260 C splitless 0 8 min 6 Trimipramine 7 Phenytoin 8 Diazepam 9 Nordiazepam 10 Diphenoxylate Barbiturates Column TR 5MS 15 m x 0 25 mm x 0 25 um Part Number 260F130P Initial Temp 150 C 0 2 min Rate 1 20
91. ansfer Line Nut 290SG001 1 Each Graphite Vespel Ferrule for Transfer Line 290SG020 10 Pack For Agilent Instruments SWAP IT GCMS Interface Kit SWAP IT GCMS Interface Nuts Ferrules Accessories 60180 794 1 Each SWAP IT GCMS Interface SWAP IT Only 60180 796 1 Each Transfer Line Nut 290SG004 1 Each Graphite Vespel Ferrule for Transfer Line 290SG021 10 Pack SWAP Tight Nut and Adaptor for S SL Injector 290SG003 1 Each Accessories SWAP Tight Nut 290SG002 1 Each SWAP Tight Ferrules Blank 290SG000 10 Pack SWAP Tight Ferrules 0 1 0 25mm 290SG025 10 Pack SWAP Tight Ferrules 0 32mm 290SG032 10 Pack Abundance 2 Time min www thermoscientific com chromatography 303 General Gas Chromatography Tools Support GC applications General Gas Chromatography Tools Description Cat No Quantity Straight Tipped Forceps 60180 770 1 Each Angle Tipped Forceps 60180 771 1 Each Pin Vice 60180 772 1 Each Magnifying Glass 60180 773 1 Each Probes 60180 774 1 Each Inspection Mirror 60180 775 1 Each Pick Up Tool 60180 777 1 Each 0 35mm Drill Bit 60180 779 1 Each 0 45mm Drill Bit 60180 780 1 Each 0 70mm Drill Bit 60180 781 1 Each Adjustable Spanner 60180 782 1 Each Tri Scale Ruler 60180 783 1 Each Shortix Capillary Column Cutter 60180 835 1 Each Shortix Capillary Column Cutter Repair Kit 60180 836 1 Each Ceramic Column Cutter 60201 318 1 Each GC Tool Kit for Thermo Scientific Instruments GC Tool Kit for Thermo Scientific Inst
92. atic hydrocarbons TR FAME 260M154P 259 D5974 Fatty androsin acids in tall oil fraction products TG 1MS Inquire 220 D5986 Oxygenates benzene toluene C8 C12 aromatics and total aromatics in finished TG 5MS 26098 1420 221 gasoline by GC FTIR D6160 PCBs in waste materials TR SimDist 260S250P 257 D6352 Boiling range distribution of petroleum fractions TG 1MS Inquire 220 TR SimDist 260S250P 257 D6417 Engine oil volatility TG 1MS Inquire 220 D6584 Free and Total Glycerin in B 100 Biodiesel TR BioDiesel G 26AF024P 261 D6729 Individual components in spark ignition engine fuels TG 1MS Inquire 220 D6730 Individual components in spark ignition engine fuels using precolumn TG 5MS 26098 2960 221 TG 624 26085 4080 229 E202 Ethylene glycols and propylene glycols TR 5 260E470P 247 E475 Di tert butyl peroxide TG 1MS Inquire 220 E1616 Acetic anhydride TG WAXMS 26088 3090 234 E1863 Acrylonitrile TR SimDist 260S250P 257 www thermoscientific com chromatography 211 GC Column Selection by US EPA Drinking Water Test Method Selected EPA Drinking Water methods are listed below with the appropriate recommended that you consult the original complete method or contact our Thermo Scientific GC column offerings In some cases there is more than technical support team for additional information or help in choosing the one phase or column dimension that can be used When in doubt it is correct column for your application Method Title Recommended Par
93. bons Mid polarity phase 35 Phenyl polysilphenylene siloxane e Pharmaceuticals Exceptionally low surface activity Low bleed even at elevated temperatures Similar to DB 35 DB 35MS HP 35 HP 35MS MDN 35 Rtx 35 SPB 35 BPX35 TRACE TR 35MS GC Columns I D Length Film Thickness Cat No Quantity 0 20mm 15m 0 33um 260C497P 1 Each 0 22mm 15m 0 25um 260C129P 1 Each 0 22mm 2bm 0 25um 260C135P 1 Each 0 25mm 15m 0 25um 260C130P 1 Each 0 25mm 30m 0 25um 260C142P 1 Each 0 25mm 60m 0 25um 260C154P 1 Each 0 25mm 30m 0 50um 260C223P 1 Each 0 32mm 30m 0 50um 260C224P 1 Each 0 32mm 30m 0 25um 260C143P 1 Each 0 32mm 60m 0 25um 260C155P 1 Each 0 53mm 30m 0 50um 260C225P 1 Each 0 53mm 15m 1 00um 260C286P 1 Each 0 53mm 30m 1 00um 260C298P 1 Each TRACE TR 1701 GC Columns Mid polarity column with alternative selectivity Applications NON POLAR e Pesticides Phase 1496 Cyanopropylphenyl Polysiloxane e PCB s Max Temps 280 C 300 C USP Listing G46 e PAH S e Organic Acids gt Mid polarity phase 14 Cyanopropylphenyl polysiloxane e Drugs gt Low bleed even at a high operating temperature e Steroids gt Excellent starting point for method development e EPA 608 8081 gt Suitable for a wide variety of applications Similar to DB 1701 Rtx 1701 HP 1701 BP10 OV 1701 007 1701 CP Sil 19 CB TRACE TR 1701 GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 2600130P 1 Each 0 25mm 30m 0
94. cePLOT TG BOND Alumina GC Columns Na SO and KCI Deactivation I D Length Film Thickness Cat No Quantity Na S0 Deactivation 0 32mm 30m Bum 26001 6020 1 Each 0 32mm 50m Bum 26001 6050 1 Each 0 53mm 30m 10um 26001 6080 1 Each 0 53mm 50m 10um 26001 6110 1 Each KCl Deactivation 0 32mm 30m bum 26002 6020 1 Each 0 32mm 50m Bum 26002 6050 1 Each 0 53mm 30m 10um 26002 6080 1 Each 0 53mm 50m 10um 26002 6110 1 Each www thermoscientific com chromatography 239 TracePLOT TG BOND Msieve 5A GC Columns Designed for separation of Ar O and other permanent gases Applications gt Specially designed coating and deactivation procedures for chromatographic e Permanent gases efficiency and the integrity of the coating porous layer gt Deactivation process yields a sharp peak for CO elution rather than the tailing e Refinery or natural gases i commonly seen in other columns gt High retention of molecular sieve permits separation of permanent gases at temperatures above ambient gt Uniform particles remain adherent to the tubing even following continuous valve cycling Similar to GS Msieve HP PLOT Molsieve CP Molsieve 5A Molsieve 5A AT Molsieve PLT 5A Rt Msieve 5A TracePLOT TG BOND Msieve 5A GC Columns I D Length Film Thickness Cat No Quantity 0 32mm 15m 30um 26003 6010 1 Each 0 32mm 30m 30um 26003 6040 1 Each 0 53mm 15m 50um 26003 6070 1 Each 0 53mm 30m 50um 26003 6100 1 Each TracePLOT TG BOND Q GC
95. dynamic Ensure that the sample concentration is suitable for the detection system Peak Area range of the detection system Inappropriate injection technique Try a different injection technique Injection parameters inappropriate Check the injection temperature Check the flow rates Non reproducible sample injection technique Evaluate the sample preparation sequences Compare the results with a series of standard injections Leaking syringe or septum Check and replace the syringe at regular intervals Check and replace septum at regular intervals Leaks at the injection Check the column connections Run a leak check Poor injection technique Carefully meter the injected amount Use a clean good quality syringe Poor split flow or ratio control Monitor the flow Replace the in line filter Poor Sensitivity with Carrier gas flow rate too low Increase the carrier gas flow rate Locate and remove possible obstructions in the carrier Increased Retention Time gas line Check the injector column ferrules Poor Sensitivity with Oven or injector parameters are not optimized Adjust the oven parameters Adjust the injector parameters Normal Retention Time Leaks in the GC carrier gas line Run a leak test and correct leaks Syringe leaks during injection Replace syringe or piston seals if applicable Split injection temperature too low Increase the temperature of the injector Column is in poor condition or wrong column type used Condition the columns C
96. e atmospheric build up in the oven 10 20 30 40 50 60 70 80 90 Gas Linear Flow Rate cm sec A van Deemter plot of efficiency against linear flow rate for three carrier gases Recommended Flow Rates and Velocities for Capillary Columns Carrier Gas 0 25 mm ID 0 32 mm ID 0 53 mm ID mL min cm min mL min cm min mL min cm min He 1 35 IN 35 6 35 H2 1 6 50 2 6 50 7 5 50 N 0 4 14 0 5 11 0 9 7 Recommended Detector Gas Flow Rates Air mL min H2 mL min Make Up mL min ECD E 35 40 FID 350 35 30 NPD 60 2 5 15 FPD 100 75 30 Unretained Compounds FID Methane ECD Methylene Chloride NPD Acetonitrile TCD MS Methane Butane PID ELCD Vinyl Chloride www thermoscientific com chromatography 327 Sag Selection of Injection Method The identification of the most appropriate injection method relies on the sample type and the boiling point to be used in the separation The diagram below summarizes this selection process Concentration Column Conditioning All Columns Except TRACE TR 1MS amp TR WaxMS It is recommended that before the column is subjected to any thermal gradients all oxygen has been removed because the presence of oxygen in the system can shorten the column lifetime Removal of oxygen can be achieved by purging the columns with oxygen free carrier gas for a minimum of 20 minutes at 40 C using an approximate head pressure of 100kPa Although all Thermo Scientific columns have been
97. ed and therefore the contamination It is also dependent on the stationary phase Generally 2mL of pentane is suitable for non polar contamination with methanol used for more polar samples Other contamination such as non volatile compounds pieces of septa or ferrule metal can result in poor peak shape due to band broadening at the injection step This can be cured by the removal of a section from the front end of the column The amount removed is dependent on the degree of contamination the size of injection and the ID of the column but generally 50cm should be sufficient As the efficiency of the column is proportional to the square www thermoscientific com chromatography 329
98. ed plunger gt Feature cone shaped 90 blunt tip National Scientific Target Precision GC Syringes for Agilent Technologies Fixed Needle PTFE Tip Plunger 23 Gauge Volume Length Agilent No Cat No Quantity Sul 42mm NS604305 1 Each 10uL 42mm 5181 8809 NS604405 1 Each SuL 42mm NS604315 6 Pack 10uL 42mm 5181 4730 NS604415 6 Pack Syringes for Agilent Technologies Fixed Needle 26 Gauge gt 26s Gauge needle gt Use with 7673 Series 7683 Series 6850 ALS gt Feature cone shaped 90 blunt tip National Scientific Target Precision GC Syringes for Agilent Technologies Fixed Needle 26 Gauge Volume Length Agilent No Cat No Quantity SuL 42mm 9301 0891 NS104303 1 Each 10uL 42mm 9301 0714 NS104403 1 Each SuL 42mm 5183 4728 NS104313 6 Pack 10uL 42mm 5181 4729 NS104413 6 Pack www thermoscientific com chromatography 313 Syringes for Agilent Technologies Fixed Needle PTFE Tip Plunger 26 Gauge Use with 7673 Series 7683 Series 6850 ALS gt 26s Gauge needle PTFE tipped plunger gt Use with 7673 Series 7683 Series 6850 ALS gt Feature cone shaped 90 blunt tip National Scientific Target Precision GC Syringes for Agilent Technologies Fixed Needle PTFE Tip Plunger 26 Gauge Volume Length Cat No Quantity Sul 42mm NS604303 1 Each 10uL 42mm NS604403 1 Each Sul 42mm NS604313 6 Pack 10uL 42mm NS604413 6 Pack Syringes for PerkinElmer Fixed Needle PTFE Tip Plunger Gas gt 23s and
99. eedle Point Cat No Quantity 25uL 51mm 26s Bevel NS620506 1 Each 100uL 51mm 26s Bevel NS620706 1 Each 100uL 50mm 238 Cone NS620703 1 Each 500uL 51mm 265 Bevel NS620903 1 Each Syringes for CTC Leap Technologies Removable Needle PTFE Tip Plunger Gas Tight Use with A200s GC Pal LC Pal HTS Combi Pal gt 26s Gauge needle gt PTFE tipped plunger gastight National Scientific Target Precision GC Syringes for CTC Leap Technologies Removable Needle PTFE Tip Plunger Gas Tight Volume Length Gauge Needle Point Cat No Quantity 10uL 51mm 26s Bevel NS606405 1 Each Syringes for Manual On Column and Septum Injection Series N Fixed Needle Bevel gt 26s and 22s Gauge needle Use with JADE or Merlin septumless injectors split and splitless mode National Scientific Target Precision GC Syringes for Manual On Column and Septum Injection Series N Fixed Needle Bevel Volume Length Needle Gauge Needle Point Cat No Quantity Sul 51mm 26s Bevel NS100301 1 Each 10uL 51mm 26s Bevel NS100401 1 Each 2byL 51mm 22s Bevel NS100501 1 Each 100uL 51mm 22s Bevel NS100701 1 Each SuL 51mm 26s Bevel NS100311 6 Pack 10uL 51mm 26s Bevel NS100411 6 Pack www thermoscientific com chromatography 315 Syringes for Manual On Column and Septum Injection Series N Fixed Needle 90 gt 22s Gauge needle Use with JADE or Merlin septumless injectors split and splitless mode National Scientific Target Precision Syringes for
100. ent original part gt All Agilent GC 5890 6890 7890 split splitless injection ports Thermo Scientific Gold Inlet Base Seals for Agilent GCs For Use with I D Cat No Quantity Single column installation 0 8mm 290GA081 10 Pack Single column installation 0 8mm 290GA082 2 Pack Dual column installation 1 2mm 290GA121 10 Pack Dual column installation 1 2mm 290GA122 2 Pack Gold Cross Inlet Base Seals for Agilent GCs Gold plating provides a surface with exceptional inertness suitable for analysis of highly active compounds gt Precision machined to provide exceptional sealing properties gt Reduces activity especially useful for analysis of pesticide PCBs phenols etc High grade stainless steel providing reproducible seal gt Direct equivalent to Agilent original part gt Compatible with all Agilent GC 5890 6890 7890 split splitless injection ports 599164 Gold Cross Inlet Base Seals for Agilent GC Instruments I D Cat No Quantity 0 8mm 290GA084 10 Pack 0 8mm 290GA083 2 Pack GC Accessoris Siltek Inlet Base Seals for Agilent GCs Siltek coating provides a surface with exceptional inertness suitable for the analysis of highly active compounds gt Precision machined tp provide exceptional sealing properties gt Reduces activity especially useful for analysis of pesticides PCB s phenols etc High grade stainless steel providing reproducible seal I D Cat No Quantity 0 8mm 290GA091 10 P
101. erating Temperature 40 F to 165 F Inlet 1 4 FNPT Outlet 1 4 FNPT Designed Leak Rate 2 x 10 ccs helium Valve Materials Body Nickel Plated Brass Seat PCTFE Diaphragm 316 Stainless Steel Replacement Indicating Cartridge Filters for VIP Valves Indicating cartridge filters to be used with VIP Valves Replacement Indicating Cartridge Filters for VIP Valves Description Indicator Change Cat No Quantity Triple Indicating Filter H20 O HCs Orange to Gray Purple to Green 60180 942 1 Each Combi Indicating Filter H 0 HC Purple to Green 60180 943 1 Each u GC Accessoris GC Installation Kit gt Includes Tubing cutter x in reamer fig in wrench in wrench in brass tees 4 in brass nuts 10 Brass front and back ferrules 10 15 2m instrument grade cleaned in copper tubing GC Installation Kit Description Cat No Quantity GC Installation Kit 60180 888 1 Each Septa A wide range to cover most applications Variety of materials and temperature limits for all applications For use in Thermo Scientific TRACE and Thermo Scientific FOCUS GCs and instruments from other manufacturers Contaminant free in individual blister packs Temperature limit 400 C Brand Material I D Cat No Quantity BTO Low Bleed Silicone 9mm 31303240 50 Pack BTO Low Bleed Silicone 11mm 31303230 50 Pack BTO Low Bleed Silicone 12 mm 31303228 50 Pack BTO Low Bleed Silicone 17mm 31303211
102. for plunger in needle syringes contain both the plunger and needle which must be changed together Replacement Seals for Syringes Replacement Seals for Thermo Scientific Syringes For Use with Cat No Quantity 0 5uL Syringes 365RK561 2 Pack 1 0uL Syringes 365RK563 2 Pack GC Accessories National Scientific Target Precision Syringes Syringes for Agilent Technologies Fixed Needle 23 265 23 26s Tapered needle Use with 7673 Series 7683 Series 6850 ALS Feature HP style dual gauge cone shaped blunt tip v cw v vy Tapered design combines strength of larger diameter 23s with narrow 26s gauge piercing for minimized evaporation and easy on column injection National Scientific Target Precision GC Syringes for Agilent Technologies Fixed Needle 23 26s Volume Length Agilent No Cat No Quantity DuL 42mm 5181 1273 NS104304 1 Each 10uL 42mm 5181 1267 NS104404 1 Each DuL 42mm 5181 8810 NS104314 6 Pack 10uL 42mm 5181 3360 NS104414 6 Pack Syringes for Agilent Technologies Fixed Needle PTFE Tip Plunger 23 265 23 26s Gauge tapered needle PTFE tipped plunger Use with 7673 Series 7683 Series 6850 ALS Feature HP style dual gauge cone shaped blunt tip vv v v Tapered design combines strength of larger diameter 23s with narrow 26s gauge piercing for minimized evaporation and easy on column injection National Scientific Target Precision GC Syringes for Agilent Technologies Fixed Needle PTFE Tip Plunger
103. h 1 Each 1 Each 24 TRACE TR 5MS GC Columns Feature a popular GCMS phase for many applications Applications NON POLAR e Hydrocarbons Phase 5 Phenyl Polysilphenylene siloxane Solvents NE o e Pesticides USP Listing G27 G36 e Herbicides Phenol gt Non polar phase 5 Phenyl polysilphenylene siloxane e Phenols Ar gt Low bleed and high stability e Amines gt High signal to noise for increased sensitivity gt High robustness to oxygen and water contamination Similar to DB 5 DB 5MS DB 5 625 XTI 5 BPX5 Rtx 5MS Rtx 5 SIIMS AT 5 AT 5MS 007 5MS SPB 5 CP Sil 8CB Ultra 2 HP 5 HP 5MS HP5 TA SPB 5 MDN 5S VF 5ms RSL 200 CB 5 OV 5 PE 5 007 2 MP 5 SE 52 SE 54 PTE 5 CC 5 RH 5ms ZB 5 TRACE TR 5MS GC Columns I D Length Film Thickness Cat No Quantity 0 10mm 5m 0 1um 260F002P 1 Each 0 10mm 10m 0 1um 260F020P 1 Each 0 10mm 20m 0 10um 260F145P 1 Each 0 15mm 25m 0 25um 260F134P 1 Each 0 18mm 20m 0 18um 260F578P 1 Each 0 25mm 15m 0 10um 260F035P 1 Each 0 25mm 15m 0 25um 260F130P 1 Each 0 25mm 15m 1 00um 260F284P 1 Each 0 25mm 30m 0 10um 260F047P 1 Each 0 25mm 30m 0 25um 260F142P 1 Each 0 25mm 30m 0 25um 260F142J 1 Each 0 25mm 30m 0 50um 260F223P 1 Each 0 25mm 30m 1 00um 260F296P 1 Each 0 25mm 60m 0 25um 260F154P 1 Each 0 25mm 60m 1 00pm 260F308P 1 Each 0 32mm 10m 0 10um 260F024P 1 Each 0 32mm 15m 0 25um 260F131P 1 Each 0 32mm 15m 1 00um 260F285P 1 Each 0 32mm 30m 0 25um
104. h 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each Quantity 2 Pack 2 Pack 2 Pack 2 Pack 5 Pack 5 Pack 5 Pack 5 Pack 2 Pack 1 Pack 5 Pack 5 Pack 2 Pack 1 Pack 1 Pack 2 Pack 2 Pack 309 Replacement Plungers for Syringes For Use with Cat No Quantity 365F1921 or 365F1931 365RP421 1 Each 36562111 or 36562161 365RP451 1 Each 365H2321 or 365H2381 365RP461 1 Each 36512561 or 36512611 365RP481 1 Each 365J2831 or 365J2881 365RP491 1 Each 365K3041 or 365K3051 365RP511 1 Each 365D1811 365RP441 1 Each 365D1561 365RP392 2 Pack 36561041 365RP382 2 Pack 365D 1791 365RP522 2 Pack 365D3741 365RP532 2 Pack 365D1611 365RP412 2 Pack 365H3771 365RP471 1 Each 365D1611 365RK351 1 Each 365D2985 365RP121 1 Each 365F3761 365RP431 1 Each 365F3988 365RP816 1 Each 36545333 365RP826 1 Each 36518630 36518635 365RP845 1 Each 365F3700 365RP922 1 Each 365H6 700 365RP926 1 Each 365J7700 365RP928 1 Each 365K8130 365K8135 365RP844 2 Each Repair Kits for Thermo Scientific Plunger in Needle Syringes Extend the life and performance and reduce cost per use of syringes Repair Kits for Thermo Scientific Plunger in Needle Syringes For Repair of Syringe Cat No Cat No Quantity 365A0411 365RK541 1 Each 365A0421 365RK241 1 Each 365A0431 365RK261 1 Each 365A0471 365RK291 1 Each 365A0481 365RK331 1 Each 365A0331 365RK321 1 Each 365B0511 365RK311 1 Each 365B0531 365RK341 1 Each Repair kits
105. hange the column Retention Times Decreasing Stationary phase deteriorated by oxygen and or water Use a carrier gas free of oxygen and water Replace or install appropriate gas filters see page287 289 Stationary phase loss due to column bleeding Reduce the column temperature Retention Times Increasing Increasing carrier leakage Check the septum and column connections Carrier gas supply running out Replace the bottle Low Reproducibility of Drifting or unstable pneumatic controller Monitor the column pressure or flow Check and replace the controller if necessary Retention Times Poor injection technique Start the run at consistent time after injection Sample size is too large Reduce the injected amount and or volume Unstable column temperature Check the main oven door and cooling flap Monitor the column temperature Retention Times are GC column is in poor condition Condition the column Change the column Inconsistent Insufficient equilibration time set on GC Increase equilibration time Poor injection Repeat with better injection technique Oven temperature programmed to rise too quickly Reduce oven temperature ramp rate Air is leaking into the system at the injector seal or Trace and repair the leak the carrier gas manifold If you need more assistance or information on specific detection systems please contact us and request our Troubleshooting Guide www thermoscientific com chromatography 325 _ GC Equation
106. heck the oven temperature ensuring that it doesn t exceed the column upper limit Recondition the column Replace the column Ensure that all interconnections and screw connections are tight Bake out the detector Clean the detector Reduce the upper column temperature Bake out the column Install a high temperature column Install oxygen filters in the carrier gas line Check the pneumatic and inlet systems for leaks Use correct gas purity with low oxygen content Isolate the detector from the electronics If noise disappears clean the collector Check the detector gas flows Condition the column Check the gas purity and install appropriate filters Reduce the detector temperature to the column temperature upper limit Tighten fittings accordingly Lower the column to the correct position 2 3mm below the tip of the jet Isolate the detector from the electronics If the spiking disappears clean the jet and the collector Increase the FID temperature to at least 150 C Reduce the flow to slightly above optimum Increase the flow to slightly above optimum Increase the flow to 40 50mL min Test the column at the optimum flow rate Clean or replace the liner Remove the last two coils from the column Increase the temperature to 5 C below the column maximum Reduce the amount and or concentration of the sample 323 GC Troubleshooting continued Symptom Peak Related Problems Double Peaks
107. henyl Polycarborane siloxane 5 Phenyl Polysilphenylene siloxane 5 Phenyl Methylpolysiloxane Proprietary 35 Phenyl Methylpolysiloxane 35 Phenyl Methylpolysiloxane 100 Dimethyl Polysiloxane Polyethylene Glycol PEG 5 Phenyl Polysilphenylene siloxane 5 Phenyl Methylpolysiloxane 35 Phenyl Polysilphenylene siloxane 5 Phenyl Polysilphenylene siloxane 8 Phenyl Polysilphenylene siloxane Na S0 Deactivated Aluminium Oxide KCI Deactivated Aluminium Oxide Molecular Sieve 5A 100 divinylbenzene Porous divinyl benzene polymer Divinylbenzene 4 vinylpyridine Divinylbenzene ethylene glycol dimethylacrylate www thermoscientific com chromatography Polarity Non Polar Non Polar Non Polar Non Polar Non Polar Non Polar Mid Polarity Mid Polarity Mid Polarity Mid Polarity Mid Polarity Mid Polarity Mid Polarity Mid Polarity Polar Polar Polar Polar Non Polar Non Polar Non Polar Non Polar Non Polar Mid Polarity Mid Polarity Mid Polarity Mid Polarity Mid Polarity Polar Polar Polar Polar Non Polar Mid Polarity Mid Polarity Non Polar Mid Polarity Non Polar Non Polar Non Polar Mid Polarity Mid Polarity Non Polar Polar Non Polar Non Polar Mid Polarity Non Polar Mid Polarity Non Polar Non Polar Non Polar Non Polar Mid Polarity Mid Polarity Polar Maximum Operating Temperature 330 C 350 C 330 C 350 C 330 C 350 C 300 C 315 C 330 C 350 C 380 C 400 C 300 C 320
108. ines e 1 1 0 1 0 1 e Nitrogen containing heterocyclics gt Midpolarity phase 35 diphenyl 65 dimethyl polysiloxane gt Developed for analysis of active basic compounds without derivatization gt Also allows analysis of neutral compounds and adsorptive compounds with oxygen groups susceptible to hydrogen bonding Low bleed at maximum operating temperature TraceGOLD TG 35MS AMINE GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 5um 26092 2110 1 Each 0 25mm 15m Tum 26092 2840 1 Each 0 25mm 30m 0 5um 26092 2230 1 Each 0 25mm 30m Tum 26092 2960 1 Each 0 32mm 15m Tum 26092 2850 1 Each 0 32mm 15m 1 5um 26092 0680 1 Each 0 32mm 30m Tum 26092 2970 1 Each 0 32mm 30m 1 5um 26092 3350 1 Each 0 53mm 15m Tum 26092 2860 1 Each 0 53mm 15m 3um 26092 3840 1 Each 0 53mm 30m Tum 26092 2980 1 Each 0 53mm 30m 3um 26092 3960 1 Each 221 www thermoscientific com chromatography TraceGOLD TG 1301MS GC Columns Low bleed excellent reproducibility and column to column consistency even with sensitive detectors like ECDs and MS A ti NON POLAR pplications Phase 6 Cyanopropylphenyl Polysiloane e Alcohols Max Temps 260 C 280 C USP Listing G43 e Volatile organics e xygenates erc selene Low to mid polarity phase 6 cyanopropylphenyl 94 dimethyl polysilo Long lifetime gt Excellent inertness gt Equivalent to USP G43 phase Similar to Rtx 1301 DB 1301 BP 624 HP 1301
109. interface The ferrules temperature tolerance is well above the limit of the injector MS interface or GC oven Unlike other ferrules SilTite Ferrules do not need re tightening after installation Please also see syringes on page 00 Quantity Part Number 10 29053488 10 29053487 10 29053486 10 29033461 10 29033460 10 29033471 10 290VT168 10 290VT165 10 290VT186 10 290VT187 10 290VT188 2 290BT239 10 29033496 10 29033497 1 290MT229 1 290MT230 17 290MT231 10 290MT221 10 290MT222 10 290MT223 5 290MT211 299 Agilent 5890 6890 and 6850 Instruments Description 15 Graphite 85 Vespel Ferrules Injectors and Detectors GC MS Interface 100 Graphite Ferrules Injectors and Detectors at Atmospheric Pressure Not for GC MS SilTite Kits GC MS Interface Split Splitless Injectors Replacement SilTite Ferrules For all SilTite Connectors SilTite Nuts GC MS Interface Split Splitless Injectors Replacement Baseplate Seals Kits contain 2 nuts and 10 ferrules Contains 2 nuts 10 ferrules and 2 base seals Ferrule Size Column ID Quantity Part Number 0 1 0 25 mm 10 290VA191 0 32 mm 10 290VA192 0 53 mm 10 290VA193 Packed Column 1 8 OD 10 290VT168 Packed Column 1 4 OD 10 290VT165 0 1 0 25 mm 10 29033496 0 32 mm 10 29033497 0 53 mm 10 290VP144 0 1 0 32 mm 10 290GA139 0 45 0 53 mm 10 290GA140 Packed Column 1 8 OD 10 290GA108 Packed Column 1 4 OD 10 290GA107 0 1
110. inute 5 minute hold MS He 30cm sec 1 0 uL Split 50 1 250 C 8 phencyclidine 9 methadone 10 cocaine 11 codeine 12 scopolamine 13 alprazolam TG 5MS 30m x 0 25mm x 0 25um 26098 1420 100 C to 220 C at 15 C minute to 330 C at 10 C minute 5 minute hold MS He 30cm sec 1 0 uL Split 50 1 250 C 5 glutethimide 6 phenobarbital 7 methaqualone 8 primidone 4 E 30 40 50 60 70 80 90 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 min 30 40 50 60 70 80 90 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 210 22 0 23 0 min Underivatized Barbituates Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 ethosuximide 2 barbital 3 methyprylon 4 aprobarbital 5 butalbital 6 amobarbital 7 pentobarbital 8 secobarbital TG 35MS 30m x 0 53mm x 1 0um 26094 2980 100 C to 280 C at 10 C minute 10 minute hold FID He AQcm sec 1 0 uL Splitless 250 C 9 meprobamate 10 carisoprodal 11 glutethimide 12 phenobarbital 13 methaqualone 14 primidone 15 carbamazepine 16 diphenylhydantoin Underivatized Mixed Basic Drugs Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 nicotine 2 benzocaine 3 cotinine 4 meperidine 5 caffeine 6 benzphetamine 7 ket
111. iodiesel M TR Biodiesel F TR Biodiesel G TR DoA5 TR DoA35 TR Dioxin 5MS TR PCB 8MS TR Bond Alumina Na S0 TR Bond Alumina KCI TR Bond Msieve 5A TR Bond Q TR Bond Q TR Bond S TR Bond U 100 Dimethyl Polysiloxane 5 Phenyl Methylpolysiloxane Proprietary Base Optimised 5 Phenyl Methylpolysiloxane Similar to 5 Phenyl Methylpolysiloxane 5 Phenyl Methylpolysiloxane 35 Phenyl Methylpolysiloxane Base Optimised 35 Phenyl Methylpolysiloxane 50 Phenyl Polysiloxane 6 Cyanopropylphenyl Methylpolysiloxane 6 Cyanopropylphenyl Methylpolysiloxane 14 Cyanopropylpheny Methylpolysiloxane 50 Cyanopropylmethyl Phenylmethylpolysiloxane Trifluoropropyl Methylpolysiloxane 90 Cyanopropyl Phenylcyanopropyl Polysiloxane Polyethylene Glycol PEG Acid Optimised Polyethylene Glycol PEG Base Optimised Polyethylene Glycol PEG 100 Dimethyl Polysiloxane 10096 Dimethyl Polysiloxane 5 Phenyl Methylpolysiloxane 5 Phenyl Polysilphenylene siloxane 5 Phenyl Polycarborane Siloxane 35 Phenyl Polysilphenylene siloxane 50 Phenyl Polysilphenylene siloxane 6 Cyanopropylphenyl Polysiloxane 14 Cyanopropylphenyl Polysiloxane 50 Cyanopropylphenyl Polysiloxane 70 Cyanopropyl Polysilphenylene siloxane Polyethylene Glycol PEG Polyethylene Glycol PEG TPA Modified Polyethylene Glygol PEG 100 Dimethyl Polysiloxane Cyanopropylpheyl Dimethyl Polysiloxane Proprietary 5 Phenyl Polysilphenylene siloxane 8 P
112. irst 95 of all GC columns used are either TG 1MS TG 5MS or TG WAXMS type columns A good starting column is a 30m x 0 25mm ID 5 Phenyl column with a 0 25um film thickness such as the TG 5MS 26098 1420 Page 221 This is a non polar column which separates predominately on boiling point but has some polar characteristics For further assistance in choosing the right column for your separation please contact our technical support help desk GC Column Selection Thermo Scientific TRACE GC Column Phase Information TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TraceGOLD TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TRACE TracePLOT TracePLOT TracePLOT TracePLOT TracePLOT TracePLOT TracePLOT Column TG 1MS TG 5MS TG SQC TG 5MS AMINE TG 5SILMS TG 5HT TG 35MS TG 35MS AMINE TG 17MS TG 1301MS TG 624 TG 1701MS TG 225MS TG 200MS TG POLAR TG WAXMS TG WAXMS A TG WAXMS B TR 1 TR 1MS TR 5 TR 5MS TR SHT TR 35MS TR 50MS TR V1 TR 1701 TR 225 TR FAME TR WAX TR WAXMS TR FFAP TR SIMDIST TR 524 TR 525 TR 527 TR 8095 TR 8270 TR Pesticide TR Pesticide Il TR Pesticide III TR Pesticide IV TR B
113. jection Volume Injection Mode 1 Acetone 2 2 Butanone 3 2 Pentanone 4 3 Pentanone 5 4 Methyl 2 pentanone 6 3 Methyl 2 pentanone 7 3 Hexanone 8 2 Methyl 3 hexanone 9 2 Hexanone 10 4 Methyl 2 hexanone 11 Mesityl oxide 40 C 5 min 10 C min to 190 C MS He 25 psi 1 6 mL min 0 5 uL Split 80 1 250 C 12 5 Methyl 2 hexanone 13 3 Heptanone 14 Cyclopentanone 15 2 Heptanone 16 Cyclohexanone 17 Octanone 18 2 Nonanone 19 2 Decanone 20 2 Undecanone 21 2 Dodecanone EPA 625 Phenols 5 ng 260018 Column Part Number Temperature Detector Type Carrrier Gas Injection Mode 1 Phenol 2 2 Chlorophenol 3 2 Nitrophenol 4 2 4 Dimethylphenol dinitrophenol 5 2 4 Dichlorophenol 6 4 Chloro 3 methylphenol TR 5MS 30 m x 0 25 mm x 0 25 um 260F142P 40 C 1 min 8 C min to 360 C FID H 12 psi Split 380 C 7 2 4 6 Trichlorophenol 8 24 Dinitrophenol 9 4 Nitrophenol 10 2 Methyl 4 6 11 Pentachlorophenol 55 10 minutes www thermoscientific com chromatography 6 0 Time min GC Applications 269 _ ENVIRONMENTAL Aromatic Pollutants 2600013 Column TR WaxMS counts 30 m x 0 25 mm x 0 25 um Part Number 260X142P Temperature 60 C Isothermal 10 min Detector Type FID Carrrier Gas He 17 3 psi Flow Rate 1 5 mL min Injection Volume 0 2 ul Injection Mode Split 100 1 250 C 1 Benzene 4 p Xylene 2
114. lf height van Deemter Equation This is a relationship that considers the effect of linear velocity on the HETP or H where A accounts for eddy diffusion B describes the molecular diffusion of the vapor in the direction of the column axis C refers to the resistance to transfer from the stationary to mobile phase and u is the linear velocity of the mobile phase H A CU GC Technical Information Carrier Gas Choice The choice of carrier gas is a compromise between a number of considerations among them efficiency and speed as well as availability safety and cost The three most common carrier gases used are nitrogen helium and hydrogen Nitrogen shows the lowest HETP making it the most efficient of the gases High quality nitrogen is readily available and inexpensive compared to other options However the optimum flow rate to achieve nitrogen s very low HETP leads to long analysis times see figure Helium has a slightly lower efficiency than nitrogen but the optimum flow rate is higher Also small changes in flow rate of helium around the optimum will not affect efficiency as greatly as with nitrogen E E A Fr LLI I For many hydrogen is the carrier gas of choice It shows higher efficiency than helium and at a higher flow rate The variation in HETP with changes in flow rate is also far lower making it more forgiving and reproducible There is however a slight risk of an explosiv
115. lumn for a NIOSH ASTM or EPA method Thermo Scientific column recommendations are given on pages 210 216 Should you need assistance with column selection or method development please contact one of our technical support desks and our highly trained team of scientists will be able to help Quick Reference Icon The reference graphic below on each column page gives easy access to the specifications of each phase type It gives a relative measure of polarity its chemistry and its maximum temperature limits as well as its USP classification NON POLAR E Pi Phase 100 Dimethyl Polysiloxane Max Temps 330 C 350 C USP Listing G2 GC Columns TG 1MS 220 T6 5MS 221 TG SQC 222 m TG 5MS Amine 223 3 TG 5SilMS 224 TG 5HT 225 TG 35MS 226 TG 35MS Amine 227 TG 1301MS 228 TG 624 229 TG 1701MS 230 TG 17MS 231 TG 225MS 232 TG 200MS 239 TG WAXMS 234 TG WAXMS A 235 TG WAXMS B 236 TG POLAR 237 TraceGOLD GC Columns TraceGOLD GC Columns offer you a leap forward in column performance delivering low bleed and superior inertness ideally suited to MS applications 219 www thermoscientific com chromatography TraceGOLD TG 1MS GC Columns Exceptionally low bleed for optimal signal to noise ratio sensitivity and mass spec integrity Annliestons NON POLAR pP rn Phase 100 Dimethyl Polysiloxane e Hydrocarbons Max Temps 330 C 350 C USP Listing G2 e PCBs i e Drugs of abuse gt N
116. lution and avoid unnecessarily long analysis times Another factor to consider is the phase ratio b which is calculated using both the internal diameter and film thickness in the following equation b Internal diameter um 4 x Film thickness um The phase ratio can be used in two ways 1 To categorize the best dimensions for an application a For volatile samples b 100 b For general samples b 250 c For high molecular weight samples b 400 2 To transfer an analysis from a column of one ID to another without changing the method substantially choose a column with a similar b value as this will have similar retention properties Film Thickness um 0 5 1 18 3 00 25 14 8 125 63 3 2 160 80 44 27 265 133 74 44 c amp ETL D Se OS ca Phase ratio B of common column dimensions D Column Length A longer column length will provide greater efficiency and resolution but this is not a linear relationship Resolution is proportional to the square root of column length so doubling the column length will increase resolution by approximately 4096 However increasing the column length will also increase the retention time Double column length twice the analysis time Generally it is recommended to use the shortest column which will perform the desired separation Additional Considerations oeveral generalizations regarding GC columns exist that you might rely on when in doubt F
117. ly Green LED and all 7 red no leak detected LEDs and audible continuous alarm significant leak detectec www thermoscientific com chromatography 305 nn GFM Pro Electronic Flowmeter Measure and monitor flow quickly and efficiently The GFM Pro Flowmeter is specifically designed for use with gas chromatography GC instruments This versatile product is an electronic device capable of measuring bidirectional volumetric flow for all types of gases Real time measurements can be made for various types of flow paths including continually changing gas types The unitis portable so it can be hand held or it also has an optional stand for bench top convenience Compact ergonomic design features side grips for added durability Easy to use interface features over range warning indicator and auto shutoff Measurement range of 0 5 500 mL min both positive amp negative flow Accuracy of 2 of flow or 0 05 mL min whichever is greater Data output via USB port Calibration traceable to NIST primary standards Explosion proof rating for flammable and explosive gases CE certified Uses 2 AA batteries Re calibration service available v wv yv v wv nv mv mv cw GFM Pro Electronic Flowmeter Description Cat No Quantity GFM Pro Flowmeter 66002 010 1 Each Soft sided Carry Case Flowmeter not included 66002 002 1 Each Negative vacuum flow range de 0 00 gt Positive flow range Display reads Display
118. m 15m 0 25um 26097 1300 1 Each 0 25mm 15m 0 5um 26097 2110 1 Each 0 25mm 15m Tum 26097 2840 1 Each 0 25mm 30m 0 25um 26097 1420 1 Each 0 25mm 30m 0 5um 26097 2230 1 Each 0 25mm 30m Tum 26097 2960 1 Each 0 32mm 15m Tum 26097 2850 1 Each 0 32mm 30m Tum 26097 2970 1 Each 0 53mm 15m Tum 26097 2860 1 Each 0 53mm 15m 3um 26097 3840 1 Each 0 53mm 30m Tum 26097 2980 1 Each 0 53mm 30m 3um 26097 3960 1 Each www thermoscientific com chromatography 223 n TraceGOLD TG 5SilMS GC Columns Incorporate phenyl groups in the polymer backbone for improved thermal stability reduced bleed and reduced susceptibility to oxidation NON POLAR i Phase Similar to 596 Phenyl Methylpolysiloxane Applications Max Temps 330 C 350 C i USP Listing G27 G36 e GC MS applications using ion trap systems e Polycyclic aromatics gt Low polarity silarylene phase with selectivity comparable to 5 e Hydrocarbons including chlorinated diphenyl 95 dimethyl polysiloxane hydrocarbons gt Designed for low bleed and outstanding inertness e Phthalates e Phenols e Amines e rganophosphate Similar to DB 5MS VF 5ms CP Sil 8 Low Bleed MS Rxi 5Sil MS BPX5 ZB 5ms Optima 5MS SLB 5 TraceGOLD TG 5SiIMS GC Columns I D Length Film Thickness Cat No Quantity 0 1mm 10m 0 1um 26096 0200 1 Each 0 25mm 15m 0 25um 26096 1300 1 Each 0 25mm 15m 0 5um 26096 2110 1 Each 0 25mm 15m Tum 26096 2840 1 Each 0 25mm 30m 0 25um 26096 1420 1 Each 0
119. menex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Phenomenex Supelco Alltech Alltech Alltech Varian Varian Varian Varian Varian Varian Agilent Agilent Agilent Agilent Agilent Agilent Agilent Agilent Supelco Quadrex Varian Varian Restek Restek Restek Restek Restek Restek Restek Supelco Recommended Thermo Scientific Alternative TG 200MS TR FAME TG 35MS TG 5HT TG 5MS TR 1 TG 1701MS TG WAXMS TR SimDist TG 1MS TG 35MS TR 5 TG 17MS TG 5HT TG 5MS TG 5SiIMS TG 624 TG WAXMS A TR FFAP TG WAXMS TR WAXMS TG BOND Alumina Na2S04 TG BOND Alumina Na2S04 TG BOND Msieve 5A TG BOND Q TG BOND Alumina KCI TG BOND Alumina Na2S04 TG BOND Msieve 5A TG BOND Q TG BOND S TR BOND U TG BOND Alumina Na2S04 TG BOND Alumina KCl TG BOND Msieve 5A TG BOND Q TG BOND Alumina Na2S04 TG BOND Msieve 5A TG BOND Alumina Na2S04 TG BOND U TG BOND Msieve 5A TG BOND Msieve 5A TG BOND Q TG BOND U TG BOND Alumina KCl TG BOND Alumina Na2S04 TG BOND Msieve 5A TG BOND Q TG BOND Q TG BOND S TG BOND U TG BOND Q 233 259 226 225 221 245 230 234 257 220 226 247 231 225 221 224 229 235 256 234 259 239 239 240 241 239 239 240 241 242 242 239 239 240 241 239 240 239 242 240 240 241 242 239 239 240 241 241 242 242 241 207 G
120. mn Part Number Initial Temp Rate Final Temp Detector Temp Carrier Gas Initial Temp Rate Final Temp Hydrocarbon Standard Mix Hydrocarbons C1 C4 Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 Methane 2 Ethane 3 Ethylene 4 Propane TR SimDist 10 m x 0 53 mm x 2 65 um 2605348P 40 C 15 C min 350 C 10 min 400 C Helium 20 mL min 80 C 15 C min 350 C 10 min TG BOND Alumina Na2S04 30m x 0 53mm x 10um 26001 6080 40 C 1 0 minute hold to 200 C at 10 C minute 10 minute hold FID He 40 0 mL min 100 uL Splitless 180 C 5 Propylene 6 n Butane 7 Acetylene 8 Propyne C24 40 20 DO BO an 40 20 on www thermoscientific com chromatography C32 T ca C36 C44 GC Applications 213 FORENSIC AND TOXICOLOGY Basic Drugs Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 amphetamine 2 methamphetamine 3 nicotine 4 cotinine 5 caffeine 6 benzphetamine 7 ketamine Neutral and Acidic Drugs Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 methprylon 2 butalbital 3 amobarbital 4 meprobamate TG 5MS 30m x 0 25mm x 0 25um 26098 1420 100 C to 220 C at 15 C minute to 330 C at 10 C m
121. mplete method Scientific GC column offerings included for your convenience There may or contact our technical support team for additional information or help in be more than one phase or column dimension that can be used When in choosing the correct column for your application Method Title Recommended Part Number Thermo Scientific Phase 801 Aerobic bacteria TR FAME Inquire 1001 Methylene chloride TG 1MS 26098 1430 1002 Chloroprene TG 1MS 26098 2960 1003 Halogenated hydrocarbons TG 624 26085 3390 1004 Dichloroethyl ether TG 1MS Inquire 1005 Methylene chloride TG WAXMS 26088 1430 1010 Epichlorohydrin TG WAXMS Inquire 1011 Ethyl bromide TG WAXMS 26088 2240 1013 Propylene dichloride TG WAXMS Inquire 1015 Vinylidene chloride TG 624 Inquire 1016 1 1 2 2 Tetrachoro 2 2 difluoroethane and 1 1 2 2 tetrachoro 1 2 difluoroethane TG WAXMS 26088 2240 1018 Dichlorodifuoromethane 1 2 dichlorotetrafluoroethane and chlorodifluoromethane TG 1MS 26099 2970 1020 1 1 2 Trichloro 1 2 2 trifluoroethane TG WAXMS 26088 1430 1300 Ketones 1 TG WAXMS 26088 2240 1301 Ketones 2 TG WAXMS 26088 2240 1302 N Methyl 2 pyrrolidinone TG 5MS 26098 2970 1400 Alcohols 1 TG WAXMS 26088 2240 1401 Alcohols 2 TG WAXMS 26088 2240 1402 Alcohols 3 TG WAXMS 26088 2240 1403 Alcohols 4 TG WAXMS 26088 1430 1450 Esters 1 TG WAXMS 26088 2240 1451 Methyl cellosolve acetate TG 5MS 26098 2970 1453 Vinyl acetate TG 5MS 26098 2970 1454 Isopropyl acetate TG 1MS 26099 2970 1457 Ethyl acetate TG WAXMS
122. n Impact lonization lonization Potential 70eV Scan 100 m z to 350 m z in 0 35 Split 50 1 8 2 Deoxy glucitol 9 Allitol 10 Mannitol 11 Galacitol 12 Glucitol 13 Myo inositol J J seen 40505 15 minutes TR 1701 30m x 0 25mm x 0 25um 2600142P 40 C 1 0 minute hold to 260 C at 10 C min 5 minute hold FID He 1 2 mL min 1 0 uL Split 50 1 250 C Mi llivaks 3 Derivatized Glucose isomer www thermoscientific com chromatography 285 GC Accessories Gas Management amp Filtration 287 Injection Port Septa 293 GC Equipment 305 GC Syringes 307 GC Accessories and Equipment Choose Thermo Scientific accessories to enhance and optimize the performance of your GC and GCMS instruments We offer a wide array of products including fittings septa gas filters liners syringes and equipment GC Accessories Click On Inline Filters Easy to use format eliminates contamination Pure gas output 99 9999 or 6 0 grade No carrier gas line contamination during filter change Easy and fast replacement without the need for tools No risk of overtightening fittings w cw Cw v VW Reuseable end fittings reduce cost of clean gas remain installed during filter replacement TUEV approved Maximum pressure 11 bar 160 psi Maximum flow 25L min Combi filter removes oxygen and moisture or moisture and hydrocarbons vv v v vw Triple filter removes oxygen moisture and hyd
123. n methyl ester 3 Dicamba methyl ester 13 Picloram methyl ester 4 Dichlorprop methyl ester 14 Quinclorac methyl ester 5 24 D methyl ester 15 DCPA Dacthal 6 Pentachloroanisole 16 Acifluorfen methyl ester 7 2 4 5 TP Silvex methyl ester 8 Chloramben methyl ester 9 2 4 5 T methyl ester www thermoscientific com chromatography 267 ENVIRONMENTAL QTM PAH Mix Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 Naphthalene 2 Acenaphthylene 3 2 Bromonaphthylene 4 Acenaphthene 9 Fluorene 6 Anthracene 7 Phenanthrene 8 Fluoranthene TG 1MS 30m x 0 25mm x 0 25um 26099 1420 100 C to 160 C at 5 C minute to 260 C at 2 C minute 1 0 minute hold MS He 1 2 mL min 1 0uL Split 50 1 250 C 9 Pyrene 10 Benzo a anthracene 11 Chrysene 12 Benzo b fluoranthene 13 Benzo a pyrene 14 Indeno 1 2 3 c d pyrene 15 Dibenzo a h anthracene 16 Benzo g h i perylene Polybrominated Diphenyl Ethers PBDE in Environmental Samples Column Part Number Temperature Detector Type Carrier Gas Injection Mode 1 Tri BDE 28 2 Tetra BDE 47 3 Penta BDE 99 4 Penta BDE 100 5 Hexa BDE 153 TR 5MS 15m x 0 25 mm x 0 1 um 260F035P Initial Temp 80 C 0 1 min 1 C sec to 300 C hold 10 min MS DSQ He PTV injection 6 Hexa BDE 154 7 Hepta BDE 183 8 Octa BDE 205 9 Nona BDE 206 1
124. n nitrosodiphenylamine 69 phenanthrene 78 3 3 dimethylbenzidine 87 benzo b fluoranthene 23 2 nitrophenol 54 dibenzofuran diphenylamine 70 anthracene 79 butyl benzyl phthalate 88 benzolk fluoranthene 24 2 4 dimethylphenol 55 2 3 5 6 tetrachlorophenol 63 1 2 diphenylhydrazine as 71 carbazole 80 bis 2 ethylhexyl adipate 89 benzo a pyrene 25 benzoic acid 56 2 3 4 6 tetrachlorophenol azobenzene 72 di n butyl phthalate 81 3 3 dichlorobenzidine 90 perylene d12 IS 26 bis 2 chloroethoxylmethane 57 diethyl phthalate 64 2 4 6 tribromophenol SS 73 fluoranthene 82 benzo aJanthracene 91 indeno 1 2 3 cd pyrene 27 2 4 dichlorophenol 58 4 chlorophenyl phenyl ether 65 4 bromophenyl phenyl ether 74 benzidine 83 bis 2 ethylhexyl phthalate 92 dibenzola h anthracene 28 1 2 4 trichlorobenzene 59 fluorene 66 hexachlorobenzene 75 pyrene d10 SS 84 chrysene d12 IS 93 benzo ghi perylene 29 naphthalene d8 IS 60 4 nitroanaline 67 pentachlorophenol 76 pyrene 85 chrysene c contaminant www thermoscientific com chromatography 265 A ENVIRONMENTAL Nitrogen Herbicides Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 Eptam 2 Sutan 3 Vernam 4 Tillam 5 Ordram 6 Treflan 7 Balan 8 Ro Neet TG 35MS 30m x 0 53mm x 0 50um 26094 2250 60 C 1 0 minute hold to 290 C at 15 C minute 5 0 minute hold FID He 2
125. n the outlet Detector base body temperature too low The sample is overloading the column If you need more assistance or information on specific detection systems please contact us and request our Troubleshooting Guide www thermoscientific com chromatography GC Technical Information be shut down and unplugged before starting Eye protection should also be worn The following table lists common GC problems encountered the possible causes and solutions for your quick reference Recommended Solutions Remove the end section of the column Replace the carrier gas cylinder Increase the pressure Check the gas controllers Check impurity levels in the gas source Use correct gas purity Replace or install appropriate Gas Filters see page 287 Perform a leak test Check the tightness of the connections on the carrier gas line Allow enough time for the column to stabilize Alter the GC program See your GC user manual for details Increase the purge flow rate Shorten the purge time Increase the solvent delay Shorten the purge time Contact your service representative Check impurity levels in the gas source Use correct gas purity Replace or install appropriate Gas Filters see page 287 Check the detector and clean it Condition column Change the column Trace and repair the leak Recondition the column Reduce the carrier gas flow Recondition the column Replace gas cylinders Replace the gas filters C
126. nalysis of common drugs of abuse Applications TRACE TR DoA 5MS widely used for the analysis and determination of a range of e Amphetamines codeine and toxicological target compounds including amphetamines codeine and morphine morphine TRACE TR DoA 35MS the recommended column for use in drug testing labs for e Carboxy THC the confirmation of THC TRACE GC Columns for Drugs of Abuse Phase I D Film Thickness Length Cat No Quantity TR DoA35 0 20mm 0 33um 15m 26AC497P 1 Each TR DoA5 0 25mm 0 25um 15m 26AF130P 1 Each TRACE TR BioDiesel GC Columns Designed for use in carbon neutral fuels development applications Applications gt TRACE TR BioDiesel M For determination of residual methanol content in e Biodiesel Biodiesel according to EN method 14110 e ASTM D 86751 gt TRACE TR BioDiesel G For the analysis of total glyceride content according e EN14214 to EN method 14105 gt TRACE TR BioDiesel F For the analysis of FAME content in biodiesel according to EN method 14103 gt TRACE TR BioDiesel G ASTM For the analysis of total glyceride content according to ASTM method D 6751 gt Specific columns developed for the determination of methanol FAMEs or glycerides TRACE TR BioDiesel GC Columns Phase I D Length Film Thickness Cat No Quantity TR BioDiesel M 0 32mm 30m 3 0um 26AA395P 1 Each TR BioDiesel G 0 32mm 10m 0 1um 26AF024P 1 Each TR BioDiesel F 0 25mm 30m 0 25um 26AX142P 1 Each TR BioDiesel G ASTM
127. ning a small percentage of tailing inhibitor TG 1MS 220 TR 1 MS 246 TR 1 245 G42 35 Phenyl 65 dimethylpolysiloxane percentages refer to molar substitution TG 35MS 226 TR 35MS 250 G43 6 Cyanopropylphenyl 9496 dimethylpolysiloxane percentages refer to molar substitution TG 624 229 TR V1 258 G46 1496 Cyanopropylphenol 8696 methylpolysiloxane TG 1701MS 230 TR 1701 251 G48 90 biscyanopropyl 10 cyanopropyl phenyl polysiloxane TG POLAR 237 www thermoscientific com chromatography 209 GC Column Selection by ASTM Method Selected ASTM methods are listed below with the appropriate Thermo Scientific GC column offerings In some cases there is more than one phase or column dimension that can be used When in doubt it is rec ommended that you consult the original complete method or contact our technical support team for additional information or help in choosing the correct column for your application Title Recommended Part Number Thermo Scientific Phase D1983 Fatty acid methyl ester composition TG WAXMS 26088 1420 234 D2245 Oils and oil acids in solvent reducible paints TR FAME 260M154P 259 D2268 High purity n heptane and isooctane TG 1MS Inquire 220 D2306 C8 aromatic hydrocarbons TG WAXMS 26088 1540 234 D2360 Trace impurities in monocyclic aromatic hydrocarbons TG WAXMS 26088 1550 234 D2426 Butadiene dimer and styrene in butadiene concentrates TR 1 260A470P 245 D2427 Determination of C2 through C5 hydrocarbons in
128. nt Instruments Description Cat No Quantity Male Nut 290SA130 5 Pack Split Splitless amp MS Starter Kit 290SA131 1 Each Split Splitless amp FID Starter Kit 290SA132 1 Each Split Splitless Injector Base Seal 290SA133 2 Pack Finger Tite Ferrules I D For Use with Cat No Quantity 0 4mm 0 1 0 25mm I D columns 29081132 10 Pack 0 5mm 0 32mm D columns 29081131 10 Pack Ferrules GC Accessories Wide range of choices for a wide range of instruments and applications Thermo Scientific ferrules are available in three different materials and various dimensions to match the instrument and capillary column ID The choice of material is dependent upon the use guidelines are given in the table 100 Graphite Ferrules Thermo Scientific 100 graphite ferrules are a soft material that Is porous to oxygen making them suitable for most applications except GC MS interface connections These easy to use ferrules form a soft grip with the column and provide a stable seal Material Type Suitable for GC MS Graphite No Graphite Vespel Yes Stainless Steel SilTite Yes 15 Graphite 85 Vespel Ferrules The mechanically robust 15 Graphite 85 Vespel ferrules have a long lifetime and are compatible with GC MS These ferrules form a strong grip with the column and cannot be reused as they form a permanent seal with the column They have a temperature limit of 350 C but must be re tightened after initial temperature c
129. nt flow too low Too large injection size Carrier gas flow rate too high Column deteriorated Column temperature too high Column too short Incorrect column choice Injection technique is not adequate Bleed from the GC column Bleed from the septum sample vial septa are contaminating the sample Recommended Solutions Inject more rapidly in a smooth motion Use a higher speed Decrease the injected amount Decrease the analyte concentrations Increase the split ratio Increase the temperature Use a thicker film column Repeat with better injection technique Replace the cylinder Replace the filter see page 287 289 Ensure the glassware is clean and contamination free Decrease the injection port temperature Use the on column injection technique Carry out adequate clean up of sample prior to injection Remove the column and bake out the inlet Use a high quality septum Replace the split vent filter Install an in line filter between the pneumatics and the inlet Increase the final oven program temperature or total run time Increase the column flow rate Increase the initial oven temperature Reduce the injection volume On column Install a retention gap On column Reduce the carrier gas flow rate Check the combustion gas flow Bake out or clean the detector Check the detector temperature and that flame is lit Inject less sample Check the column position Replace or repair the syringe
130. od 527 features the robust low bleed performance required for analysis of pesticides and flame retardants gt TRACE TR 8270 US EPA Solid Waste Test Method 8270 gt TRACE TR 8095 US EPA Method 8095 for Explosives Testing featuring high max temperature and low surface activity TRACE GC Columns for Specific EPA Methods e Pesticides e Flame retardants e Explosives Phase I D Length Film Thickness Cat No Quantity TR 524 0 18mm 20m 1 0um 26RV495P 1 Each TR 525 0 25mm 30m 0 25um 26RX142P 1 Each TR 527 0 25mm 30m 0 25um 26RF142P 1 Each TR 8095 0 32mm 12m 0 25um 260P123P 1 Each TR 8270 0 25mm 30m 0 5um 26RF223P 1 Each TR 8270 0 25mm 30m 1 0um 26RF296P 1 Each TRACE GC Columns for Dioxin and PCB Analysis Designed to meetthe requirements of high resolution GC MS methods Applications TRACE TR Dioxin 5MS Specifically designed for Dioxin and Furan testing e Dioxins PCDDs gt Wide coverage of the 17 cogeners with the highest toxicological significance e Furans PCDFs gt TRACE TR PCB 8MS meets the requirments for HR GCMS analysis of PCB s e PCB Congeners Low bleed TRACE GC Columns for Dioxin and PCB Analysis Phase I D Length Film Thickness Cat No Quantity TR PCB 8MS 0 25mm 50m 0 25um 26AJ148P 1 Each TR Dioxin 5MS 0 2bmm 60m 0 25um 26AF154P 1 Each TR Dioxin 5MS 0 25mm 30m 0 1um 26AF047P 1 Each TR Dioxin 5MS 0 2bmm 60m 0 1um 26AF059P 1 Each TRACE GC Columns for Drugs of Abuse Specifically designed for the a
131. ode 1 diethylamine 2 pyridine 3 morpholine 4 phenol 5 aniline 6 2 chlorophenol 7 diethylenetriamine TG 5MS Amine 30m x 0 32mm x 1 0um 26097 2970 120 C to 220 C at 10 C minute FID Hydrogen 40 cm min 1 0 uL Split 25 1 300 C 8 octylamine 9 1 methyl 2 pyrrolidinone 10 2 nitrophenol 11 2 6 dimethylaniline 12 nicotine 13 2 nitroaniline Primary Amines min 0 5 10 Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 methylamine 2 dimethylamine 3 trimethylamine 4 ethylamine 5 isopropylamine 15 20 25 30 35 40 45 TG 35MS Amine 30m x 0 53mm x 1 0um 26092 2980 35 C 5 minute hold Isothemal FID He 35 cm sec 1 0 uL Split 10 1 250 C 6 tert butylamine 7 n propylamine 8 diethylamine 9 sec butylamine Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 trimethylamine 2 dimethylamine 3 ethylamine 4 methylamine 5 isopropylamine TG WAXMS B 30m x 0 53mm x 1 0um 26086 2980 45 C Isothermal FID Hydrogen 40 cm sec 1 0 uL Direct Injection 250 C 6 n propylamine 7 tert butylamine 8 diethylamine 9 sec butylamine Residual Solvents Class 1 Column Part Number Temperature at 10 C min 20 minute Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1
132. on polar 100 dimethyl polysiloxane e Gasoline range organics GRO gt Equivalent to USP G2 e Refinery gases e Essential oils e Pesticides Similar to Rxi 1ms DB 1 DB 1ms HP 1 HP 1ms Ultra 1 SPB 1 Equity 1 VF 1ms CP Sil 5 CB Low Bleed MS TraceGOLD TG 1MS GC Columns I D Length Film Thickness Cat No Quantity 0 1mm 10m 0 1um 26099 0200 1 Each 0 25mm 15m 0 25um 26099 1300 1 Each 0 25mm 15m 0 5um 26099 2110 1 Each 0 25mm 15m Tum 26099 2840 1 Each 0 25mm 30m 0 25um 26099 1420 1 Each 0 25mm 30m 0 5um 26099 2230 1 Each 0 25mm 30m Tum 26099 2960 1 Each 0 25mm 60m 0 25um 26099 1540 1 Each 0 25mm 60m 0 5um 26099 2350 1 Each 0 25mm 60m Tum 26099 3080 1 Each 0 32mm 15m 0 25um 26099 1310 1 Each 0 32mm 15m 0 5um 26099 2120 1 Each 0 32mm 15m Tum 26099 2850 1 Each 0 32mm 30m 0 25um 26099 1430 1 Each 0 32mm 30m 0 5um 26099 2240 1 Each 0 32mm 30m Tum 26099 2970 1 Each 0 32mm 60m 0 25um 26099 1550 1 Each 0 32mm 60m 0 5um 26099 2360 1 Each 0 32mm 60m Tum 26099 3090 1 Each 0 53mm 15m 0 5um 26099 2130 1 Each 0 53mm 15m Tum 26099 2860 1 Each 0 53mm 15m 1 5m 26099 3340 1 Each 0 53mm 30m 0 5um 26099 2250 1 Each 0 53mm 30m Tum 26099 2980 1 Each 0 53mm 30m 1 5um 26099 3360 1 Each 0 53mm 60m 1 5um 26099 3370 1 Each TraceGOLD TG 5MS GC Columns The most widely used MS phase in gas chromatography Applications i Semivolatiles Phase 5 diphenyl 95 dimethyl polysiloxane e Phenols Max Temps 330 C 350 C USP Listing G
133. on tetrachloride 18 Benzene 19 1 2 Dichloroethane 20 Trichloroethene Explosives TR 8095 12m x 0 32 mm x 0 25 um 260P123P 200 pg uL HMX 2 000 pg uL 80 C 5 min 20 0 C min to 225 C 225 C Mass Spec Methane 2 5 mL min Helium 5 0 mL min Constant Flow Basic 1 0 21 1 2 Dichloropropane 22 Dibromomethane 23 Bromodichloromethane 24 cis 1 3 Dichloropropene 25 Toluene 26 trans 1 3 Dichloropropene 27 1 1 2 Trichloroethane 28 Tetrachloroethene 29 1 3 Dichloropropane 30 Dibromochloromethane 1 Nitrobenzene 2 2 Nitrotoluene 3 3 Nitrotoluene 4 4 Nitrotoluene 5 Nitroglycerin 400 600 800 10 00 31 1 2 Dibromoethane 32 Chlorobenzene 33 Ethylbenzene 34 1 1 1 2 Tetrachloroethane 35 m Xylene 36 p Xylene 3 o Xylene 38 Styrene 39 Bromoform 40 Isopropylbenzene 6 2 6 Dinitrotoluene D3 ISTD 7 2 6 Dinitrotoluene 8 1 3 Dinitrobenzene 9 2 4 Dinitrotoluene 10 2 4 6 Trinitrotoluene www thermoscientific com chromatography GC Applications 41 Bromobenzene 42 1 1 2 2 Tetrachloroethane 43 1 2 3 Trichloropropane 44 n Propyl benzene 45 2 Chlorotoluene 46 1 3 5 Trimethylbenzene 47 4 Chlorotoluene 48 tert Butylbenzene 49 1 2 4 Trimethylbenzene 50 sec Butylbenzene 11 1 3 5 Trinitrobenzene 12 PETN 13 4 Amino 2 6 dinitrotoluene 14 RDX 15 3 5 Dinitroaniline OT 1 2 3 4 5 56 O10101 OT OT OT I 8 g 0
134. pre conditioned we recommend that they are conditioned after installation by following these steps 1 Heat the column from 50 C to the maximum operating temperature at 5 C min and hold for one hour The maximum operating temperatures for all TRACE GC columns are provided below It is important to stay within the maximum temperature range for the column 2 Monitor the detector signal during conditioning until a stable baseline is reached Due to the factory pre conditioning of the column this should be case of thick films and polar phases Maximum Operating Temperatures for TraceGOLD and TRACE GC Columns Column Maximum Operating Temperature Column Maximum Operating Temperature Column TG 1MS 330 C 350 C TG 5MS 330 C 350 C TG SQC 330 C 350 C TG 5MS AMINE 300 C 315 C TG 5SILMS 330 C 350 C TG 5HT 380 C 400 C TG 35MS 300 C 320 C TG 35MS AMINE 220 C TG 17MS 300 C 320 C TG 1301MS 260 C 280 C TG 624 240 C TG 1701MS 260 C 280 C TG 225MS 240 C TG 200MS 320 C 340 C TG POLAR 275 C TG WAXMS 260 C TG WAXMS A 250 C TG WAXMS B 220 C TR 1 films TR 1MS TR 5 TR 5HT TR 5MS TR 35MS TR 50MS TR V1 TR 1701 TR 225 TR FAME TR WAX TR WAXMS TR FFAP 340 C 360 C for films lt 1 0um 300 C 320 C for films 1 5 to 3 0um 280 C 300 C for films gt 3 0um 370 C 380 C 340 C 350 C for films lt 1 5um 280 C 300 C for films gt 1 5um 380 C
135. r Change Capacity Moisture Inert Carrier Air H Gray to White 7 2g H O Oxygen Inert Carrier Green to Gray 1L 0 Hydrocarbon Inert Carrier Air H 12g n butane Combi Inert Carrier Purple to Green 1 89 H0 6g HCs Triple Inert Carrier Orange to Gray 1 8g H20 500mL 0 4g HCs Purple to Green Super Clean Cartridge Filters Description Base Included Cat No Quantity Moisture Cartridge Filter with Indicator No 60180 819 1 Each Oxygen Cartridge Filter with Indicator No 60180 820 1 Each Hydrocarbon Cartridge Filter No 60180 821 1 Each 3 Cartridge Pack 1 x Triple 2 x HC H 0 Combi Filters No 60180 822 1 Each 4 Cartridge Pack 1 x O 1 x H 0 2 x HC Filters No 60180 823 1 Each Indicating Triple H 0 O HCs No 60180 824 1 Each Indicating Triple H 0 02 HCs He Preconditioned for GCMS No 60180 825 1 Each Indicating Combi HC H 0 No 60180 826 1 Each 4 Cartridge Kit 1 x O 1 x H20 2 x HC Filters Yes 60180 827 1 Each 3 Cartridge Kit 1 x Triple 2 x HC H 0 Combi Filters Yes 60180 828 1 Each 1 Cartridge Kit 1 x Indicating Triple He Preconditioned for GCMS Yes 60180 829 1 Each 1 Cartridge Kit 1 x Triple He Preconditioned for GCMS Yes 60180 830 1 Each Twin HC Filters For High Flow Base Plate LC MS No Indicator No 60180 831 1 Each High Flow Twin H 0 Filters Air Generators No 60180 832 1 Each High Flow Cartridge Pack 2 x HC No indicator for LCMS No 60180 839 1 Each High Flow Cartridge Pack 2 x HC with indicator for LEMS
136. reads Display reads Display reads Display reads over range flow values under range flaw values flow values 500 mLimin 0 50 mL min 0 50 mL muin 500 mlumin Thermo Scientific GC Syringes Autosampler Syringes for Thermo Scientific Instruments Autosampler Syringes for Thermo Scientific Instruments Volume Needle Type Length Gauge TipStyle TriPlus AS3000 AS2000 Al Type Cat No Quantity 0 5uL Plunger in Needle 50mm 23 Cone X X Split PTV 36504045 1 Each 0 5uL Plunger in Needle 75mm 31 Cone Manual OC 36500500 1 Each O5pl Plunger in Needle 80mm 26 Cone and 36504046 1 Each DuL Fixed 50mm 26 Cone split PTV 36504047 1 Each SuL Fixed 50mm 23 Cone X X X 36503701 1 Each Sul Fixed 50mm 26 Cone X X split PTV 36500505 1 Each Sul Removable 75mm 31 Cone Manual OC 36500510 1 Each bul Fixed 80mm 26 Cone X spitlessand 365020251 Each 10uL Removable 42mm 28 Cone X 365D1611 6 Pack 10uL Fixed 50mm 26 Cone X X X 365D3711 1 Each 10uL Fixed 50mm 26 Cone X X X 365D1856 6 Pack 10uL Fixed 50mm 25 Cone X X X X Split PTV 36500525 1 Each 10uL Fixed 50mm 23 Cone X X X X PTV SSL Split 36520060 1 Each 10uL Removable 50mm 26 Cone X X 365D1841 1 Each 10uL Removable 50mm 23 Cone X X X 365D3731 1 Each Merlin Valve 10uL Fixed 80mm 23 Cone X X SSL Splitless 36520061 1 Each OC in PTV 10uL Fixed 50mm 23 26 Cone X X Metin Valve 36500580 1 Each 10uL Fixed Gas Tight 50mm 23 Cone X 365D3741 1 Each 10uL Fixed 80mm 2 Cone X X ae 36502019 1 Each SS 10uL Remo
137. rocarbons Click On Inline Filters For Gas Indicator Change Capacity Moisture Inert Carrier Air H 219 H O Oxygen Inert Carrier 3L 0 Hydrocarbon Inert Carrier Air H 36g n butane Indicating Triple Inert Carrier Red to White 3g H 0 400mL 0 5g HCs Purple to Green Triple Inert Carrier 6g H Q 1L O 12g HCs Combi Inert Carrier 10g HQ 18g HCs Click On Inline Filters Type Cat No Quantity Moisture Filter 60180 801 1 Each Oxygen Filter 60180 802 1 Each Hydrocarbon Filter 60180 803 1 Each Combi 02 H20 60180 804 1 Each Triple H20 02 HCs 60180 805 1 Each Triple H20 02 HCs He Preconditioned for GCMS 60180 806 1 Each Indicating Triple 02 H20 HCs He Preconditioned for GCMS 60180 808 1 Each Combi Moisture and Hydrocarbons 60180 843 1 Each End fitting Brass 0 125 in 60180 809 2 Pack End fitting Steel 0 125 in 60180 810 2 Pack End fitting Brass 0 25 in 60180 811 2 Pack End fitting Steel 0 25 in 60180 812 2 Pack Double ended Connector to Connect Filter to Indicator 60180 813 1 Each Replacement O rings 60180 833 1 Each Wall mounting clamp 60180 834 4 Pack www thermoscientific com chromatography 287 Super Clean Cartridge Filters Replace easily without tools 99 9999 pure gas or 6 0 grade output No carrier gas line contamination during cartridge change Cost effective TUEV approved Max pressure 11 bar 160 psi vv v v 4 Max flow 7L min Cartridge Type For Gas Indicato
138. rophenol 7 2 4 Dinitrophenol 3 2 4 Dimethylphenol 8 4 Nitrophenol 4 2 4 Dichlorophenol 9 2 Methyl 4 6 dinitrophenol 5 4 Chloro 3 methylphenol 10 Pentachlorophenol 10 00 12 00 14 00 16 00 18 00 20 00 EPA 502 2 Volatile Organic C Column Part Number USEPA 502 2 mix Injection Mode Split Ratio Injection Volume Initial Temp Injection Temp Rate 1 Rate 2 Liner Type Final Temp Carrier Gas Carrier Gas Flow Average Linear Velocity Detector Type Full scan 1 Dichlorodifluoromethane 2 Chloromethane 3 Vinyl chloride 4 Bromomethane 5 Chloroethane 6 Trichlorofluoromethane 7 1 1 Dichloroethene 8 Dichloromethane 9 trans 1 2 Dichloroethene 10 1 1 Dichloroethane EPA 8095 Column Part Number sample Initial Temperature Rate 1 Final Temperature 1 Detector Type Reagent Gas Type Reagent Gas Flow all segments Carrier Gas Carrier Gas Flow Left Carrier Method Mode Injection mode Sample volume uL ompounds TR V1 30 m x 0 25 mm x 1 4 um 260V332P 200 ppm in Methanol Split 50 1 1 uL 40 C 1 min 250 C 6 C min to 210 C 15 min to 240 C 4 mm ID Single Taper Liner 240 C 5 min Helium 22 8 psi 1 3 mL min 35 cm sec at 40 C Mass Spectrometer 45 450 11 2 2 Dichloropropane 12 cis 1 2 Dichloroethene 13 Bromochloromethane 14 Chloroform 15 1 1 1 Trichloroethane 16 1 1 Dichloropropene 17 Carb
139. ruments Description Cat No Quantity Capillary Tool Kit for Thermo Scientific GCs 60180 784 1 Each GC Tool Kit for Agilent Instruments Description Cat No Quantity Capillary Tool Kit for Agilent GCs 60180 786 1 Each GC Accessories GLD Pro Gas Leak Detector Aids in quickly locating and identifying gas leaks The GLD Pro Gas Leak Detector is specifically designed for use with gas chromatography instruments Detection of leaks allows the user to reduce detector noise provide a stable baseline reduce carrier gas by minimizing waste and maximize the lifetime of the analytical column by minimizing the presence of oxygen and other impurities in the carrier gas Suitable for detection of a wide range of laboratory gases Push button on off switch Push button zero function Automatic shutoff 5 minutes LED light indicator for intensity of leak Rechargable battery up to 6 hrs operation Durable storage case Probe holder One year warranty v v cw cw Y vv vY GF WH GLD Pro Gas Leak Detector Description Cat No Quantity GLD Pro Leak Detector 66002 001 1 Each Small Probe Adaptor 66002 003 1 Each Soft sided Carry Case Leak Detector not included 66002 002 1 Each Green LED and all 3 yellow Green LED and 4 red LEDs and audible continuous LEDs small leak detected alarm significant leak detected N 200 S E E Probe Reference e H eference gt Lj 5 Ze e C gt Green LED on
140. s Adjusted Retention Time t An analyte s retention time tg minus the elution time of an unretained peak tm tr tm Adjusted retention time is also equivalent to the time the analyte spends in the stationary phase Capacity Factor k Expression that measures the degree of reten tion of an analyte relative to an unretained peak where tp is the retention time for the sample peak and tm is the retention time for an unre tained peak A measurement of capacity will help determine whether retention shifts are due to the column capacity factor is changing with retention time changes or the system capac ity factor remains constant with retention time changes tet tm k Thus the higher the capacity factor the longer the retention time Effective Theoretical Plates N A measure of a column performance that accounts for the effects of unretained elution time where tr is the adjusted retention time and o is the standard deviation of the peak ta 2 el This value also remains constant as retention gaps and guards are used Depending on the method of peak width calculation different efficiencies can be reported This leads to two popular measures t 2 N 16 Where W is the tangential peak width 13 4 peak height tr Y N 5 54 Where W is the width measured at half height 50 peak height 326 41 HEEP H Height Equivalent to an Effective Plate Her L
141. s Sampling Fixed Needle Gas Tight Cat No NS600511 NS600611 NS600711 NS600811 NS600911 NS600013 NS600033 NS600053 NS600073 With PTFE tipped stainless steel plungers Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each Volume Sul 10uL 250uL 1mL 2 5mL 5mL Needle Length 51mm 51mm 51mm 51mm 51mm 51mm Gauge 26s 26s 22S 22S 228 228 00s Needle Point Side hole Side hole Side hole Side hole Side hole Side hole Cat No NS600304 NS600404 NS600804 NS600002 NS600022 NS600042 Quantity 1 Each 1 Each 1 Each 1 Each 1 Each 1 Each GC Accessories Syringes for CTC Leap Technology Headspace Fixed Needle Gas Tight gt For Combi Pal Headspace Autosampler gt PTFE tipped stainless steel plunger National Scientific Target Precision Syringes for CTC Leap Technology Headspace Fixed Needle Gas Tight Volume Needle Length Gauge Needle Type Cat No Quantity 10uL 51mm 26s Bevel NS606401 1 Each 1 0mL 56mm 22s side hole NS620013 1 Each 2 5mL 56mm 22s side hole NS620023 1 Each 5 0mL 56mm 22S Side hole NS620049 1 Each Syringes for On Column Fused Silica Removable Needle Stainless steel plunger National Scientific Target Precision Syringes for On Column Fused Silica Removable Needle Volume Needle Length 0 D Cat No Quantity Sul 100mm 0 23mm NS142304 1 Each 10uL 100mm 0 23mm NS142404 1 Each Syringes for On Column Fused Silica
142. s Tapered needle National Scientific Target Precision GC Syringes for Agilent Technologies Replacement Needles 23 26s Volume Length Agilent No Cat No Quantity Sul 42mm 5182 0832 NS834308 3 Pack 10uL 42mm 5181 3319 NS834408 3 Pack Syringes for Agilent Technologies Fixed Needle Super Elastic Plunger 23 265 23 26s Tapered needle super elastic plunger Use with 7673 Series 7683 Series 6850 ALS Feature cone shaped 90 blunt tip v cw v vy Tapered design combines strength of larger diameter 23s with narrow 26s gauge piercing for minimized evaporation and easy on column injection National Scientific Target Precision GC Syringes for Agilent Technologies Fixed Needle Super Elastic Plunger 23 26s Volume Length Agilent No Cat No Quantity Sul 42mm N A NS164304 1 Each 10uL 42mm N A NS164404 1 Each Syringes for Agilent Technologies Fixed Needle 23 Gauge gt 23s Gauge needle Use with 7673 Series 7683 Series 6850 ALS gt Feature cone shaped 90 blunt tip National Scientific Target Precision GC Syringes for Agilent Technologies Fixed Needle 23 Gauge Volume Length Agilent No Cat No Quantity Sul 42mm 9301 0892 NS104305 1 Each 10uL 42mm 9301 0713 NS104405 1 Each Sul 42mm 5182 0875 NS104315 6 Pack 10uL 42mm 9301 0725 NS104415 6 Pack Syringes for Agilent Technologies Fixed Needle PTFE Tip Plunger 23 Gauge gt Use with 7673 Series 7683 Series 6850 ALS gt 23s Gauge needle PTFE tipp
143. s polar columns Applications e Alcohols e Pesticides e xygenates e PCB cogeners e Aroclor mixes Similar to NON POLAR Phase Max Temps USP Listing 14 Cyanopropylphenyl Polysiloxane 260 C 280 C G46 Mid polarity phase 14 cyanopropylphenyl 86 dimethyl polysiloxane Fully characterized for long term reproducibility column to column consistency and low bleed Optimal for confirmation analysis Equivalent to USP G46 phase Rtx 1701 DB 1701 HP 1701 SPB 1701 VF 1701 CP Sil 19 CB TraceGOLD TG 1701MS GC Columns I D 0 1mm 0 25mm 0 25mm 0 25mm 0 25mm 0 25mm 0 25mm 0 25mm 0 25mm 0 25mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 32mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 0 53mm 00s Length 10m 15m 15m 15m 30m 30m 30m 60m 60m 60m 15m 15m 15m 15m 30m 30m 30m 30m 60m 60m 60m 60m 15m 15m 15m 15m 15m 30m 30m 30m 30m 30m 60m 60m 60m 60m 60m Film Thickness 0 1um 0 25um 0 5um Tum 0 25um 0 5um Tum 0 25um 0 5um Tum 0 25um 0 5um Tum 1 5um 0 25um 0 5um Tum 1 5um 0 25um 0 5um Tum 1 5um 0 25um 0 5um Tum 1 5um 3um 0 25um 0 5um Tum 1 5um 3um 0 25um 0 5um Tum 1 5um 3um Cat No 26090 0200 26090 1300 26090 2110 26090 2840 26090 1420 26090 2230 26090 2960 26090 1540 26090 2350 26090 3080 26090 1310 26090 21
144. t Number Thermo Scientific Phase 501 3 Trihalomethanes TG 624 26085 3960 229 502 1 Volatile halogenated compounds TG 624 26085 4080 229 TR 5MS 260F396P 248 502 2 Volatile organic compounds TG 624 26085 4080 229 TG 624 26085 3320 229 503 1 Volatile aromatic amp unsaturated organics TG 624 26085 4080 229 TR 5MS 260F396P 248 504 EDB and DBCP TR 5MS 260F396P 248 TG 5MS 26098 2240 221 504 1 EDB and DBCP TR 5MS 260F396P 248 TG 5MS 26098 2240 221 506 Phthalates and adipates TG 1MS 26099 1430 220 TG 5MS 26098 1430 221 507 Organonitrogen and organophosphorus pesticides TG 5MS 26098 1420 221 TG 17MS 26089 1420 231 509 Ethylene thiourea TG 1701MS 26090 1420 230 TG WAXMS 26088 1300 234 513 Dioxin TG 5MS 26098 1540 221 515 2 Chlorinated herbicides TG 5MS 26098 1430 221 TG 17MS 26089 1430 231 524 1 Volatile organic compounds TR 524 26RV495P 260 TG 624 26085 4080 229 TG 624 26085 3320 229 524 2 Volatile organic compounds TR 524 26RV495P 260 TG 624 26085 4080 229 TG 624 26085 3320 229 525 1 Semi volatile organic compounds TR 525 26RX142P 260 TG 5MS 26098 1420 221 525 2 Semi volatile organic compounds TR 525 26RX142P 260 TG 5MS 26098 1420 221 527 Selected pesticides and flame retardants TR 527 26RF142P 260 TG 5MS 26098 1420 221 548 1 Endothall TG 1MS 26099 1430 220 TG 5MS 26098 1420 221 551 Chlorinated disinfection by products chlorinated solvents TG 5MS 26098 1420 221 TG 1701MS 26090 2240 230 552 Haloacetic acids TG 1701MS 26090 1430 230 TG 35MS 26094
145. te column because of the wide range of options However the choice can be simplified by considering a number of questions about the planned separation his section provides useful information to help you determine the most suitable column for your analysis Column Selection for Existing or Regulated Methods This section provides a number of tools to aid in selecting the most appropriate product from the TRACE family of GC Columns The Thermo Scientific TRACE Phase table lists details for the wide array of phases offered in the TraceGOLD TRACE and TracePLOT GC column ranges The GC Column Selection by Manufacturer table provides a quick cross reference for TRACE columns to other GC columns If you are following an ASTM NIOSH or US EPA method please refer to the Column Selection by Method tables for the best Thermo scientific product Method Development Considerations When first developing a method you should consider these column characteristics to determine the best column for the separation A Column Phase B Internal Diameter C Film Thickness D Column Length A Column Phase In GC the separation of two analytes occurs due to differences in their interaction with the stationary phase therefore a phase must be chosen that matches the properties of the sample For example if the components have different boiling points greater than 2 C a non polar column such as the TG 1MS is recommended If the products differ primarily in
146. te esters TG WAXMS 26088 2980 234 D3695 Volatile alcohols in water by direct aqueous injection GC TG WAXMS 26088 2980 234 D3710 Boiling range distribution of gasoline and gasoline fractions TR SimDist 2605348P 257 TR SimDist 26053478 257 D3725 Fatty acids in drying oils TR FAME Inquire 259 D3760 Isopropylbenzene cumene TG WAXMS 26088 1550 234 TG 1MS Inquire 220 D3797 o Xylene TG WAXMS 26088 2360 234 D3798 p Xylene TG WAXMS 26088 2360 234 D3871 Purgeable organic compounds in water using headspace sampling TG 624 26085 4080 229 D3893 Purity of methyl amyl ketone and methyl isoamyl ketone TG 624 26085 3960 229 D3973 Low molecular weight halogenated hydrocarbons in water TG 624 26085 3960 229 D4059 PCBs in insulating liquids TG 5MS 26098 1540 221 TR PCB 8MS 26AJ148P 260 D4415 Dimer in acrylic acid TG WAXMS 26088 1430 234 GC Column Selection Method Title Recommended Part Number Thermo Scientific Phase D4443 Residual vinyl chloride monomer content in ppb range in homo and co polymers by headspace GC TG 624 26085 3960 229 D4735 Trace thiophene in refined benzene TG WAXMS 26088 2250 234 D4773 Propylene gycol monomethyl ether dipropylene glycol monomethyl ether and propylene TR 5 260E470P 24 glycol monomethy ether acetate D4806 Denatured fuel ethanol for blending with gasoline for use as automotive spark ignition TG 1MS Inquire 220 engine fuel D4815 MTBE ETBE TAME DIPE tert Amyl Alcohol and C1 to C4 Alcohols in gasoline TR 1 260A
147. th the stationary phase Increases retention and resolution but also peak diffusion Change column dimensions Longer column Smaller ID Increase film thickness Can provide discrimination based on time spent in stationary phase Change the phase More polar columns retain polar compounds better and vice versa providing analyte discrimination Preliminary method development TraceGOLD TG 5MS Increase speed Increase temperature ramp rate Reduces the distribution constant analytes spend less time in the stationary phase Increase carrier linear flow rate Decreases interaction with the stationary phase Shorter column Decrease film thickness Analyte spends less time in stationary phase Consider UltraFast GC Can reduce analysis times by a factor of 20 Method optimization GC Troubleshooting Before you start any troubleshooting it is essential to observe safe laboratory practices Know the chemical and physical properties of any solvents used and have the appropriate Material Safety Data Sheets MSDSs readily available All electrically powered instruments should Symptom Baseline Related Problems Baseline Drifting Accumulation of stationary phase Carrier gas cylinder pressure too low to allow control Drifting carrier gas or combustion gas flows Accumulation of impurities in the column Baseline Falling Carrier gas leak in the system Column is baking out Baseline Falling
148. that the Thermo Scientific TRACE column range has less than half the bleed of other popular columns Robustness Moisture and oxygen pose a danger to GC columns Oxygen contamination can come from many sources leading to shortened lifetimes increased bleed and increased cost TRACE GC columns have been manufactured with improved phase bonding to minimize the risk of damage due to contaminated carrier gas or difficult samples Reproducibility 28 a As well as focusing on individual column performance we work to improve column to column reproducibility arising from major improvements in the production processes A column bought today will have the same characteristics or better as one obtained a year or ten years from now Guaranteed Performance All TRACE columns have passed rigorous testing procedures to ensure the highest possible performance and are delivered with a serialized certificate to show their performance and assist with traceability All Thermo Scientific columns come with a 100 guarantee If for any reason the column does not perform up to our claims we will replace it with one that does Technical Support Our quality technical support will help you solve your problems quickly via phone our web resource center or the technical section of this catalog Please refer to the GC Column Selection Guide on page 204 for information to help you select the appropriate column for your separation If you are looking for a co
149. the tubing for essentially no particle release Applications gt Mid polarity Divinylbenzene 4 vinylpyridine solid phase e Non polar and polar compounds gt Particles incorporated to the walls of the tubing for essentially no particle release Similar to CP PoraPLOT S Supel G45 Rt S BOND TracePLOT TG BOND S GC Columns I D Length Film Thickness Cat No Quantity 0 32mm 15m 10um 26006 6000 1 Each 0 32mm 30m 10um 26006 6030 1 Each 0 53mm 15m 20um 26006 6060 1 Each 0 53mm 30m 20um 26006 6090 1 Each TracePLOT TG BOND U GC Columns Polar columns incorporating particles to the walls ofthe tubing for essentially no particle release Applications gt Polar Divinylbenzene ethylene glycol dimethylacrylate phase e Analysis of polar and nonpolar gt Particles incorporated to the walls of the tubing for essentially compounds no particle release Similar to HP PLOT U Rt U BOND CP PoraPLOT U CP PoraBOND U Supel N PLOT TracePLOT TG BOND U GC Columns I D Length Film Thickness Cat No Quantity 0 32mm 15m 10um 26007 6000 1 Each 0 32mm 30m 10um 26007 6030 1 Each 0 53mm 15m 20um 26007 6060 1 Each 0 53mm 30m 20um 26007 6090 1 Each TracePLOT Particle Traps for GC Instruments Provides a safeguard from dislodged particles entering the detector gt Provides a safeguard from dislodged particles entering the detector TracePLOT Particle Traps for GC Instruments Description I D Cat No Quantity PLOT Particle Trap 2 5m x
150. thyl arachidate 12 Methyl behenate 13 Methyl cis 13 docosenoate 14 Methyl tetracosanoate 1 3 60 e be a is ae 7 8 Tene mini FAMES C8 C24 Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 Methyl octanoate 2 Methyl decanoate 3 Methyl decanoate 4 Methyl myristate 5 Methyl palmitate 6 Methyl palmitoleate 7 Methyl stearate Alditol Acetate Mixture Column Part Number Initial Temp Program Rate Final Temp Carrier Gas Detector Injection Mode 1 Erythritol 2 2 Deoxy ribitol 3 Rhamnitol 4 Fucitol 5 Ribitol 6 Arabinitol 7 Xylitol Derivatized Sugars Acylated Column Part Number Temperature Detector Type Carrier Gas Flow Rate Injection Volume Injection Mode 1 Derivatized Fructose 2 Derivatized Glucose isomer GC Applications TG POLAR 30m x 0 25mm x 0 25um 26082 1420 100 C 0 5 minute hold to 195 C at 25 C minute 1 minute hold to 250 C at 10 C minute 3 minute hold MS He 1 2 mL min 0 1uL Split 100 1 250 C 8 Methyl oleate 9 Methyl linoleate 10 Methyl linolenate erm A oo 50 55 11 Methyl arachidate Tire miri 12 Methyl behenate 13 Methyl cis 13 docosenoate 14 Methyl tetracosanoate Relative Abundance TR FAME 30 m x 0 25 mm x 0 25 um 260M142P 190 C 1 min 3 C min 260 C 10 min He 50 kPa MS Electro
151. thylpolysiloxane e Organochlorine pesticides and Max Temps 300 C 320 C herbicides USP Listing G42 e Pharmaceuticals gt Mid polarity phase 35 diphenyl 65 dimethyl polysiloxane e PCB cogeners gt Equivalent to USP G42 phase e Aroclor mixes e Sterols e Rosin acids e Phthalate esters Similar to Rtx 35 BP 35 HP 35 SPB 35 SPB 608 TraceGOLD TG 35MS GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 15m 0 25um 26094 1300 1 Each 0 25mm 15m 0 5um 26094 2110 1 Each 0 25mm 15m Tum 26094 2840 1 Each 0 25mm 30m 0 25um 26094 1420 1 Each 0 25mm 30m 0 5um 26094 2230 1 Each 0 25mm 30m Tum 26094 2960 1 Each 0 32mm 15m 0 25um 26094 1310 1 Each 0 32mm 15m 0 5um 26094 2120 1 Each 0 32mm 15m Tum 26094 2850 1 Each 0 32mm 30m 0 25um 26094 1430 1 Each 0 32mm 30m 0 5um 26094 2240 1 Each 0 32mm 30m Tum 26094 2970 1 Each 0 53mm 15m 0 5um 26094 2130 1 Each 0 53mm 15m Tum 26094 2860 1 Each 0 53mm 15m 1 5um 26094 3340 1 Each 0 53mm 15m 3um 26094 3840 1 Each 0 53mm 30m 0 5um 26094 2250 1 Each 0 53mm 30m Tum 26094 2980 1 Each 0 53mm 30m 1 5um 26094 3360 1 Each 0 53mm 30m 3um 26094 3960 1 Each TraceGOLD TG 35MS AMINE GC Columns Chemically altered tubing surface reduces tailing and eliminates the need for column priming a NON POLAR Applications Phase Modified 35 Phenyl Methylpolysiloxane for Basic Compounds e Amines including alkylamines Max Temps 200 C 220 C diamines triamines and ethanol Vor isting N A am
152. um 26082 5060 1 Each 0 53mm 30m 0 1um 26082 0490 1 Each 0 53mm 30m 0 2um 26082 5070 1 Each 0 53mm 60m 0 1um 26082 0610 1 Each 0 53mm 60m 0 2um 26082 5080 1 Each www thermoscientific com chromatography 237 GC Columns TG BOND Alumina 239 TG BOND Msieve 5A 240 TG BOND Q 241 TG BOND O 242 TG BOND S 242 TG BOND U 242 TracePLOT Accessories 242 TracePLOT GC Columns Thermo Scientific TracePLOT GC Columns offer the latest innovation in PLOT column technology providing reproducible analyses of permanent gases hydrocarbons and solvents TracePLOT TG BOND Alumina GC Columns Na SO and KCl Deactivation Optimized for linear and quantitative analysis of polar unsaturated hydrocarbons Applications gt Strong bonding to prevent particle generation suits these columns to valve e C1 C5 hydrocarbons switching operations without damage to injection and detection systems from particle release e Unsaturated hydrocarbon isomers i gt Columns to which water has adsorbed may be regenerated to restore full efficiency and selectivity gt Each column has been tested to ensure proper film thickness 1 3 butadiene selectivity propadiene and methyl acetylene resolution trans 2 butene and 1 butene and coating efficiency 1 3 butadiene Similar to Alumina PLOT AT Alumina CP Al203 KCI CP AI203 Na2S04 GS Alumina GS Alumina KCl HP PLOT M HP PLOT S Rt Alumina BOND KCI Rt Alumina BOND Na2S04 Tra
153. um 260R225P 1 Each TRACE TR 225 GC Columns Reliable and reproducible performance Applications NON POLAR i E gol MEM Esters FAMES Phase 5096 Cyanopropylpheny Polysiloxane e Carbohydrates Max Temps 230 C 260 C USP Listing G7 e Neutrol Sterols gt Mid polarity phase 50 Cyanopropylphenyl polysiloxane gt Low bleed even at elevated temperatures gt Outstanding robustness for difficult separations gt Manufactured to minimize risk of damage from contaminated carrier gas Similar to DB 225 HP 225 RTX 225 BP225 TRACE TR 225 GC Columns I D Length Film Thickness Cat No Quantity 0 25mm 60m 0 25um 260Y154P 1 Each 0 25mm 15m 0 25um 260Y130P 1 Each 0 25mm 30m 0 25um 260Y142P 1 Each 0 32mm 25m 0 25um 260Y137P 1 Each 253 www thermoscientific com chromatography TRACE TR WAX GC Columns General purpose high polarity columns Applications NON POLAR e Esters Phase Polyethylene Glycol PEG Max Temps 260 C 280 C for films 1 0um Alcohols 240 C 260 C for 1 0um films e Glycols gt Polar phase Polyethylene glycol e Aromatic isomers gt Highly crosslinked and fully deactivated gt Solvent washable Similar to DB Wax BP20 Rtx Wax Stabilwax HP20M HP Wax HP INNOWax Supelcowax 10 AT Wax Nukol CP Wax52CB SUPEROX II Carbowax PE WAX ZBWAX TRACE TR WAX GC Columns I D engt Film Thickness Cat No Quantity 0 10mm 10m 0 1um 260W020P 1 Each
154. vable Gas Tight 75mm 31 Cone Manual OC 36500520 1 Each 50uL Removable Gas Tight 50mm 25 Bevel X 365G2161 1 Each 50uL Removable 50mm 23 Cone X LV Splitless 36503015 1 Each 100uL Removable 50mm 25 Bevel X 365H2301 1 Each 100uL Removable Gas Tight 50mm 23 Side hole X X see Note 36520050 1 Each 100uL Removable Gas Tight 50mm 25 Bevel X 365H2381 1 Each 100uL Removable Gas Tight 50mm 23 Cone X X X LV Splitless 36500495 1 Each 250uL Fixed Gas Tight 50mm 25 Bevel X 36512561 1 Each 250uL Removable Gas Tight 50mm 25 Bevel X 36512611 1 Each 250uL Removable Gas Tight 80mm 26 Cone X X LVOC 36500490 1 Each 250uL Removable Gas Tight 50mm 23 side hole X X X see Note 36520051 1 Each 1 0mL Removable Gas Tight 50mm 23 Bevel X 365K3041 1 Each Syringe 36520051 is to be used when performing PTV LVI injections with a dedicated liner for thermo labile compounds liner 45352060 Compatible with Merlin Microseal device installed on BEST PTV and with AS2000 and TriPlus autosamplers for liquids www thermoscientific com chromatography 307 Autosampler Syringes for Agilent Instruments Autosampler Syringes for Agilent Technologies Volume 0 5uL 0 5uL 0 5uL Sul Sul Sul Sul Sul Sul 10uL 10uL 10uL 10uL 10uL 10uL 10uL 10uL Needle Type Removable Removable Removable Fixed Fixed Fixed Fixed Fixed Fixed Fixed Fixed Fixed Fixed Fixed Removable Fixed Fixed Length 42mm 42mm 42mm 42mm 42mm 42mm 42mm 42mm 42mm
155. ycles All varieties of ferrules are supplied in contaminant free individual blister packs allowing removal of an individual item without risk of contamination to the other supplied items Ordering Information Thermo Scientific Instruments Description 100 Graphite Ferrules not GC MS interface 15 Graphite 85 Vespel Ferrules TRACE Cold On Column Injectors Injectors and Detectors Brass Nut GC MS Interface SilTite Kit GC MS Interface Replacement SilTite Ferrules Must be used in conjunction with brass nut PN 290BT239 Kit contains 2 SilTite nuts and 10 ferrules TRACE and FOCUS Injectors and Detectors Ferrule Size Column ID 0 1 0 25 mm 0 32 mm 0 53 mm 0 1 0 25 mm 0 32 mm 0 53 mm Packed Column 1 8 OD Packed Column 1 4 OD 0 1 0 25 mm 0 32 mm 0 53 mm 0 1 0 25 mm 0 32 mm 0 1 0 25 mm 0 32 mm 0 53 mm 0 1 0 25 mm 0 32 mm 0 53 mm Replacement SilTite Nuts t Equivalent to PN 29013488 29013487 amp 29013486 previously sold in quantities of two www thermoscientific com chromatography Temp Limit C Re usable 450 Yes 350 No 500 No SilTite Metal Ferrules oil ite metal ferrules and nuts are made from the same material and have the same thermal expansion coefficient The SilTite ferrule forms a strong permanent airtight seal around the capillary column eliminating leaks The base of the ferrule is flat and forms a perfect seal with the MS
156. yringes for Manual On Column and Septum Injection Replacement Needles Blunt Volume Length Gauge Needle Point Cat No Quantity Sul 2 51mm 265 90 blunt end NS832302 3 Pack 10uL 2 51mm 26s 90 blunt end NS832402 3 Pack 25 100uL 2 51mm 22s 90 blunt end NS832502 3 Pack 250 500uL 51mm 22s 90 blunt end NS832602 3 Pack Syringes for Accurate Dosing of Liquids Fixed Needle Side Hole Gas Tight gt Suitable for liquid or gas samples gt 26s and 22s Gauge needles gt PTFE tipped stainless steel plunger eliminates frozen plungers National Scientific Syringes for Accurate Dosing of Liquids Fixed Needle Side Hole Gas Tight Volume Length Gauge Needle Point Cat No Quantity Sul 51mm 26s Bevel NS600301 1 Each Sul 51mm 26s Blunt End NS600302 1 Each 10uL 51mm 26s Bevel NS600401 1 Each 10uL 51mm 26s Blunt End NS600402 1 Each 25uL 51mm 22s Bevel NS600501 1 Each 2byL 51mm 22s Blunt End NS600502 1 Each BOuL 51mm 26s Bevel NS100601 1 Each BOuL 51mm 225 Blunt End NS600602 1 Each 100uL 51mm 22s Bevel NS600701 1 Each 100uL 51mm 22s Blunt End NS600702 1 Each 250uL 51mm 26s Bevel NS100801 1 Each 250uL 51mm 22 Side Hole NS600804 1 Each 500uL 51mm 22s Bevel NS600901 1 Each 500uL 51mm 22s Blunt End NS600902 1 Each 500uL 51mm 22s side Hole NS600904 1 Each 1mL 51mm 22s Bevel NS600000 1 Each 1mL 51mm 22s Blunt End NS600001 1 Each 1mL 51mm 22s side Hole NS600002 1 Each 5mL 51mm 22s Bevel NS600040 1 Each 5mL 51mm 22s Blunt End NS600041 1 Each

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