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1. Some of the keys must be operated in pairs to enter certain functions In such cases the keys should be activated in the following sequence VOLUME FUP soises aneo A N EEEE AENEA KENES Increase volume VOLUME FDOWN sticsmrpsccundasncaicndsysWarcanditorndarracdddsveaicnsaniincian Decrease volume STAR To E O EE Start dispense operation VOLUME FST AR NT ccasecnctcrensaciceiccclateuaiintotticecnddesteceeestdedecdsiele Continuous dispense Oe E ESE E cepa deed E E Stop dispense panic button SPEEDFUP erretiroen Increase dispense speed to max 255 SPEEDTDOWN vsgeccadecntecnzacidcen Decrease dispense speed from 255 to 180 INTER FS OM wes cacrseespactsocstanoncersaenacceaneatereten Set interval time in seconds INE 2 a parssees SoconceeSacetecs eenncedecacmnersssenedes set number of dispenses ST OPFIN GEIR ALS wcesssecrosedtnereceazet Stop amp cancel interval dispense mode PE DART perene E E a Set default 200 Ir sieer ienn iea E EOE EE Increase the calibrated volume GALIDOW N cisec ses datenestactace tamensessiescosteen Decrease the calibrated volume CAL FRAN GE sere onise seine ceisieedsantatenendsdeyiscebereeeecsdesiaecbaks Moves the decimal point Page 5
2. mean value into the unit by pressing CAL UP to increase the displayed volume or CAL DOWN to decrease D The unit is now ready for use and you can now set the volume you would like to dispense Calibration using other than the default calibration value Press CAL START to display the default calibration value of 1 000ml 2 Press CAL RANGE to move the decimal place so that the unit displays the volume in the range in you prefer for example if your work involves dispensing ml s rather than p s move the decimal point to display 10 00 3 Press and hold VOLUME UP or VOLUME DOWN until the desired volume for calibration is displayed 4 Carry out five dispenses and establish the gravimetric volume dispensed in each operation 5 Calculate the mean delivery volume 6 Enter the calculated mean value into the Unoverse unit by pressing CAL UP to increase the displayed volume or CAL DOWN to decrease the displayed volume T The unit is now ready for use Page 6 3 The choice of tubing The unit can work either with fixed length tubing 75mm long within the tube clamp or with continuous tubing which in effect does not have any length restriction In both cases the correct tube clamps have to be installed in the clamp There is one size of clamp for the fixed clamp tubing which is supplied as part of the tube For the continuous tubing there are three sizes of clamps 1 Ma
3. transfer metering and dispensing In contrary to centrifugal and gear pumps peristaltic pumps handle fluids of various viscosities are self priming and can operate in either flow direction With no valves seals or packing to come in direct contact with the pumped fluid they are ideal for pumping high purity amp corrosive fluids and for contamination free dosing The principle of the peristaltic pump is based on a tube which is squeezed by a series of rollers As a general rule the higher the number of rollers and the smaller the tube diameter the lower are the flow rates but better is the accuracy and precision The 9100 controller is equipped as a standard with 3 roller system and 2 0mm ID tube This tube diameter together with maximum speed delivers a flow rate of 50ml min This combination offers an ideal tool for applications which require volumes between 500ul and 50ml For smaller dispense volumes use the 1 0mm ID tube The pump is also designed to work in continuous mode The highest dispense accuracy is achieved by using a semi rigid tube on the outlet of the pump We recommend thin wall tubing such as FEP tubing ID1 5mm X OD2 1mm or PVC tube Page 1 1 The peristaltic tube 5 Adjusting the dispense volume Press keys VOLUME UP or VOLUME DOWN to enter the volume nearest to your desired The peristaltic tube is made from volume Santoprene and the connectors are Nylon PA Please make sure the reagents you in
4. 12VDC 0 5A Environmental operating teMp cccceecceeeeeseeeeeeeeeeeeeeaees 10 C to 40 C Environmental storage temp cccccseccsseceeeeeseeeeeseeeseeeees 4 C to 40 C SCILOGEX SCILOGEX LLC 500 Four Rod Road Ste 122 Berlin CT 06037 USA Tel 860 828 5289 FAX 860 828 5389 The CE sign certifies that the instrument Email info scilogex com meets the requirement of the EEC www scilogex com in to the specified test methods directives and has been tested according UNOVERSE 9100 Electronically controlled dispensing pump User Manual ISS1 11 Chemical compatibility chart 13 FAQ 1 Q Why does the pump stalls or runs slower than expected when new _ a S o nA A A new Santoprene tube is stiff when new so has to be shaped for some time Aceti id Chroni id M It Sil It i pr aa r f before it gains it s elasticity Run the pump in continuous mode for a total of approx 5 minutes with the clamp lever half open to start with gradually moving he clamp lever to fuly cose positon e life of a peristaltic tube d A The life of a peristaltic tube depends on many variants such as speed the reagent it is pumping and temperature In general you should expect approximately 800 hours operation from one tube Fluoboric acid Nickel salts Sulfur dioxide Ammonium hydrox Fluosilicic acid Nitric acid 10 Sulfuric acid dil ide 3 Q Why does the displayed value sometime jump in dou
5. Box contains The following Unoverse 9100 pump conitroller cccccseeecseeeeeeeeeees Cat No 9100 000 PSU output 12V 0 3A with universal plug adapters Cat No 6025 This instruction MANUAL sin dainsscvousensudvandondeuaredmecusitiuadewansaauds Cat No 9100 6001 ID 2 0 Santoprene tube cece cceececeeeeeseeeeeeeeeeeeeeeees Cat No 9000 502 Accessories amp spares Silicone Tubing ID 1 0mm complete with connectors 006 Cat No 9000 504 Silicone Tubing ID 2 0mm complete with connectors 006 Cat No 9000 505 Santoprene Tubing D 1 0mm complete with connectors Cat No 9000 501 Santoprene Tubing ID 2 0mm complete with connectors Cat No 9000 502 Santoprene tubing ID 2 00mm1meter running length Cat No 9000 506 Silicone tubing ID 1 00mm1meter running length ccceee Cat No 9000 507 Silicone tubing ID 2 00mm1meter running length cccee Cat No 9000 509 Silicone tubing ID 3 00mm1meter running length ccee Cat No 9000 508 Unoverse 9100 wall mounting bracket Stand cccsseeeeeeeeeeeees Cat No 9100 001 FOGL O NI eea ai meer keen lee ee ener sw Sere eee nae meen eee eet Cat No 6013 Product Specification Mains Voltage cccsscccseecceeeceseeseeeeeeeeeees 100V 240V 0 3A MAX 47 63Hz Power Supply Unit output a tcicssiecanestincnacsetiousneysieicineesttorenitietenmmeyste
6. OWN keys enter the number of seconds or 10Xsec you wish to have between the dispenses from 1 second to 99 seconds 4 Press INTERVALS and the second set of digits will flash This digits denote the number of dispenses you wish to have from 1 to 98 dispenses 5 Using the UP amp DOWN keys enter the number of dispense events between 1 and 98 6 Press INTERVALS and the display will show the volume The colon between the two sets of digits flashes to indicate that an interval dispense mode has been entered into the unit You can now adjust the volume as indicated in the previous paragraph T Press START and the controller will dispense the set volume in the interval mode which you have entered into the unit 8 Press STOP INTERVALS button to stop the intervals mode The flashing colon will disappear from the display 9 To change any of the interval parameters simply press the INTERVALS key again and enter new parameters 10 Panic stop You can press the STOP button at any point throughout the dispense mode to terminate the automated dispense operation when you have finished Whenever the pump is not in use for long periods of time it is important to release the pressure off the tube This will reduce the possibility of the tube s permanent deformation and ensure that accuracy precision is maximised Release the pressure by lifting the pressure lever 1 C Repla
7. ble figures A This happens when dispensing small volumes with the ID2 0mm tubing Following the calibration procedure the instrument s mathematical calculation divides the volume to be dispensed by the number of pulses received from the motor s encoder and stores this value If the volume per rotor rotation is relatively large the ratio of pulses to volume is coarse In these circumstances the required volume input does not divide into stored values and therefore the calculator will Sete aie eden a eee fee weber nic aad ID1 0mm tube the dispensed volume per rotor rotation is small enough Calcium salts lodine and solutions Phthalic acid Zinc salts i P pe a to allow single ul per displayed digit ee a E Little or no effect on Satoprene 4 Q Can leave the unit switched ON throughout the day A Yes you can The dispenser requires very little energy when the pump is not running so continuous power into the unit will not harm it ee e e e e Q Why can t I set slower dispense speed A The motor s speed is controlled via the voltage supply to the motor Too low voltage and the pump s motor will stall in particular when the tubing is new and the resulting load on the motor is higher 6 Q Can I dispense hot reagents using the dispenser A Yes the dispenser to works safely with media temperatures of up to 100 C Be aware that the internal electronics could be damaged by any ingress of fluids or steam va
8. cing the tube 3 seconds intervals 8 events For work in small volumes use the ID 1 0mm tube which is available as an accessory Lift the lever and remove the pump s cover Pull out both tube holders d f th Repl 11 Note that in the dispense process the display shows the A E cc a seconds left before next dispense and the running event with a new tube GOCE 12 Continuous dispense To dispense your chosen volume continuously at the interval time you selected enter 99 as the number of repeats This will prompt the unit to dispense continuously until the STOP button is pressed Remember to Page 7 check the tubing condition from time to time Page 2 4 Gravimetric pump calibration procedure Pump flow performance is subject of many factors among them the condition of the peristaltic tube and the viscosity of the reagent It is therefore important that you calibrate the pump before it is commissioned and at periodic intervals IMPORTANT CHOOSE THE CALIBRATION VOLUME THAT MATCHES THE RANGE YOU ARE MOST LIKELY TO USE IN YOUR APPLICATION The default calibration volume is 1 000 You can however choose any other calibration volume which is most suitable for your application 1 Press CAL START to display the default calibration value of 1 000 Zi Carry out five dispenses into a vessel and establish the gravimetric volume dispensed in each operation 3 Calculate the mean delivery volume 4 Enter the calculated
9. p to open position in order to relieve the pressure whenever the pump is not being used for long periods or overnight 11 Exclusion If the equipment is used in a manner not specified by the manufacturer the protection provided by the equipment might be impaired This unit is NOT suitable for use in explosion hazard environments Page 8 1 A Unpacking Remove the packing materials unpack the pump controller and the power supply unit Make sure that you have all the following components Unoverse 9100 pump controller ccccccseccsseessseeeeeees Cat No 9100 000 Power ot 86 2 Ak U1 0 eee eee eee ae eer eee Cat No 9100 004 ID 2 0 Silicone tube as scncicndiccccesaedoneadsoneciesuedateesdedemncomeactucnens Cat No 9000 509 Please contact your supplier immediately if you notice any one of the components is missing or damaged Note Do not attempt to assemble a unit using damaged components Retain the packaging so it can be used for future shipping The plug in power supply unit is Switch Mode and automatically adjusts itself to the mains power supply characteristics It will work with any mains voltage supply from 100V to 240V The power supply unit is shipped with three alternative plug adaptors to fit European American and UK power outlets Select the correct adaptor for your needs and clip it into the power supply 2 General information on peristaltic pumps Peristaltic tube pumps are ideal for fluid
10. pours Moderate effect Carbon tetrachloride Ethyl chloride Trichloroethylene Perchloroethylene Severe Chlorobenzene Freon Lacquer Toluene Chloroform Gasoline unleaded Naphtha Page 9 7 Changing the pumps direction The pump controller can be used for dispensing or aspirating reagents The slide switch on the left side of the unit sets the direction that the pump rotor rotates 8 Pump speed adjustment To adjust the dispense speed press SPEED UP to increase or SPEED DOWN to decrease You can adjust the speed from a maximum of 255 to a minimum of 180 9 Continuous dispense mode To run the pump continuously press VOLUME START You can stop the pump at any point by pressing the STOP button The pump displays Cont to indicate continuous running Please note running the dispense tubes dry over a long period will shorten their life 10 Care amp maintenance The control unit is maintenance free The peristaltic tubes however require replacement as soon as excessive wear or a large variation in dispense volumes are noticed The operational life of the tubes is a function of the speed load and materials being dispensed Avoid running the tubes dry for longer than a few minutes Check the peristaltic tubes weekly for signs of excessive wear and replace if required Pump tubes which remain clamped in the pump will deform with time Therefore rotate the tube clip at the top of the pum
11. rked 1 for ID1 0mm tube 2 Marked 2 for ID 2 0mm tube a Marked 3 for ID 3 0mm tube The easiest roller position for tube replacement is when one roller is at the top of the pump You can turn the roller wheel with your fingers until you reach this positioning When using continuous tubing make sure that the tube is fitted so that it is in contact with the inner surface of the tube clamp Page 3 4 Preparing the pump for use Plug the supplied PSU into your power socket and the low voltage plug into the socket on the left side of the unit switch it on by pressing the ON button The green LED will illuminate indicating that the unit is operational The display will temporarily read 9100 and then default to the value 1 000 This value is the factory setting Note the direction of flow The pump is reversible using the slide switch so you can return any unused reagent back into the reservoir Pump direction slide switch Front Lower tube IN Upper tube OUT Back Lower tube OUT Upper tube IN Remote pulse such as foot switch Accessory or pulse from a robotic processor Power ON indicator On Off switch Accepts 2 5mm mono plug Power socket for 12V DC 0 3A Page 4 3 The Control Panel The keys on the control panel are assigned with functions to calibrate the pump set the volume to be dispensed set speed and interval of dispense
12. tend to use are compatible with these materials See Chart Make sure the tubes terminate in a receiving vessel and press START to begin dispensing For priming or to dispense more than the set volume hold down the START key 6 Interval Dispense You can set the unit to dispense the desired volume for a number of times in predefined intervals This feature is useful in repeatable operations either in manual mode or when the dispense head is held by a robotic arm 1 A Clamping the peristaltic tube The pump controller is delivered with a ID 2mm Santoprene tube In order to reduce deformation caused by clamping the pressure lever is supplied in the open position To set repeat dispensing 1 Interval time setting Select between intervals of 1 99 sec or 10 to 990 seconds Press and hold down the INTERVAL key and press DOWN key to select 1 to 99 seconds or UP key for 10 to 990 seconds If you are not sure in which mode the Before use ensure you turn the lever The pressure lever moves the pump cover towards the down to the fully clamped position rollers and thus clamps the tube between the cover and instrument is enter the desired mode prior to any further the rollers programming 1 B Releasing the peristaltic tube 2 Press INTERVALS the display flashes the first two digits to the left These digits denote the time in seconds between the dispense operations 3 Using the UP amp D
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