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Infinityplus Installation Planning

1. pressure exceeds 90 PSI L Three way diverting Compressed i ae ball valve 1 2 in NPT 1 2 in NPT ME es ae VE female male amp 300 SCFH alle ST or greater Output must be 90 PSI 1 2 in or greater N Shut off z NQ copper feed valves i 1 TEN Tifa if o i 80 PSI WO Yi vo gt FAL JE Anti vibration option Compressed Let an Nr nitrogen ot ES To air management box 93 99 9 300 SCFH or greater Customer Supplied Varian Supplied Figure 5 Setup for Switching Gas Supplies 32 Infinityplus Installation Planning 01 999176 00 B1001 3 6 Compressed Nitrogen Gas 3 6 Compressed Nitrogen Gas During low temperature operation below room temperature of the variable temperature accessory a compressed nitrogen gas supply from a cylinder or a fixed line is required that is dry oil free and magnetically clean e g free of rust with a dew point of 193 C 80 K The flow pressure and filtration rates through the regulators are the same as those listed for the compressed air supply Itis acceptable to operate below room temperatur
2. 1 4 in 1ft 01 999176 00 B1001 Infinityplus Installation Planning 57 Chapter 6 Room Layouts 58 Infinityplus Installation Planning 01 999176 00 B1001 A accessibility of site 15 accessory cabinet 16 20 acetone 42 A frame for chain hoist 42 air conditioning requirements 27 33 air filtration 33 ambient temperature requirements 26 for temperature stability 26 intake filter 33 separate power line 33 to reduce humidity levels 26 air dryer assembly 31 air freight delivery 16 air reservoir 31 air supply main 31 air termination fitting 32 ball valve 31 high humidity areas 31 prefilter 31 air ventilation 26 ambient humidity 26 ambient temperature 27 antistatic spray 34 antivibration systems 23 automatic teller machine ATM cards caution 9 B back up device 35 ball valve 31 building inspector 29 C cardiac pacemaker wearers 43 cardiac pacemakers 43 cautions defined 7 CD ROM drive 35 ceiling height 21 centerline to floor distance 25 CFM rated fans for ventilation 26 chain hoist 42 codes 29 color CRTs 24 compressed air supply 31 compressed nitrogen gas flow and pressure rates 33 supply requirements 33 variable temperature accessory 33 computer preparation 34 CP MAS Module electrical outlets 31 crate unpacki
3. compressed nitrogen val a x a x 7 di gt SES lt 53 Q 5 300 89 Console power Workstation power N N pr 5 gauss Ser 125 line Internet amp phone lines 1 4 in 1ft Infinityplus Installation Planning 55 01 999176 00 B1001 Chapter 6 Room Layouts Illustrations for Room Layout ser i T cl 5 gauss Pal line You can use the illustrations on this 7 page as to scale component representations Cut the components i out and use Blank Grid for Room Layout on page 57 to build your room 300 89 layout AA N N Pa e wn 72 cb a lt Infinityplus Accessory console cabinet o px 1 4 in 1ft 56 Infinityplus Installation Planning 01 999176 00 B1001 Blank Grid for Room Layout
4. 3 8 Telephone and Internet Access page 33 3 9 Electrostatic Discharges page 34 3 10 Sun Workstation Preparation page 34 Verify the configuration with a Varian Inc representative before designing the room layout Site preparation must conform with federal state and local codes which take precedence over recommendations in this guide Approval by a building inspector might be necessary 3 1 Line Voltage Variation Infinityplus spectrometers require one line at 220 Vac 10 7 single phase for the console one for the accessory rack and one for each power amplifier The computer workstation requires either 120 Vac or 220 Vac Current ratings are listed in Table 14 Measure and record the ac line voltage for 48 hours using a suitable power line analyzer such as the BMI Model 4800 or equivalent Provide a copy for the Varian installation engineer Requirements are the following Long term voltage variations slow average do not exceed 7 of nominal line tap voltages Short term voltage variations sag or surge with a duration between several milliseconds and several seconds do not exceed 10 of nominal line tap voltage Line transients impulse with a duration between 1 us and 800 us do not exceed 50 V peak above or below nominal line tap voltage These transients must be measured at the power plug with a load connected that draws the same power as the spectrometer AC line frequency does no
5. 60 Infinityplus Installation Planning storage media 34 stray field data 44 magnetic field plots 44 magnetic field profiles 24 magnetic field warning signs 51 magnetic interference 20 23 Magnetic Leg 20 magnetic media caution 9 man command 36 memory amount 35 metal objects warning 7 Miscellaneous Crate 16 modifying the instrument 8 monitor degaussing coil 42 moving crates 13 17 moving equipment 16 moving van delivery 16 N name service 38 NFS server 37 NIS or NIS server 38 nitrogen contact with body 8 nitrogen gas requirements 33 nitrogen gas supply low temperature operation requirements 41 magnetic nitrogen gas container 41 precooling requirements 41 purity requirements 41 VT accessory 41 nitrogen refill volumes 27 nitrogen supplies 39 NMR work table 20 NMR work table weight 16 O Object Code License Form 13 online documentation 36 opening crates 16 17 operating frequencies 26 operating frequency 25 Order Acknowledgment form 13 17 P pacemaker warning 7 pacemakers 43 peripherals printer requirements 36 X server software requirements 36 postdelivery instructions 16 posting requirements 51 power conditioning system 30 power line analyzer 29 power outages frequent and short 30 power stick 21 power supplies uninterrupted 30 pregnancy hazard 44 pressure gauge 32 printer requirements 36 prosthetic parts warning 7 01 999176 00 B1001
6. cm in kg Ib Accessory cabinet 74 29 1 55 21 7 78 30 6 68 150 Magnetic Leg 65 5 26 41 16 1 45 7 18 66 30 NMR work table 71 28 178 70 152 60 48 107 53 contains floor plans for the NMR laboratory area or room The plans are suggestions and not specifications The standard arrangement places the power bay s to the right of the console as viewed from the front However cable lengths are long enough to allow the power bay s to be placed to the left of the console if that orientation works better for a particular site All cabinets have casters for easy movement allowing the system to be placed in a location as small as that illustrated in Chapter 6 Room Layouts on page 53 as long as sufficient space exists for the cabinets to be moved to provide for access to all sides The minimum dimensions do not include compensation for external magnetic and rf interference that may be present When setting up a spectrometer you should try to keep the 5 gauss line inside the lab The console power bay and workstation must be outside the 5 gauss line see section 2 7 Magnetic Environment page 23 If this criteria can not be met please consult with your Varian representative Each individual site must be analyzed to ensure optimum system performance 2 2 Accessibility of Site The site must provide adequate access for the routine delivery of supply dewars containing liquid helium and nitrogen The site must a
7. field values 0 5 1 0 1 5 2 0 2 5 3 0 Radial distance from magnet CL m Figure 11 Stray Field Plots for 600 89 Magnets 3 5 4 0 01 999176 00 B1001 Infinityplus Installation Planning 49 Axial distance from magnet CL m Chapter 5 Stray Magnetic Fields 50 0 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 Radial distance from magnet CL m Figure 12 Stray Field Plots for 800 63 2 2K Magnets 5 0 800 63 2 2 magnet field values 5 5 6 0 Infinityplus Installation Planning 01 999176 00 B1001 5 3 Posting Requirements for Magnetic Field Warning Signs 5 3 Posting Requirements for Magnetic Field Warning Signs The strong magnetic fields that surround a superconducting magnet are capable of causing death or serious injury to individuals with implanted or attached medical devices such as pacemakers or prosthetic parts Such fields can also suddenly pull nearby magnetic tools equipment and dewars into the magnet body with considerable force which could cause personal injury or serious damage Moreover strong magnetic fields can erase magnetic media such as tapes and floppy disks disable the information stored on the magnetic strip of automated teller machine ATM and credit cards and damage some watches To warn of the presence and hazard of strong magnetic fields the customer is responsible for posting clearly visible signs warning of magnetic field hazards This responsibility includes measuring stray fields with a gaussm
8. magnet Generally keep the PC beyond the 5 gauss perimeter of the magnet Refer to the Installation Planning Guide for magnet field plots Never operate solids high power amplifiers with liquids probes Never operate the solids high power amplifiers with a liquids probe The high power available from these amplifiers can easily destroy liquids probes Use the appropriate high power probe with the high power amplifier Take electrostatic discharge ESD precautions to avoid damage to sensitive electronic components Wear a grounded antistatic wristband or equivalent before touching any parts inside the doors and covers of the spectrometer system Also take ESD precautions when working near the exposed cable connectors on the back of the console B1001 Infinityplus Installation Planning 9 SAFETY PRECAUTIONS Radio Frequency Emission Regulations 10 The covers on the instrument form a barrier to radio frequency rf energy Removing any of the covers or modifying the instrument may lead to increased susceptibility to rf interference within the instrument and may increase the rf energy transmitted by the instrument in violation of regulations covering rf emissions It is the operator s responsibility to maintain the instrument in a condition that does not violate rf emission requirements Infinityplus Installation Planning 01 999176 00 B1001 Introduction This guide assists in selecting and preparing a site to install a Varian In
9. 5 Ib ft Presence or movement of ferromagnetic objects over 45 kg 100 Ib such as pushcarts hand trucks gas cylinders 2 to 5 gauss Presence or movement of ferromagnetic objects over 450 kg 1000 Ib such as small delivery trucks automobiles pallet movers forklifts and elevators 1 to 2 gauss Presence or movement of ferromagnetic objects over 34 000 kg 75 000 Ib such as trains large trucks Magnetic Field Objects Affected by the Magnetic Field 15 gauss line or closer 5 to 15 gauss 2 to 5 gauss 1 to 2 gauss Cardiac pacemakers ferromagnetic implants and unrestrained ferromagnetic objects such as tools keys electronic equipment analog watches magnetic data storage media and credit cards Cardiac pacemakers and electronic equipment such as shielded CRTs computers shielded image intensifiers and shielded photomultiplier tubes Very sensitive electronic equipment such as unshielded image intensifiers and photomultiplier tubes Extremely sensitive electronic equipment such as linear accelerators electron microscopes and CRTs 24 The CRT in color monitors needs to be degaussed in magnetic fields above to 2 gauss Above 5 gauss color monitors may need additional shielding to prevent display distortion Sun workstations and peripherals are also affected by the magnetic field refer to Section 3 10 Sun Workstation Preparation on page 34 for a discussion of magnetic field considerati
10. 55 41 46 6 36 2 500 89 AS a a a 74 44 b 39 1 46 0 400 89 AS a a a 63 37 b 36 3 36 2 300 89 40 a a 59 b b 35 7 36 2 200 89 a a a 56 b b 35 1 36 2 a Where no radial position is given the point is within the cryostat body b The axial point is in the cryostat bore Compare with the magnet centerline CL distance 5 2 Stray Field Plots 44 This appendix shows typical stray field data and plots for each magnet The values are typical but may vary between individual magnets Gauss levels should be checked after a particular magnet has been installed The values in Table 23 were provided by Oxford technical documentation Table 24 lists the distance from the magnet centerline to the floor for high field magnets Infinityplus Installation Planning 01 999176 00 B1001 5 2 Stray Field Plots Table 23 Stray Field Data for NMR Magnet Systems Axial Distance from Magnet Radial Distance from Magnet Magnet Systems Center Line Center Line MHz mm Tesla gauss m gauss m 1 5 10 25 1 5 10 25 200 89 4 69 4 6 2 65 2 05 1 49 3 50 2 00 1 60 1 15 300 89 7 04 4 7 2 75 2 20 1 63 3 75 2 20 1 75 1 26 400 89 AS 9 39 2 9 1 8 1 5 1 17 2 30 1 3 0 80 0 74 400 89 9 39 6 5 3 80 3 00 2 21 5 15 3 05 2 40 1 74 500 89 AS 11 74 4 0 25 1 90 1 45 3 10 1 75 1 40 0 96 600 89 14 09 8 55 5 00 3 97 2 92 6 75 3 95 3 14 2 32 800 63 2 2K 18 81 13 00 7 60 6 0 4 41 10 25 6 0 4 75 3 51 Table 24 Magnet Centerline to Floor Magnet
11. 921351 Japan Tokyo 3 5232 1211 Korea Seoul 2 3452 2452 Mexico Mexico City 5 523 9465 Netherlands Houten 30 635 0909 Norway Oslo 9 86 74 70 Russian Federation Moscow 95 241 7014 Spain Madrid 91 472 7612 Sweden Solna 8 445 1601 Switzerland Zug 41 749 88 44 Taiwan Taipei 2 2698 9555 United Kingdom Walton on Thames England 1932 898 000 United States Palo Alto California Varian Inc NMR Systems Customer Sales Support 650 424 5145 Service Support Palo Alto California 1 800 356 4437 E mail customer support nmr varian com North American Service Manager 6440 Dobbin Rd Ste D Columbia MD 21045 410 964 3065 Venezuela Valencia 41 257608 We at Varian will make every effort to ensure that the ownership of your new NMR spectrometer is a lasting productive and pleasurable experience 12 Infinityplus Installation Planning 01 999176 00 B1001 Chapter 1 Site Selection and System Delivery Sections in this chapter 1 1 Installation Planning Process this page 1 2 Site Selection page 14 1 3 Transport Route and System Shipping Dimensions page 15 1 4 System Shipment page 16 Varian s delivery responsibility ends at the Varian factory shipping dock or at the customer s receiving dock depending upon the type of insurance obtained by the customer In either case for 200 through 600 MHz magnets the customer must provide a moving
12. Acknowledgment form determines owner responsibility FOB PALO ALTO or FORT COLLINS Transfer of ownership occurs when the shipment leaves the factory The customer is responsible for claims for shipping damage Upon request Varian will provide assistance in filing claims FOB DESTINATION Transfer of ownership occurs at customers point of receipt Varian is responsible for claims for shipping damage Damage discovered fifteen or more days after delivery generally cannot be recovered Such damage will be at the expense of the customer 2 As soon as possible move the shipment to a clean dry location preferably the installation site Move the crates in an upright position Do not drop or mishandle The crates are packed with G force and tip and tell indicators that record mishandling If one or more crates cannot be moved into the installation site because of doorway clearance leave the affected crate in a clean safe dry location Again do not open any crate except with direct instructions from an authorized Varian representative In particular the crate containing the magnet has components that could be irreparably damaged if opened incorrectly 3 Contact Varian to schedule the visit of an installation engineer after the shipment is moved to the installation site the utilities are installed and non Varian installation parts and supplies listed in the Installation Supplies and Equipment section are received For install
13. Electrical Outlets Table 14 lists the electrical outlets circuits requirements of system components The sections below details the requirements of each componenit If you have the choice between two voltages in the range it is generally better to choose the high voltage side since sites tend to suffer sags more than increases in voltage The specification of 220 10 7 Vac means that you can operate at voltages as low as 204 6 Vac That voltage is a minimum and not recommended any sags in that voltage level may lead to problems Table 14 contains information for how to improve the operating conditions when in this low voltage region Twistlok style connectors are recommended to reduce the risk of accidentally disconnecting power during operation Due to the large number of plug configurations world wide Varian does not ship end connectors on cords Obtaining appropriate local connectors is the customers responsibility Table 14 Electrical Outlets Circuits Requirements Usable Cable NERO Fe Electrical Requirements Operation in 190 205 Va Length pr en single phase at 50 60 Hz Range Asian Market Circuits 8 ft Host workstation and 2 100 125 Vac 15 A Ok peripherals minimum or 220 240 Vac 15 A 16 ft Infinityplus two 1 220 10 7 Vac 20 A Step up cabinet console 15 ft CMA amplifier each 1 220 10 7 Vac 30 A Step up CH 9F 20 ft AMT amplifier each 1 220 10 7 Vac 15 A Jumper select X or Y band 18 ft Infinit
14. Systems Distance From Magnet MHz mm Centerline to Floor m 200 89 1 12 300 89 1 12 400 89 400 89 AS 1 13 500 89 AS 1 15 600 89 1 23 800 63 1 44 01 999176 00 B1001 Infinityplus Installation Planning 45 Chapter 5 Stray Magnetic Fields 200 89 magnet field values 5G Axial distance from magnet CL m 0 5 1 0 1 5 2 0 Radial distance from magnet CL m Figure 6 Stray Field Plots for 200 89 Magnets 300 89 magnet field values Axial distance from magnet CL m 0 5 1 0 1 5 2 0 Radial distance from magnet CL m Figure 7 Stray Field Plots for 300 89 Magnets 46 Infinityplus Installation Planning 01 999176 00 B1001 5 2 Stray Field Plots 400 89 magnet field values Axial distance from magnet CL m 0 5 1 0 1 5 2 0 2 5 3 0 Radial distance from magnet CL m Figure 8 Stray Field Plots for 400 89 Magnets 400 89 AS magnet field values Axial distance from magnet CL m 0 5 1 0 1 5 2 0 2 5 3 0 Radial distance from magnet CL m Figure 9 Stray Field Plots for 400 89 AS Magnets 01 999176 00 B1001 Infinityplus Installation Planning 47 Chapter 5 Stray Magnetic Fields 500 89 AS magnet field values Axial distance from magnet CL m 0 5 1 0 1 5 2 0 2 5 3 0 3 5 Radial distance from magnet CL m Figure 10 Stray Field Plots for 500 89 AS Magnets 48 Infinityplus Installation Planning 01 999176 00 B1001 Axial distance from magnet CL m 5 2 Stray Field Plots 600 89 magnet
15. a flow rate 400 8 AS 2 through the pressure of 19 LPM 40 SCFH at 207 kPa 500 89 AS 3 30 psig For low temperature operation use 600 89 3 prepurified grade gas 99 99 800 63 2 2 K 5 CAUTION To avoid movement caused by magnetic field attraction helium gas and nitrogen gas cylinders made of magnetic material must be kept outside the 5 gauss limit of the magnet and firmly secured Face Mask and Thermal Gloves If cryogenic helium or nitrogen contacts living tissue a serious injury similar to a burn can occur Order appropriate safety coverings for use during dewar servicing including a mask that protects the face completely and a loose fitting pair of thermal gloves WARNING Avoid helium or liquid nitrogen contact with any part of the body If liquid helium or nitrogen contact living tissue a serious injury similar to a burn can occur Never place any part of your body directly over the helium and nitrogen exit tubes on top of the magnet If helium or nitrogen contacts the body seek medical attention especially if the skin is blistered or the eyes are affected Heat Gun Acquire a 1600 W heat gun Dayton Model 27046 or equivalent and heavy duty extension cord for thawing ice accumulation and drying out moisture on dewar servicing equipment CAUTION These heat guns contain ferrous magnetic materials Nonferromagnetic Ladder Acquire a 180 cm 6 ft nonferromagnetic ladder for reaching the top of the dewar while i
16. and Weights i 20 Table 7 Ceiling Minimum Height sise 21 Table 8 Interaction Between a Magnetic Field and Common Objects 0 00 0 seeseeeseeseeteceeeeeees 24 Table 9 Operating Frequencies for NMR Spectrometers ii 25 Table 10 Operating Frequencies for Common Nuclei 26 Table 11 Liquid Helium Displacement for Room Ventilation Considerations 26 Table 12 Ambient Temperature and Relative Humidity iii 27 Table 13 Helium and Nitrogen Refill Intervals and Volumes i 27 Table 14 Electrical Outlets Circuits Requirements iii 30 Table 15 Compressed Air Pressure for Nitrogen and Air i 32 Table 16 Maximum Air Conditioning Requirements i 33 Table 17 Host Computer Requirements sn 35 Table 18 Preinstallation Worksheet for Solaris ii 37 Table 19 Initial Onsite and Short Notice Liquid Helium Supplies iii 40 Table 20 Initial Onsite Liquid Nitrogen Supply ie 40 Table 21 Helium Gas Supply onermisseisssmrrvrbinivsinniaiesinestseksrsrerrberabidsislesskertb dente 41 Table 22 Stray Field Data for Oxford Magnets at ACGIH Exposure Values 44 Table 23 Stray Field Data for NMR Magnet Systems ie 45 Table 24 Magnet Centerline to Floor ss 45 01 999176 00 B1001 Infinityplus Installation Planning 6 SAFETY PRECAUTIONS The foll
17. and air lines to the appropriate accessories Table 15 Compressed Air Pressure for Nitrogen and Air System Configuration Pressure at Device Flow Rate System with optional antivibration systems 552 kPa 80 psig 0 067 LPM 0 14 SCFH Infinityplus VT and purge 552 kPa 80 psig 169 LPM 360 SCFH Infinityplus spinning 552 kPa 80 psig 141 LPM 300 SCFH Total source required is 600 SCFH minimum 3 5 Switching Gas Supplies Varian Inc recommends using a three way or diverting ball valve to allow switching of gas sources With this valve installed each supply line will have a shut off valve and regulator on the supply side of the switching valve The first stage regulators can be omitted if the line pressure downstream of the regulator will be less than 90 PSI with the regulator in line Asa general practice both VT and spinning will run off of nitrogen gas or compressed air the sources are not normally different for the two outputs Varian Inc does not recommend using a quick connect fitting to switch sources since they usually introduce a significant flow restriction Varian Inc supplies a Tee fitting with adaptors to go from 1 2 inch NPT female fitting to the connections for the air management box and the MAS speed controller A 3 8 inch hose barb fitting is included as an alternate input in the Tee in case the 1 2 inch NPT is not available Refer to Figure 5 Optional first stage regulators if line
18. and possibly extensive damage to the magnet It could also cause a sudden dangerous release of nitrogen and helium gases from the dewar Except when transferring nitrogen or helium be certain that the relief valves are secured on the vent tubes Caution Notices Observe the following precautions during installation operation maintenance and repair of the instrument Failure to comply with these cautions or with specific cautions elsewhere in Varian manuals violates safety standards of design manufacturing and intended use of the instrument Varian assumes no liability for customer failure to comply with these precautions CAUTION CAUTION CAUTION CAUTION 01 999176 00 Keep magnetic media ATM and credit cards and watches outside the 5 gauss perimeter from the centerline of the magnet The strong magnetic field surrounding a superconducting magnet can erase magnetic media such as floppy disks and tapes The field can also damage the strip of magnetic media found on credit cards automatic teller machine ATM cards and similar plastic cards Many analog wrist and pocket watches are also susceptible to damage from intense magnetism Refer to the manuals supplied with the magnet for the size of the specific 5 gauss stray field This gauss level should be checked after the magnet is installed Keep the PCs beyond the 5 gauss perimeter of the magnet Avoid equipment damage or data loss by keeping PCs well away from the
19. crew to move the shipping crates holding the system from the delivery truck or storage location to the installation site For 750 MHz magnets and larger depending on contract terms Varian may provide a moving crew 1 1 Installation Planning Process Use the following steps to prepare for delivery of the system Refer to the chapters in this guide for further details Consult knowledgeable individuals such as plant facilities personnel for assistance in implementing these instructions 1 Check the SHIP BY date on the Varian Order Acknowledgment form Use this date as a target for completing installation preparations If you anticipate any delays in site readiness and need to delay shipment notify the factory at least 90 days in advance Select the site for installing and operating the system Note a site survey is standard with most Infinityplus spectrometer systems Review the considerations described in Section 1 2 on page 14 and make sure the site conforms to the requirements listed in Chapter 2 Installation Site Requirements on page 19 Prepare the installation site including electrical outlets compressed air supply and air conditioning as described in Chapter 3 Site Preparation on page 29 Make any computer preparations required also described in Chapter 3 Order supplies and equipment for installation and startup operation as described in Chapter 4 Installation Supplies on page 39 Make arran
20. field This gauss level should be checked after the magnet is installed Only qualified maintenance personnel shall remove equipment covers or make internal adjustments Dangerous high voltages that can kill or injure exist inside the instrument Before working inside a cabinet turn off the power switch located on the back of the console and or the power switch on the individual high power amplifier then disconnect the ac power cords If you are unsure of the location for the power switches contact your Varian Inc service representative Do not substitute parts or modify the instrument Any unauthorized modification could injure personnel or damage equipment and potentially terminate the warranty agreements and or service contract Written authorization approved by a Varian Inc product manager is required to implement any changes to the hardware of a Varian NMR spectrometer Maintain safety features by referring system service to a Varian service office Do not operate in the presence of flammable gases or fumes Operation with flammable gases or fumes present creates the risk of injury or death from toxic fumes explosion or fire Leave area immediately in the event of a magnet quench If the magnet dewar should quench sudden appearance of gasses from the top of the dewar leave the area immediately Sudden release of helium or nitrogen gases can rapidly displace oxygen in an enclosed space creating a possibility of asphyxiatio
21. or hme0 for Ultras or 10 100baseT Ethernet boards IP Address Use 192 9 200 1 for non networked spectrometers or your network IP number for all other networked systems Name Service Choose NIS not NIS Choose NIS Domain Name Example our domain Name Server Host Name Example ourserver Name Server IP Address Example 195 5 2 25 Subnet Mask Example 255 255 255 0 Time Zone Examples US Mountain US Pacific US Eastern System Configuration Type Choices Server Standalone or Dataless Client Choose standalone Disk Layout Disk layout sizes vary according to disk size 01 999176 00 B1001 Infinityplus Installation Planning 37 Chapter 3 Site Preparation Obtaining the IP Address Your Sun workstation must have a unique Internet Protocol IP network address if your Sun workstation is to be attached to a network Consult your network administrator about the address If the software is being installed on a Sun workstation that is already connected to a network the command ypcat hosts grep uname n can be used to display the IP address of your Sun workstation Note the use of back quotes in this command If NIS is not enabled use the command cat etc hosts grep uname n Selecting a Subnet Mask The subnet mask is a number that is used to split IP addresses into the network Internet and host parts If your site does not use multiple subnets use the defau
22. should contain only a small percentage of nylon and be installed over antistatic pads Alternatively regular use of a good quality antistatic spray can help considerably in alleviating the problem Whenever a printed circuit board must be touched or handled the person should wear grounded wrist straps CAUTION Many components in the system contain highly sensitive electronic devices that must be protected from electrostatic discharges by proper floor coverings and grounding practices A person walking across a nylon carpet or wearing synthetic fabrics can generate an electrostatic charge that can discharge to the next object that is touched If this happens to be the system the system components can be damaged An overly dry atmosphere also tends to create an electrostatic charge As with any system based on integrated circuits the system is susceptible to static spikes both those generated on the power line and those generated in the lab area that must be suppressed 3 10 Sun Workstation Preparation 34 Varian NMR spectrometers are operated using a Sun workstation as a host computer Regardless of whether the Sun was purchased from Varian or separately certain preparations are required Some of these preparations have been outlined previously in the section Electrical Outlets on page 30 The following sections contain additional considerations Magnetic Field Considerations The spectrometer host workstation system and magne
23. temperature operation using the variable 400 89 AS 325 temperature accessory a refrigerant is required 500 89 AS 700 Most commonly this is liquid nitrogen in the VT 600 89 700 cooling bucket or the optional Kadel long run 800 63 2 2 K 2000 time liquid nitrogen dewar Helium Gas Supply Table 21 lists the recommended number of helium gas cylinders A regulator must be provided Each cylinder should hold at least 8000 liters 285 ft3 The helium gas must be the highest purity available no less than 99 995 or U S Bureau of Mines Grade A A magnetic helium gas container can be used provided the unit remains outside the 5 gauss limit of the magnet and the cylinder is firmly secured to avoid movement caused by the magnetic field 40 Infinityplus Installation Planning 01 999176 00 B1001 4 1 Required Installation Supplies and Equipment Nitrogen Gas Supply for Magnet Installation During installation one cylinder of nitrogen gas is Table 21 Helium Gas Supply required for precooling the magnet and for transfer of liquid nitrogen A regulator must be provided A Magnet field Helium gas magnetic nitrogen gas container can be used if it is MHz cylinders outside the magnet 5 gauss limit and the cylinder is firmly secured to prevent attraction to the magnet 200 89 2 If the system is equipped with the variable temperature 309 93 accessory a nitrogen gas supply is required The gas 400 83 2 must be dry and chemically pure with
24. than 5 gauss outside the room If a minimum configuration is necessary the customer must ensure the safety of people who need to pass through the 5 gauss regions Compressed air amp compressed nitrogen a 300 89 D S Console power Workstation power x 5 gauss Internet amp phone lines 1 4 in 1ft 54 Infinityplus Installation Planning 01 999176 00 B1001 Recommended Room Layout for a 300 89 System The room dimensions are about 5 9 m x 5 9 m 19 5 ft x 19 5 ft The Infinityplus cabinet is 111 cm x 78 cm 44 in x 31 in The high power amplifier cabinet is 55 cm x 78 cm 22 in X 31 in each The accessory cabinet is 56 x 79 cm 22 in x 31 in Typical table size is 178 cm x 152 cm 70 in x 60 in The magnet is 69 cm x 69 cm 27 in x 27 in A distance of 1 m 3 ft should be maintained around the standard cabinet The magnet should be at least 0 6 M 2 ft from the wall Compressed air amp
25. that exceeds the house pressure Attach to the valve a minimum I cm 0 5 in pipe terminated with a 1 2 inch male National Pipe Thread NPT The termination fitting should be within 6 m 20 ft of the planned location of the accessory cabinet A first stage air regulator see Figure 5 capable of 2 psi is also suggested upstream from the ball valve when 90 PSI or greater can be reached at the output In areas where humidity is high or where moisture in the air supply is a problem consider installing a prefilter with an automatic drain to help prevent overload of the filter In extreme cases an air dryer assembly may be necessary The source should include a reservoir and be capable of delivering the air pressures in kilopascals or pounds per square inch gauge and flow rates in liters per minute or standard cubic feet per hour after filtering as given in Table 15 Designing to the flow rates stated in Table 15 should allow for optimum life from your compressor and allow your delivery system to maintain a high quality of air A coalescing filter and particulate filter 01 999176 00 B1001 Infinityplus Installation Planning 31 Chapter 3 Site Preparation are required and must be supplied and installed by the customer The particulate filter should be capable of filtering to 0 1 micron The installation engineer will install on your air termination fitting a Varian supplied assembly that includes a 0 to 690 kPa 0 to 100 psi pressure gauge
26. the system components and Chapter 6 Room Layouts on page Table 4 Infinityplus Cabinets Dimensions and Weights System Height Width Depth Weight y cm in cm in cm in kg lb Infinityplus console 124 5 49 110 7 43 6 78 30 7 281 620 Infinityplus amplifier cabinet 142 3 56 55 3 21 8 78 30 7 272 600 1 cabinet for 1 3 channels 2 cabinets for 4 channels 01 999176 00 B1001 Infinityplus Installation Planning 19 Chapter 2 Installation Site Requirements Table 5 Magnet Dimensions with Stand or Legs Attached Magnet Bore Height Width Depth Magnet Weight Wih MHz mm mn mlin cmn Weight Antivibration in in kg Ib kg Ib 200 89 230 90 5 79 31 79 31 391 860 456 1005 300 89 230 90 5 79 31 79 31 399 878 506 1115 400 89 230 90 5 79 31 79 31 410 902 660 1456 400 89 AS 230 90 5 79 31 79 31 410 902 660 1456 500 89 AS 258 101 6 98 38 98 38 1250 2756 600 89 258 101 6 79 31 79 31 796 1755 800 63 2 2K 349 7 137 6 118 3 46 6 118 3 46 6 3000 6600 Notes 1 Dimensions and weights are typical and can vary 5 cm 2 in or 44 5 kg 10 1b from crate to crate 2 AS represents actively shielded magnets 3 Magnets with in the weight column ship standard with the antivibration legs Table 6 System Accessories Dimensions and Weights Height Width Depth Weight Configuration cm in cm in
27. 00 89 AS 203 80 123 44 152 60 1049 2308 600 89 203 80 94 37 128 50 5 781 1722 800 63 2 2 K 290 114 210 84 210 84 3000 6600 Actively shielded magnets are designated by AS Dimensions and weights are typical and can vary 5 cm 2 in or 4 5 kg 10 1b from crate to crate Table 2 Cabinet Dimensions as Shipped with Crate and Pallet Height Width Depth Weight Came cm in cm in cm in kg Ib Infinityplus console 158 62 125 49 104 41 354 780 Infinityplus amplifier cabinet 168 66 71 28 112 44 313 690 1 cabinet for 1 3 channels 2 cabinets for 4 channels calculating vertical horizontal and turning clearances and evaluating the structural strength of passageways Moving the larger crates of the system requires a forklift or hydraulic pallet mover which must be considered when calculating accessibility For an installation site at a different level from the delivery location be sure that the lifting equipment such as a forklift or an elevator is capable of handling the combined weight and size of the shipping crates and the moving equipment 01 999176 00 B1001 Infinityplus Installation Planning 15 Chapter 1 Site Selection and System Delivery Table 3 System Accessories Dimensions as Shipped with Crates and Pallets as Appropriate ii Height Width Depth Weight r cm in cm in cm in kg Ib Accessory cabinet 94 37 72 28 97 38 90 1
28. 98 Miscellaneous Crate 145 57 130 51 104 41 154 339 NMR work table 31 12 188 74 115 45 89 196 If it is not possible to gain access to the installation site unless the system is uncrated contact a Varian representative for further instructions Do not uncrate the system except upon direct instructions from an authorized Varian representative To avoid unnecessary expense be sure moving personnel and equipment are ready for the shipment on the delivery day 1 4 System Shipment The method of shipping and the current conditions at the destination determine the extent of the receiving preparations The Varian Order Acknowledgment form indicates the shipping method for the order The following service is usually provided Air Freight System is delivered to unloading dock or other easily accessible outside unloading point Factory to destination transit time is about two days not including time to clear customs Motor or Moving Van System is delivered to an easily accessible interior location or any interior location to which freight can be easily transported by movable dolly Excluded is transport in elevators that cannot support the weight of the shipment or up stairways Factory to destination within the United States is about eight days Selecting a Local Shipping Company Confirm that the local shipping company uses a vehicle that will allow the magnet to be transported in an upright position for all transport me
29. Installation Planning Infinitypius NMR Spectrometer Systems Pub No 01 999176 00 Rev B1001 NOTICE Varian Inc was acquired by Agilent Technologies in May 2010 This document is provided as a courtesy but is no longer kept current and thus will contain historical references to Varian For more information go to www agilent com chem he Agilent Technologies Installation Planning Infinitypus NMR Spectrometer Systems Pub No 01 999176 00 Rev B1001 AVI TAS VA AJ IAN Installation Planning Infinityplus NMR Spectrometer Systems Pub No 01 999176 00 Rev B1001 Revision history A0101 Initial release B1001 Minor changes including Table 14 Technical contributors Joe Dumais Mark Stevenson Tom Benzel Kevin Geohring Technical writer Dan Steele Mike Miller Copyright 2001 by Varian Inc 3120 Hansen Way Palo Alto California 94304 http www varianinc com All rights reserved Printed in the United States The information in this document has been carefully checked and is believed to be entirely reliable However no responsibility is assumed for inaccuracies Statements in this document are not intended to create any warranty expressed or implied Specifications and performance characteristics of the software described in this manual may be changed at any time without notice Varian reserves the right to make changes in any products herein to improve reliability functi
30. No Antivibration System 21 Magnet Weight Distribution With Antivibration System oo ee 22 2 5 Floor Vibration Level Requirements ss 23 2 6 Magnet Support Requirement sisi 23 Floor Anchoring Requirements ss 23 2 7 Magnetic Environment _ ieaie a ioiii 23 2 8 Radio Frequency Interference In Band i 25 29 Ventilation min an A nn 26 2 10 Ambient Temperature and Humidity ii 26 2 11 Helium and Nitrogen Refill Volumes and Intervals i 27 Chapter 3 Site Preparation sine 29 3 1 Line Voltage Variation ii 29 3 2 Uninterrupted Power Supply siens 30 43 Electrical Outlets x rai a 30 3 4 Compressed Air Supply i 31 3 5 Switching Gas Supplies sisi 32 3 6 Compressed Nitrogen Gas ieina iiss 33 3 7 AC Power and Air Conditioning sisi 33 3 8 Telephone and Internet Access eceeseseceeeeseesesseeeseeseceseseeaeeseeseseeceeesaaes 33 3 9 Electrostatic Discharges sicari la lalla lana ala a dui 34 01 999176 00 B1001 Infinityplus Installation Planning 3 Table of Contents 3 10 Sun Workstation Preparation ss 34 Magnetic Field Considerati ns sunonvmvsanibednvmid hk ddan keiserinne kad d dd 34 SUO Worksta HONS lia era deans vane ie 35 SU PETE be 35 Solans Media Liliana 35 Solars Installato c ca aaa 35 SUD DOGE Ut lia 36 Sun Workstation Preparation Checklist eceseessceeseeseeseseeeeeeseseeens 36 Co
31. Q quench 26 R radio frequency emission regulations 10 RAM requirements 35 receiving preparations 16 refill intervals 27 refill volumes 27 relief valves warning 9 reproductive hazard 44 reservoir for air 31 rf interference 20 25 room layouts 53 S safety precautions 7 9 sales centers 12 scheduling installation 17 server 36 service centers 12 Ship By date 13 shipping crate damage 17 shipping method 16 signs 51 site accessibility 15 site size requirements 19 site survey 13 size of site 19 Solaris CD ROM 35 collecting system and network information 36 Solaris operating system software 35 solids high power amplifiers caution 9 solvents 42 spectrometer frequency ranges 25 stand alone 37 step down transformer 31 stingers 42 stray field plots 25 43 44 streaming tape cartridge 34 structural floor loading rating 21 subnet mask 38 Sun peripherals 35 Sun workstation 34 Sun workstations 35 sunlight 27 supplies 39 supply dewars 20 supporting the magnet 23 surge current 33 surge protection 31 42 T temperature stability 26 thermal gloves 41 tip and tell indicator 15 17 transfer of ownership 17 transfer tube 21 42 Tygon tubing 42 01 999176 00 B1001 Index U uname n command 37 uncrating system 16 UPS systems 30 V van delivery 16 Varian sales and service centers 12 ventilation 26 vertical magnetic fields 24 vibration in flo
32. Systems Leg Placement and Sizes 22 Infinityplus Installation Planning 01 999176 00 B1001 2 5 Floor Vibration Level Requirements 2 5 Floor Vibration Level Requirements The floor must be sufficiently rigid to reduce the vibration from adjacent dynamic loads to a negligible level defined as no single peak vibration greater than 20 ug acceleration from 5 to 100 Hz For sites exceeding this specification antivibration equipment is necessary Sites with vibrations below 5 Hz exceeding 5 ug are not recommended for the installation of any spectrometers Use of Firestone tire antivibration systems are not generally recommended at sites with vibrations below 20 Hz or at any site with large vibrations in the horizontal direction Ground floor or basement sites are generally preferred for systems because the natural resonant frequencies of most building structures are typically at low frequencies and horizontal in direction Measurements are made with an analyzer Ono Sokki Model CF 200 field FFT analyzer Hewlett Packard Model 3561A signal analyzer or equivalent using 16 RMS time averages and with a seismic accelerometer that has 10 V g sensitivity Wilcoxen Model 731 or equivalent 2 6 Magnet Support Requirement The magnet has a high center of gravity and could tip over during an earthquake or after being struck by a large object Therefore the magnet must be supported either by ropes attached to the ceiling or by bolting the magnet legs to the f
33. a be taken to the area safely Can cryogen transfers be made quickly and safely 3 Finally look at the area as a whole with the following considerations Look foran area large enough to contain the magnet and as much of the 5 gauss static field as possible The area should have the minimum ceiling height described in Section 2 3 Ceiling Height Requirements on page 21 When an acceptable space has been found look for steel and iron in the immediate area Consider the structural steel of the building iron pipes machinery etc Look in the near area for elevators vehicular traffic large transformers and other large amounts of steel and iron Consider the ability to control the movement of ferromagnetic objects such as elevators automobiles or carts within the magnetic field Consider adequate access for the delivery of dewars containing liquid helium and nitrogen Consider public access that might pass through the 5 gauss zone Consider escape routes in case of emergency including a magnet quench Consider the location of sensitive electronic equipment that might be affected by the magnetic field This includes dryers compressors and other such equipment See Section 2 7 Magnetic Environment on page 23 and Chapter 5 Stray Magnetic Fields on page 43 For an exact definition of gauss line boundaries refer to Section 5 2 Stray Field Plots on page 44 for more informatio
34. acing e g a magnet that holds 30 liters of LHe will require a fan that can displace about 784 ft of helium gas 2 10 Ambient Temperature and Humidity 26 Table 12 lists the required ambient temperature ranges temperature stability and humidity levels for the site For optimal performance the ambient temperature around the magnet should not vary Magnet homogeneity is optimized if the ambient temperature stability is Infinityplus Installation Planning 01 999176 00 B1001 2 11 Helium and Nitrogen Refill Volumes and Intervals maintained for the duration of an experiment and between shimming Sunlight should never shine directly on the magnet or the area surrounding the magnet If necessary install an air conditioning system to maintain the required conditions Keep the air conditioning system operating continuously to stabilize the temperature and humidity surrounding the spectrometer system The air flow from the room heating and cooling system must not blow on the magnet Do not allow moisture to collect on in or around the system At high altitudes above 5000 ft the cooling efficiency for the electronics is lower This can be compensated for by lowering the room temperature by one or two degrees from the room temperature specification Table 12 Ambient Temperature and Relative Humidity Temperature Relative Humidity Mode C F Noncondensing Operational range 17 to 24 60 to 75 20 to 80 Optimum 20 68 40 to 60 Temp
35. ations in the United States telephone the Installation Department at 650 424 4587 01 999176 00 B1001 Infinityplus Installation Planning 17 Chapter 1 Site Selection and System Delivery 18 Infinityplus Installation Planning 01 999176 00 B1001 Chapter 2 Installation Site Requirements Sections in this chapter 2 1 Site Size this page 2 2 Accessibility of Site page 20 2 3 Ceiling Height Requirements page 21 2 4 Structural Strength of Floor page 21 2 5 Floor Vibration Level Requirements page 23 2 6 Magnet Support Requirement page 23 2 7 Magnetic Environment page 23 2 8 Radio Frequency Interference In Band page 25 2 9 Ventilation page 26 2 10 Ambient Temperature and Humidity page 26 2 11 Helium and Nitrogen Refill Volumes and Intervals page 27 The Infinityplus NMR spectrometer has certain site requirements which are described in this chapter Factors to consider when selecting the installation site include Site size and ceiling height Accessibility to the delivery location Floor rigidity and structural strength Magnetic and radio frequency environment Air ventilation ambient temperature and humidity 2 1 Site Size The site must be large enough to allow free access to all sides of the cabinet magnet and accessories for operation maintenance and cryogenic service Table 4 Table 5 and Table 6 list the dimensions of
36. be addressed immediately to avoid delays and additional costs One person Ve el Infinityplus Figure 1 Infinityplus Cabinet and Oxford Magnet 01 999176 00 B1001 Infinityplus Installation Planning 11 Introduction from the customer s institution should be appointed to coordinate site planning and preparation This person should represent all users of the system in dealing with Varian and the facility planner or architect Contacting Varian Varian s staff of thoroughly trained service specialists throughout the world is your assurance of always receiving prompt attention You can access information at www varianinc com nmr using the Contact Us button or For product sales and service information contact one of the Varian sales offices Argentina Buenos Aires 114 783 5306 Australia Mulgrave Victoria 3 9566 1138 Austria V sendorf 1 699 96 69 Belgium Brussels 2 721 48 50 Brazil Sao Paulo 11 829 5444 Canada Ottawa Ontario 613 260 0331 China Beijing 10 6846 3640 Denmark Herlev 42 84 6166 France Orsay 1 69 86 38 38 Germany Darmstadt 6151 70 30 Italy Milan 2
37. cording to Varian specifications Configuration and Peripherals Printers should be parallel Centronics and must be capable of accepting PostScript Sufficient RAM for a full page of PostScript is required this might be more than the minimum supplied depending on the plotter and paper size X server software must be capable of supporting RSH REXEC XDM or XDMCP Collecting System and Network Information The Solaris installation program prompts you to enter some system and network information before installation begins You can save time by collecting this information now before booting from the Solaris CD ROM Use the Table 18 to record your system information Each field on the worksheet is described below If your system is not connected to a network you need to know or create only the Host name root password and the time zone If your system is on a network you need additional information described in the following sections If unsure contact your network administrator System Configuration Type You are asked to configure your Sun workstation as one of the following server standalone or dataless client server is a system that provides network services such as Infinityplus Installation Planning 01 999176 00 B1001 3 10 Sun Workstation Preparation file transfer and storage space A standalone system is a system that contains its own hard disk and bootup files A dataless client sometimes called diskless client
38. discuss the health risks of being in proximity to magnetic fields Wearers of metal prosthetics and implants should contact their physician to determine if a danger exists Refer to the manuals supplied with the magnet for the size of the specific 5 gauss stray field This gauss level should be checked after the magnet is installed WARNING Keep metal objects outside the 10 gauss perimeter from the centerline of the magnet The strong magnetic field surrounding the magnet attracts objects containing steel iron or other ferromagnetic materials which includes most ordinary tools electronic equipment compressed gas cylinders steel chairs and steel carts Unless restrained such objects can suddenly fly towards the magnet causing possible personal injury and extensive damage to the probe dewar and superconducting solenoid The greater the mass of the object the more the magnet attracts the object Only nonferromagnetic materials plastics aluminum wood nonmagnetic stainless steel etc should be used in the area around the magnet If an object 01 999176 00 B1001 Infinityplus Installation Planning 7 SAFETY PRECAUTIONS Warning Notices continued WARNING WARNING WARNING WARNING WARNING WARNING WARNING is stuck to the magnet surface and cannot easily be removed by hand contact Varian service for assistance Refer to the manuals supplied with the magnet for the size of the specific 10 gauss stray
39. e solvents are needed to clean the magnet parts before assembly Acetone should never be used for general cleaning as it can damage some plastics and paints 4 2 Recommended Laboratory Supplies and Equipment 42 In addition to the required installation supplies and equipment the following items are recommended Cryogenic equipment rack Electrical power surge protector Monitor degaussing coil Cryogenic Equipment Rack Various items are used around the magnet for routine maintenance and handling including a helium transfer tube a flutter tube Tygon tubing and stingers To protect the cryogenic equipment from damage and to keep it conveniently available provide a rack to hold the items A 1 2 m x 2 4 m 4 ft x 8 ft peg board hung on a laboratory wall with wood or plastic pegs works very well Electrical Power Surge Protector To protect the delicate electrical components of the Sun workstation monitor disk drive unit CPU base etc a good quality surge protector should be inserted in the power circuit serving the components A single surge protector with six outlets should suffice if the components are located relatively close to one another Contact an electronic professional for advice on quality surge protection in your area If a UPS is to be used for line conditioning a surge protector is unnecessary See Chapter 3 3 Electrical Outlets on page 30 for power ratings Monitor Degaussing Coil The workstat
40. e using compressed air so long as the dew point is low enough to prevent condensation in the coldest part of the system usually the cooling apparatus 3 7 AC Power and Air Conditioning Use Table 16 to help determine maximum surge current and air conditioning requirements A filter on the air conditioning unit intake and special air filtration is required in installations exposed to corrosive gases salt air or unusual dirt or dust conditions The air conditioning system requires a power line separate from the spectrometer system Table 16 Maximum Air Conditioning Requirements For standard systems and host workstations System Power Surge Current Heat output kW A BTU hr Infinityplus two cabinet console3 1 7 70 5800 Accessory cabinet 0 02 68 Computer and monitor 0 24 22 824 Printer 0 057 19 200 AMT amplifiers X or Y band 1 2 23 4000 CMA H band 0 6 2050 Pulsed Field Gradient Amplifier 0 3 1025 1 Decay time lt 150 ms 2 Conversion of the unit of heat energy between BTU and the amount of system power is calculated using 1 kWh 3413 BTU 3 Measurements are only for the standard acquisition and rf console which does not share an ac power branch with the host workstation 4 Measurements are only for the host workstation which does not share an ac power branch with the acquisition and rf console 3 8 Telephone and Internet Access Varian Inc requires locating a voice telephone line near
41. er the power duct behind the console Infinityplus Amplifier Cabinets Each CMA amplifier in this cabinet requires 220 Vac single phase 30 A service Each AMT amplifier requires 220 Vac single phase with 20 A service It is best to have the power connection off to the side of the console unless there is about three feet of clearance behind the console The power bay can be on either side of the console but it is usually to the right as viewed from the front Infinityplus Accessory Cabinet One 220 Vac single phase 15 A outlet for the accessory cabinet The cabinet has its own distribution strip Other Accessories and Test Equipment At least six outlets are needed within 1 8 m 6 ft of the host workstation standard cabinet and magnet The outlets must have ground connections and provide a minimum of 2 30 KVA at the local single phase line voltage 120 Vac at 20 A or 230 Vac at 10 A 3 4 Compressed Air Supply The house compressed air supply must provide a source of air that is clean dry and free of contaminants with a dew point of 40 C 40 F minimum The delivery pipes should be at least 1 2 inch copper piping specified as air handling lines Install a ball valve on the permanent outlet of the air supply line The ball valve must be rated at least 860 kPa 125 psi or 9 kg cm with an open diameter matched to the copper piping If the house line pressure is greater than this level the valve must be rated at a level
42. erature stability 1 0 1 8 Storage shipping range 20 to 60 4 to 140 8 to 80 2 11 Helium and Nitrogen Refill Volumes and Intervals Table 13 lists typical refill volumes and intervals for helium and nitrogen Locating a reliable local source of liquid helium and nitrogen is particularly important Use the values listed in Table 13 when making arrangements for an on going supply of liquid helium and liquid nitrogen Note that refill volumes vary 20 to 40 depending on the refill efficiency and conditions Table 13 Helium and Nitrogen Refill Intervals and Volumes Magnet Bore Helium Refill Interval Helium RE Nitrogen Refill Interval Nitrogen Refill MHz mm days Joe days Volume liters liters 200 89 LH203 203 68 14 61 200 89 LH365 365 112 14 67 300 89 LH203 203 68 14 61 300 89 LH365 365 112 14 67 400 89 180 60 14 67 500 89 120 90 18 121 600 89 90 60 18 121 800 63 2 2 K 60 328 14 167 01 999176 00 B1001 Infinityplus Installation Planning 27 Chapter 2 Installation Site Requirements 28 Infinityplus Installation Planning 01 999176 00 B1001 Chapter 3 Site Preparation Sections in this chapter 3 1 Line Voltage Variation this page 3 2 Uninterrupted Power Supply page 30 3 3 Electrical Outlets page 30 3 4 Compressed Air Supply page 31 3 5 Switching Gas Supplies page 32 3 6 Compressed Nitrogen Gas page 33 3 7 AC Power and Air Conditioning page 33
43. erformance Base level graphics work fine with Spinsight Higher performance graphics configurations e g Creator Elite are also compatible with Spinsight Either 8 bit or 24 bit graphics are supported Sun Peripherals A CD ROM drive is required to load the Solaris and Spinsight software onto the host workstation The CD ROM drive might not automatically be included with a Sun workstation it is included when the Sun computer is part of a NMR spectrometer purchase While loading the software remotely is possible loading the software locally is preferred Often the remote computer is password protected and thus requires the presence of the system administrator to enter the password and grant access Should any troubleshooting or software reloads be required the process would be complicated by the need for the system administrator A back up device such as a tape drive is strongly recommended Solaris Media Sun workstations whether purchased from Varian or another source include the UNIX right to use license If you purchase a Sun workstation through Varian a current version of Solaris on a CD ROM is included If you purchase the Sun workstation from another source you must purchase a copy of the Solaris CD ROM or make sure a copy is available At least one copy of the CD ROM available for the installation is required Note that the Varian supplied media might not be for the latest version of Solaris It is however the lat
44. ertically to adjacent floors and additional signs may be needed there 01 999176 00 B1001 Infinityplus Installation Planning 51 Chapter 5 Stray Magnetic Fields 3 Magnet area danger signs Figure 15 Post at each entrance to the magnet area Be sure each sign is outside the 5 gauss perimeter A10 GAUSS A 5 GAUSS I WARNING WARNING Tools and Equipment Pacemaker Metallic Implant Hazard Strong magnetic fields are present that can Strong magnetic and rf fields are present that make magnetic items suddenly fly towards the can cause serious injury or death to persons magnet which could cause personal injury or with implanted or attached medical devices serious damage Do not take tools equipment such as pacemakers and prosthetic parts Such or personal items containing steel iron or persons must not go closer to the magnet than other magnetic materials closer to the magnet this sign until safety at a closer distance is than this sign identified by a physician or device manufacturer Dewars Magnetic Media ATM Credit Cards The stray field of the magnet can pull a Strong magnetic fields are present that can magnetic dewar into the magnet body causing erase magnetic media disable ATM and credit serious damage Use only nonmagnetic cards and damage some watches Do not take stainless steel dewars Do not use iron or steel such objects closer to the magnet than this sign dewars during servicing Pa N 8725000200 2050 10 Mag S
45. est supported by Varian In case of doubt please contact Varian Solaris Installation All Sun computers for use with an Infinityplus system are configured at the Fort Collins factory If you have directly purchased the Sun computer from a source other than Varian 01 999176 00 B1001 Infinityplus Installation Planning 35 Chapter 3 Site Preparation 36 Inc the computer must be shipped to the Fort Collins factory to be properly loaded with software Preinstalled Solaris cannot be used with Spinsight and Infinityplus Sun Documentation Solaris contains extensive online documentation For these reasons full Sun UNIX documentation is not included with the purchase of a Sun workstation whether from Varian or another source Full Solaris documentation is available at http docs sun com Full hardcopy documentation is available from Sun through SunExpress but such documentation is not required for installation or use of the system Sun Workstation Preparation Checklist Sun workstation is an Ultra or SPARCstation capable of running Solaris 2 6 or newer Hard disk space is 4 GB or larger RAM is 64 MB or more CD ROM drive is installed locally or readily accessible on a networked computer Solaris CD ROM is available If you have purchased the Sun workstation from a source other than Varian Sun workstation shipped to Fort Collins factory for proper configuration Sun workstation and peripherals installed and configured ac
46. eter Radio frequency emissions may also pose a danger to some individuals The rf emission levels from Varian NMR equipment have been measured and compared to the IEEE ANSI C95 1 1991 standard For further information refer to the RF Environment section of the Installation Planning Guide Warning Signs Varian provides signs to help customers meet this posting responsibility These signs must be posted according to the following requirements before the magnet is energized 1 10 gauss warning signs Figure 13 Post along the 10 gauss perimeter of the magnet so that a sign can be easily seen by any person about to enter the 10 gauss field from any direction Refer to the manuals supplied with the magnet for the size of a typical 10 gauss stray field Check this gauss level after the magnet is installed Note that the stray field may extend vertically to adjacent floors and additional signs may be needed there A sign is not required if the 10 gauss field extends less than 30 cm 12 in beyond a permanent wall or less than 61 cm 24 in beyond the floor above the magnet 2 5 gauss warning signs Figure 14 Post along the 5 gauss perimeter of the magnet so that a sign can be easily seen by any person about to enter the 5 gauss field from any direction Refer to the manuals supplied with the magnet for the size of a typical 5 gauss stray field Check this gauss level after the magnet is installed Note that the stray field may extend v
47. finityplus NMR superconducting spectrometer system including preparing the Sun workstation Using the predelivery and postdelivery checklists provided and following the information presented should bring about a smooth transition from delivery to installation Figure 1 illustrates a Infinityplus cabinet and an Oxford magnet This guide contains the following chapters Chapter 1 Site Selection and System Delivery describes how to plan for the installation of an NMR spectrometer This chapter also discusses system delivery and provides a table of shipping dimensions for NMR components Begin in this chapter Chapter 2 Installation Site Requirements lists the factors to consider when selecting the installation site Chapter 3 Site Preparation describes the many factors to consider electrical cooling safety supplies and so forth when preparing the installation site Chapter 4 Installation Supplies describes the supplies required and recommended for the system installation Chapter 5 Stray Magnetic Fields provides magnetic field safety hazard data and shows stray field plots for each magnet system Chapter 6 Room Layouts provides information for laying out the NMR room Importance of Communication In planning the system installation good communications are essential between the customer the facility planner or architect and Varian on a frequent basis Any questions or problems must
48. gements for workers and equipment to move the system upon delivery to the installation site as described in Section 1 4 System Shipment on page 16 Read carefully sign and mail to Varian the Object Code License Form Note that acceptance of the products on the Order Acknowledgment form constitutes acceptance of the terms stated in the Object Code License Form whether the form is signed or not 01 999176 00 B1001 Infinityplus Installation Planning 13 Chapter 1 Site Selection and System Delivery 1 2 Site Selection Site selection is the process of finding a location for the magnet providing the least interference from the building it occupies The selection of an optimum site is determined almost entirely by the high magnetic fringe field of the system The process of selection can be complex because of the interaction of the magnetic field with the surrounding environment Chapter 2 Installation Site Requirements describes in detail all the factors to consider when selecting a site 1 Begin by looking for a site with a series of general requirements in mind The placement of the magnet is the primary consideration How will the field from the magnet affect its neighbors What will the building and its contents do to the quality of the magnet field Can the system be delivered to the site 2 The second requirement is access Will the site limit public access in surrounding areas Can magnetic storage medi
49. hausted from the magnet will displace oxygen and cause dia i Magnet Bore LHe Maximum Volume asphyxiation if not properly ventilated MHz mm liters During a magnet quench the evaporated helium is exhausted from the manifold 200 89 76 through the pressure relief valves The 300 89 76 amount of gas exhausted depends on the 400 89 AS 69 amount of liquid helium in the magnet at the 500 89 AS 130 time of the quench Table 11 lists the 600 89 115 approximate total amount of liquid helium possible for each magnet system but it is 800 63 450 unlikely that a magnet quench will boil off the total amount listed in Table 11 Also remember that vented helium gas fills the room from the ceiling down so place fans and ducts accordingly Direct return vents leading to a local cold water air conditioning unit may ingest enough cold gas to result in freezing and possibly rupturing the chiller The expansion ratio of liquid helium at room temperature is about 740 1 which means that one liter of liquid helium expands to about 740 liters of helium gas For fans rated in LPM liters per minute multiply the LHe maximum volume listed in Table 11 by 740 to get an idea of helium gas the fan should be capable of displacing For fans rated in CFM cubic feet per minute multiply the LHe maximum volume listed in Table 11 by 26 13 includes expansion ratio to get an idea of the total amount of helium gas that the fan should be capable of displ
50. ion Planning 59 Index hoist clearance 15 host name 37 host workstation magnetic field considerations 34 host workstation requirements 35 host workstation electrical outlets 31 humidity levels for a site 26 I Infinityplus Accessory Cabinet electrical outlets 31 installation department 17 installation equipment 39 installation site preparation 29 installation site requirements 19 installation supplies 39 interference rf 25 Internet Protocol network address 38 IP address 38 isopropyl alcohol 42 L laboratory size requirements 19 ladder 41 lifting equipment 15 line conditioner 29 line voltage variation 29 liquid helium boiloff 40 caution about dewars 39 expansion ratio 26 initial supply 40 locate a reliable source 27 39 refill volumes and intervals 27 supply 40 supply dewars 39 liquid nitrogen adaptor for rubber tubing 40 boiloff 40 locate a reliable source 27 39 recommended quantities 40 refill volumes and intervals 27 storage containers 40 supply requirements 40 VT accessory operation 40 VT cooling bucket 40 LPM rated fans for ventilation 26 M magnet crate 15 17 magnet field homogeneity 24 magnet quench warning 8 magnet tipping hazard 23 magnet transport 16 magnetic environment 23 magnetic field considerations for computers 34 magnetic field exposure 44 cardiac pacemakers 43 effects on equipment 24 reproductive hazard 44 risk to pregnancy 44
51. ion monitor can gradually become somewhat magnetized due to its proximity to the magnet This condition can be corrected with a degaussing coil If the host workstation system is to be located near the edge of the 1 2 gauss stray field of the magnet the degaussing coil is a necessity For example GC Electronics model 9317 1801 Morgan St Rockford IL 61102 815 968 9661 Infinityplus Installation Planning 01 999176 00 B1001 Chapter 5 Stray Magnetic Fields Sections in this chapter 5 1 Safety Hazards of Strong Magnetic Fields this page 5 2 Stray Field Plots page 44 5 3 Posting Requirements for Magnetic Field Warning Signs page 51 The magnetic field is typically the biggest concern when planning for an NMR system This chapter contains magnetic field safety information and stray field plots 5 1 Safety Hazards of Strong Magnetic Fields The potential safety hazards of strong magnetic fields for devices such as certain pacemakers must be understood and planned for A set of plots indicating the magnitude of the stray fields for each type of magnet is included in Section 5 2 Stray Field Plots on page 44 These plots show typical levels of stray field Actual levels may vary and should be checked after a particular magnet has been installed WARNING Cardiac pacemaker wearers must remain outside the 5 gauss perimeter from the magnet until safety is clearly established An NMR superconducting magnet generates s
52. is a system without its own hard disk and uses an NFS server for the operating system storage and other services For the purposes of Spinsight you must install your system as a standalone system Selecting a Host Name Each computer on a network has a host name that uniquely identifies the computer If you already have a version of UNIX installed you can use the command uname n from within a shell to display this information for a Sun workstation When choosing a host name make sure the name you select is unique within both your local area network and if applicable your name service domain In many networks the choice of a host name is left up to the owner of the Sun workstation subject to the requirement of uniqueness A host name can be up to 64 uppercase or lowercase characters It is strongly recommended that you use all lowercase characters in the host name because some networking software that might be used in other computers on the network could require lowercase host names Choose a name that starts with a lowercase letter followed by any combination of lowercase letters numbers or hyphens The name however cannot end with a hyphen Table 18 Preinstallation Worksheet for Solaris Category Your Configuration Host Name Example mysystem If VNMR is to be installed as well as Spinsight do not use inova inovaauto gemcon or wormhole Primary Network Interface Use le0 for 10baseT Ethernet boards
53. larger capacity liquid helium storage dewars is used with the magnet additional ceiling clearance may be necessary In general the ceiling height must be at least twice the height of liquid helium storage dewar above the floor Some magnets can be provided with optional hinged top loading components that reduce the minimum ceiling height requirements Contact Oxford for details this must be specified when ordering the magnet Leg antivibration i e vibration isolation systems do not increase the ceiling height requirements Table antivibration systems add 20 32 cm 8 in 2 4 Structural Strength of Floor Contact a plant engineer structural engineer or registered civil engineer to confirm that the magnet and antivibration system as applicable does not exceed the structural floor loading rating The site floor also must have sufficient structural strength to support the combined weight of the entire spectrometer system and all moving equipment during installation Table 4 Table 5 and Table 6 Magnet Weight Distribution With No Antivibration System This section describes weight distribution for magnets without antivibration systems The weights of the magnets including stands are given in Table 5 200 89 300 89 400 89 and long hold magnets The stands for these magnets consist of three legs as shown in the plan view in Figure 2A Because the legs are hollow the surface contact with the floor is only 167 74 cm 26 sq in t
54. loor Magnet dimensions and weights are listed in Table 5 A structural engineer should be contacted to determine the best restraint method that meets local seismic requirement variations If overhead ropes are used the ceiling of the building should be evaluated for structural strength The ropes should have a small amount of slack so that building vibrations are not transmitted to the magnet These vibrations can cause artifacts to appear in the NMR spectra Floor Anchoring Requirements All systems with antivibration legs must be anchored to the floor The antivibration system used incorporates the dampening mechanism as an integral part of the magnet leg As a result the legs are not rigidly attached to the magnet In order to work properly they must be firmly attached to the floor This floor attachment also prevents the tipping of the leg in the case of an earthquake or being struck by a large object Depending on the seismic requirement the size of the magnet and the floor material floor anchoring alone may not be adequate A structural engineer should be contacted for recommendations Anchoring to the floor is a standard procedure for many other types of equipment Varian expects that the customer s plant or maintenance personnel can usually accomplish anchoring the leg Varian supplies four 1 2 inch diameter anchor bolts for each leg A minimum depth of 2 5 in is required for each bolt 2 7 Magnetic Environment The site must have a mi
55. lso be accessible for system delivery as described in Section 1 3 Transport Route and System Shipping Dimensions on page 15 20 Infinityplus Installation Planning 01 999176 00 B1001 2 3 Ceiling Height Requirements 2 3 Ceiling Height Requirements The ceiling must provide Table 7 Ceiling Minimum Height sufficient headroom to insert the liquid helium 7 n Minimum With transfer tube into the n ard Ceiling ee Hinged Components magnet dewar and the mm emin cm in storage dewar The height n EE ai of the ceiling or that part 9992 2180230 2 gt ITO of the ceiling located 300 89 314 123 6 295 116 directly above the magnet 400 89 314 123 6 295 116 without obstructions such 400 89 AS 314 123 6 295 116 as lighting and heating 500 89 AS 333 131 319 126 ducts must A 600 89 343 135 Not applicable greater than the minimum 800 63 2 2k 400 157 5 Not applicable heights listed in Table 7 If you buy the helium level option the helium level probes are furnished with a flexible section as standard thus allowing all magnets to be installed within minimum ceiling heights listed in Table 7 All dimensions include 110 mm to clear the top of the cryostat These ceiling minimums allow enough headroom to insert the standard helium flutter tube and refill transfer tubes into the magnet dewar They also allow use of the standard power stick for running up the magnet field However if one of the
56. lt number otherwise consult your network administrator For a Sun workstation connected to a network the command cat etc netmasks can be used Selecting the Name Service Type The name service prompt allows choosing between NIS NIS and none Choose NIS not NIS You will need to enter the host name and the IP address of the computer from which you receive the service If you choose none you are not prompted for additional information Ask your network administrator what name service the network uses Entering the host Name and IP Address of the Name Server With NIS as the name service type it is assumed that there is another computer on the network that is the current NIS server You are asked to enter the host name and IP address of the server that provides the name service On an existing computer the server s name can be displayed by entering the command ypwhi ch The server s IP address and other information can be displayed by entering the command ypcat hosts grep ypwhich Again note the use of back quotes Domain Name The domain name is the name assigned to a group of computers that are administered together All computers in the group domain are accessed by the same NIS or NIS maps Your network administrator should be able to provide the domain name You can also find your domain name by entering the command domainname Setting the Time Zone Solaris software uses world time zones and automatically adj
57. me studies suggest a link between magnetic field exposure and adverse reproductive effects the body of medical data available is not clear enough to draw any firm conclusions regarding risks to pregnancy Static magnetic field associated with the NMR spectrometer magnets are not considered by the scientific community at this time to comprise a risk to pregnancy or a reproductive hazard An article by the American Conference of Governmental Industrial Hygienists ACGIH entitled Threshold Limit Values and Biological Exposure Indices 5th ed states the following TLVs Threshold Limit Values refer to static magnetic flux densities to which it is believed that nearly all workers may be repeatedly exposed day after day without adverse health effects These values should be used as guides in the control of exposure to static magnetic fields and should not be regarded as a fine line between safe and dangerous levels Routine occupational exposures should not exceed 60 milliteslas mT equivalent to 600 gauss whole body or 600 mT 6000 gauss to the extremities on a daily 8 hour time weighted average basis A flux density of 2 teslas 20 000 gauss is recommended as a ceiling value Table 22 Stray Field Data for Oxford Magnets at ACGIH Exposure Values Magnet Type Radial Distance cm Axial Distance cm MHz mm 0 6kG 6kG 20kG 0 6kG 6kG 20kG eee n 800 63 2 2K 129 52 24 171 84 59 57 6 40 3 58 4 600 89 75 15 14 105
58. n Make sure you have enough ventilation in case of a quench Refer to Section 2 9 Ventilation on page 26 14 Infinityplus Installation Planning 01 999176 00 B1001 1 3 Transport Route and System Shipping Dimensions 1 3 Transport Route and System Shipping Dimensions sok If possible move the crates with a forklift or hydraulic pallet mover directly to the installation site The crates must remain upright CAUTION Move the crates in an upright position Do not drop or mishandle The crates are packed with G force and tip and tell indicators that record mishandling Be especially careful about moving the magnet crate If one or more crates cannot be moved into the installation site because of doorway clearance leave the affected crates in a clean safe dry location Do not open any crate except with direct instructions from an authorized Varian representative The installation site must be accessible from the delivery location with adequate clearance for system crates and moving equipment including magnet hoist throughout the access route Refer to Table 1 Table 2 and Table 3 for the dimensions and weights needed for Table 1 Magnet Dimensions as Shipped with Crate and Pallet Magnet Bore Height Width Depth Weight MHz mm cm in cm in cm in kg Ib 200 89 185 73 94 37 128 50 5 456 1003 300 89 185 73 94 37 128 50 5 464 1021 400 89 AS 185 73 94 37 128 50 5 571 1259 5
59. n Do not return until the oxygen level returns to normal Avoid liquid helium or nitrogen contact with any part of the body In contact with the body liquid helium and nitrogen can cause an injury similar to a burn Never place your head over the helium and nitrogen exit tubes on top of the magnet If liquid helium or nitrogen contacts the body seek immediate medical attention especially if the skin is blistered or the eyes are affected Wear eye protection when spinning a sample with the probe outside the magnet A rotor crash can shatter a rotor and cause eye injury when spinning a sample in a probe that is not installed in a magnet Wear eye protection Support the magnet and prevent it from tipping over The magnet dewar has a high center of gravity and could tip over in an earthquake or after being struck by a large object injuring personnel and causing sudden dangerous release of nitrogen and helium gasses from the dewar Therefore the magnet must be supported by at least one of two methods 8 Infinityplus Installation Planning 01 999176 00 B1001 SAFETY PRECAUTIONS Warning Notices continued WARNING with ropes suspended from the ceiling or with the antivibration legs bolted to the floor Do not remove the relief valves on the vent tubes The relief valves prevent air from entering the nitrogen and helium vent tubes Air that enters the magnet contains moisture that can freeze causing blockage of the vent tubes
60. ng 16 credit cards caution 9 cryogen equipment 42 cryogen refill intervals 27 cryogen refill volumes 27 cryogen warning 41 cryogenic equipment rack 42 D dataless client 37 01 999176 00 B1001 Index daylight savings time 38 degaussing coil 42 delivery of supplies 20 delivery responsibility 13 delivery services 16 domain name 38 domainname command 38 E electrical outlet requirements 30 4 channel system 31 amlifier cabinets 31 host computer and peripherals 31 Infinityplus cabinet 31 test equipment outlets 31 VT CP MAS 31 electrical power surge protector 42 electrostatic discharge 34 antistatic spray 34 carpeting requirements 34 caution 34 floor coverings 34 grounding 34 preventing 34 equipment rack 42 expansion ratio of liquid helium 26 F face mask 41 fans for ventilation 26 flammable gases warning 8 floor structure strength 21 floor vibration 23 floor vibration measurement 23 flutter tube 42 FOB block 17 frequencies for common nuclei 26 ranges 25 G gauss levels 44 G force indicator 15 17 Graphics hardware 35 GX graphics 35 H heat gun 41 helium contact with body 8 helium gas supply 40 cylinder requirements 40 magnetic helium gas container 40 purity requirements 40 helium refill volumes 27 helium supplies 39 helium liquid expansion ratio 26 high altitudes sites 27 high power amplifiers cautions 9 hoist 41 Infinityplus Installat
61. nimum of environmental magnetic fields Common sources of magnetic interference are fluctuating loads on adjacent power lines radio or television transmissions heavy duty transformers elevator motors and similar electromagnetic devices Allow a separation of at least 4 6 m 15 ft between the magnet and other high field electromagnets elevators or forklift trucks 01 999176 00 B1001 Infinityplus Installation Planning 23 Chapter 2 Installation Site Requirements Similar separation distances must also be maintained between the magnet and anything that can cause a detrimental effect on the field homogeneity or the structural integrity of the magnet Conditions that could interfere with the magnet include but are by no means limited to a wall with metal sheathing or steel studding a concrete support column with steel reinforcing bars and a storage area containing steel dewars for cryogenic storage Each site must be carefully analyzed to ensure optimum performance of the system See Table 8 for examples of objects that affect or are affected by the magnetic field Stray field data for radial and axial distances for each magnet are given in Table 23 Table 8 Interaction Between a Magnetic Field and Common Objects Magnetic Field Objects That Affect the Magnetic Field 15 gauss line or closer 5 to 15 gauss All ferromagnetic construction materials except small amounts of steel reinforcing bar normally not exceeding 11 kg m 2
62. nn ufalonand Periphefal iui 36 Collecting System and Network Information ii 36 Chapter 4 Installation Supplies nes 39 4 1 Required Installation Supplies and Equipment _ i 39 Liquid Heluim Supply uc aa 40 Liquid Nitrogen Supply sila 40 HEN GE SUP see 40 Nitrogen Gas Supply for Magnet Installation n 41 Face Mask nd Thermal COVES iaia 41 TE RE ii ii RR NS 41 NonterroniasnenciLadder urine 41 LE KG EE E E RR re SE 41 Isopropyl Alcohol and Acetone Solvents i 42 4 2 Recommended Laboratory Supplies and Equipment 42 Cryogenie Equipment Rack 42 Electrical Power Surge Protector arie 42 Monitor Degaussing Goil sus minimale 42 Chapter 5 Stray Magnetic Fields 43 5 1 Safety Hazards of Strong Magnetic Fields i 43 Pacemakers cicala die 43 Magnetic Field Exposure 44 5 2 Str y Field PIOtS siii 44 5 3 Posting Requirements for Magnetic Field Warning Signs i 51 KE SE NE lia ta 51 Chapter 6 Room Layouts incinta 53 Minimum Space for 2300 89 Systeri iii 54 Recommended Room Layout for a 300 89 System ii 55 TMS PAGS Or ROOM LAYOUT i 56 Blank Grid for Room Layout li ao 57 li RER re eee ee re re 59 4 Infinityplus Installation Planning 01 999176 00 B1001 List of Figures Figure 1 Infinityplus Cabinet and Oxford Magnet 11 Figure 2 Plan Views of Floor Contact Point
63. nserting and removing the helium transfer tube The ladder should be sturdy and self supporting with rubber feet A somewhat taller 250 to 300 cm 8 to 10 ft ladder is recommended for 800 MHz magnets Hoist Consult Varian Installations to determine if Varian will provide a hoist A hoist must be available to remove the magnet from the crate assemble it and move it into place The capacity of the hoist depends on the weight of the magnet being installed Table 5 on page 20 specifies magnet weights Allow a safety factor of at least 100 above the weight 01 999176 00 B1001 Infinityplus Installation Planning 41 Chapter 4 Installation Supplies shown Be sure adequate space is available for bringing the hoist and magnet in through the lab door WARNING Death or serious injury may result if the magnet is lifted with improperly assembled or improperly rated equipment The hoist can be a chain hoist suspended from a moveable mechanism such as an A frame or it can be permanently fixed above the area designated for the magnet such as a beam A vertical lifting device is required for magnets with anti vibration legs this vertical lifting device would eliminate the need for a cherry picker type device Consult your plant facilities department or authorized Varian representative to ensure that adequate facilities are available Isopropyl Alcohol and Acetone Solvents Obtain 1 pint 500 cm each of isopropyl alcohol and acetone Thes
64. on or design Varian does not assume any liability arising out of the application or use of any product or circuit described herein neither does it convey any license under its patent rights nor the rights of others Inclusion in this document does not imply that any particular feature is standard on the instrument Infinityplus is a trademark of Varian Inc Sun and the Sun logo are trademarks of Sun Microsystems Inc SPARC and SPARC station are trademarks of SPARC International Tygon is a trademark of DuPont Company Ethernet is a trademark of Xerox Corporation Oxford is a registered trademark of Oxford Instruments Ltd Other product names are trademarks or registered trademarks of their respective holders Table of Contents SAFETY PR CAUTIONS es iaia 7 pe Te iii 11 Chapter 1 Site Selection and System Delivery 13 1 1 Installation Planning Process iii 13 LA Ste Sel cti n cca lio iaia 14 1 3 Transport Route and System Shipping Dimensions ii 15 1 4 System Shipment sura 16 Selecting a Local Shipping Company ss 16 Postdelivery Inspection cusiria iaia aa 16 Chapter 2 Installation Site Requirements s rrnnnnnvnnnnnnnvvnnnnnnnnnnnnnnnvnnnnnnnnnen 19 LI SES ila a 19 2 Accessibility OL SHE siii 20 2 3 Ceiling Height Requirements eee eeeeeceeeeeceeeeseeseseesseeaesseseeeeesseeeeeaes 21 2 4 Structural Strength of Floor 21 Magnet Weight Distribution With
65. ons Because the magnetic field exists both horizontally and vertically the effect of the field on persons electronic equipment computers and other objects located above and below the magnet must be considered Pacemaker hazard and other signs warning that a magnetic field is present may be needed in the space on the next floor above the magnet and on the floor below the magnet Figure 4 shows the typical elliptical profile of the vertical axial stray magnetic fields for the 400 500 600 750 and 800 MHz magnet systems drawing is not to scale Refer to Section 5 2 Stray Field Plots on page 44 for stray magnetic field values Table 24 lists the distances from the magnetic field centerline to the floor Infinityplus Installation Planning 01 999176 00 B1001 2 8 Radio Frequency Interference In Band Combining that data with the data in Table 23 allows you to determine how far the fields extend above your ceiling and below your floor t Typical 5 gauss Centerline to vertical zone 5 gauss see Table 23 eni on page 45 ypical 10 gauss vertical zone Centerline to 10 gauss see Table 23 on page 45 Magnet room floor v Centerline to floor see Table 24 on page 45 WM Jd Figure 4 Typical Vertical Stray Fields for High Field Magnets 2 8 Radio Frequency Interference In Band The site should be checked for radio Table 9 Operating Frequencies for frequency interference rfi at o
66. or 23 vibration in floor measurement 23 voltage variations 29 VT CP MAS Module electrical outlets 31 Ww warning signs 51 warnings defined 7 work table 20 workstation preparation 34 world time zones 38 X X server software requirements 36 Y ypcat command 38 ypwhich command 38 Infinityplus Installation Planning 61 Index 62 Infinityplus Installation Planning 01 999176 00 B1001
67. otal which creates relatively high point loading This loading is only a concern if the floor covering is soft 01 999176 00 B1001 Infinityplus Installation Planning 21 Chapter 2 Installation Site Requirements A B Ro 40 cm 15 75 in R 27 3 cm R 32 7 cm 12 875 in konst 10 75 in een 5 in annular O D base p Magnets Magnets with antivibration tires 200 89 200 89 300 89 300 89 400 89 400 89 LH magnets 400 89AS Figure 2 Plan Views of Floor Contact Points of Magnet Stands Magnet Weight Distribution With Antivibration System This section describes weight distribution for magnets installed with antivibration systems Magnet weights including stands and antivibration systems are listed in Table 5 200 89 300 89 400 89 500 89 600 89 and 800 63 magnets The antivibration system for these magnets consists of dampening equipment integrated into the magnet legs All of these magnets are supported by three legs as illustrated in Figure 3A Figure 3B and Figure 3C i kast B 3 leg pads on floor eg pads on floor 36 8 x 27 9 cm 14 5 x 11 in per LL pr R 50 cm 7 DAG 19 72 in R inside 41 a inside oo 2 N Nus 89 cm 35 in i 600 89 Magnet 7 800 63 oa N amp C 3 leg pads on floor 33 0 x 36 8 cm 13 x 14 5 in Ss p ka ii 7 R es 44 7 cm 17 6 in Magnet 500 89AS Figure 3 Magnet Leg Antivibration
68. owing warning and caution notices illustrate the style used in Varian manuals for safety precaution notices and explain when each type is used WARNING warnings are used when failure to observe instructions or precautions could result in injury or death to humans or animals or significant property damage CAUTION Cautions are used when failure to observe instructions could result in serious damage to equipment or loss of data Warning Notices Observe the following precautions during installation operation maintenance and repair of the instrument Failure to comply with these warnings or with specific warnings elsewhere in Varian manuals violates safety standards of design manufacturing and intended use of the instrument Varian assumes no liability for customer failure to comply with these precautions WARNING Persons with implanted or attached medical devices such as pacemakers and prosthetic parts must remain outside the 5 gauss perimeter from the centerline of the magnet The superconducting magnet system generates strong magnetic fields that can affect operation of some cardiac pacemakers or harm implanted or attached devices such as prosthetic parts and metal blood vessel clips and clamps Pacemaker wearers should consult the user manual provided by the pacemaker manufacturer or contact the pacemaker manufacturer to determine the effect on a specific pacemaker Pacemaker wearers should also always notify their physician and
69. r countries For a list of Varian offices see Contacting Varian on page 12 52 Infinityplus Installation Planning 01 999176 00 B1001 Chapter 6 Room Layouts This section provides some suggested NMR room layouts The illustrations in this section are drawn approximately to scale When designing room layouts be sure to account for horizontal radial stray fields that can extend beyond the walls and vertical axial stray fields that can extend above the ceiling and below the floor Refer to Section 5 2 Stray Field Plots on page 44 for actual stray field plots for your magnet Refer to Figure 6 on page 46 through Figure 12 to find the stray field for your magnetic field strength and scale the layout accordingly 01 999176 00 B1001 Infinityplus Installation Planning 53 Chapter 6 Room Layouts Minimum Space for a 300 89 System The room dimensions are about 4 7 m x 5 5 m 15 5 ft x 18 2 ft The Infinityplus cabinet is 111 cm x 78 cm 44 in x 31 in The high power amplifier cabinet is 55 cm x 78 cm 22 in X 31 in each The accessory cabinet is 56 x 79 cm 22 in x 31 in Typical table size is 178 cm x 152 cm 70 in x 60 in The magnet is 69 cm x 69 cm 27 in x 27 in A distance of 1 m 3 ft should be maintained around the standard cabinet The magnet should be at least 0 6 M 2 ft from the wall Varian Inc does not recommend using minimum space configurations due to the presence of stray fields greater
70. r near the NMR Spectrometers operating frequencies of the spectrometer listed in Table 9 and most common nuclei Proton Frequency Frequency Range listed in Table 10 The level of any MHz MHz interference should be attenuated to an electrical field strength of less than 150 UV 200 12 to 215 m at the site of the magnet Interference or 300 12 to 325 cross talk often occurs when two 400 12 to 430 spectrometers are located in the same room 500 12 to 538 referenced to the same power system or 600 12 to 645 operating at the same frequency 750 12 to 807 to 800 12 to 860 01 999176 00 B1001 Infinityplus Installation Planning 25 Chapter 2 Installation Site Requirements Table 10 Operating Frequencies for Common Nuclei 4 6975 7 0463 9 3950 11 744 14 092 17 616 18 790 Nuclei Tesla Tesla Tesla Tesla Tesla Tesla Tesla IH 199 75 299 75 399 75 499 75 599 75 749 75 799 75 VF 18791 282 00 376 07 470 15 564 23 705 34 752 38 31p 81 96 121 34 161 82 202 30 242 78 303 50 323 74 13c 50 22 75 36 100 51 125 65 150 80 188 56 201 09 295 39 68 59 55 79 41 99 28 119 14 149 98 158 87 2H 30 66 46 01 61 36 76 71 92 06 115 09 122 77 ISN 20 24 30 37 40 51 50 64 60 77 76 97 81 04 39K 9 32 13 99 18 65 23 32 27 99 34 99 37 32 2 9 Ventilation Air ventilation must be adequate to displace Table 11 Liquid Helium Displacement for the liquid helium gas during a quench Room Ventilation Considerations Gaseous helium or nitrogen ex
71. r varians Ree ie Fe variane Figure 13 10 Gauss Warning Sign Figure 14 5 Gauss Warning Sign Amm STRONG MAGNETIC AND RADIO FREQUENCY FIELDS ARE PRESENT Magnetic Media and Tools and Equipment ATM Credit Cards Strong magnetic fields are Strong magnetic fields are present that could erase present that could make some magnetic media such as magnetic items suddenly fly floppies and tapes disable ATM towards the magnet body which and credit cards and damage could cause personal injury or some watches serious damage Do not take such objects closer Do not take tools equipment to the magnet than the or personal items containing 5 GAUSS WARNING signs steel iron or other magnetic materials closer to the magnet than the 10 GAUSS WARNING signs Pub No 87 250801 00 BO694 Magnet Area Entrance Danger Sign Figure 15 Magnet Area Danger Sign Stray magnetic fields can reach beyond the published distances when two or more magnetic fields intersect or when the field extends over large ferromagnetic masses or structures steel doors steel construction beams etc In this case the customer must measure the stray field using a gaussmeter to determine how the 5 and 10 gauss fields are altered contact a scientific instrumentation supplier for information on acquiring a gaussmeter You can request additional signs from Varian by telephoning 1 800 356 4437 in the United States or by contacting your local Varian office in othe
72. s of Magnet Stands i 22 Figure 3 Magnet Leg Antivibration Systems Leg Placement and Sizes in 22 Figure 4 Typical Vertical Stray Fields for High Field Magnets i 25 Figure 5 Setup for Switching Gas Supplies i 32 Figure 6 Stray Field Plots for 200 89 Magnets iii 46 Figure 7 Stray Field Plots for 300 89 Magnets ii 46 Figure 8 Stray Field Plots for 400 89 Magnets iii 47 Figure 9 Stray Field Plots for 400 89 AS Magnets 47 Figure 10 Stray Field Plots for 500 89 AS Magnets i 48 Figure 11 Stray Field Plots for 600 89 Magnets ii 49 Figure 12 Stray Field Plots for 800 63 2 2K Magnets iii 50 Figure 13 10 Gauss Warning Sign sens 52 Figure 14 5 Gauss Warning Sign ss 52 Figure 15 Magnet Area Danger Sign iii 52 5 Infinityplus Installation Planning 01 999176 00 B1001 List of Tables Table 1 Magnet Dimensions as Shipped with Crate and Pallet 15 Table 2 Cabinet Dimensions as Shipped with Crate and Pallet ii 15 Table 3 System Accessories Dimensions as Shipped with Crates and Pallets as Appropriate 16 Table 4 Infinityplus Cabinets Dimensions and Weights ii 19 Table 5 Magnet Dimensions with Stand or Legs Attached ii 20 Table 6 System Accessories Dimensions
73. t to quench 01 999176 00 B1001 Infinityplus Installation Planning 39 Chapter 4 Installation Supplies Liquid Helium Supply To prevent unnecessary loss of the a Table 19 Initial Onsite and Short Notice Liquid supply request delivery just prior to the scheduled visit of the Varian installation Heine Supplies engineer Table 19 lists the amount of liquid helium LHe recommended at Magnet Bore Initial Supply Short Notice inetalletion MHz mm liters Supply liters The amount of loss due to boiloff as the 200 89 300 200 magnet is cooled varies An initial LHe 300 89 300 200 supply about 50 more than the amount 400 89 300 300 expected to be necessary for cooling 400 89 AS 300 300 down the magnet is usually adequate 500 89 AS 1000 600 however an additional supply for Von 600 89 1000 600 delivery on short notice is also advisable should the initial amount be insufficient 800 63 2 2 K 3000 1000 Table 19 shows the quantities recommended Liquid Nitrogen Supply Table 20 Initial Onsite Liquid Table 20 lists the recommended amount of liquid Nimogeh supply nitrogen LN LN storage containers suffer a M ar Initial Suppl loss of contents from boiloff so request delivery pe Ge SURRE pe MHz liters of the supply just prior to the scheduled visit of the installation engineer Provide an adaptor for 200 89 325 connecting 9 mm 3 8 in ID rubber tubing to 300 89 325 the LN container 400 89 325 For low
74. t vary by more than 0 5 to 1 0 Hz Installing a line conditioner and regulator is strongly recommended By providing protection against transients and improving line regulation total system up time improves and the electronic components within the system last longer In many locations 01 999176 00 B1001 Infinityplus Installation Planning 29 Chapter 3 Site Preparation a good power conditioning system can pay for itself within a few years Contact a local power consultant for suitable equipment in your area 3 2 Uninterrupted Power Supply If your site experiences frequent and short less than 10 minutes power outages you should consider installing an uninterrupted power supply UPS UPS systems are limited in how long they can supply power when house power is out Consider the placement of a UPS when planning your lab If you want to use a single UPS it must have output for 220 Vac and 120 Vac and it must be installed such that both the NMR console and the host workstation can use it If the UPS does not provide a 220 Vac output use a step up transformer to boost the 208 Vac output to 220 Vac You can purchase an autotransformer from Varian Part No 01 901886 00 Due to the large current draw solids systems often require more than one UPS which may also need an autotransformer To determine the power rating for the UPS in kW refer to Table 16 on page 33 and add the values KW for the accessories with your system 3 3
75. the host workstation This telephone enables interactive troubleshooting between the customer and Varian support personnel Varian also strongly recommends that Internet access be provided during and after system installation By providing external access to the spectrometer technical problems can be 01 999176 00 B1001 Infinityplus Installation Planning 33 Chapter 3 Site Preparation quickly analyzed by the engineering and scientific staff at Palo Alto After the system is installed applications related questions can be answered in real time by Varian s NMR applications people As a matter of policy Varian provides online support during installation and during the warranty period If direct access to the Internet is not technically feasible a high quality analog telephone line can be used If internal security policies preclude ready modem or Internet access to the spectrometer contact Varian s installation department for a list of options that might satisfy security concerns 3 9 Electrostatic Discharges Electrostatic discharges less than 15 kV generally do not result in any perceivable errors or problems Discharges greater than 15 kV however might result in loss of data and errors perceivable to the operator Discharges greater 25 kV can cause damage to the equipment To prevent electrostatic discharge damage the system should be installed on vinyl covered floors and be properly grounded If carpeting is installed the carpet
76. thods that will be used See Table 1 Table 2 and Table 3 for dimensions and weights of major system components Contact the shipping company locally about the service usually rendered If moving equipment will be required at the site obtain help from the plant facilities department or an outside moving service Sea freight or motor freight without air cushion suspension is not recommended for long distance delivery of systems Postdelivery Inspection When the system is delivered follow the instructions below to inspect for shipping damage before moving the crates Do not open any crate CAUTION Do not open any crate except with direct instructions from an authorized Varian service representative In particular the crate containing the magnet has components that could be irreparably damaged if opened incorrectly 16 Infinityplus Installation Planning 01 999176 00 B1001 1 4 System Shipment 1 Upon delivery check for shipping damage but do not open any shipping crates except with direct instructions from an authorized Varian service representative Examine crates for shipping damage and document any apparent damage as follows Note the nature of the damage on the carrier s waybill b Request an inspection and written damage report by a representative of the carrier c Contact the insurance company d Forward a copy of the damage report to the local Varian representative In case of damage the FOB block on the Varian Order
77. tic storage media hard disk streaming magnetic tape cartridge etc must be located at a sufficient distance from the magnet such that the magnetic field cannot damage the data For a Sun workstation this specification is less than 5 gauss The distances at which this gauss level is present are different for each kind of magnet and must be taken into account when planning the room size See the field plots in Section 5 2 Stray Field Plots on page 44 for typical distances Infinityplus Installation Planning 01 999176 00 B1001 3 10 Sun Workstation Preparation at which various gauss levels exist for particular magnets but be aware that these distances vary somewhat for each magnet and should be checked after a magnet is installed Sun Workstations Infinityplus spectrometers Table 17 Host Computer Requirements require a Sun host computer that meets the requirements Ite Requirement listed in Table 17 m Er EE EE Host computer Sun Ultra 5 or better have at least 64 megabytes Solaris version Solaris 2 6 or later MB of RAM but 128 MB is RAM 64 MB minimum 128 MB recommended CDE requires preferred 24 MB of RAM Solaris and Hard disk 9 GB preferred 4 GB minimum Spinsight require a minimum Graphics 8 or 24 bit color total hard disk space of 3 GB Peripherals CD ROM drive is required Monitors can be any size Tape backup device recommended Graphics can be plain or the GX version the GX series provides higher p
78. trong magnetic and electromagnetic fields that can inhibit operation of some cardiac pacemakers which could result in death or serious injury to the user Consult the pacemaker user s manual contact the manufacturer or confer with a physician to determine the effect on a specific pacemaker Varian provides signs with each system to warn pacemaker wearers of this hazard Post the signs according to Section 5 3 Posting Requirements for Magnetic Field Warning Signs on page 51 Pacemakers Cardiac pacemaker wearers must not enter a zone that would subject a cardiac pacemaker to a magnetic intensity that could cause adverse effects In many instances this zone includes space on the floors directly above and or below the magnet For assistance in determining the effect of a system on pacemaker consult the pacemaker user s manual contact the pacemaker manufacturer or confer with a physician to determine the effect on a specific pacemaker Actual levels vary and should be checked after a particular magnet has been installed 01 999176 00 B1001 Infinityplus Installation Planning 43 Chapter 5 Stray Magnetic Fields Magnetic Field Exposure NMR workers are often exposed to high levels of static magnetic fields At this time no conclusive scientific evidence exists indicating adverse health effects at current exposure levels Current exposure levels are generally indicated as levels equal to or less than those in Table 22 Although so
79. usts for daylight savings time if appropriate Time zones are specified by name such as US Central Disk Layout Your Sun workstation must contain at least one hard disk drive 38 Infinityplus Installation Planning 01 999176 00 B1001 Chapter 4 Installation Supplies Sections in this chapter 4 1 Required Installation Supplies and Equipment this page 4 2 Recommended Laboratory Supplies and Equipment page 42 Certain supplies not provided by Varian such as helium and nitrogen supplies must be obtained by the customer before the Varian installation engineer can start the installation 4 1 Required Installation Supplies and Equipment The installation engineer will need the following non Varian supplies and equipment during installation Liquid helium supply Liquid nitrogen supply Helium gas supply Nitrogen gas supply Face mask and thermal gloves Heat gun Nonferromagnetic ladder e Hoist e Isopropyl alcohol and acetone Locating a reliable local source of liquid helium and nitrogen is particularly important As soon as possible after ordering a system make arrangements for an initial delivery and an ongoing supply of liquid helium and nitrogen CAUTION Specify that supply dewars be made of nonmagnetic materials A magnetic supply dewar next to the magnet can damage the magnet solenoid A magnetic supply dewar can also be pulled into the magnet possibly damaging the magnet or causing the magne
80. yplus accessory 1 90 132 Vac 15 A Operate in lower cabinet 190 240 Vac 15 A voltage range The console and each proton fluorine amplifier require a dedicated autotransformer i e step up transformer see Section 3 2 on page 30 30 Infinityplus Installation Planning 01 999176 00 B1001 3 4 Compressed Air Supply Host Workstation and Peripherals The host workstation and accessories require a minimum of two 120 Vac or one 220 Vac single phase power outlets Varian Inc provides a power distribution strip with six outlets If your location has ac voltages outside the specified voltage range in Table 14 you should check with your local Varian service center for power outlet requirements Locations with ac voltages over 125 Vac might need at least one step down transformer To minimize ground loop interference electrical outlets should all be on the same 20 A service Surge protection is strongly recommended Infinityplus Two Cabinet Console The standard two cabinet console requires a dedicated single phase continuous duty 220 Vac power line with 20 A minimum service for up to 4 channels Terminate this line within 3 m 10 ft of the center of the standard two cabinet console with a fused quick disconnect switch box or circuit breaker It is usually best to have the power duct on the left off to the side of the cabinet unless there is enough room to leave the console about three feet from the wall If there is room cent

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