ekspert™ ultraLC Systems Site Planning Guide
Contents
1. 19 inches 20 inches 151 5 Ib ekspert ultraLC 110 system 475 mm 500 mm 67 kg 147 Ib 69 kg with a cooled column oven 19 inches 20 inches 151 5 Ib ekspert ultraLC 110 HTC Configurations ekspert ultraLC 110 HTC 855 mm 500 mm N A 48 85 kg system 37 5 inches 20 inches 107 7 lb ekspert ultraLC 110 XL system 1030 mm 500 mm N A 61 35 kg with an uncooled column oven 46 5 inches 20 inches 135 3 Ib ekspert ultraLC 110 XL system 1030 mm 500 mm N A 64 85 kg with an cooled column oven 46 5 inches 20 inches 143 Ib ekspert ultraLC 110 HTS Configurations ekspert ultraLC 110 HTC 1138 mm 500 mm N A 50 85 kg system 48 6 inches 20 inches 112 1 Ib ekspert ultraLC 110 XL system 1313 mm 500 mm N A 63 35 kg with an uncooled column oven 57 6 inches 20 inches 139 7 Ib ekspert ultraLC 110 XL system 1313 mm 500 mm N A 66 85 kg with an cooled column oven 57 6 inches 20 inches 147 4 Ib ekspert ultraLC 110 XL Configurations ekspert ultraLC 110 XL system 330 mm 500 mm 58 kg 155 Ib 62 kg 136 Ib 13 inches 20 inches ekspert ultraLC 110 XL system 505 mm 500 mm 70 5 kg 155 Ib 74 5 kg with an uncooled column oven 20 inches 20 inches 163 5 Ib Site Planning Guide ekspert ultraLC Systems 13 of 18 Site Requirements Table A 1 System Footprint and Weight Continued System ekspert ultraLC 110 XL system with an cooled column oven Width 505 mm 20 in2. PAL HTX xt User Manual Installation and Operation 7 Note For regulatory and safety information for the ekspert ultraLC 110 and 110 XL a Note Ifthe site preparation tasks are not complete when the AB SCIEX Field Service Employee FSE arrives the scheduled installation will be postponed Customer Site Planner Responsibilities Select the desired configuration and verify that adequate space is available Refer to Site Layout Requirements on page 13 Provide all required electrical receptacles Refer to Electrical Requirements on page 15 Provide the required laboratory ventilation Refer to Ventilation Requirements on page 16 Provide a printer and the required software Refer to Computer and Software Requirements on page 16 e Verify that the requirements for the operating environment are met Refer to Environmental Requirements on page 17 e Provide the required solutions and laboratory equipment required to complete the installation Refer to Customer Supplied Reagents and Equipment on page 17 Complete the checklist in Site Planning Checklist on page 9 and return it to the Field Service Employee FSE scheduled installation date 4 Note The FSE will follow up the checklist is not received prior to the Site Planning Guide ekspert ultraLC Systems 7 of 18 Customer and FSE Responsibilities FSE Responsibilities e Review the checklist and discuss outstanding issues with the sit
3. and provided when the Cliquid software is purchased with an AB SCIEX mass spectrometer Triazine Standard Mixture AB SCIEX PN 4376887 Shipped separately from the system ekspert ultraLC Systems Site Planning Guide 18 of 18
4. ad 8 Chapter 2 Site Planning Checklist 0000 eee 9 Customer Information 0 0000 aaa 9 7 9 Comments 7 10 0 28 ka AZ and 1 clu M Te 7 11 Appendix A Site Requirements llllllll 13 Site Layout Requirements 2 6 0 0 cee ee RR n 13 Electrical Requirements 15 Protective Earth Conductor 000s 15 System Electrical Specifications ccc eens 15 Ventilation Requirements n eee 16 Computer and Software Requirements 0000 16 Environmental Requirements 17 Customer Supplied Reagents and Equipment 2 2055 17 Laboratory Supplied Requirements 00 17 AB SCIEX Supplied Requirements 18 Site Planning Guide ekspert ultraLC Systems RUO IDV 05 0862 A D5031371 C 5 of 18 Contents eksigent part of AB SCIEX ekspert ultraLC Systems Site Planning Guide 6 of 18 Customer and FSE Responsibilities This guide is for the site planner the individual responsible for preparing the facility for the installation of the ekspert ultraLC system systems refer to the ekspert ultraLC Systems Hardware User Guide For regulatory and safety information for ekspert ultraLC 110 HTC systems refer to the HTC PAL PAL HTC xt User Manual Installation and Operation For regulatory and safety information for ekspert ultraLC 110 HTS systems refer to the HTS PAL HTX PAL PAL HTS xt
5. 80 To 2000 m 70 db autosampler 50 F to 104 F ultraLC 110 HTC 4 C to 40 C 75 maximum To 3000 m 62 db autosampler 39 F to 104 F ultraLC 110 HTS 4 C to 40 C 75 maximum To 3000 m 62 db autosampler 39 F to 104 F ultraLC 110 XL 10 C to 40 C 20 to 80 To 2000 m 70 db autosampler 50 F to 104 F Pump 5 C to 40 C 20 to 80 To 2000 m 70 db 41 F to 104 F Column oven 5 C to 40 C 30 to 80 To 2000 m N A 41 F to 104 F Customer Supplied Reagents and Equipment Return to checklist Laboratory Supplied Requirements General equipment and consumables Disposable gloves Pipetting accessories pipettors and tips PEEK tubing 0 005 inch i d 1 16 inch o d red 4 meters or more and cutter Glassware Measuring cylinders 100 mL 1000 mL HPLC bottles 1000 mL e Glass autosampler vials 1 mL 1 5 mL or 2 mL Caps for all autosampler vials Consumables and Reagents Ammonium formate minimum 10 g MS grade methanol HPLC grade water Site Planning Guide ekspert ultraLC Systems 17 of 18 Site Requirements MS grade isopropanol MS grade acetonitrile AB SCIEX Supplied Requirements The following consumables are required for the HPLC MS system test and the Cliquid9 System Suitability Test They are supplied with Cliquid Phenomenex 00B 4424 B0 Synergi 4 um Fusion RP 80A 50 x 2 mm columns PN 4376878 Required for use with the Cliquid software
6. ches Length 500 mm 20 inches Weight Without Cooling 74 kg 162 5 Ib Table A 2 Weights and Dimensions of Individual Components With Cooling 78 kg 171 Ib cooled sample Equipment Height Width Length Weight ultraLC 110 autosampler 510 mm 300 mm 360 mm 19 kg 42 Ib 20 inches 12 inches 14 inches ultraLC 110 autosampler 575 mm 300 mm 360 mm 21 kg 46 5 Ib with cooling option 27 inches 12 inches 14 inches ultraLC 110 HTC 648 mm 545 mm 385 mm 16 85 kg autosampler with the 25 5 inches 21 5 inches 15 2 inches 37 1 Ib cooled sample compartment ultraLC 110 HTS 648 mm 828 mm 385 mm 18 85 kg autosampler with the 25 5 inches 32 6 inches 15 2 inches 41 6 Ib compartment ultraLC 110 XL 540 mm 330 mm 480 mm 26 kg 57 5 Ib autosampler 21 inches 13 inches 19 inches ultraLC 110 XL 620 mm 330 mm 480 mm 30 kg 66 Ib autosampler with 24 5 inches 13 inches 19 inches cooling option LC pump 120 mm 300 mm 500 mm 16 kg 35 Ib 5 inches 12 inches 20 inches Column oven optional 600 mm 170 mm 345 mm Without cooling 24 inches 7 inches 13 5 inches 12 5 kg 27 5 Ib With cooling 16 kg 35 Ib d Note Specifications for individual components does not include optional accessories Table A 3 Distances From To Maximum Distance Computer Auosampler Jl Note For optimum performa
7. e planner Supply all fittings plugs and cables required to connect the LC system to the electrical receptacles Setup ekspert ultraLC equipment sold and supported by AB SCIEX e Test the system to the specifications in the Data Log During Installation The FSE unpacks the system sets up the system and then confirms its operation After the system is set up the FSE performs installation tests Technical Support AB SCIEX and its representatives maintain a staff of fully trained service and technical specialists located throughout the world They can answer questions about the system or any technical issues that may arise For more information visit the web site at www absciex com ekspert ultraLC Systems Site Planning Guide 8 of 18 Site Planning Checklist Customer Information Organization Address City Country Telephone Site planner contact name E mail address Requirements Table 2 1 Site Planning Checklist Requirements Complete The site is not designated as BioSafety Level 3 BSL 3 or BSL 4 Site Layout Requirements Refer to Site Layout Requirements on page 13 The installation location can accommodate the equipment dimensions If the requirements cannot be met contact the FSE Electrical Requirements Refer to Electrical Requirements on page 15 An electrical outlet is provided for each component of the system aut
8. ekspert ultraLC Systems Site Planning Guide RUO IDV 05 0862 A December 2013 This document is provided to customers who have purchased AB SCIEX equipment to use in the operation of such AB SCIEX equipment This document is copyright protected and any reproduction of this document or any part of this document is strictly prohibited except as AB SCIEX may authorize in writing Software that may be described in this document is furnished under a license agreement It is against the law to copy modify or distribute the software on any medium except as specifically allowed in the license agreement Furthermore the license agreement may prohibit the software from being disassembled reverse engineered or decompiled for any purpose Warranties are as stated therein Portions of this document may make reference to other manufacturers and or their products which may contain parts whose names are registered as trademarks and or function as trademarks of their respective owners Any such use is intended only to designate those manufacturers products as supplied by AB SCIEX for incorporation into its equipment and does not imply any right and or license to use or permit others to use such manufacturers and or their product names as trademarks AB SCIEX warranties are limited to those express warranties provided at the time of sale or license of its products and are AB SCIEX s sole and exclusive representations warranties and obligat
9. for the Functional Tests are available Product Familiarization Obtain and review system documentation Go to www eksigent com Comments ekspert ultraLC Systems Site Planning Guide 10 of 18 Site Planning Checklist Exceptions Signoff Complete the checklist and return it to the FSE email specified below on or before the Return date Completion date yyyy mm dd acknowledge that all installation requirements as specified in this document have been met Return date yyyy mm dd Site Planner contact name FSE name 7 i O SE ema 7 Site Planning Guide ekspert ultraLC Systems 11 of 18 Site Planning Checklist eksigent part of AB SCIEX ekspert ultraLC Systems Site Planning Guide 12 of 18 Site Requirements Site Layout Requirements Return to checklist Note The site must not be designated BioSafety Level 3 BSL 3 or BSL 4 AB SCIEX does not install service or repair equipment in areas designated BSL 3 or BSL 4 Table A 1 System Footprint and Weight System Width Length Weight Without With Cooling Cooling ekspert ultraLC 110 Configurations ekspert ultraLC 110 system 300 mm 500 mm 51 kg 112 Ib 53 kg 12 inches 20 inches 116 5 Ib ekspert ultraLC 110 system 475 mm 500 mm 163 5 kg 139 5 Ib 69 kg with an uncooled column oven
10. ions AB SCIEX makes no other warranty of any kind whatsoever expressed or implied including without limitation warranties of merchantability or fitness for a particular purpose whether arising from a statute or otherwise in law or from a course of dealing or usage of trade all of which are expressly disclaimed and assumes no responsibility or contingent liability including indirect or consequential damages for any use by the purchaser or for any adverse circumstances arising therefrom For research use only Not for use in diagnostic procedures The trademarks mentioned herein are the property of AB Sciex Pte Ltd or their respective owners Eksigent is a division of AB Sciex LLC AB SCIEX is being used under license 2013 AB Sciex Pte Ltd Printed in Canada AB Sciex LLC 1201 Radio Road Redwood City CA 94065 USA ekspert ultraLC Systems Site Planning Guide 2 of 18 Revision History Revision Reason for Change Date December 2073 Site Planning Guide ekspert ultraLC Systems RUO IDV 05 0862 A D5031371 C 3 of 18 Revision History eksigent part of AB SCIEX ekspert ultraLC Systems Site Planning Guide 4 of 18 Contents Chapter 1 Customer and FSE Responsibilities 0 0202 00 7 Customer Site Planner Responsibilities 0 7 FSE Responsibilities 8 Du nng Installati n PPS 8 Technical SUDO dodo dde icol Re Rie debeo doe e d RU eere
11. nce make sure that the column outlet is as close to the ion source as possible ekspert ultraLC Systems 14 of 18 Site Planning Guide Site Requirements Electrical Requirements Return to checklist installation of all electrical supplies and fixtures and make sure that all A WARNING Electrical Shock Hazard Use only qualified personnel for the installations adhere to local bylaws Power surges line spikes and transient energy sources can impede instrument operation Ensure that the instrument s electrical supply is adequately protected from these conditions and includes a correctly installed protective earth conductor A qualified electrician must install or inspect the earth conductor before the system components are connected The system requires four electrical outlets one each for Autosampler e PumpA e PumpB Column oven optional The ultraLC 110 HTC and HTS autosamplers require an additional outlet for the cooled sample compartment a Note The AC mains supply cables provided with the ultraLC 110 HTC and HTC An autosamplers and their cooled sample compartment are 3 m 118 inches in length The cables provided with the other system modules are 2 5 m 99 inches in length If the power cables are too far from the AC mains supply outlet the customer must supply extension cords Protective Earth Conductor Return to checklist The mains supply must include a correctly installed pro
12. osampler pump A pump B and optionally the column oven The mains supply includes a correctly installed protective earth conductor Ventilation and Waste Collection Requirements Refer to Ventilation Requirements on page 16 Installation of plumbing and ventilation fixtures complies with local biohazard regulations and safety standards Ventilation of the laboratory environment in which the mass spectrometer will be used complies with local regulations and the air exchange rate is appropriate for the work performed Site Planning Guide ekspert ultraLC Systems 9 of 18 Site Planning Checklist Table 2 1 Site Planning Checklist Continued Requirements Complete Computer and Software Requirements Refer to Computer and Software Requirements on page 16 A network printer or a dedicated printer and necessary print drivers are available The Analyst 1 6 software or a later version is installed on the acquisition computer An account with Administrator privileges is available for the FSE Environmental Requirements Refer to Environmental Requirements on page 17 The ambient temperature and relative humidity meet the requirements for the individual components Materials Required for Routine Operation Refer to Customer Supplied Reagents and Equipment on page 17 All required LC equipment and supplies are available Consumables and reagents
13. por in excess of occupational exposure limits WARNING Potential Radiation Hazard Biohazard or Toxic Chemical Hazard Use only qualified personnel for the installation of plumbing and ventilation fixtures and make sure that all installations follow local bylaws and biohazard regulations The venting of fumes and disposal of waste must be in accordance with all federal state provincial and local health and safety regulations and that the air exchange rate is appropriate for the work performed per hour in laboratories Note Inthe United States OSHA 29 CFR Part 1910 1450 requires 4 to 12 air changes Computer and Software Requirements Return to checklist A network or dedicated printer including any necessary print drivers The ekspert ultraLC software requires the Analyst 1 6 software or a later version to be installed on the acquisition computer For requirements for the acquisition computer see the nstallation Guide for the Analyst software The FSE must be logged in to the acquisition computer with Administrator privileges to install the ekspert ultraLC software ekspert ultraLC Systems Site Planning Guide 16 of 18 Environmental Requirements Return to checklist Table A 5 Requirements and Specifications Site Requirements System Ambient Relative Humidity Altitude Noise Temperature non condensing Level ultraLC 110 10 C to 40 C 20 to
14. tective earth conductor that must be installed or checked by a qualified electrician before connecting the LC system components conductor Any interruption of the protective conductor is likely to make the A WARNING Electrical Shock Hazard Do not intentionally interrupt the protective installation dangerous System Electrical Specifications Table A 4 contains the electrical specifications for the HPLC system components s Note Specifications are subject to change without notice Contact your FSE for the Al latest specifications Site Planning Guide ekspert ultraLC Systems 15 of 18 Site Requirements Table A 4 Electrical Specifications System Power Nominal Input Frequency Consumption Voltage ultraLC 110 autosampler 200VA 950700240 50Hzor60Hz ultraLC 110 HTC autosampler 150 W 100 V to 240 V 50 Hz or 60 Hz ultraLC 110 HTS autosampler 150 W 100 V to 240 V 50 Hz or 60 Hz ultraLC 110 XL autosampler 450 VA 100 4 V 50 Hz or 60 Hz t 0 Pump 150 VA 100 V to 240 V 50 Hz or 60 Hz Column oven 550 VA maximum 115 V to 230 V 50 Hz or 60 Hz Ventilation Requirements Return to checklist WARNING Potential Radiation Hazard Biohazard or Toxic Chemical Hazard Make sure that the laboratory is equipped with adequate ventilation to maintain solvent vapor within local occupational exposure limits The use of an organic solvent as part of a rinse protocol may release solvent va
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