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Chrompack CP 9050 Liquid sampler manual

1. OM GS CER GT CD ON Mr The sampler loose the memory the sampler was without power a long time and the sampler has to stay one day with power on until the ballery the battery 15 discharged has more than 3 3 V m am roy SA JL JR GL 42 G 1_ di LL m Gm Gm Gm Cro Gm Gm CERO CORR RR CERTO RR EF UO UAR LL CHEM RD UAR EF GR EMO GR AS CT mo Gm Cm Cum 1 step 2 step 3 step 4 Step 5 188 5 step CURE push 3 x V screw and move the part A downstairs to distance 0 fix screw ATTENTION these steps are 10 do affer every syringe ch
2. 103013 103012 INJECTION HEAD SERIALNUMBER 10301 UP 001 9204 DESCRI SUPPLIER ae ra e g 498 eU ae Dt LATI e i E Sae tutto ovn exu nn 1 ttt Deme xat NO ML UM erat n TOURA ot Pole Te Ae m EP CP PART db ENS ER 001 5086 20 INJECTION UNIT BOARD 82 19013 001 5086 30 FLEX CABLE li POLE _ 103012 001 5386 CABLE WITH BOARD 81 1192764 7 INJECTION BOARD 3 INJECTION HEAD SERIALNUMBER 10070 10500 DOC 001 2004 ee NUMBER NUMBER j01 5086 20 INJECTION UNIT BOARD 82 FLEX CABLE 11 POLE 001 5086 10 CABLE WITH BOARD B1 001 5050 INJECTION BOARD 77 119395 7 SUPPLIER DESCRIPTION CP PART INJECTION HEAD SERIALNUMBER 10001 10069 DOC 001 9004F SUPPLIER DESCRIPTION c5 e 01 5046 20 INJECTION UNIT BOARD 32 001 5086 30 FLEX CABLE _ 001 5086 1 INJECTION BOARD Bi 103008 001 5090 INJECTION BOARD 3 103005 505300 REV 1 01 ar SEVERAL PARTS DOC E EE HE 5 al Let Mu sib O EE E NUM
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5. Installation 2 6 MOUNTING CONNECTING AN EXTRA RS232 PLUG AND CABLES IN THE CP 9001 2 GC For the 5232 communication with the DATA ACQUISITION SAMPLER sampler a 25 pin femaie RS232 connector with cabie has to be mounted next to the 25 pin female connector for e the data acquisition see Figure 2 3 NOTE case of an old CP 9901 two 3 mm holes have to be drilled in the mounting plate for the 25 pin pesgeesq connect The cable from the connector must be routed through the electronic compartment of the CP 9001 2 to the SATELLITES 5232 board and connected with the 5 pin plug at CM3 see Figure 2 2 A cable with 25 pin male connectors at both sides must be connected between Figure 2 3 Data Acquisition Sampler and the 25 pin sampler connector at the Satellite Connections back of the CP 9001 2 and the 9 pin connector at the back of the CP 9050 sampler marked Serial Use the 25 9 pins converter delivered with the instrument 4 case one or two have been installed the cable with he AS pin connector coming from the 9001 2 must be connected to the Pin connector at the CP 9050 sampler marked IN OUT C4 2 7 REPLACING THE STANDARD COVERS OF THE CP 9001 GC BY SAMPLER COVERS The eft hand cover over the flow controls mounted with two screws the middle cover over the detector and injector area mounted with two screws the hinges for the middie cover mounted with two screws each and
6. SPECIAL TOOL P N 794 Weld Equip Sales bv ANTISTATIC HELD SERVICE KIT __ S7OQAD HELMONDNL RAWING NUMBER DATE MEAM 31 04920 42225 16430 Telefax 31 04920 36222 M iT r 1 v 8 1 SECTION 8 PREVENTIVE MAINTENACE LIABILITIES SCHEDULES amp MAINTENEANCE PROCEDURES 8 2 INTRODUCTION 8 3 PREVENTIVE MAINTENANCE 8 4 MAINTENANCE PROCEDURES 505300 REV 1 00 m INTRODUCTION When properly maintained the CP9050 will provide years of troublefree operation To keep the CP9050 operating at its best performance and reliability it s very important that it receives preventive maintenance 505300 REV 1 00 PREVENTIVE MAINTENANCE Daily by end user Check septum and liner of injection port If required repiace septum and clean the liner of the injection port Check wash solvent empty waste vial if required Check the syringe contamination plunger movement and needle tip damage Before a first run after several hours of interrupted operation perform 3 5 wash cycles to condition the syringe Weekly by end user Check wash solvent and waste vial septa These septa are part of an effective syringe cleaning concept replace them regularly to avoid sample cross contamination Check syringe If require
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8. 1 1 1 R p mama r m Rs hs ian M JIS au E JopjouuJe 94 1145 7 d M3JIS dj SAJOS 1 3 TO A TR MM 2 ee ut NM m m n NEN m am m NE MES E r ma 5 3 ADJUSTING PROBLEMS WITH THE SAMPLER CONFIGURATION After installation and of repair or removing the sampler it s necessary to do the sampler configuration explicit the INJECTION POSITION and REFERENCE ADJUST Even after doing those adjustments it can happen that the syringe needle is not in the middle of the sample vial and or Wash Waste vial To solve this problem you must follow the flow chart describing the reference and wash waste adjustment Start Configuration mes Uxersmaniuai page 2 12 for details REFERENCE ADJUST Refer to the users manual 2 10 12 p SMPL penetration See usersmanual page 2 10 13 details Check if the syringe neadiae 15 positioned in the middie af the sample cap ee he meddle 7 Ha correct 5 correct 7 Tha example should corrected 2 t tha night This 12 adjust Try ta adjust the tray with the four inB
9. eMLOELAY TIME TIME START of sampler INJECTION Figure 3 4 Timing of seal opening in relation to syringe movement The pneumatically controlled seal of the must be opened before the syringe can enter the TP OCI The timing can be seen in Figure 3 4 The seal will be opened as soon as the syringe injection head reaches its position above the TP OCI and wili be closed when the syringe reaches the programmed injection depth In this way the seal is open for the shortest time possible The signal for opening the seal comes from the CP 9050 sampler a contact closure of a relay available via the in connector at 9050 sampler marked IN OUT This relay contact is wired M series with relay VLV 3 for a front and in series with relay VLV 4 for arear TP OCI Relays VLV 3 and VLV 4 are switched based on the dipswitch settings at the RS232 board presence of one or two TP OGIS Sampler activation Page 1 Line 12 SAMPLER 51 front or rear injection port With PRE INJECTION DELAY Second part of Page 4 Line 9 see Section 3 6 the time between reaching the injection depth and the injection can be programmed With POST INJECTION DELAY Second part of Page 4 Line 10 see Section 3 6 the time between the injection and the withdrawal of the syringe from the injection port can be programmed Good starting values for injection delays PRE INJECTION DELAY INJ DELAY 2s
10. and Revision 2 xx software Five important software modifications have been implemented with the release of software revision 2 xx for the CP 9001 In case of selecting the CP 9010 9050 sampler in Page 1 Line 12 a new set of Pages 4 and 8 will become visible In case of selecting a 940 941 sampler Page 4 and 8 are the same as in Software revision 1 b Baseline recording subtraction is not possible anymore Therefore Page 2 Line 3 and 4 show optional c Relevant Page 8 parameters VIAL RANGES METHODS plus some extra parameters of Page 7 AUTOSTART and RESTART TIME will be saved in EEPROM at the sacrifice of GC method 12 s a consequence only eleven GC methods can be programmed in Page 5 d Revision 2 xx software enables control of the temperature programmable on column injector TP OCI which is often used in combination with the CP 9010 or the CP 9050 automatic liquid sampler 505300 REV 1 00 3 8 1 3 8 Programming VLV EXT 1 or VLV EXT 2 in a Tx program will only disable the default START or STOP function of that relay In software revision 1 xx both default START and STOP functions were disabled in case VLV EXT 1 and or VLV EXT 2 had been programmed in a Tx program e 505300 REV 1 00 3 8 2 cae 3 10 Sampler in out connector Cable P N 738434 The and with the 2 pole connector is to contro TP OCI The other two wires shoukt only used for NOH integrated istand alone sampler
11. g L05 GONG Y PEE fy OOM YEH SLOHIS EL 2 4 SCHO40 472 54 7 mit F hrungs ed SCHO amp amp auf 01 Spiel abgestimti A 3 2 DIN 125 2 195 CS QN A 2 5 DIN Q34 A 2 10 DIN 912 DIN 439 2 nm Rm ee 1534 RN RR RTT 1 3955 eec B Exo ae 20 DIN 912 2 Ir 4 ols la 054 002 054 M3x5 DIN 965 2 1 a M M B4 M IN 912 y rm x Um 812 2 mum o mm T GO 4 5 LLL 32 125 AZ M3 DIN 834 EL Raw L R8 045 9 44 5286 191 ruck eder ind J 3 2 BIN 6797 2 baxs DIN 912 42 VKM 13052 Gutekunst M3 DIN 034 4A2 5088 3 2 DIN 125 2 M3x8 DIN 965 A2 3 6 DIN 312 42 M3 DIN 934 2 014125 Typ 03 03036 DIN125 Typ 03 031046 SCHOSS8 SCHOS35 8046 O27 M2 5x3 OIN 913 AZ DIN 912 4A2 5 DIN 6798 DOSO M3x8 DIN 812 4A2 M3x6 DIM 9g12 4A7 S TON d qe SCH O41 Gewinde in Teil SCHO45 n B engeklebt DIN 705 A2 SCHOS9 M2 5x3 DIN 813 42 042 0 52 97 Gefestiqungsschelle M 2 4 0 51 3 DIN S65 A7 934 A72
12. If a programmed vial range is processed a in front of the line number of that vial range will mark that condition When resetting the CP 9001 2 LINE 10 RESET 0 these marks disappear if ali programmed injections were done so all programmed vial ranges will be completed and have in front of ail vial ranges restarting the CP 9001 2 by pressing the START key or the START RESET button starts the sampler all over again with the first injection of the first vir u of the first programmed vial range 3 12 CHROMPACK Operation NOTE NOTE NOTE NOTE 9050 AUTOMATIC LIQUID SAMPLER In case a sampler GC run is stopped after one or more injections were done and one wants to start all over again the CP 9001 2 must be reset LINE 10 RESET 0 otherwise the sampler continues with the next injectioni in case a vial range is changed or just pressing three times ENTER after selecting a vial range by selecting LINE X the CP 9001 2 will be reset in the same way as with LINE 10 RESET 0 The programmed values for VIAL RANGES and coupled METHODS are stored in EEPROM Switching the CP 9001 2 off and on again makes the last programmed values active again LINE 8 PRIORITY PRIORITY SAMPLE During a sampier GC run a priority sample can be programmed Enter the viai number for the priority sampie followed by a decimal point and the method number to be used with that priority sample Exam
13. NUMBER 001 9204 INJECTION HEAD 02753 2 2 7 Di m olt oc 1 001 5073 CABLE ARM ASSEMBLY BASE BODY 001 5286 CABLE INJ HEAD BASE BODY 102764 REAR VIEW SERIAL 4 10129 10300 DOC 001 1002 A SUPPLIER O 001 9004 INJECTION HEAD 1 001 9003 ARM ASSEMBLYO1 9003 N DESCRIPTION gt t M C 001 9202 BASE BODY 001 5073 A CABLE ARM ASSEMBLY BASE BODY 001 5286 10 CABLE INJ HEAD BASE BODY N C 22505300 1 01 REAR VIEW SERIAL 10070 10128 DOC 001 1002 SP ee mO to a i e t EE 5 ow d E sa a t SV II e 207 t fuu t Qo ort U VU 4 Yee Do Ptol Dae Rows 1 t DORDE ye nif c 2 Et tot oon T E 7 Ula DIEM CAT FoU aet htt DUM x 1 ect UN X nz ata T F t Tan Sra 3 2 Po 27 001 9004 INJECTION HEAD 102752 001 9003 ARM ASSEMBLY01 9003 001 9002 BASE BODY CABLE ARM ASSEMBLY BASE BODY 001 5286 10 CABLE INJ HEAD BASE BODY 102763 FRONT VIEW SERIAL 10001 10069 DOC 001 1000F SUPPLIER NUMBER DESCRIPTION ALS CP AUTOSAMPLER SERIAL 30301 UP DOC 001 1202 2 SU
14. LINE 3 CLEAN SLV NUMBER OF PRE INJECTION SOLVENT CLEAN FLUSHES 0 99 default 0 This parameter specifies the number of times the syringe 5 washed with soivent before sampling PRE INJECTION SAMPLE CLEAN FLUSHES and or FILL STROKES NOTE filling the needie with solvent before sampling one can compensate for needle dead volume PRE INJECTION SOLVENT CLEAN FLUSHES gt 0 In that case PRE INJECTION SAMPLE CLEAN FLUSHES and FILL STROKES must be set to CHROMPACK 3 9 ome CP 9050 AUTOMATIC LIQUID SAMPLER NOTE NOTE Operation LINE 4 SOLV PLUG SOLVENT PLUG 0 5 in steps of 0 1 pi default 0 pi SOLVENT PLUG R PLUG will be used in the so called sandwich injection technique where soivent and sample be separated by an air plug With PRE INJECTION SOLVENT CLEAN FLUSHES one can get a solvent plug with the volume of the while here the SOLVENT PLUG programmed solvent volume programmed value plus the needle volume When using a SOLVENT PLUG the conditions PRE INJECTION SAMPLE CLEAN FLUSHES 0 FILL STROKES 0 must be fulfilied not possible to enter a value for this parameter RANGE blinking check the above mentioned conditions Bo not program a total volume INJ VOL AIR VOL SOLV PLUG AIR PLUG which is bigger than the total syringe volume LINE 5 AIR PLUG AIR PLUG 0 5 in steps of 0 1 defauit 0 pi AIR PL
15. Number of pre injection solvent clean flushes 0 99 Number of pre injection sample clean flushes 0 99 Number of fill strokes 0 99 Fill volume for fill strokes 0 5 0 10 Number of post injection solvent clean flushes 0 99 Injection port front rear Air plug after sample 5 0 10 Sandwich solvent and air plug before sample 0 5 0 10 6 3 1 6 3 nm CP 9050 AUTOMATIC LIQUID SAMPLER Feature Specifications Viscosity delay 0 8 3 5 Plunger speed during filling 0 1 25 5 pl s cene Plunger speed during injection 0 1 25 5 ml s Status information CP 9001 2 Method storage capacity Output control signals Power 7 Line voltage Frequency Dimensions x x d weight 505300 REV 1 00 Pre injection delay 0 25 5 Post injection delay 0 25 5 51 Free programmable vial ranges 1 7 can be coupled with GC methods 1 11 Priority sample position 1 105 analyzed with programmed GC method 4 11 Warning limit for plunger stroke counter 0 9800 Septum counters ifront and rear Programmed and actual plunger stroke count Humber of sampled vial Actual injection per vial Active GC method Completed vial range 9 sets of sampler parameters battery backup CP 9110 TP OCI Control relay 40 V max 110 240 V 50 or 60 HZ 60 x 40 x 25 8 Specifications are subjects to change 501749 6 3 2 S
16. See Figure 1 1 and 1 2 for details The Injection Head s function is to transport liquids either from vial to viai or from vial to the injection port of the GC The Injection Head carries the syringe and provides the two essential movements of the syringe Lowering the syringe to let the needle pierce the septum of the vial until the tip is well submerged into the vial s liquid Moving the plunger up and down for taking and dispelling liquids The syringe carrier holds the syringe the syringe itself is locked by the syringe fixing lever while the head of the plunger is fixed by a screw loaded plunger holder The needle guide pushed down by springs holds the needle of the syringe and centers the needle in the septum cap of the injection port it also functions as sample vial detector The njection Head is fastened to the crossrail by two hex screws These two screws can be reached by mounting holes in the back wall of the injection head There is one electrical flat cable connection between Injection Head and Crossrail and one electrical flat cable connection between Crossrail and Instrument Base Unit The Crossrail provides the movement of the Injection Head from solvent and waste vial along the sample tray to the injection port s For the adjustment of the injection point the crossrail has to be moved towarts the iniector s till the Syringe Carrier can easily reach the used
17. 1 Resets the front injection septum counter to zero After changing the septum of the front injection port the septum counter must be reset In case of a temperature programmed column injection port TP this counter can be used to see if cleaning of the TP is needed or if the seal must be replaced CHROMPACK 3 13 came CP 9050 AUTOMATIC LIQUID SAMPLER Operation NOTE NOTE 3 8 2 Resets the rear injection septum counter to zero After changing the septum of the rear injection port the septum counter must be reset In case of a TP this counter can be used to see if cleaning of the TP is needed or if the seal must be replaced 3 Resets the plunger stroke counter to zero After cleaning replacing a syringe the plunger stroke counter must be reset RESET oniy works in non run model This might also be a good time to change the Snap cap with septum on the Waste and Solvent viall STATUS INFORMATION PAGE 8 AND STATUS PAGE The second part of 8 shows up after pressing RUN CONTROL SAMPLER tront rear SEPTUM 0 0 SET PL COUNT ACT PL COUNT VIAL INJ VIAL ACT ACTIVE METHOD This Page contains status information Most information is updated after an injection SEPTUM INJECTION COUNTER as a reminder for exchanging a septum Septum counters for front and rear injection port are given After every injection the septum counter of the injectio
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19. CHROMPACK CP 9050 Automatic Liquid Sampler Reference Manual CHROMPACK Herculesweg 8 P O Box 8033 4330 EA MIDDELBURG The Netherlands Tei 31 118 671000 Fax 31 118 633118 a a 6 505299 REV 02 BTW CONTENTS OF THIS MANUAL SECTION 0 SAFETY PRECAUTIONS SECTION 1 INTRODUCTION SECTION2 INSTALLATION SECTION 3 OPERATION SECTION 4 MAINTENANCE SECTIONS TROUBLE SHOOTING SECTION 6 ORDERING INFORMATION INDEX Safety information SECTION 0 SAFETY INFORMATION 0 1 Safety information 0 2 General safety precautions om machen Rap m 22 oH ko s ge nt mo can IC C ET CP 9050 AUTOMATIC LIQUID SAMPLER Page 0 3 0 4 CHROMPACK Safety information CP 9050 AUTOMATIC LIQUID SAMPLER 0 4 WARNING a d E HX a 2 Y LI 4 b SAFETY INFORMATION In accordance to Chrompack s commitment to customer service and safety this instrument and its accompanying documentation complies with the CE NEN 5509 specifications To prevent any injury to the user or any damage to the instrument it is essential that you read the information in this chapter If this manual is not in your mother language and if you have problems understanding the text we advise you to contact your Chrompack office for assistance Chrompack cannot accept responsibility for any damag
20. Mark those dimensions on the new to mount crossrail and then loosen the Allen head screws at position A and B in order to remove the legs To mount the replacement crossrail proceed in reverse order through the steps 505300 REV 1 00 3 7 1 eco 3 7 After replacing the crossrail special attention should be paid to the alignment of the sampler on the GC Check the injection positions and the WASH WASTE vial positions in the same way as done during the first installation For a better sliding of the injection head you can put some grease on both the square sliding bars inside the crossrail DX MOLYKOTE grease P N 084202 IMPORTANI NOTE After exchanging mechanical or electronically parts it s mandatory to set the configuration parameters See usermanual page 2 8 505300 REV 1 00 3 7 2 3 8 Chromatograph Software changes The Chrompack CP 9001 GC has two different software versions available 1 Revision 1 xx a 940 941 One shot samplers and b 910 911 Automatic Liquid samplers 2 Revision 2 XX a 940 941 One shot samplers and CP 9010 Automatic Liquid sampler c CP 9050 Automatic Liquid sampler NOTE The Chrompack CP 9002 GC is standard equipped with software to control 940 941 One shot samplers and the CP 9010 9050 Automatic Liquid Samplers There is no special software required The ALS 910 911 samplers are no longer supported by this software Comparison between Revision 1
21. Volume Injections per vial Installation Installing a syringe Instrument Base Unit Introduction K Keyboard locking L Last vial M Maintenance Method parameters Motor speeds Mounting the sampler N Normal injection Number of injection points 0 On column injector Operating hints Operation Options special sampler parameters Ordering information 3 14 2 8 2 14 2 12 2 14 3 8 3 10 3 7 3 7 3 19 2 1 2 9 1 1 3 6 3 20 3 12 4 3 2 23 2 17 2 7 CHROMPACK CP 9050 AUTOMATIC LIQUID SAMPLER INDEX P Plunger count 3 14 Start signal source 2 11 2 12 Plunger count warning limit 3 13 Status information 3 14 3 15 Plunger speed 3 10 Summary of programming 3 20 Plunger stroke counter 2 13 Symptom Post injection delay 3 11 Air bubbles 5 5 Post injection solvent clean flushes 3 8 Cross contamination 5 5 Post injection time 3 11 Does not start 5 5 Pre injection delay 3 11 Excessive noise 5 5 Pre injection sample clean flushes 3 8 Pre injection solvent clean flushes 3 9 Pre injection time 3 11 Low detector signal 5 6 Priority sample 3 13 Lower repeatability 5 6 Programming Picks up vials 5 4 Special sampler parameters 3 9 Skips vials 5 4 Standard sampler parameters 3 7 Wrong penetration depth 5 5 Run Control Sampler 3 12 Wrong X position 5 5 Syringe R Carrier 2 9 Ready active state 2 11 Cleaning 4 3 Reference adjust 2 15 Filling test 2 18 Reset function
22. CP 9050 AUTOMATIC LIQUID SAMPLER TIMETABLE FOR MAINTENANCE Daily Check septum and liner of injection port If required replace septum and clean the liner of the injection port Check wash solvent empty waste vial if required Check the syringe contamination plunger movement and needle tip damage Before a first run after several hours of interrupted operation perform 3 5 wash cycles to condition the syringe use the option in UTILITIES page of the CP 9050 Automatic Liquid Sampler Wee Check wash solvent and waste vial septa These septa are part of an effective syringe cleaning concept replace them regularly at least every 1 2 weeks to avoid sample cross contamination Because also the Snap cap might be getting soft under the influence of solvent it is advised to change the septum and Snap cap together Check syringe If required clean the syringe The syringe has to be replaced every 2 3 months depending on use SYRINGES The 9050 sampler uses standard Hamilton 700 series syringes 5 or 10 ul with needle length of 51 mm an OD of the needle of 0 47 mm gauge 265 and point style 1 which means the needle has a bevel of 17 and is slightly bent inward Therefore protecting it from blockages Special syringes with slightly thicker 0 52 mm gauge 255 needles can be used as weil for packed splitter and splitless injectors with septum cap For the on column injector the needle must have
23. CP 9050 AUTOMATIC LIQUID SAMPLER Troubie shooting CHROMPACK Ordering information CP 9050 AUTOMATIC LIQUID SAMPLER SECTION 6 ORDERING INFORMATION Page 6 1 INCLUDED PARTS 6 3 _ 82 ACCESSORIES CONSUMABLES 6 3 6 3 SPARE PARTS 6 3 CHROMPACK Ordering information CP 9050 AUTOMATIC LIQUID SAMPLER 6 1 INCLUDED PARTS 6 2 ACCESSORIES CONSUMABLES Part no Description Quantity 10201 Crimp top vial 1 ml 100 pc 10375 Crimp top vial 1 ml with 0 1 removable conical insert 100 pc 10210 Aluminum crimp cap with septum for 10201 10375 100 pc 10381 Removable conical insert 0 1 ml 100 pc 10231 Hand crimper for 10200 10375 10210 1 738200 Crimp top vial 10 mi 125 pc 10223 Polyethylene snap cap with septum 100 pc 10227 Polyethylene snap cap 100 pc 10225 Replacement septum red for 10223 100 pc 11223 Hamiiton 75N Syl syringe 1 11224 Hamilton 701N 104 syringe 1 11330 Sixpack of 701N 10 syringes 1 pc 8670 Syringe cleaner 220 240V 1 pc 8672 Syringe cleaner 110V 1 pc 8665 Cleaning Kit with cleaning wires and cleaning solution 1 pc 8154 Cleaning solution 70 ml 1 pc 10041 Septa Chromsep Blue 9 mm 30 pc 10036 Septa ChromSep Red 9 mm 30 pc 738668 Included part kit CP 9050 without Reference manual 1 734918 silicon seals for TP on coiumn injector 10 pc 737903 Vertical air duct 1 pe 6 4 SPARE PARTS Part no Description Quantity 735649 Connection cable RS232 board DB25 female connector 1 73564
24. POST INJECTION DELAY INJ DELAY 10s NOTE Relay 2 is used for switching the fan cooling of the TP Relay VLV 3 is used single TP case of dual TP relays VLV 3 and 4 are used 3 16 CHROMPACK Operation CP 9050 AUTOMATIC LIQUID SAMPLER 3 10 OPERATING HINTS Vial positions The 7 x 15 tray can contains 105 viais in 7 rows of 15 columns The first row is marked with column numbers 1 2 3 14 some positions of the next rows are marked with vial numbers OOQOOCOOCOCOCOCOCOOCOCOQCZQO QC 55 7 T um 77 OQOOQOCGCOOCOQCGOCQOQOQOC C CC C _ Co C et 5 CC 1 2 3 4 5 6 7 a 3 10 11 12 13 14 Figure 3 5 7 x 15 tray with vial positions Solvent Vial Estimate the volume of solvent needed for the programmed number of INJECTIONS and programmed number of PRE and POST INJECTION SOLVENT CLEAN FLUSHES per injection Be sure there will be enough solvent in the solvent vial Waste vial Estimate the volume of waste collected by the programmed number of INJECTIONS and the programmed number of SAMPLE and SOLVENT CLEAN FLUSHES Wetting a syringe Before starting a series of injections it is wise to wet the by solvent sample flush strokes This be done by starting a GO sampier run The sampler starts if programmed with PRE INJECTI
25. SMUO41 1 THE PROFESSIONALS CHOICE mem Chrampack is nol responsible for pnnting enor and reserves the aght to change spacificabions designs and picas without notice and liability Capynght Chrempack infemational 6 1 SECTIONS TSB s ENGINEERING CHANGES PRODUCT NOTES AND EQUIPMENT RELATED PRODUCTS 6 2 TSB s AND ENGINEERING CHANGES 6 3 PRODUCT NOTES AND EQUIPMENT RELATED PRODUCTS 505300 REV 1 00 TSB s and ENGINEERING CHANGES 505300 REV 1 00 CHROMPACK Manual Update Distribution Service manual 9050 sampler 031 instrument CP 9050 Date 31 January 1997 Subject Update manual from REV 1 10 to REV 1 13 Originator Jan Vos Enclosures 3 pages Author Jan Vos Eile Service Manual CP _op50 505300 of pages d Dear Colleagues Au 1 Remove front page add front page REV 1 13 2 Remove page 2 7 REV 1 01 in section 2 add REV 1 02 2 Please insert this page in section 6 gt SM031 1 NENNEN FROM CHROMATOGRAPHERS FOR CHROMATOGRAPHERS Chrompack is not responsible for printing errors and reserves the right to change specifications designs and prices without notice and liability Copyright International omen CHROMPACK Manual Update Distribution Service manual CP 9050 505300 No 024 nstrument CP 9050 autosampler Date 24 September 1996 Subject Update manual from REV 1 05 to REV 1 10 Originator Jan Vos Enclosures 5 pages Author Jan Vos
26. SYMPTOMS CHECKS AND SOLUTIONS CHECKING PROCEDURES ADVANCED SERIAL LINK TEST CHROMPACK CP 9050 AUTOMATIC LIQUID SAMPLER Page 5 3 5 4 5 4 5 7 5 7 Iw ee Trouble shooting CP 9050 AUTOMATIC LIQUID SAMPLER 5 1 SAMPLER ERROR MESSAGES CP 9001 2 DISPLAY The CP 9001 2 has five error messages related to sampler operation NOT INSTALLED CHECK SAMPLER UNDEFINED VIAL RANGE PL COUNT EXCEEDED SAMPLER ERROR No communication possible with sampler RS 232 interface board not present Cables between RS232 interface board and sampler not connected CP 9050 sampier switched off CP 9050 sampler not in STANDBY mode while receiving a START command Starting the CP 9001 2 while the CP 9050 sampier is still busy in mode one or more are marked in case the keyboard of tha CP 9050 sampler was not locked switching the sampler on while the CP 9050 sampler was activated in the CP 9001 2 Page 1 Line 12 5AMPLER 51 it is possible to press the U or key these states the sampler cannot be started In CONFIGURATION SETUP mode switching the sampler on with the M key pressed while the CP 9050 sampler was activated in the CP 9001 2 Page 1 Line 12 SAMPLER 51 In CONFIGURATION SETUP mode the sampler cannot be started One or more vial ranges do have a zero for the first vial The actual plunger count is higher than the programmed warning limit The syringe mus
27. 1 Line 12 SAMPLER 51 the CP 9001 2 gets information from the sampler about the syringe size and tray these values must be programmed during setup of the sampler The defauit values and data ranges for the sampler parameters in the CP 9001 2 are set according to the syringe and tray installed Page 8 the RUN CONTROL SAMPLER Page of the CP 9001 2 links GC methods to vial ranges of the sampler Up to seven vial ranges can be defined while overlap between the vial ranges is possible If no method is specified with the vial range all vials of this range wili be processed with the sampler parameters programmed in the active memory of the CP 9001 2 The CP 9050 sampler itseif can store up to nine sampler methods sampler method hoids only the sampler parameters of Page 4 of the CP 9001 2 which are maintained even when the power to the CP 9050 sampier is switched off When the CP 9001 2 is started with the sampler active Page 1 Line 12 SAMPLER 51 ali sampler parameters to be used are downloaded to the sampler incase GC method was specified with the vial range this GC method will be loaded in the active memory of the CP 9001 2 and the sampler parameters from the active memory the parameters of Page 4 of the CP 9001 2 will be downloaded to the sampler f no GC method was specified with the range the sampler parameters from the active memory the parameters of Page 4 of the CP 9001 2 will be downloaded directly to the s
28. 12 2102 NUMBER OF INJECTION PORTS 2 42 2103 WASHING POSITION 2 12 2404 START CYCLE SIGNAL 2 12 2 10 5 SYRINGE VOLUME 2 12 2106 TRAY SELECTION 2 13 2 10 7 BCD ACTIVE STATE 2 13 2 10 8 START CYCLE BUZZER 2 13 2 10 9 MANUAL INJECTION BUZZER 2 13 2 10 10 BARCODE SCANNER 2 13 2 10 11 INJECTION POINTS POSITION 2 14 2 10 12 REFERENCE ADJUST 2 15 2 10 13 SAMPLE VIAL PENETRATION 2 16 2 10 14 CLEANING VIALS PENETRATION 2 18 2 10 15 MOTOR SPEED 2 17 2 10 16 PLUNGER TEST 2 18 2 10 17 SERIAL LINK BAUDRATE 2 19 2 10 18 SERIAL LINK TEST 2 19 2 10 19 POSITION SENSORS TEST 2 19 2 10 20 RESET TO DEFAULT 2 20 241 TABLES OF CONFIGURATION METHOD AND UTILITY PARAMETERS 2 20 CHROMPACK 2 1 Installation CP 9050 AUTOMATIC LIQUID SAMPLER 2 1 NOTE 2 2 GENERAL The installation comprises Assembling the CP 9050 sampler b Software update of ihe CP 9001 2 GC c installing the RS232 board in the CP 9001 2 GC d Mounting connecting an extra RS232 plug and cable in the CP 9001 2 GC e Replacing the standard covers of the 9001 GC by the sampler covers f Replacing standard septum cap s by sampler septum cap s d Mounting the CP 9050 sampler h System setup and adjustment procedures If CP 9001 2 and CP 9050 sampler were ordered together steps b to can be skipped only the assembling of the sampler the mounting of the sampler and the system setup and adjustment procedures have to be done lf the sampler was order
29. 1k0 BUZZER 11 ____ 27 512 ii PAD IC3 PCO ADO 5 iD HAG CLAV PAl IC2 PCi ADI 12 ____ e gk Pastel PCR AD2 4 1 1 TEST 13 ee hs 112 PC4 113 Serielle Schnittstelle 30 100nf4 PCS ADS _14 I00nP4 C76 2106 E m 103 C77 TCT ADT 49 ____ 97 22 8 12 111 74HC574 s 28 lic 8 1 9 PB2 Al0 5 4 T 190 4 11 Tour ee T2oUT TEIN 55 PD5 35 PB5 A13 13 i 1 6 14 7 15 m si ENN F y AS 23 s 15 122 xj RNYOSPRODI ji 120 06 Anatenerung H2 5112 74 574 L tajen 11212 415 617 8 1 hcl REED RELAIS KEYBO HODA LIB REL3 FEYB1 soe m HODB VZTBY REL4 he D Vis TRO a m g XIRO VPPE pir 13 i31 SIL3 29227 777 734 4 PHIA po 130 1 12 131 112 4 15 5 7 8 D15 Ansteverung RL EMEN 2480524 PIST 1 SER 1 _ MIN RELAIS 5 D Vp d R25220 amp 198 RNO PRO10 SILI _ alal el sf gre al NS a g 2 d d MOSI R26220R R24 2208 i9 j 4HCOO0 pi s 7 143 212 5115 amp 8 ERN PAA RNYOBPE100 m 140 ao vt ml m
30. CONFIGURATION PARAMETERS Parameter Possible values INJECTION POINTS 1 2 3 4 WASH POSITION LEFT RIGHT START SIGNAL GC READY REMOTE SYRINGE VOLUME 2 5 10 gl TRAY SELECTION 4 8 6 14 7 15 10 20 BCD ACTIVE STATE HIGH LOW START CYCLE BUZZ ON OFF MANUAL INJ BUZZ ON OFF BAR CODE SCANNING ON OFF INJECTION POSITION 0 1 2 3 REFERENCE ADJUST SAMPLE PENETRATION WASH PENETRATION SOLVENT WASTE MOTOR SPEED 1mm sec SYRINGE MOVE UP 50 125 SYRINGE WASH DOWN 50 125 SYRINGE SAMPL DOWN 50 125 SYRINGE INJECT 50 125 SOLVENT PULL UP O 1415 1 250 SOLVENT EJECT 0 1605 4 250 SAMPLE EJECT 0 15 1 250 SYRINGE TEST 0 1 1 250 X amp y axis SPEED 1tmm s 50 125 SYRINGE TEST 0 1 FILLING 0 50 SERIAL BAUDRATE 600 1200 2400 4800 9600 SERIAL LINK TEST POS SENSOR TEST RESET TO DEFAULT NOTE 1 The OF INJ POINTS must be set at 2 even if only one injection port is available 2 Only important when non standard connections options are made used 9050 AUTOMATIC LIQUID SAMPLER installation 2 10 1 CONFIGURATION To enter the Configuration menu turn power off then while still pressing the M key turn power on After the initialization cycle the following message is displayed Press V to enter this option Select configuration parameter with gt or Press to enter the selected parameter MODIFY the value of the selected paramet
31. CP 9050 AUTOMATIC LIQUID SAMPLER 5 4 CHECKING PROCEDURES For all these checking procedures the CP 9050 sampler must be in CONFIGURATION SETUP mode Switch on 9050 sampier with key pressed The display shows CONFIGURATION blinking Activate CONFIGURATION by pressing V key and step through the CONFIGURATION PARAMETERS with the or keys at the control terminal of the CP 9050 sampler tili the display shows the right PARAMETER blinking To escape from CONFIGURATION SETUP mode just press the C key 5 4 1 ADVANCED SERIAL LINK TEST In normal operation mode of the CP 9050 sampler an easy check can be done with the CP 9001 2 by setting the sampler mode page 1 Line 12 to 50 51 With sampler mode 50 the display of the CP 9050 sampler shows FST LST INJ METH MI U 1 101 1 1 Which means the keyboard of the CP 9050 has been unlocked With sampler mode 51 the display of the CP 9050 sampler shows 5 1114 Which means the keyboard of the CP 9050 has been locked NOTE By setting the sampler mode to 51 communication in both directions from 9004 2 GC to CP 9050 sampler and vice versa is checked What happens is the GC asks the sampler for the programmed tray and syringe and after getting the right answers from the sampler locks the keyboard of the sampler A different test for the serial link was described in Section 2 10 8 SERIAL LINK TEST CHROMPACK
32. File Service Manual CP 9050 505300 No of pages 6 Dear Colleagues 1 Remove front page add front page REV 1 10 2 Remove the front page REV 1 00 in section 5 add page 1 01 3 Add section 5 5 4 Please insert this page in sectlon 6 5 024 1 FROM CHROMATOGRAPHERS FOR CHROMATOGRAPHERS Chrompaek is not responsible for printing errers and reserves the right to change specifications designs and prices without notice and liability Copyright Chrompack Intemational caeci CHROMPACK Technical Service Bulletin Distribution Salessup Servrep No 7924 BTW No xxxx Instrument CP 9050 autosampler Date 24 September 1996 Subject Configuration Originator STANG Enclosures None Author Jan Vos File TSB binder Total no of pages 3 Dear colleagues After installation and of reparation or removal of the sampler it necessary to do the sampler configuration particularly the INJECTION POSITION and REFERENCE ADJUST Even after doing these adjustments it may happen that the syringe needle is not in the middle of the sample vial and or Wash Waste vial To solve th s problem you should follow the flow chart in which the reference and wash waste adjustments are described NOTE This information will be included in the service manual 505300 by means of a manual update which will be issued later TSB7924 1 FROM CHROMATOGRAPHERS FOR CHROMATOGRAPHERS Chro
33. Gaerilache Zogin fer ALS ser 020 0320 _ Datum Mame 1704 98 Grunfeld Norm nem Tolerzaz 7158 T MU 001 5303 a rr Em pore el es MM Reparalur Kil REPRIR_KYT iur ALS 104 230 ENTM er HL IR m Mme Punt 12 00 Adapters abel 4320 f r y Motor 8024 M AMP co 7 a T Pesitien UL m 0 7 000 mam M Pet Na nomo ns re ee mm _ _ aaar o parlache gt ALS 10070 10300 O 1 2 2405 Datum Name 170458 Grunield Reparatur Kit EPAIK_K IT harm Anaeryng atum Nare mL Toleranz 04718 00 ALS 106 001 1002 2 HOV 1 B 1 5304 rrr i T B SCHO96 E 001 8032 SCHOSSC TIPM MOd 09 Cri
34. GmbH Konrad Zuse Strafe 1 ALS Injektorkopft komplett T A 07745 Jena L4 2 posos S 09179404 HHE 17PM M002 08 113 Ergatzteil Stromlaufplan M 0 V c lt gt v Tastatur bindungskabel 001 4072 irme s Flachbandkabel A amp WG20 RM1 27 l4pol Pfostenverb PFL14 Leiterpl verb LPVI4 Leiterpl verb LPV14 auf APP 001 4091 gel tet auf Display gel tet Keyboard 001 4091 LER BACKLIGHT Lotverbindung zwischen AFP 001 4091 und Display gt Litze rot ca 30mm SILL LCD DISPLAY SEIRO L2012 C blau ca 30mm RHOSPEOIO BT 1 BHALYTIEK FP Jana GmbH Konrad Zuse Strafa 1 Tastatur Display 07745 Jena sees Stromlaufplan 31892 2262 54 9 2 m eack 2 3 95 4 5 6 SEL i DOC HR _APP CODE 9800 5 232 CABLE FORM A4 M M 1 1213 B 3564900 CHROMPACK B U RAE Reve S0 OOLFOSE 934 4557 4OYdHOHH DUAL 5232 BOARD CHROMPACK 7 3 D _ PORT 4 FROM CP9001 am PORT B MAINBOARO RES 59 4 12 Ce td ee 22 al o on 4 B
35. INCLUDED PARTS CP9050 11223 HAM SYRINGE 75 Spl 699007 ALLEN KEY 4MM 699009 ALLEN KEY 2 5MM 699008 ALLEN KEY 1 5MM 84339 ALLEN KEY 1 2 7 738200 CRIMP TOP VIAL 10225 DISC FOR PE SNAPCAP 5 50ML 10227 SNAPCAP REPL ONLY S 50ML 1 1 E 505300 REV 1 01 L gt 9050 220 230V 50Hz 738436 PART NUMBER DESCRIPTION 735436 CP9050 220 230V 50 2 LIQUID SAMPLER STANG 220 240V PROTECTION COVER SCHR PV 4 12079875 SCREW M4X12D7985SV WASHER 4 3D125 SV 4 4 alz 2 61634 847032 SCREW M3X6 ST ZINC PLATED 735648 PCB ASSY DUAL RS232 BOARD 735649 CABLE ASSY RS232 INTERFACE 757650 SEPTUM CAP 505299 MANUAL REF 9050 LIQUID SAMPLER 734469 OPTIONBOARD BRACKET BORGCLIP PRINT GUIDE 3306 SCREW 2 5X6 D84RVS NUT ZK M2 5 D934 SV CABLE 2XDSUB MALE 25P 9 WIRES ADAPTER DSUB25FEMALE DSUBSMAL CABLE ASSY CP9050 SPLS TP OCI STICKER CE 10 1 COVER ASSY 9002 SCREW M4Xl10D73B5Ek5 INCLUDED PARTS CP9050 731877 153005 177830 737712 947244 738668 AA O03 n0 505300 REV 1 01 PARTS NEEDED FOR 9050 BUILD ON 900 SERIES PARTS NEEDED e COVER ASSY CP9050 CP9001 ___ 1 2 CP9002 UPTO SERIAL 737732 7237732 737732 NUMBER COMM INTERFACE ASSY IS NOT 736589 736589 NEEDED N REMOTE CABLE CP9050 TO GC CABLE CP9050 TO TP OCI CP TP OCI NOT 738434 73843
36. The last part of these messages can be seen in the display of the CP 9050 sampler NOTE See section 5 4 1 ADVANCED SERIAL LINK TEST for further testing 2 10 19 POSITION SENSORS TEST The sensor state is displayed as 1 active 0 inactive AL INJECTION UNIT on LEFT side XR INJECTION UNIT on RIGHT side Y INJECTION UNIT back S SYRINGE up FL PLUNGER pulied up SMP VIAL detected IMPORTANT the motors are powered off Do not try to program any position after this test If necessary turn power off and re enter the configuration program CHROMPACK 2 19 CP 9050 AUTOMATIC LIQUID SAMPLER Installation EXAMPLE CHECKING THE SAMPLE VIAL DETECTION SENSOR The CP 9050 sampler can detect whether a vial is inserted in the selected sample number position This is done by checking how deep the needle guide moves when the syringe carrier moves down for sampling If no vial is inserted the quide moves down to the sample tray and the switch is not activated ihe state of the switch is indicated at the display The adjustment is checked as follows 1 Activate CONFIGURATION by pressing the V key while turning on the power 2 Activate Parameter POS SENSORS TEST value SMP 0 3 insert vial in position 2 of the sample tray 4 Move injection head by hand to the first sample position 5 Shift the needle guide down by hand slowly while observing the vial switch indication at the display It should be O at
37. VOLUME parameter must be set to zero LINE 5 CLEAN SLY injection NOTE FLUSHES LINE 6 1NJ PORT available LINE 7 5 NOTE 3 8 Iw Operation CP 9050 AUTOMATIC LIQUID SAMPLER 3 8 PROGRAMMING SPECIAL SAMPLER PARAMETERS By entering a 1 in LINE 7 OPTIONS a new page with additional parameters shows up SAMPLER OPTIONS l AIR VOL l 2 FILL VOL 2 3 lt CLEAN SLV 0 4 SOLV PLUG D 5 PLUG 0 6 VISCOSITY 0 7T FILL SPEED 5 8 INJ SPEED 5 9 INJ DELAY 0 gt ING DELAY 0 INJ TIME 0 0 SPECIAL 1 0 5 0441 AIR VOL l LINE 1 AIR VOL AIR VOLUME 0 5 pl in steps of 0 1 ul defauit 1 gel The air plug pulled up after taking the sampie after all programmed fill strokes can reduce evaporation from the needle The plug can also be used for the hot needle injection technique NOTE not program a total volume INJ VOL AIR VOL SOLV PLUG AIR PLUG which is bigger than the total syringe volumel LINE 2 FILL VOL FILL VOLUME 0 5 in steps of 0 1 pi default 2 5 This parameter specifies the minimum volume used for the FILL STROKES if the programmed INJECTION VOLUME is higher than the FILL VOLUME the INJECTION VOLUME will be used for ali FILL STROKES NOTE The FILL VOLUME is used for FILL STROKES and PRE INJECTION SAMPLE CLEAN FLUSHES the totai syringe volume is used for PRE and POST INJECTION SOLVENT CLEAN FLUSHES
38. Viscosity Sec Plunger speed FILL 0 4 25 5 Plunger speed gl s 0 1 25 25 Select inj Rear Front Rear Splitter PRE sec 0 99 Splitter POST sec 0 99 Delay PRE 0 999 0 3 Delay POST sec 0 999 0 3 Clean Syringe SOLVENT eo UTILITY PARAMETERS Table 111 UTILITY PARAMETERS Display Inject Samp Meth Single 1 1 Vic Washing Cycles 1 syringe 1 Vic Inject Pre Pst Manual 0 0 V Select Row X Tray V Start Cycle Delay x 1 min vic 2 22 CHROMPACK Operation CP 9050 AUTOMATIC LIQUID SAMPLER SECTION 3 OPERATION Page 3 1 INJECTION TECHNIQUES 3 3 3 2 SYRINGES 3 5 3 3 PREPARING VIALS 3 5 3 4 ACTIVATING THE SAMPLER PROGRAM 3 6 3 5 PROGRAMMING STANDARD SAMPLER PARAMETERS 3 7 3 6 PROGRAMMING SPECIAL SAMPLER PARAMETERS 3 9 3 7 PROGRAMMING THE RUN CONTROL SAMPLER PARAMETERS 3 12 3 8 STATUS INFORMATION PAGE 8 AND STATUS PAGE 3 14 3 9 TEMPERATURE PROGRAMMABLE ON COLUMN INJECTOR 3 16 3 10 OPERATING HINTS 3 17 3 11 SUMMARY OF PROGRAMMING 3 20 Ve ene Operation CP 9050 AUTOMATIC LIQUID SAMPLER 3 1 INJECTION TECHNIQUES With the CP 9050 sampier plunger in barrel syringes are used which means the needle volume of the syringe used has to be taken in account what stays in the syringe after injection depends upon injection technique used sample GC param
39. an OD of 0 47 mm to make it possible to get into a 0 53 mm column or retention gap NOTE the 5 and 10 pi syringes have a maximum plunger fill and inject speed of 25 sdisec Cleaning Clean the syringe as recommended by the syringe manufacturer Blocked needles can be cleaned with appropriate cleaning wires or with a little air pressure in the barrel in case of septum blockage Dirty glass barreis can be cleaned with suitable solvents as Hamiiton Cleaning Solution Dirty plungers can be wiped off with a fibre free cloth Do not touch the plunger with your hands SEPTA Low bleed septa should always be used in packed splitter splilless and wide bore injection ports because these produce the lowest background noise Two types of high temperature low bleed septa are recommended one for temperatures up to 375 C Chromsep Blue and the other for temperatures up to 400 C Chromsep Red With the CP 9050 sampler and the point of the syringe in good shape septa need to be replaced after 150 200 injections case the needie tip of the syringe has been damaged septa can start leaking very soon CHROMPACK 4 3 Ver orm CP 9050 AUTOMATIC LIQUID SAMPLER Maintenance CHROMPACK Va 5 1 5 2 5 3 5 4 5 4 1 Trouble shooting SECTION 5 TROUBLE SHOOTING SAMPLER ERROR MESSAGES CP 9001 2 DISPLAY SAMPLER ERROR MESSAGES 9050 SAMPLER DISPLAY SAMPLER ERRORS
40. as 2 the cycle counter will be set at 30 after starting the STATUS Page will be updated Cycle counter overflow Since it is possible but not useful think of septum to program many injections per vial the situation may arise where the number of injections per vial range exceeds 999 in that case the cycle counter will overflow Samoler mode For starting the sampler it is required that the sampler mode Page 1 Line 12 has been set to 54 in the active memory of the CP 9001 2 the method coupled to vial range the sampler mode must also be set to 51 Solvent plug amp Air plu If values for SOLVENT PLUG and AIR PLUG are not accepted blinking data range be aware of the conditions required for entering values in this case PRE INJECTION SAMPLE CLEAN FLUSHES 0 FILL STROKES 0 Changes of sampler parameters At the start of a vial range the sampler parameters will be downloaded to the CP 9050 sampler lf no method was programmed with the vial range the sampler parameters of the active memory will be downloaded but only at the start of that vial range So changes made in the active memory will become active at the start of that vial range Incase a method was programmed with the vial range the sampler parameters of that method will be downloaded but oniy at the start of that vial range So changes must be made in the GC method itself via EDIT METHOD Page 5 Line 3 and these changes will become active at th
41. can order the following parts 1 Injector head board 2 103013 see drawing encircled number 11 2 Injector head board 1 P N 103008 see drawing encircied number 18 3 Cable 103012 see drawing encircled number 31 Note This information and drawing will be included in the service manual 505300 by means of a manuat update which will be issued later TSB7921 1 FROM CHROMATOGRAPHERS FOR CHROMATOGRAPHERS DZ Chrompack is not responsible for printing errors and reserves right to change specifications designs and prices without notice and liability Copyright Chrompack Intemational U7 7 Tae SCHWARIZ 19 12 95 Poo wa Es CRPOO4 ee ke ill ee De es ee o ae IE n 4 4 Technical Service Bulletin Distribution SE SM SRICP No 7911 BTW No xxxx Instrument CP 9000 with CP 9050 Date 4 June 1996 Subject Retrofit kit for CP 9050 installation on a CP 9000 Originator J rgen Lips Enclosures None Author Jan Vos File TSB blnder Service manual CP 9050 Total no of pages 1 Dear colleagues The Retrofit kit for the CP 9000 to install a CP 9050 sampler is now available Please order the parts separately 738668 Included parts CP 9050 719948 Eprom CP 9000 VLVARDY German 719949 Eprom CP 9000 VLV4RDY English 737732 Gover assy CP 9002 177840 Cable G
42. cap 5mm 50 units and the required injection depth see section 2 9 2 figure 2 6 to the in step 2 displayed value and store with V Typical value for splitter 1339 splitless 1259 and TP 1306 NOTE 1 Before starting to grogram the positions of the injection points make sure the Injection Head in it s HOME position and also that you do not move the Injection Head during the programming Otherwise you have to restart programming because the programmed does not match the actual value 2 The best is to program all three values rougly and when the injection position is neary reached then adjust exactly 3 The M key allows to check the already stored X and Y positions of the running injection point the PENETRATION Z is reset to a safe value WARNING always use C to leave a parameter when no adjustments where made V always overwrite your stored values in this case with the safe penetration value 4 n case of a TP it s advised to do the programming without syringe to avoid damaging the silicone seal inside the TP OCI 2 10 12 REFERENCE ADJUST Press V to enter the programming X AXIS x 0 1 mm REFERENCE 2944 Position in 0 1 mm To adjust the Reference position align the right edge of the Injection Head with the Right Arm Support of the Instrument Base Unit see 19 2 8 with t 4 keys in a step by step brief action on the key or continuous
43. max min 5 Solvent Waste Sample Splitter Slt Spltless REMARKS 400 measured at needlee penetrated 1 3 into vial 650 measured when needle nearly touched the bottom of the vial e 2505 measured at needle just passing the neck of the vial 4502 measured at needle located halfway the vial 260 measured at needle just passing the neck of the vial 5502 measured when needie nearly touched the bottom of tho vial 9 This Value should have been 1367 put value 1339 is the maximum depth this sampler can be adjusted Recalculation from steps to mm 9900 15 steps This manual belongs SERVICE CP 9050 AUTOMATIC LIQUID SAMPLER P N 505300 SECTION CONTENTS 0 Safety information 1 Reference drawings 2 Components legend amp Spare parts 3 Removal Replacement amp Adjustment Procedures 4 Schematic diagrams 5 Troubleshooting amp Checks 6 TSB s Engineering Changes Product Notes and Equipment Related Products 7 Special Tools 8 Preventive Maintenance Liabilities Schedules amp Maintenance Procedures 9 Principle s of operation 10 Reference manual Chrompack is not responsible for printing errors and reserves the right to change specifications designs and prices without notice and liability All rights reserved This manual or any part thereof may not be reproduced in form without written permission from th
44. of 0 47 mm gauge 265 and point style 1 which means the needle has a bevel of 17 and is slightly bent inward Therefore protecting it from blockages Special syringes with slightly thicker 0 52 mm gauge 255 needles can be used as weil for packed splitter and splitless injectors all with septum cap For the on column injector the needie must have an OD of 0 47 mm to make it possible to get into a 0 53 mm column or retention gap Note The maximum plunger fill and inject speed for 5 and 10 gi syringe is 25 3 3 PREPARING VIALS Selecting sample solvent waste vials Standard 2 mi viais 2 mi vials with 0 1 mi inserts or 0 1 conical vials can be used in the 7 x 15 tray Dimensions OD s 11 6 mm height 30 38 mm For the solvent and waste vials 10 ml vials are used Dimensions OD 22 5 mm height 48 mm Filling sample vials For obtaining reliable high performance resuits with the sampler and preventing contamination or injection volume problems do fill the vials half full or a little bit more If the vials are almost empty the contribution from previous sample injection or solvent washes may affect the sampie cross contamination dilution effect If the vials are almost full a vacuum may interfere with the syringe measuring a precise volume Capping sample vials Use a crimper to put on the airtight crimp caps sure the cap is airtight you can the cap by hand easily the is too lo
45. original status IMPORTANT NOTE After exchanging mechanical or electronically parts it s mandatory to set the configuration parameters See usermanual page 2 89 505300 REV 1 00 3 5 2 3 6 eme EXCHANGING THE PROCESSOR BOARD Disable the SAMPLER CONTROL PROGRAM on page i of the CP 900x GC by entering code 50 on line 12 The CP 9050 keyboard is not locked anymore Write down all method and system parameters in a table as shown on page 2 21 2 22 of the Reference manual Section i0 of this binder Turn the instrument off and disconnect the power cord NOTE It is impossible to exchange the processor board while the sampler is installed on the GC 1 You must take the sampler from the GC first camere Remove the sample tray Pull the crossrail with injectionhead to the front of the sampler Remove the top cover by loosening the 8 phillips headscrews on both Sides and on the top Loosen also the 3 allen head screws that fit into the bottom plate Disconnect all the plug connections on the processor board Please write down the colors of the wires coming from the transformer and their position in the green connector Remove the transformer by loosening the 2 screws in the bottom of the sampier that hold the transformer bracket Push the crossrail back to it s rear position for easier access of the lower screws that fix the processor board Use a iong stem hex wrench to loosen the seven alien hexscrews t
46. to heat water etc CP 9050 AUTOMATIC LIQUID SAMPLER Safety information 0 6 CHROMPACK ku Introduction CP 9050 AUTOMATIC LIQUID SAMPLER 1 1 1 2 1 2 1 1 2 2 1 2 3 1 2 4 1 3 1 4 SECTION 1 INTRODUCTION GENERAL HARDWARE INJECTION HEAD CROSSRAIL INSTRUMENT BASE UNIT CONTROL TERMINAL SOFTWARE GENERAL OPERATION 1 4 1 4 1 4 1 5 1 5 1 6 CHROMPACK 1 1 introduction CP 9050 AUTOMATIC LIQUID SAMPLER 1 1 GENERAL The CP 9050 Automatic Liquid Sampler can handie up to 105 liquid samples divided in up to 7 vial ranges coupled to as GC methods The sampler uses standard syringes while kinds of injection techniques are possible 1 2 HARDWARE Figure 1 1 shows the main parts of the CP 9050 Automatic Liquid Sampler CONTROL TERMINAL CROSSRAIL 1 2 3 INJECTION HEAD 4 SYRINGE CARRIER 2 SYRINGE 8800659 066060600056 5 INSTRUMENT BASE UNIT 7 TRAY CCS S SY Y Y Deni eme at Sa mi sad a 8 SOLVENT BOTTLE 9 WASTE BOTTLE eo ao 1 L eee Figure 1 1 Main Parts CP 9050 Automatic Liquid Sampler CHROMPACK 1 3 CP 9050 AUTOMATIC LIQUID SAMPLER 1 2 1 INJECTION HEAD 1 PLUNGER HOLDER 2 SYRINGE 3 SYRINGE FIXING LEVER 4 NEEDLE GUIDE Figure 1 2 Syringe Carrier 1 2 2 CROSSRAIL Introduction
47. way key pressed IMPORTANT 1 This programming must be done mecum every time the arm positlon has a been modified MECHANICAL 1 BE 2 The Sample Tray and Cleaning Vials Holder positions are RELATED to the s Holder Reference adjustment Figure 2 8 CHROMPACK 2 15 CP 9050 AUTOMATIC LIQUID SAMPLER Installation 2 10 13 SAMPLE VIAL PENETRATION SMPL PENETRATION Allows to adiust the needle penetration in the sample vials Press V to enter the programming PENETR x0 1 mm SAMPLE 1 0277 L Penetration Depth in 0 1 mm Detected vial Since it is not possible to see how far the needle penetrate into the vial proceed as follows 1 Measure the distance from septum to the desired penetration depth use a spare capped vial 2 Put a capped vial in position 1 of the tray 3 Move the syringe downwarts with 1 key until the needle just touches the septum of the vial 4 Move the syringe further downwarts with the 1 key over the distance measured in step 1 2 10 14 CLEANING VIALS PENETRATION WASH PENETRATION C 12 amp penetration depth in solvent and waste vials can be individually adjusted Press V to enter the programming x 0 1 mm SOLVENT 0030 L Penetration Depth in 0 1 mm Select the SOLVENT or WASTE vial with lt or and adjust penetration with 21 4 IMPORTANT Vali
48. your index finger of your other hand push the srew loaded plunger clamp up so that the plunger head slips into the plunger holder Push the syringe in position and push the plunger clamp down then fix the screw again Finally the syringe can locked by turning the white syringe fixing lever 90 Move the plunger holder down as far as possible to adjust dead volume to zero fixed by a hexagonal nut NOTE 1 Standard Hamilton syringes can be used 700 series 5 amp 10 Figure 2 7 Syringe carrier with syringe 2 The maximum piunger fill and inject instailed speed for 10 pi syringe maximum 25 3 Proper working depends on the syringe state and the following points have to be assumed Straight needle plunger freely slipping no plunger leakage 4 It s a good practice to execute some cleaning cycles Utilities 2 9 4 CLEANING VIALS Use standard 10 ml vials Fill a vial with an appropriate solvent and put it into the right place of the vial holder Place an other empty vial on the left side for waste solvent Remark To prevent plopping off of the snapcap it s advised to change the snapcap with septum on a regular base CHROMPACK 2 9 CP 9050 AUTOMATIC LIQUID SAMPLER Installation 2 9 5 NOTE 2 9 6 ADJUSTING DEPTH FOR SAMPLE SOLVENT PICKUP AND WASHING These adjustments are only required if one wants other settings than the defauit settings For these adjustments i
49. 0 sampler page Page 4 is programmable the sampler is off pressing START starts GC starting the CP 9010 or CP 9050 sampler Page 8 RUN CONTROL HODS can be active The CP 9010 or CP 9050 sampler pages Page 4 amp 8 are programmable the sampler is on pressing START starts a GC cycle while starting the CP 9010 or CP 9050 sampler Page 8 RUN CONTROL SAMPLER will be active The 94X sampler page Page 4 is programmable the sampler is off pressing START starts a GC without starting the 94X sampler Page 8 RUN CONTROL METHODS can be active The 94X sampler page Page 4 is programmable the sampler is on pressing START starts a GC cycle with starting the 94X sampler Page 8 RUN CONTROL METHODS can be active Before programming the CP 9050 sampler page Page 4 one has to activate the sampler at least once after power up of the CP 9001 2 by entering 51 for SAMPLER By doing this the CP 9001 2 gets information from the CP 9050 sampler about installed programmed syringe size and viai tray The defauit values and programmable data ranges will be set according to the installed programmed syringe size and vial tray See Section 2 10 CONFIGURATION PARAMETERS about programming the syringe size and vial tray in case the CP 9050 sampler has been activated the keyboard of the CP 9050 sampler will be locked the function keys ML VI U and C disappear in the display FST LST INJ and METH stay visible on the di
50. 3 CP 9050 AUTOMATIC LIQUID SAMPLER Safety information Skin puncture Indicates sharp or suddenly moving parts such as injection needles that may cause injury od Hot surface indicates parts that may cause burns when touched B Cryogenic frostbite Contains extremely cold materiat such as liquid nitrogen carbon 1 dioxide that may cause injury when handled carelessly CATDLEM FROSIITE 1 M M Static discharge warning Item contains parts or information that can be damaged by electrostatic discharge Take care for proper grounding before handling Do not touch Touching this item may result in damage to the instrument or personal injury 0 2 GENERAL SAFETY PRECAUTIONS 1 The installation of this instrument will normally be carried out by an experienced Chrompack service engineer Any damage to the system that occurs during unpacking when it is not carried out in the presence of a Chrompack service engineer will result in the rejection of a warranty claim This instrument should be placed in a suitable location with sufficient ventilation to remove gases and vapors Space around the instrument must be sufficient to enable cooling of the instrument Before plugging the instrument in or turning the power on always make sure that the voltage and fuses are set appropriately for your local power supply Do not turn on the instrument if there is a possibility of a
51. 3 13 3 19 Installation 2 9 Resetting to default values 2 20 2 21 Specifications 3 5 4 3 RS232 cable plug 2 6 Wetting 3 17 RS232 interface board 2 5 T S Test sample pickup depth 2 10 Sensors 5 8 Sample wash depth 2 10 Serial Link 5 7 Sampler cover 2 8 Syringe filling 5 8 Sampler errors Time out method programming 3 17 CP 9001 2 5 3 Timetable for maintenance 4 5 QCP 9050 5 4 3 16 Symptoms checks and solutions 5 4 Tray 3 17 Sampler methods 1 6 Numbering 3 17 Sampler mode 3 19 Select 2 11 Sandwich injection 3 3 3 4 Septa 4 3 U Septum cap 2 7 Utility parameters 2 23 Septum counter 3 14 Software 1 5 v Software update 2 4 Vials 3 5 3 17 Solvent pickup depth 2 10 Capping 3 5 Solvent plug sandwich 3 3 3 4 Cleaning 2 9 Solvent wash depth 2 10 Detection Sensor 2 19 Spare parts 6 3 Positions 3 17 Splitter splittess 3 11 Ranges 3 12 specifications 3 5 Viscosity delay 3 10 1 4 CeOOMPACK 19 02 98 11 46 31 118671331 EP wee CP Nederland 4 001 001 31 118671331 i 4 004 5282 2 42 43 i j alter Alander a 36 Alt t al TE i Leliterplatte 37 34 6001 2 440 4 Best ckungspton BS Dea 1 8 4 49 6 amp Bow B b CHROMPACK NEDERLAND CHROMPAC
52. 4 supplied cabie POSSIBLE BH INCLUDED PARTS 9050 738668 EPROM GERMAN NOTE 1 9001 NEEDS RS232 BOARD REV 1 04 OR HIGHER SOFTWARE REV 2 OR HIGHER ALSO 941 AND TO OCT NOTE 2 For the CP9001 and 9002 kit is available to upgrade the GC to make it suitable for the 9050 P N 738436 2 505300 REV 1 01 2 12 J MAINBOARD ASSY 2307 SERIALN 10001 10069 002 5301 oS T asus ue 2177 NUMBER 257 F BACKPANEL ASSY 5282 MAINBOARD SERIALNUMBERS 10001 10300 102765 CABLE FOR Y MOTOR TRANSFORMER HOLDER 5131 TRANSFORMER CONNECTORS 230V SERIALN 10301 UP LINE FILTER 102395 MAINBOARD ASSY 110V SERIALN 10001 10069 002 5302 SUPPLIER DESCRIPTION _ CP PART NUMBER MEME a NUMBER 257 F BACKPANEL ASSY 5282 MAINBOARD SERIALNUMBERS 10001 10300 4300 CABLE FOR Y MOTOR 5 67 TRANSFORMER HOLDER 5135 TRANSFORMER CONNECTORS 110V SERIALN 10301 UP 102762 5132 LINE FILTER 102395 MAINBOARD ASSY 230V SERIALN 10070 10300 001 5303 SUPPLIER DESCRIPTION CP PART NUMBER HEN E 7 NUMBER 257 BACKPANEL ASSY 100 FLATCABLEZ C 1300 c SCHOE 5131 TRANSFORMER CONNECTORS 230V SERIALN 10301 UP tos T Doc 709 2989 apa 2 CYP PP 6 LINE FILTER 102395 Ci 201 PIGGY BAG N C 505300 REV 1 01 0 EEE E 001 5304 iv to su PESE pel LC SEN S4 CP PART BACKPANEL ASSY N
53. 4502 measured at needle located halfway the vial e 2602 measured at needle just passing the neck of the vial 550 measured when needle nearly touched the bottom of the vial o This Value should have been 1367 but value 1339 is the maximum depth this sampler can be adjusted Recalculation from steps to mm GOOG 15 steps is Imm OOOO0 605300 REV 1 02 SECTION 4 SCHEMATIC DIAGRAMS Page Title SHEET 4 2 MAINBOARD ALS R AFP 001 5283 1 3 4 3 MAINBOARD ALS R AFP 001 5283 2 3 4 4 MAINBOARD ALS R AFP 001 5283 3 3 4 5 TRANSFORMER CONNECTIONS DM 4 6 TRANSFORMER WIRING 7 4 7 CABLE OVERVIEW SAMPLER ALS104 CP l i 4 8 CARRIER ARM TRAGARM KOMPLETT APP 001 9003 l 1 4 9 INJECTION ARM INJEKTORKOPF AFP 001 9204 1 1 4 10 DISPLAY AND KEYBOARD AFP 001 5121 1 1 4 11 RS232 CABLE 3564900 1 1 4 12 5232 CABLE 3564900 1 1 4 13 DUAL RS232 ROARD V1 06 735647 1 1 4 14 DUAL RS232 BOARD V1 06 735648 1 1 NOTE There is actual page numbering the reference drawings the nubering as given on this page in the column just indicates in which order the drawings must be inserted 505300 REV 1 01 r 224 1 a E 22 a 20 ate d Maa TE UL t un roo pa ors e o Re 7 g 4 2 1 0nF3 2 4 R52 C62 24 574
54. 5090 nection unit 001 5086 30 board 1 flex cahle connector 001 5086 1 injection unit board 1 with ZIP ijne connector Bears 02 0498 __ ____________ i ___ _____ LJ _________ __ __ 1 Adapterxabei f r y Motor 8024 AMP con Oberflache Ms3steo Poston Penis m EE RR NR ALS 104 001 10007 2 2300 ee ee eee mu BENE Toleranz 097168 _________ ____________ __ ust Anderung Datum DY Nr I Ua cocina lt ee 34T mn3a Pd x 1 ee ee 44 Zust Anderung Mame 4 52 Adapter abel f r 3024 AMF cor oberfisrhe wis 711 o ALS seen 1001 0069 Ham tor EN Aa iio Norm i 4 ALS TA UC GOOF Poi ee 1 Reparatur Kit REPAIR DINT168 mil Let EN x ee mmm i 37 4 500 Adapterkabel f r y Motor 6024 pom i 2
55. 8 5232 board 1 pc 177830 RS232 cable 2 x 25 pin male connectors 1 pc 737650 Septum cap for CP 9010 and 9050 samplers 1 pc 163371 Adapter DSUB 25 Female DSUB 9 Male 1 CHROMPACK 2 x Solvent waste vial with polythene snap cap and dise 10 1 x Allen hex key 4 mm 1 x Allen hex key 2 5 mm long t x Allen hex key 1 5 mm 1 x Allen hex key 1 3 mm 1 x Syringe 5 gal 1x Reference Manual 8 3 mme Ordering information CP 9050 LIQUID SAMPLER 6 4 CHROMPACK INDEX INDEX rene CHROMPACK CP 9050 AUTOMATIC LIQUID SAMPLER 1 1 INDEX A Aborting an injection cycle Accesories consumables Activating the sampler program Active method Active vial Actual injection Air plug sandwich Air volume air plug Assembling the sampler B Buzzer Change of sampler parameters Checking procedures Cleaning Wash position Configuration parameters Control Terminal Crossrail Cycle counter Cycle counter overflow D Default values Dip switch settings RS232 board Fill Speed Strokes Volume First vial G GC methods H Hardware Hot needle injection 3 18 8 3 3 15 3 14 3 14 3 10 3 9 2 3 2 13 3 19 5 7 2 9 2 12 2 8 2 10 2 11 1 5 1 4 3 19 3 19 2 22 2 5 3 10 3 8 3 12 1 6 1 3 3 3 CP 9050 AUTOMATIC LIQUID SAMPLER Included parts Injection Counter Depth Head Point Point Position Port Selection Speed Techniques
56. ANODIZE BLACK MATT ort e UNT MM TOLERANCES UNLESS OTHERWISE STATED 5922 FORM DIMENSIONS x 2 ANGLE 0 5 05 NAME FL REMARKS 04 A4 DATE 30 06 93 REMOVE SHARP EDGES 0 2 BURR FREE 05 we CODE 110 SHEET OF 1 1 01180 71000 HERCULESWEG 8 CHROMPACK RE Fh THE NETHERLANDS FAX 01180 33118 WOCH 7 38 31 FRONTVIEW CP 9002 THE HETHE PLANO 2 1 SECTION 2 COMPONENTS LEGEND amp SPARE PARTS t 1 1 1 RO BO B2 MJ 2 E XD 0 3 3 LO LO BO Dc 1 NOTE CHAPTER CONTENTS DOC NO Front view serial 10301 001 1202 1 of 2 Rear view serial 10301 001 1202 2 of 2 Rear view serial 10129 10300 001 1002A Rear view serial H 10070 10128 001 1002 Front view serial 100001 10069 001 1000F ALS CP AUTOSAMPLER 22041 001 1202 2 GRUNDPLATTE BASE BODY COMPLETE 110V 220V 001 9202 1 2 ARM ASSEMBLY 001 9003 INJECTORKOPF INJECTION HEAD 001 9204 INJECTION HEAD serial 10031 001 9204 INJECTION HEAD serial 10070 10128 001 9004 INJECTION HEAD serial 10001 10069 001 9004F SEVERAL PARTS 2 COVER ASSY CP9050 ON CP9001 9002 COMM INTERFACE ASSY INCLUDED PARTS CP9050 UPGRADE KIT FOR THE CP9001 CP9002 PARTS NEEDED FOR 9050 BUILD ON CP900X SERIES CONTENTS OVERVIEW MAINBOARD KIT ASSY S CONT
57. BER tof p AS MU Dos tret Trl Itu au Ei Doa wat T VERIS 4 to 20 DOGR E Mega T mo ex m tt san co aet an t 001 8052 X AXIS MOTOR ASSY 10300 524058 axis woroR O O 301 8043 02005 SCHOS7 z AXIS MOTOR PULLEY SSS 001 8224 Y AXIS MOTOR ASSY WITH MOLEX CONNECTOR SERIALN 10301 UP SCHO95 AXIS MOTOR 5 036 MOTOR PULLEY rj gt te eio Ie Se DRE el B ose TER FA L N E a ee kite Y ue 4 4 D i tke T x I nU GI E SIX EM phe ome 121 toos 2 Inline C 02754 m E ALO 001 8024 Y AXIS MOTOR ASSY WITH AMP CONNECTOR i02991 LEE SERIALN 10001 10300 WC N C 524945 7046 65320 N C SCHO6O GUIDE 505300 REV 1 01 COVER ASSY PART NUMBER 737732 COVER ASSY CP9050 CP9001 9002 9003 Dod ttt 4 84 0544 t t ei 1 01 7 m te PRIEST a rs 40 ore Ure sott xr NN e a Rc el 4 4754 gt 4 7 tard E COMM INTERFACE ASSY 736589 PART ER DESCRIPTION um 736589 COMM INTERFACE ASSY 735648 PCB ASSY DUAL 5232 BOARD INCLUDED PARTS CP9050 738668 PART NUMBER DESCRIPTION 738668
58. C 1 Pia alate bh M 5282 MAINBOARD SERIALNUMBERS 1000 1 10300 TRANSFORMER CONNECTORS 110 SERIALN 10301 UP LINE FILTER 102995 c C 505300 REV 1 01 ume NOTE SECTION 3 REMOVAL REPLACEMENT amp ADJUSTMENT PROCEDURES CHAPTER CONTENTS General procedures for electronic modules Adjusting the needle guide Exchanging the injection head Exchaning the front panel with display and keyboard Exchanging the processor board Exchanging the crossrail Software changes Standard connection In out connector In out connector cable CP9001 9002 connections BCB output connector Serial connector 55232 Options connector Penetration depth range for samplers FOR THE SAMPLER CONFIGURATION PROGRAM SEE THE REFERENCE MANUAL SECTION 2 10 1 505300 REV 1 01 i 3 2 GENERAL PROCEDURE FOR ELECTRONIC MODULES In general always use the given sequence in the adjustments The numbers between brackets e g 15 refer to the Reference drawings section 1 unless there is a figure shown on the same page Installation of the replacement component is generaliy the reverse of the removal sequence WARNING DISCONNECT POWER CORD PRIOR TO REMOVAL OF ANY COMPONENT DURING REPAIR WORK IT S MANDATORY TO USE ANTISTATIC PRECAUTIONS TO PREVENT DAMAGE 505300 REV 1 00 ADJUSTING THE NEEDLE GUIDE Insert
59. C connection to CP 9050 Best regards Jan Vos 587911 1 FROM CHROMATOGRAPHERS FOR CHROMATOGRAPHERS EEEN Chrompack is not responsible for printing errors and reserves the right io change specifications designs and prices without notice and Kability Copyright Chrompack Intemational yu tege m CHROMPACK Technical Service Bulletin Distribution SE SM SR CP No 7913 BTW No xxxx Instrument CP 9050 Date 4 June 1996 Subject First release service manual CP 9050 sampler Orlginator STANG Enclosures None Author Jan Vos File TSB binder Total no of pages 1 Dear colleaques am pleased to announce that the SERVICE MANUAL for the CP 9050 autosampler is ready now This manual is an addition to the users manual and provides detailed and specific technical information about the sampler You will notice that the amount of information is given very clearly and the table of contents will help you to find your specific needs It is strongly recommended to study the contents of the manual in detail since it will extend you knowledge of the CP 9050 sampler The 9050 service manual can be ordered as usual Please use part number 505300 hope that this manual will make your life in the field easier and wish you a lot of success with your service efforts Best regards Jan Vos TSB7913 1 FROM CHROMATOGRAPHERS FOR CHROMATOGRAPHERS Chrompack not responsible for print
60. CTION HEAD serial 10001 10069 901 9004 1 15 REPAIR KIT 230V serial 10001 10069 001 5301 1 16 REPAIR KIT 110 serial 10001 10069 001 5302 1 17 REPAIR KIT 230V serial 10070 10300 001 5303 1 18 REPAIR KIT 110V serial 10070 10300 001 5304 1 19 SEVERAL PARTS 1 20 Mounting bracket for option and RS232 board 734905 01 1 21 Septum cap for use with CP 9050 sampler 376500 02 1 22 PRONTVIEW CP 9002 738317 318 319 01 NOTE The DOC NO at the reference drawings refers to the header The encircled numbers at the reference drawings refer to the numbers given in the coiumn ITEM NO of section 2 There is no actual page numbering on the reference drawings the numbering as given on this page in the column PAGE indicates in which order the drawings must be inserted 505300 REV 1 01 just 2 54 201 ii CETTE li a 3 3 pn x 39 E006 100 N 066 100 1413 204000752 a a 1 c C L c n 4 A LA 80003 x R 27 t a D c gt ON gt ce an pc rj fi Cc C C C 001 9202 1 V ELOS LO0 006 00 4 m 01 9809 100 GSE GUI N A 006 100 0001752101 M3 SANTIN THIIS MON 006 100
61. ECTION 7 SPECIAL TOOLS 7 2 ANTI STATIC MAT 505300 REV 1 00 omer HRT ae ee ee eee eee DIU P N 737947 do Oe ee eo A Matenal is 016 thick light blue static dissipative 395 10mm Surface Resistance is 1 x 1017 ohms Snap Stud Pockets and edges are heat sealed Ground 8 Ground cord is permanently nveted to matenal with Cord X banana tack for wnst strap and an additional 395 10 mm snap stud for grounding second item required C The attached ground cord is a 5 long 105 strand high flex copper wire with black PVC insulation OD is 100 It is with a Mueller No 95 grounding clip D amp E Veicro closure kit can be folded and held in small package for tool box or briefcase Folds lo 8 x 10 i25 22 5 in 7 Hol stamped permanent Always connect both ground cord and wnst strap and test For proper grounding before beginning work around static sensitive components 16430 includes one 14840 adjsutable elastic wnsIband and one 14010 six foot coiled wrist ground A cord See Drawings 14840 and 14010 Also available as 16440 without wnstband and Corn Two pockels 12 5 and 9 5 heat sealed 10 hold 100 5 or components 6430 Mat Portable wAWnst Strap 20x22 Mat Portable No Strap 20 22
62. ENERAL SAFETY PRECAUTIONS l 10 11 The installation of this instrument will normally be carried out by an experienced Chrompack service engineer Any damage to the system that occurs during unpacking when it is not carried out in the presence of a Chrompack service engineer will result in the rejection of a warranty claim This instrument should be placed in a suitable location with sufficient ventilation to remove gases and vapors Space around the instrument must be sufficient to enable cooling of the in strument Before plugging the instrument in or turning the power on always make sure that the voltage and fuses are set appropriateiy for your local power source Do not turn on the instrument if there is possibility of any kind of electrical damage Instead disconnect the power cord and contact your Chrompack office The supplied power cord must be inserted into a power outlet with a protective earth ground connection When using an extension Cord make sure that the cord is also properly grounded Do not change the external or internal grounding connections as this could endanger you and or damage the instrument The instrument is properly grounded when shipped You do not need to make any changes to the electrical connections or to the instruments chassis to ensure safe operation When working with this instrument follow the regulations for GLP Good Laboratory Practice Take care to wear safety glasses and app
63. ENTS OVERVIEW MAINBOARD KIT ASSY S The header DOC NO at the parts lists refers to the box DOC NO of the drawings of section 1l The numbers in the column SUPPLIER NUMBER refer to tne numbers at the reference drawings of section 1 Parts with a dash in the column ITEM NO are not drawn in the reference drawings of section 1 Parts with in the column CP PART NO are not codified as available spare part For further parts breakdown of electronic units refer to section 4 505300 REV 1 01 FRONT VIEW SERIAL 10301 DOC 001 1202 1 of 2 IU t eia 2 mm LI 1 LUI te Qe ESSE LS IAE r nC du C feno 97 e uj cr Pe SH es IPS qun 21 PH DOSE SPI SUPPLIER E MEW I ec ip SHREVE i NUMBER i uo NIE t 001 9204 INJECTION HEAD 102753 901 9202 BASE BODY watt ATE ura ys s 1 NU mU H mmm 7 nan Ix 5 i Dive 4 5 tns esa UU dara ow Le PEEL M LI REAR VIEW SERIAL 10301 DOC 001 1202 2 of 2 ore SUPPLIER DESCRIPTION
64. ILL tuj 23 Di the 5 E 1 FTIIT oa Co Ts DUAL HS52328 BOARD 735648 wer FORM A3 CODE 130 Ps SHEET 1 OF 1 03 30 03 93 5540 1 03 MIDDELBURG 14 05 93 5697 1 04 THE NETHERLANDS EGER ee 1 05 LN uie Lm 1 Lud n E m TROUBLE LIST Trouble Reason Correction poor reproducibility zero volume adjustment is incorrect picture A 7 UU CMM the syringe needle breaks or dented the septum of the vials or the injector is too hard try another septum or an other syringe recommendation 10g the syringe plunger dented or is fixed zero volume adjustment is incorrect picture the syringe picks up the vials the position of the needle guide isn t correct to the syringe picture B or the sleding rods are dirty ihe sampler skips vials the high of the vials isn t analogue as the adjusting before repeat in the config menu the point vial penetration the inJ head position is sideways ofthe the inj head was changed x y pos x position config menu reference adjust vial position or the arm was shifted x pos y postlion picture or the mainboard was changed y pos Attention repeate in the config menu the in position the inj head position is sideways ofthe arm holder was shift shift the left armholder picture E wast and clean vials the y mo
65. K NEDERLAND B V Boerhaaveplain 7 4624 VT Bergen op Zoom The Netherlands Postbus 250 4600 AG Bergen op Zoom The Netherlands Telefoon 0 194 282834 AX Telefax 0 164 282828 E mail cpinfogzeelandnet ni To Jan Vos From Hans van Bergen Company CP M burg R amp D Date 11 29 96 Country NL Subject 505300 CP9050 Fax nr pap yr Ref INTJVOOS DOC VERZONDEN Total numbers of pages incl front page 1 CC Beste Jan A zoekende in het serv manual van de CP9050 dacht ik mijn informatie op blz 3 13 te kunnen vinden volgens de index blz 3 1 laatste blz is nr 13 Edoch geen blz 3 13 te vinden wel nr 3 14 met andere informatie ats die ik nodig heb Is dit een foutje of mis ik deze blz gewoon Indien ja kan ik een copie krijgen C Bij voorbaat mijn dank x Hans van Bergen lt CUSTOMER SUPPORT service 827 v 99 21 S31 M VASA wine Eo AD 7 CP Nederland 80017003 31 118671331 CHROMPACK NEDERLAND CHROMPACK NEDERLAND B V Bergen op Zoom The Netherlands rai Bargan op Zoom The Netherlands Teietax 0 164 282828 To Company CP M burg R amp D 11 20 98 Country NL 505200 0050 Fax et 003 Total numbers of pages incl frontpage 1 Bests Jan zoekende in het manual van CP9050 dacht informatie op biz 3 13 te kunnen vinden volgens de index biz 3 1 lantste biz ia nr 13 Edoch goon biz 3 13 te vinde
66. M FLAT CABLE SERIALN 10130 UP 102767 5073 ARM CABLE SERIALN 10070 10129 02766 507 03003 SCHO24 016 c 3033 53003 8031 02998 SCHO22 c SCH023 02557 5 021 SCHO36 SCHO20 SIDE COVER ACHOI2 SCHOI6 X AXIS BELT ML 103000 SCHO62 X AXIS BELT CLAMP 5083 ARM LEFT LIMIT SENSOR 103001 SCHO11 ARM SLIDE C C 7 E ELS SSF had HP Q as m OLIO O OJ x zm o MD 27 C 505300 REV 1 01 li INJECTORKOPF INJECTOR HEAD ASSY DOC 901 9 Re d P 204 NUMBER 00 25 0 502020222 NUMBER SCHO47 SYRINGE SUPPORT 5286 CABLE WITH BOARD 1 SERIALN 10300 UP 5086 1 INJECTION BOARD 1 SERIALN 10001 10069 5086 10 CABLE WITH BOARD 1 SERIALN 10070 10300 8043 Z AXIS MOTOR ASSY 1 034 MOTOR HOLDER 043 LEVER 044 LEVER SHAFT 030 INJECTOR BODY HEAD SCH102 NEEDLE GUIDE SPRING SCH038 20 TEETH PINION SCHO35 REFLECTOR 5090 INJECTION BOARD 3 032 UPPER COVER 031 INJECTOR HEAD COVER SCHO39 INJ HEAD BASE PLATE SCHO45 NEEDLE GUIDE SCH041 IS PART OF NEEDLE GUIDE 5086 20 INJECTOR BOARD 2 5086 30 FLEX CABLE 11 POLE 505300 REV 1 01 2 2 2 103004 103015 103006 102764 103008 102763 203009 03010 03011 Z DERSE 2 A zr de Fey Ql lt 12 gt un
67. M2x4 DIM B4 A 5086 30 lac 1 ato RE man nu a LL oe eee UB 001 5086 20 injection unit board 2 wilh ZIP line connector 001 5086 30 flex cable without connector 001 5286 infection unit board 1 with connector with round cable and connect Mestad Uberflache d less 20 58 5 in head ipmann 020498 senem in LL Gm mu 001 9704 inj head 001 5090 injection unit board 321 Q Menge mr ra mm BH n a M rm 001 5086 20 injection unit board 2 x with ZIP ling connector in head 001 5090 injection unit board 1 001 5086 30 flex cable without carnnector 001 5086 10 injection unit board 1 with ZiP line connector with round cable and connect inj head EN 001 9004 X Gatun SES r rn r er ee mam Lo ee 001 5086 20 injection unit board 2 ini with ZIP tine connector head 001
68. NG Check rolling smoothness Lubrication grease LOOSE PULLEY Lubrication silicon oil ARM ASSEMBLY See section 1 DOC NO 003 ARM HOLDERS Tightening of the fixing screws BELLOWS Aspect Before checking the next parts please remove the injection head and the bellows CARRIAGE ASSEMBLY Check bearing and slide Lubrication bearing and slide grease BELT Beit tension Belt clamp tightening LOOSE PULLEY Lubrication silicon oil 505300 REV 1 00 8 4 1 iNJECTION HEAD See section 1 DOC NO 094 GEARS AND RACK Check bearing and slide Lubrication silicon oil NEEDLE GUIDE SPRINGS Check for smoothness Lubrication silicon oil VIAL SENSOR REFLECTOR Adjust if necessary Fixing screws NEEDLE GUIDE STOPS Adjust if necessary Fixing screws Remove the Injector head cover for checking BELT Belt tension Belt clamp fixinq screw LOOSE PULLEY Lubrication Silicon oil FLEXSTRIP CABLE Visible inspection HEAD LOCKING Visible inspection Efficiency 505300 REV 1 00 8 4 2 PRINCIPLE S OF OPERATION 505300 REV 1 00
69. Netztrafo 230V 2xFlachsteckkupolung RS 531 569 001 5131 2xAbdeckung RS 531 475 4xAderendhulse tsotiert fur Smm 8050 5 T TR 1 SchrumpfschL auch 3 Netztrafo 2xFlachsieckkupplung RS 531 469 001 5135 ev 2xAbdeckung RS 531 475 E i 3 JP Leiterpl verb LPVI1O BU LE 2 5 X Mator HMB l17PHM MOOZ u8 4 43 3 112 LP X Endlage rechta AFP 001 5084 AMP BL 281796 3 AMP SL 281598 3 LP X Endlage links AFP 001 5083 D Sub SLO9 LK JPA Voc 3 5 4 Konrad Zuse Strafe 1 5 5 07745 EArunkabel Jena GmbH Tragarm komplett AFP 001 9003 Stromlaufplan 1 Blatt Hub Motor 1 7 E i 5 2 HY200 1507 OD50AXO04 4 B ExsaAtzteil H 001 8042 4 3 T Wopf LP oben 001 5088 Ersatztail H O01 50845 20 STI LEI 5x1 BU LEI 5x1 001 5050 e JPL 68100 010 Flexkabel 10 119 001 5037 Ersatzteil NW 00 5086730 BERG 68101 010 suf FACE 2 bastuckt werden Kennzeichnung von Pin auf LP ist alschl STi D Sub SL15 LKH _ _ ____ iu _ 4 p a c 3 id Kopf LP unten mit R ndkabel 001 5286 Jena
70. ON SOLVENT CLEAN FLUSHES PRE INJECTION SAMPLE CLEAN FLUSHES FILL STROKES and so on If the sampler cycle is interrupted before injection no internal counters are incremented and the GC sampler can be started again without the need for resetting You can also use the WASHING SYRINGE parameter in the UTILITIES page of the CP 9050 see table page 2 23 In this case wetting your syringe will be done with solvent only CHROMPACK 3 17 CP 9050 AUTOMATIC LIQUID SAMPLER Operation NOTE 3 18 FST LST INJ METH M 01 101 1 1 V CP 9050 sampler display When the sampler mode CP 9001 2 Page 1 Line 12 is set to 51 the keyboard of the CP 9050 sampler will be locked no keys are active anymore with the exception of the key When the GC Sampler combination is started the CP 9050 display changes to INJECT SAMP METH SINGLE A Y where X is the processed and Y the sampler method used Aborting an injection cycle With the C key it is possible to abort the started cycle even when the keyboard of the sampler is locked in the sampling phase of the CP 9050 sampler only the sampler stops hoid situation Now there are two possibilities 1 after pressing the key the sampler continues where it was stopped 2 after pressing the C key a second time the sampler and CP 9001 2 will be stopped If the syringe is already contaminated or filled the sample is automatically thrown away and the s
71. P 9050 sampler must be equipped with software revision 2 or higher The software revision number can be found in the upper line of page 10 of a CP 9001 e g REVISION 2 01 NOTE With software revision 1 only 94X and 91X type sampiers can be controlled 2 4 CHROMPACK 2 5 Installation 9050 AUTOMATIC LIQUID SAMPLER INSTALLING THE RS232 INTERFACE BOARD IN THE CP 9001 2 GC A CP 9001 2 meant to control a CP 9050 sampler must be equipped with a revision 1 04 or higher R5232 interface board The revision number of the R 3232 interface board can be found at the printed circuit board This RS232 interface board has to be installed in one of the two slots at the basic control board of the CP 9001 2 Figure 2 2 shows the required dip switch jumper setting and interface cable to the sampler connector If no TP has been installed all positions of dipswitch S1 must be set to OFF In that case the TP cannot be programmed Page 1 Line 13 shows optional If one TP has been installed only position 1 must be set to ON and in case of two TP OCI s position 2 must be set to ON Page 1 Line 13 shows TP OCI which means the TP OCI is programmable A E pe ENS i tee 31 EE 1xOCl 2xOCcl UM gd 1 04 CHROMPACK ART Fiqure 2 2 RS232 Board Switch Jumper Settings and Cable Connection CHROMPACK 2 5 CP 9050 AUTOMATIC LIQUID SAMPLER
72. PPLIER 7 7 005 WASH WASTE VIAL SPRING DESCRIPTION 7 22 505300 REV 1 01 GRUNDPLATTE BASE BODY COMPLETE 110 220v DOC 001 9202 1 2 DESCRIPTION NAR 1 OH NUMBER 5031 TRANSFORMER SOLDER GROUP SERIALN 10001 10300 NC 8224 Y AXIS MOTOR ASSY WITH MOLEX CON SERIALN 102754 8024 Y AXIS MOTOR ASSY WITH AMP CON SERIALN 10001 10300 SCHO63 SENSOR INDEA at 2 310 SCH68 TRAY HOLDERS AXIS BEARING ASSY BELT ATTACHMENT Y AXIS N C 102992 5121 DISPLAY KEYBOARD ASSY 7 053 FRONT COVER NC RAIL C REAR COVER WITH SILKSCREEN 02996 BODY BASE PLATE 001 5132 LINE FILTER 102995 i colo Ur c so D You can use this mainboard only after first updating with the Mainboard assy s For assy contents see page 2 12 505300 REV 1 01 mrt re o TT TRAGER KOMPL ARM ASSY DOC 001 9003 DESCRIPTION 2 12220 tepran raan 5 ped aag dna de da es PE 1 te tart MARS iS inks stat PN EUST Q4 dla DHE Whe Pala oec MENO FIC as eR SCHO14 15 TEETH LOOSE PULLEY 102755 SCHOIS PULLEY SHAFT 5073 B AR
73. TR CLEAN SLV INJ PORT of the sampler page Page 4 Line 1 6 If required get access to the special sampler parameters AIR VOL FILL VOL CLEAN SLV SOLV PLUG AIR PLUG VISCOSITY FILL SPEED INJ SPEED INJ DELAY gt INJ DELAY INJ TIME AND gt INJ TIME by entering 1 in Page 4 Line 7 OPTIONS and program the special sampler parameters If required save the GC method Page 5 Line 1 If required repeat steps 2 to 6 or program methods via EDIT METHOD Page 5 Line 3 Program one or more vial ranges in Page 8 Line 1 7 and GC methods if no method is specified METH 0 with the vial range all vials of this range will be processed with the sampler parameters programmed in the active memory of the CP 9001 If required program the PLUNGER COUNT WARNING LIMIT and RESET the ACTUAL PLUNGER COUNT and SEPTUM COUNTERS If one wants to start all over again reset the sampler GC by entering 0 in Page 8 Line 10 RESET It 5 pest to use RESET 0 before starting a new series of injections to be sure the sampler starts with the first injection of the first vial in the first vial range programmed many cases the history of the sampter GC combination is not known exactly 3 70 CHROMPACK Maintenance bu SECTION 4 MAINTENANCE 41 TIMETABLE FOR MAINTENANCE UT 042 SYRINGES 43 SEPTA oca CHROMPACK CP 9050 AUTOMATIC LIQUID SAMPLER Page 4 3 4 3 4 3 Maintenance 4 4 2 4 3
74. UG and SOLVENT PLUG wiil be used in the so called sandwich injection technique where solvent and sample will be separated by the programmed AIR PLUG When using a SOLVENT PLUG and AIR PLUG the conditions PRE INJECTION SAMPLE CLEAN FLUSHES 0 and FILL STROKES 0 must be fuifiitedl not possible to enter a value for this parameter DATA RANGE blinking check the above mentioned conditions Do not program a total INJ VOL AIR VOL SOLV PLUG AIR PLUG which is bigger than the total syringe volumel LINE 6 VISCOSITY VISCOSITY DELAY 0 9 9 s in steps of 0 1 s default 0 5 s parameter specifies the delay between sample pullup and sample ejection while sampling win FILL STROKES The same delay time is used after the last fill stroke before the syringe will be taken out of the vial This feature is especially useful for handling viscous samples LINE 7 FILL SPEED PLUNGER SPEED while pulling up sample 0 1 25 ifs in steps of 0 1 defauit 5 5 The speed of the upward plunger movement during sampling PRE INJECTION SAMPLE CLEAN FLUSHES and FILL STROKES can be set here This feature is especially useful for handling viscous samples LINE 8 INJ SPEED PLUNGER SPEED while injecting 0 1 25 pi s in steps of 0 1 ul s default 25 ulis The speed of the downward plunger movement during injection can be set here So if a fast or slow injection has to be performed the plunger speed be set here accordin
75. Update Distribution Service manual CP 9050 505300 No 023 Instrument CP 9050 autosampler Date 3 September 1996 Subject Update manual from REV 1 00 to REV 1 05 Originator Stang Enclosures drawing Author Jan Vos File Service Manual CP 9050 505300 No of pages 6 Dear Colleagues 1 Remove front page add front page REV 1 05 2 Remove DOC NO CRPO004 in section 1 add the including drawing 3 Remove pages 2 7 2 8 and 2 11 in section 2 add the pages with REV 1 01 4 Please insert this page in section 6 5 023 1 FROM CHROMATOGRAPHERS FOR CHROMATOGRAPHERS _ Chrompack is not responsible for printing errors and reserves the right io change specifications designs and prices without notice and liability Copyright Chrompack Intemational came CHROMPACK Technical Service Bulletin Distribution SE SMISRICP No 7921 BTW No instrument Sampler CP 9050 Date 2 September 1996 Subject Spare parts Injector head Originator Stang Enclosures CRP Injection head Author Jan Vos File TSB binder Service manual Total no of pages 2 Dear colleagues Inside the injector head you will find two printed circuit boards connected by a soldered flat cable Due to the serviceability exchanging this connection can give problems Therefore the supplier has changed this connection in such a way that it is much easier to replace If the problem is related to these boards you
76. ____ 7x18 0x14 _ BCD Active State _________ Start Buzz owon Manual inj Buzz Bar Code Scanning Injection Position X as 0 1 x mm 7 4482 7 Y as 0 1 x 6 960 6 Penetration 0 1 x mm 30 1339 30 Reference Adjust X as 0 1 x mm 7 4482 1522 Sample Penetration Penetration Depth 30 547 30 Wash Penetration Solvent Penetration 0 1 x mm 30 547 30 Waste Penetration 0 1 x mm 30 Motor Speed x 1 mm sec Syringe MOVE UP 50 125 WASH DOWN 50 125 SAMPt DOWN 50 125 4 50 125 Solvent PULL UP 01 pif sec 1 250 EJECT 1 250 Sample EJECT 1 250 Syringe TEST 0 1 1 250 X amp Y axis SPEED 1mm sec 50 125 oyringe test Filling 0 1 0 100 1 Serial Baudrate x 100 6 12 24 48 96 5 Serial Link Test Pos Sensors Tes ____ _ ____ CHROMPACK P 9050 AUTOMATIC LIQUID SAMPLER Installation METHOD PARAMETERS Table 11 METHOD PARAMETERS RANGE DEFAULT METH em Injection MODE SPECIAL pape ft Volume SOLVENT 0 5 0 Volume AIR 0 5 0 Volume SAMPLE pl 0 1 Volume AIR 0 Clean Syringe SOLVENT PRE 0 99 Clean Syringe SAMPLE PRE 0 99 Filling Vol gal 0 1 5 0 2 5 Number Fillstrokes 0 99 7
77. a clean syringe with the nominal needle length of 5imm Loosen the set screws at the needle guide stops 3 with a 1 3 mm hex key Now the needle guide is no longer under spring load and may be moved up or down until the needle tip is about 0 5mm inside the needle guide 6 Fasten the allen hex screws of both the needle guide stops Double check the set position by cautiously pushing up the needle quide until the needle tip may be sensed with the finger Check the gap below the needle quide stops to be 0 omm 1 INJECTION HEAD 2 PLUNGER HOLDER 3 NEEDLE GUIDE STOP 2X 4 SYRINGE 4 SYRINGE FIXING LEVER NEEDLE GUIDE 505300 REV 1 00 3 4 EXCHANGING THE COMPLETE INJECTION HEAD Turn the instrument off and disconnect the power cord Remove the syringe Push the injection head to the lefthand side of the crossrail Gently unplug the flatcable that is connected to the injection head Use an allen hex key to loosen the two screws holding the injection head to the cross side The upper and lower screw can be exposed by moving the syringe carrier by hand up or down so that the hole in the syringe carrier is lined up with one of the screws To mount the replacement injection head proceed in the reverse order 1 INJECTION HEAD 2 SYRINGE CARRIER 3 SYRINGE 4 INJECTION HEAD FIXING SCREWS 505300 REV 1 00 3 5 EXCHANGING THE FRONT PANEL WITH DISPLAY AND KEYBOARD Disable
78. ampler The sampier method number used for storage 1 9 depends on the value of SPECIAL INJECTION METHODS oniy normal injection is possible in Page 4 of the CP 9001 2 Default SPECIAL 1 which means that all sampler parameters are stored in sampler method 1 used for normal injection GC method is a method of the CP 9001 2 containing GC and sampler parameters GC methods are stored in the CP 9001 2 sampler method is a method of the CP 9050 sampler containing only sampler parameters methods are stored in the sampler 1 6 CHROMPACK Installation CP 9050 AUTOMATIC LIQUID SAMPLER SECTION INSTALLATION Page 2 1 GENERAL 2 3 22 ASSEMBLING THE CP 9050 SAMPLER 2 3 2 3 CABLE CONNECTIONS CP 9050 2 4 24 SOFTWARE UPDATE OF THE CP 9001 GC 2 4 2 5 INSTALLING THE 5232 INTERFACE BOARD IN THE CP 9001 2 GC 2 5 2 6 MOUNTING CONNECTING AN EXTRA RS232 PLUG AND CABLES IN THE CP 9001 2 GC 2 6 2 7 REPLACING THE STANDARD COVERS OF THE 9001 GC BY SAMPLER COVERS 2 6 2 8 REPLACING STANDARD SEPTUM CAP S BY SAMPLER SEPTUM CAP S 2 7 2 9 MOUNTING THE CP 9050 SAMPLER 2 7 29 1 _ SETTING THE CONFIGURATION PARAMETERS 2 8 29 2 ADJUSTING THE INJECTION DEPTHS FOR DIFFERENT INJECTION PORTS 2 8 293 INSTALLING A SYRINGE 2 9 2 94 VIALS 2 9 295 ADJUSTING DEPTH FOR SAMPLE SOLVENT PICKUP AND WASHING 2 10 296 CONFIGURATION SETUP AND ADJUSTMENT PROCEDURES 2 10 2 10 CONFIGURATION PARAMETERS 2 11 2 10 1 CONFIGURATION 2
79. ange d b distance solve screw a and move the par upstairs mount the syringe check fhe position j correction picture solve screw b and move the part 8 downstairs fixing the syringe plunger power on in syringe fest blinking casignce x m _ ___ y vA or Or on PICTURE B reflector area sensor TE hs LIE i DETAIL A sieding rods wrong correc f wrong solve the screws 1 push the needle guide in fhe same position like the needte split fix fhe screws 1 solve the screw 2 and correct the reflector position rm needle guide MUN T PO DETAIL A N PICTURE OOOQOOOOQOOQQQO COO C AX XX 19 9 IC f optokoppler for y direction nnm rnm Grundplatte kompl 7 ER amm d mcm m L eee plaslic washers there are problems a
80. cated on the right side of the CP 9050 one in front and one in the rear position The thirt hole is located in the bottom plate of the Instrument Base Unit under the Sample Tray The position of the sampler is hereby fixed Unpack the Sample Tray and place it into the Instrument Base Uniton Make sure that the Sample Tray is placed in the correct way which means the 2 pins in the Instrument Base Unit fit into the bottom of the Sample Tray and the vial numbering can be read The installation of the sampler can be divided in five steps a SETTING THE CONFIGURATION PARAMETERS Section 2 9 1 b ADJUSTING THE INJECTION DEPTHS Section 2 9 2 C INSTALLING A SYRINGE Section 2 9 3 d CLEANING VIALS Section 2 9 4 ADJUSTING DEPTH FOR SAMPLE SOLVENT PICKUP AND SAMPLE SOLVENT WASHING Section 2 9 5 CHROMPACK 2 7 CP 9050 AUTOMATIC LIQUID SAMPLER Installation 2 9 1 2 9 2 SETTING THE CONFIGURATION PARAMETERS a Connect the power cord b Switch on the sampler while pressing the key on the control terminal The display shows CONFIGURATION blinking C Press the V key to enter this option d Follow the procedure given in Section 2 10 1 2 10 20 CONFIGURATION ADJUSTING THE INJECTION DEPTHS FOR DIFFERENT INJECTION PORTS For packed splitless and on column injection it is best to inject as deep as possible into the injection port For splitter injection splitter injection port or splitter split
81. d clean the syringe The syringe might have to be replaced every 2 3 months depending use Cleaning of the syringe by end user Clean the syringe as recommended by the syringe manufacturer Biocked needles can be cleaned with appropriate cleaning wires Dirty glass barrels can be cleaned with suitable solvents as Hamilton Cleaninq Solution Dirty plungers can be wiped off with a fibre free cloth Do not touch the piunger with your hands When cleaning doesn t help replace the syringe Replacing septa by the end user bleed septa should always be used in packed splitter splitless and wide bore injection ports because these produce the lowest background noise Two types of high temperature low bleed septa are recommend one for temperatures up to 375 C Chromsep Blue and the other for temperatures up to 400 C Chromsep Red With the CP 90 sampler and the point of the syringe in good shape septa need to be replaced after 150 200 injections In case the needle tip of the syringe has been damaged septa can start leaking very soon 505300 REV 1 00 MAINTENANCE PROCEDURES The next points of maintenance should carried out every year BODY ASSEMBLY Remove arm assembly rear cover right cover caution take care of the Keyboard display cable See section 1 DOC NO 02 Y AXIS MOTOR Fixing nuts Y AXIS BELT Tightening of the belt attachment Tighteninq of the clamp Belt tension Y AXIS BEARI
82. date V ONLY when SOLVENT and WASTE penetration are programmed 2 16 CHROMPACK Installation 9050 AUTOMATIC LIQUID SAMPLER 2 10 15 MOTOR SPEEDS Motor speeds are in 1mm sec unless mentioned different The default values have proven good results and should be changed only if really necessary rrr SYRINGE MOVE UP 80 V C Syringe moving upwarts With 11 or 4 values can be changed SYRINGE WASH DOWN 80 1 C Syringe moving down to cleaning vials With 1 or values can be changed SYRINGE SAMPL DOWN 8 V C Syringe moving down to sampie vial With 1 values can be changed SYRINGE INJECT 100 V1 C Syringe moving down to iniect sample With or 4 values can be changed Plunger pulling up solvent With 1 or 4 values can be changed SOLVENT EJECT 150 V Plunger ejecting solvent With t or 4 values can be changed CHROMPACK 2 17 CP 9050 AUTOMATIC LIQUID SAMPLER SAMPLE EJECT 200 IV IC installation Plunger ejecting sample during filling strokes With or values can be changed SYRINGE TEST 0 1 50 LL GL AL With 1 or 4 values can be changed Plungerspeed when testing your syringe or checking your dead volume n amp Y AXIS SPEED tmm sec 100 V C speed with which the Injection Head moves to the injec
83. ds can be programmed in Page 5 Without sampler the five METHODS and the METHOD MODE in RUN CONTROL METHODS will be saved as well d One can control a temperature programmable on column injector TP which can be used with the CP 9050 liquid sampler The way the is used be selected in Page 1 Line 13 one or two TP 5 with free programmable temperature or temperature coupied to the oven temperature In case of free programmable TP 5 the relevant parameters show up in Page 7 Line 16 and up CHROMPACK 1 5 CP 9050 AUTOMATIC LIQUID SAMPLER Introduction NOTE 1 4 NOTE NOTE NOTE Programming VLV 1 or VLV 2 in Tx program only disable the default START or STOP function of that relay in software revision 1 0X both default START and STOP functions were disabled in case VLV 1 and or VLV 2 had been programmed in a Tx program In case of a TP relay VLV 2 is used for switching the fan cooling of the TP OCI VLV 3 is used for the opening of the seal of the front TP and VLV 4 is used for the opening of the seal of the rear TP GENERAL OPERATION The CP 9001 2 with software release 2 or higher can store up to eleven GC methods A GC method holds all GC parameters of Page 1 2 3 4 most of the parameters of Page 7 and some parameters of Page 10 Thus the sampier parameters of Page 4 are included in a GC method When the CP 9050 sampler is activated Page
84. e Section 2 13 Ignore this message and the subsequent message After change of sampler software EPROM Ignore if it was not caused RESET TO DEFAULT see Section 2 13 or sampler software exchange EPROM for Every time a motor moves towards a switch the distance moved is checked against the maximum possible travelling distance If the switch is not activated after this distance either the switch is defective or the motor does not move Check cables connections See Section 2 10 19 POSITION Similar case as above but the switch remains activated This message indicates a software error and should normally not appear If the message persists call for NOTE in a few cases the data range given in the CP 9001 2 is greater than the CP 9050 sampler can accept 52 SAMPLER ERROR MESSAGES CP 9050 SAMPLER DISPLAY WARNING SAMPLER SETUP LOST This message is displayed if the checksum calculated correct this message press Weak backup battery on Control Board CHECK BATTERY ON See WARNING SAMPLER SETUP LOST CPU MODULE service to repiace the batteries SWITCH NOT DETECTED due to a mechanical or electronic failure SENSORS TEST SWITCH ALWAYS CLOSED ERROR N service 5 3 SAMPLER ERRORS 5 CHECKS AND SOLUTIONS Symptom Iniection n id picks up vials Check if the sy needle is completely retracted into the needle guide when in its home position and uncer power Touch with your finger th
85. e or injury caused by misunderstanding of the information in this manual indications in the manual This manual contains warnings and precautionary statements that can prevent personal injury instrument damage and loss of data if properly followed Statements of this nature are called to your attention by the following symbols The NOTE calis attention to procedure practice or the like which if not correctly performed or adhered to could result in inadequate functioning of the instrument The WARNING calls attention to a procedure practice or the like which if not correctly performed or adhered to could result in personal injury or damage to the product Indications on the instrument Specific symbols drawing attention to safety hazards have been applied on appropriate places on the nstrument The following symbols can be encountered Instruction manual symbol Indicates that the user should refer to the manual before operating the equipment Indicates dangerous voltage terminals fed from the interior by voltage exceeding 1000 V must be so marked Protective conductor terminal For protection against electrical shock in case of a fault Used with field wiring terminals to indicate the terminal which must be connected to ground before operating equipment Radioactive hazard Indicates that the instrument contains radioactive components which may cause personal injury when handled incorrectly CHROMPACK 0
86. e publishers Issued by Chrompack Int Service Department Copyright 9 May 1998 by Chrompack 505300 REV 1 67 aree 0 1 SECTION 0 SAFETY INFORMATION PAGE DESCRIPTION 0 2 Safety information 0 4 General safety precautions 505300 REV 1 00 tone SAFETY INFORMATION In accordance to Chrompack s commitment to customer service and safety this instrument and its accompanying documentation complies with the CE NEN 5509 specifications To prevent any injury to the user or any damage to the instrument it is essential that you read the information in this chapter If this manual is not in your mother language and if you have problems understanding the text we advise you to contact your Chrompack office for assistance Chrompack cannot accept responsibility for any damage or injury caused by misunderstanding of the information in this manual Indications in the manual This manual contains warnings and precautionary statements that can prevent personal injury instrument damage and loss of data if properly followed Statements of this nature are called to your attention by the following symbols NOTE The NOTE calls attention to procedure practice or the like which if not correctly performed or adhered to could result in inadequate functioning of the instrument WARNING The WARNING calls attention to a procedure practice or the like which if not correctly performed or adhered to could resu
87. e set to zero NUMBER OF FILL STROKES 0 99 default 7 This parameter specifies the number of pull ups using the FILL VOLUME This parameter serves to controi the filling of the syringe It may happen that air bubbles remain below the plunger after pull up By moving the plunger down fast after a pull up these air bubbles can be If zero is selected for FILL STROKES the plunger will be pulled up only once using the If you want a solvent plug with the volume of the syringe needle on top of the sample to compensate for needie dead volume PRE INJECTION SOLVENT CLEAN FLUSHES gt 0 this NUMBER OF POST INJECTION SOLVENT CLEAN FLUSHES 0 99 default Q This parameter specifies the number of times the syringe is washed with solvent after the If the sampler is stopped in the sampling phase before injection but after taking some sample the syringe is cleaned with the programmed number of SOLVENT CLEAN INJECTION PORT front rear default rear Here one can select the injection port to be used in case a front and a rear injection port are Message ENTER 1 to program 0 1 default 0 By entering a 4 in this line a new page with additional parameters shows up This page contains parameters that need to be changed less frequently For further detaiis see Section 3 6 PROGRAMMING SPECIAL SAMPLER PARAMETERS Entering a 1 is the only way to get access to the additional parameters NOTE LINE 4 FILLSTR worked out NOTE INJECTION
88. e start of that vial range A RESET 0 Page 8 Line 10 resets the sampler to the first injection of the first vial range Default values for a programmed syringe In case one wants to use a syringe with a different capacity e g change from a 5 to a 10 ul syringe this capacity has to be programmed in the CONFIGURATION PARAMETERS of the CP 9050 sampler see Section 2 10 amp 2 10 1 Activating the sampler by setting the sampler mode Page 1 Line 12 to 51 the CP 9001 2 gets the syringe size from the sampler and adjusts the data ranges of the syringe related parameters accordingly If no GC method was loaded during activation of the sampler the sampler parameters will be set to default values if a GC method was loaded the values of the sampler parameters do not change to default values CHROMPACK 3 19 E om CP 9050 AUTOMATIC LIQUID SAMPLER Operation 3 11 SUMMARY OF PROGRAMMING The programming of the CP 9050 sampler can be summarized in nine steps 1 2 3 4 5 6 7 8 Activate the sampler by entering 51 in Page 1 Line 12 SAMPLER By doing this the CP 9001 2 gets information from the CP 9050 sampler about installed programmed syringe size and vial tray The default values and programmable data ranges will be set according to the instaliad programmed syringe size and vial tray Program the six standard sampler parameters INJ VOL INJ VIAL CLEAN SMP FILLS
89. e underside of the needle holder If the needle tip can be detected the needle is not fully retracted if not fully retracted check the length of the syringe needle used nominal length is 51 mm 2 the needle length is OK adjust the needle guide position Loosen the screws in the needie quide stops just below both springs of the needle quide with the 1 3 mm Allen hex key Shift the needle quide in the right position needle point about 0 5 mm retracted and fasten the screws in the needle quide stops CHRON T CK Troubie shooting CP 9050 AUTOMATIC LIQUID SAMPLER Symptom Sampler seems to skip samples If skipping samples is an intermittent problem it is most likely that you are using vials that too long or too short so that the vial detector does not function properly for every vial Check the height of vials against the specified height see Section 3 3 PREPARING VIALS Symptom Injection head moves to wrong X position when picking up sample or solvent Check if the right vial tray has been selected during CONFIGURATION SETUP see Section 2 10 CONFIGURATION PARAMETERS Symptom Wrong syringe needle penetration depth after adjustment solvent waste sample inject position A common error is that the adjusted penetration depth is not actually stored with the key and the old depth is remained See Sections 2 10 11 2 10 14 for adiusting the penetration depth at solvent waste sample and in
90. ed separately one or more of the nine steps have to be taken ASSEMBLING THE CP 3050 SAMPLER After unpacking position the main body of the instrument on a flat table Unpack the Crossrail and the Injection Head Place the Crossrail on the LEFT and RIGHT Arm Support of the Instrument Base Unit and tight it up with the 2 hexagonal screws Connect the flat cable of the Crossrail with the Instrument Base Unit Take the Injection Head and keep one of the screws on the long 2 5 mm Allen hex key and line up the hole in the black syringe carrier plate with the upper hole in the back panel of the injection head The two holes in turn need to be aligned with the upper hole in the cross slide and the screw has to be pushed through and tightened to mount the injection head while the guidance pins in the cross slide fit into the holes in the back panel of the injection head Now slide the syringe carrier downwards until the hole in the black syringe carrier plate lines up with the lower hole in the of the back panel of the injection head The second mounting screw can be inserted and tightened Connect the flat cable to the injection head CHROMPACK 2 3 CP 9050 AUTOMATIC LIQUID SAMPLER Installation 2 3 CABLE CONNECTIONS Check if the Instrument you received has the right voitage OPTIONS SERIAL BCD OUTPUT GC IN OUT fb Figure 2 1 Back panel 9050 2 4 SOFTWARE UPDATE OF THE CP 9001 GC CP 9001 meant to control a C
91. ed through the split vent 17 hydrogen is used as the carrier gas or if toxic compounds are analyzed the spiit vent must be connected via external tubing to a proper fume hood The same applies for the exhaust of the detector When measuring gas flow rates through an FID or NPD never measure air and hydrogen together They should be measured separately to minimize explosion nazard Cold compounds such as carbon dioxide liquid nitrogen may cause severe burns Refer to Chrompack manual Cryogenic frostbite Cat 505079 for detailed information When handling sharp objects such as fused silica or stainless steel capillaries or capillary columns traps syringes etc avoid puncture of the skin Never try to repair or replace any component that is not described in this manual without the assistance of a Chrompack service engineer Unauthorized repairs or modifications will resuit in rejection of warranty claims Always disconnect the power cord before attempting any type of maintenance Note that capacitors inside the instrument may still be charged even if the instrument is turned off Use proper tools when working on the instrument to prevent danger for yourself and or damage to the instrument Only use fuses of the type and current rating specified Do not use repaired fuses and do not short circuit the fuse holder Damage can result if the instrument is stored under unfavorable conditions for prolonged periods e g subject
92. er with 1 or 4 Update and Quit with VI Discard and Quit with C 2 10 2 NUMBER OF INJECTION POINTS set the number of injection points 1 4 2 V IC Set this value at 2 even if oniy one injection port is available 2 10 3 WASHING POSITION WASH POSITION LEFT C Set to LEFT with or 4 d 2 10 4 START SIGNAL ee START SIGNAL REMOTE V Set to REMOTE with or 2 10 5 SYRINGE VOLUME set to volume of syringe used with 1 or 4 2 12 CHROMPACK installation CP 9050 AUTOMATIC LIQUID SAMPLER 2 106 TRAY SELECTION SELECTROWXCOL ROW X COL TRAY 7 X 15 SELECTROWXCOL Set the 7 x 15 tray with or 1 2 107 BCD ACTIVE STATE Sets the active logical level 800 ac ACTIVE STATE HIGH V1 C Select HIGH or LOW with t or Only important if this option is available and used 2 10 8 START CYCLE BUZZER START CYCLE BUZZ ON C Select ON or OFF with t or 4 2 10 9 MANUAL INJECTION BUZZER MANUAL INJ BUZZZ ON C Select ON or OFF with 1 4 2 10 10 BARCODE SCANNING This option is not available although on and off can be selected CHROMPACK 2 13 9050 AUTOMATIC LIQUID SAMPLER Installation 2 10 11 INJECTION POSITION INJECT POSITION No 0 Injection position 0 rear injection port Injection position 1 front injection port One or two injection points can be programmed depending on hardware pre
93. eters and sampter parameters With the CP 9050 sampler different injection techniques can be used normal hot needle sandwich Since many parameters are programmable not only pre injection solvent and or sample cleaning post injection solvent cleaning etc but also speed of injection and residence time before and after injection all kinds of injection techniques can be optimized To show the possibilities of these samplers three examples of injection techniques wiil be discussed a A HOT NEEDLE INJECTION b ASIMPLE SANDWICH INJECTION c A MORE ELABORATE SANDWICH INJECTION In these examples we assume the needle volume is 1 0 2 of sample or solvent evaporates from the needle during injection a A HOT NEEDLE INJECTION After sampling 1 1 the total amount of sample in barrel needle is 2 pl as be seen after taking 1 gal air plug 2 By programming a pre injection detay of a few hundred milliseconds the needle can be heated before injection During injection part of the sample in the needle evaporates thus after injection 3 stays 0 8 In this way we have injected 2 0 8 1 2 ul of sample assuming no discrimination during the 1 2 3 evaporation from the needle Figure 3 1 Hot needle injection CHROMPACK 3 3 car 9050 AUTOMATIC LIQUID SAMPLER Operation b A SIMPLE SANDWICH INJECTION A possibility to inject the sarnpied amount more precisely will be whe
94. gly 3 10 CHROMPACK cero Operation NOTE NOTE CP 9050 AUTOMATIC LIQUID SAMPLER LINE lt INJ DELAY PRE INJECTION DELAY 0 99 9 s in steps of 0 1 s defauit 0 3 s After the syringe moves down into the injection port a certain delay time can be programmed before the sample will be injected In case of a fast injection one can select a short delay time and in case of the so called hot needle injection technique this delay time must be set long enough to warm up the needie in case of temperature programmabie on column injection ports OCI s this time sets the time the pneumatic seal is closed before injection see Section 3 9 TEMPERATURE PROGRAMMABLE ON COLUMN INJECTOR LINE 10 gt INJ DELAY POST INJECTION OELAY 0 99 9 s in steps of 0 1 s default 0 3 s This parameter specifies the delay between injection and the moment the syringe will be pulled out of the injection port This delay time can be useful for controlling the evaporation from the needle case of temperature programmable on column injection ports TP OCI s this time sets the time after the injection when the syringe will be withdrawn LINE 11 INJ TIME INJECTION TIME for valve switching 0 999 s in steps of 1 s default 0 s This parameter specifies the time between start of the sampier cycle and injection practice to be effective the programmed time shouid be longer than the time between start of sampler cycle and
95. hat hold the board to the black instrument chassis Carefully lift the board vertically out of the housing Remove the EPROM by means of a chip puller Read also the procedure Exchanging an EPROM on the next page Insert the EPROM in the corresponding socket of the replacement processor board 505300 REV 1 00 3 6 1 3 6 To install the replacement board proceed in reverse order through the above mentioned steps Even though all plugs and its advisable sockets are keyed and therefor prevent mix up wires to double check these connections before turning on the instrument IMPORTANT NOTE After exchanging mechanical or electronically parts it s mandatory to set the configuration parameters See usermanual page 2 8 M 505300 REV 1 00 Exchanging the crossrail HB i Disable the SAMPLER CONTROL PROGRAM on page 1 of the CP 9001 2 GC by entering code 50 on line 12 The 9050 keyboard is not locked anymore Turn the instrument off and disconnect the power cord Remove the injection head Refer to page 3 4 for more information about the injection head Disconnect the crossrail flatcable that is plugged into the processor board Loosen the Allen head screws of the crossrail leg at the right hand side oniy C Carefully measure the distance between the left crossrail end and the left leg D and between the right crossrail leg and the right end E
96. ing errors and reserves the right to change specifications designs and prices without noce and liabdity 2 Copyright Chrompack Inlematiaral 6 3 PRODUCT NOTES AND EQUIPMENT RELATED PRODUCTS 505300 REV 1 00 CP 9050 SAMPLER Feature AUTOMATIC LIQUID Specifications Tray capacity Sample capacity Syringes Minimum sample volume Injection volume Injection on to Reproducibility Control of the sampler Programming via sampler Programming via CP 3001 2 505300 REV 1 00 Injection into 2 injection ports front or rear Stepper motor driven movements speed of all movements programmable Removable sample tray 105 vials 7 rows of 15 vialal 2 ml or 0 1 ml 2 ml vial with 0 1 ml insert Standard Hamilton 700 series 5 or 19 pl ul 0 1 ml insert Programmable in steps of 0 1 pl up te 5 10 pl Packed splitter splitless wide bore and temperature programmed on column injection ports lt 1 0 1 pol n C4 n C45 in n C packed column The sampler is controlled 9001 2 ac Syringe capacity 5 10 pl Number of injection ports 2 front or rear Vial detection on off Buzzer at start of cycle on off Motor speeds Sample penetration depth Solvent penetration depth Waste penetration depth Injection depth separately programmable for both injection ports Injection volume 9 5 0 10 wl Number of injections per vial 1 99
97. injection this time depends on the number of fill strokes and the number of pre injection sample solvent clean flushes LINE 12 INJ TIME POST INJECTION TIME for valve switching 0 999 s in steps of 1 s default 5 This parameter specifies the time between injection and deactivation of a valve REMARK Line 44 and 12 are not being used Because the CP 9050 is a fully integrated Liquid Sampler programming of a valve is done by using the TX table of the CP 9001 2 Example One wants to activate a splitter splitless valve connected t relay 3 VLV 3 of the CP 9001 2 before iniection This valve must stay activated till 2 minutes after injection The following parameters must be programmed TX program page 3 1 Time 0 Valve Ext 3 2 Time 2 Valve Ext 3 Note If the TX program of the CP 9001 2 relay 3 VLV 3 is programmed at time zero it will be activated when the sampler cycle starts so before the GC The time between start of the sampler and start of the GC program is dependent on the activities of the sampler number of clean strokes fill strokes etc Two minutes after injection relay 3 will be deactivated CHROMPACK 3 11 6 mo CP 9050 AUTOMATIC LIQUID SAMPLER Operation LINE 13 SPECIAL Choice of sampler method The default value is 1 which means sampler parameters will be loaded from the CP 9001 2 to method 1 of the sa
98. injection port s This can easily be done by means of the allen hex screws which tighten the Crossrail on the Instrument Base Unit 1 2 3 INSTRUMENT BASE UNIT The Instrument Base Unit houses the electronics the control terminal and the tray compartment which is partially open at the bottom At the left of the Instrument Base Unit viais for solvent right and waste left can be inserted The Instrument Base Unit is mounted with three screws on top of the sampler cover of the CP 9001 2 GC 1 4 CHROMPACK Introduction CP 9050 AUTOMATIC LIQUID SAMPLER 1 2 4 1 3 NOTE NOTE CONTROL TERMINAL The Control Terminal is used during setup for programming the CONFIGURATION PARAMETERS The normal programming of METHOD PARAMETERS is done via the CP 9001 2 keyboard and display The Control Terminal contains a two line liquid crystal display LCD and a keyboard with eight keys On the first line of the display and sometimes at the beginning of the second line there is a description of the menu or the parameter Values are displayed on the second line below the corresponding description A selected parameter value a value that can be changed is displayed as blinking On the keyboard the key set C V selects the different functions Methods Utilities Clear and Validate The four arrow keys are used to input values The parameter to be changed is selected by pressing the or key until it is displayed as b
99. ject position Symptom Sampler does not start a sample injection cycle First of all check for error messages in the displays of the CP 9001 2 and CP 9050 sampler some error messages are delayed for about 6 seconds since retries are done if commands not accepted If no error messages were seen check Page 10 Line 4 SAMPL ERR value other than 0 means the last occurred error Since this error will not be cleared automatically enter a zero for this line and retry if the symptom persists check again Page 10 Line 4 SAMPL ERR Now a value other than 0 shows the real error code see Section 5 1 SAMPLER ERROR MESSAGES CP 9001 2 DISPLAY Sampler not activated by entering 51 Page 1 Line 12 5AMPLER 901X on Undefined vial ranges Symptom Excessive noise from syringe plunger or any other drive Turn the instrument off and check if syringe plunger syringe carrier or injection head X slide when being moved by hand let you feel any resistance If smooth and even movement results there 1s no indication that any of the motors are faulty or any excessive mechanical resistance exists Since certain frequencies of the stepper motors can cause a resonance in the different instrument parts change the speed of the motor where the noise originates see Section 2 10 15 MOTORS SPEED A change up or down will most likely eliminate the noise problem It should be noted that this problem will not hurt the instrument symptom Sy
100. l mi mi ml bl e 2 217 t 2 JU e D 212 Ahnateuerung 415672 RNYOSPE100 AHALYTIK FP Jena Gui 31745 Jana 1 An R W d rd E u H T 2 3 4 J 9 d C Le C 5 n gt LPHLAS zur Tastatur Stromlaufplan Fant Main board ALS R 001 9293 Alatt 1 3 BlEtter iacu uada NA ua Se IMotortreiber 1 3 10 3 11 120 121 2 122 123 PH2B 100nF4 BLISF Xi Motortreiher H2 SUM UM VHOT 135 O0nF4 132 133 100n 4 Injektorkopfkabel Pin 1 dieser Buchsenleiste mus bei der Bestiickung auf Pin 4 der 25 poligen Buchsenleiste seini PHIB 5 T tNotortreiber vod VMOT M3A I4D 141 PH4AA VOC 51 1001074 C42 190 1 142 M4C 143 M3D PH4B M4D VCC 100nF4 100 4 BLOTE VHOT GND AL GHD Voc M3B MIA M3D 5 100uF 1 C47 100nF4 Cit 1001274 Armkabel AHATL TTIK FP Jona Fonrad fuse Stroafe 1 Mainboard ALS R 07745 Jana Motor 4 15 12 Drester AFP 001 5283 epe Stromlaurplan ML FLAME ERE T ne PUE
101. l volumes check the sample penetration depth see section 2 10 13 Determine if the caps are being crimped property by attempting to rotate the cap by hand Loose caps may cause selective loss of lighter components from a sample Adjust crimping tool correctly Symptom Results show cross contamination between samples Make sure you have septa on your wash solvent and waste vials They are an important part of the cleaning mechanism Change them at least every 1 2 weeks including Snap cap Push down the plunger holder before starting a run and check if the plunger tip touches the needie Make sure the dead volume of your syringe needie is not excessive Good syringes have a needie with dead volumes less than 1 pl typically 0 6 Use an appropriate wash solvent and program at least 5 POST INJECTION SOLVENT CLEAN FLUSHES Increase the number of flushes and observe if the cross contamination diminishes Use PRE INJECTION SAMPLE CLEAN FLUSHES and or PRE INJECTION SOLVENT CLEAN FLUSHES to reduce cross contamination further Check if the syringe fills completely when washing If several cleaning cycles are programmed and many samples are processed vacuum in the solvent vial and overpressure in the waste vial may build up Cut away a segment of the solvent and waste septa to assure equalization of pressure CHROME adr o m cu cm tt mo mmm n BEEN SU m Trouble shooting
102. less injection port in splitter mode it as advisable to inject less deep especially in case the insert has been filled with glass beads and or glass wool The syringes used do have a needle length of 51 mm Figure 2 6 shows recommended injection depths for packed splitless splitter and on column injection For adjusting the injection depth follow the procedure given in Section 2 10 11 40mm 48mm Um aya c E un 2222 SPLITTER SPLITLESS TP PACKED Figure 2 6 injection depth for packed splitter splitless and on column injection INJECTION POINTS POSITION When adjusting the injection depth it is handy to know the depth of the guidance part in the septum cap used for packed splitter or splitless injection port or in the guidance part of the temperature programmable on column injector TP which in both cases is 5 mm 2 8 CHROMPACK tnstallation CP 9050 AUTOMATIC LIQUID SAMPLER 2 9 3 INSTALLING SYRINGE IMPORTANT l PLUNGER HOLDER For safety reasons it s advised to shut 2 SYRINGE off the power everytime a syringe have 3 SYRINGE FIXING LEVER to be adjusted 4 NEEDLE GUIDE Install the syringe in the syringe carrier Take care when inserting the syringe with one hand that the needle is threaded into the hole of the needle guide Slide the rim on top of the barrel a little bit in the slot meant for it and while holding the upper part of the plunger holder with
103. linking The value is increased with the t key and decreased with the key If a low or high limit is reached the value wraps around to the other end of the valid range If a value having valid range of 1 to 200 is 10 and shouid be set to 180 it is faster and more convenient to use the 1 key so the value wraps around to 200 Holding the arrow key pushed down speeds up the changing of the value SOFTWARE Five important software modifications have been implemented with the release of software revision 2 or higher for the 9001 2 a can contro CP 9050 sampler or a CP 9010 sampler or 94X One Shot Sampler in case of selecting the 9050 sampler in Page 1 Line 12 a new set of Pages 4 and 8 will become visible in case of selecting a 94X sampler Page 4 and 8 are as with software revision 1 CP 9001 2 meant to control a CP 9050 sampler must be equipped with software revision 2 or higher In case of 91X samplers CP 9001 2 software revision 1 must be used which can control a combination of 94X and 91X sampiers b Baseline recording subtraction is not possible anymore Therefore Page 2 of the CP 9001 2 shows optional for Line 3 and 4 Relevant Page 8 parameters VIAL RANGES with coupled METHODS PL COUNT and SEPTUM counters plus some extra parameters of Page 7 AUTOSTART and RESTART will be saved in EEPROM at the sacrifice of GC method 12 As a consequence only eleven GC metho
104. lt in personal injury or damage to the product Indications on the instrument Specific symbols drawing attention to safety hazards have been applied on appropriate places on the instrument The foliowing symbols can be encountered Instruction manual symbol Indicates that the user should refer to the manual before operating the equipment Indicates dangerous voltage terminals fed from the interior by voltage exceeding 1000 V must be so marked Protective conductor terminal For protection against electrical shock in case of a fault Used with fieldwiring terminals to indicate the must be connected to ground before operating equipment 505300 REV 1 00 SAFETY INFORMATION continued Radioactive hazard Indicates that the instrument contains radioactive components which may cause personal injury when handled incorrectly Skin puncture Indicates sharp or suddenly moving parts such as injection needies that may cause injury Hot surface Indicates parts that may cause burns when touched Cryogenic frostbite Contains extremely cold materiai such as liquid nitrogen carbon dioxide that may cause injury when handled carelessly Static discharge warning Item contains parts or informa tion that can be damaged by electrostatic discharge Take care for proper grounding before handling Do not touch Touching this item may resuit in damage to the instrument or personal injury 505300 REV 1 00 om men G
105. med in the CP 9050 liquid sampler The first part of Page 4 contains parameters for daily use The second part of Page 4 accessible by putting a 1 in Line 7 OPTIONS contains parameters that will be changed less frequently Explanation of the parameters data ranges and defaults given for 5 wl syringes LINE 1 INJ VOL INJECTION VOLUME in gi 0 5 in steps of 0 1 ul default 0 5 jul This parameter specifies the volume to be sampled and injected Since plunger in barrel syringes are used needle volume has to be taken in account By filling the needle with solvent PRE INJECTION SOLVENT CLEAN FLUSHES gt 0 one can compensate for needle dead volume In that case PRE INJECTION SAMPLE CLEAN FLUSHES and FILL STROKES must be set to zero LINE 2 INJ VIAL NUMBER OF INJECTIONS PER VIAL 1 89 default 1 This parameter specifies the number of times each sample will be injected CHROMPACK 3 7 9050 AUTOMATIC LIQUID SAMPLER Operation LINE 3 lt CLEAN SMP NUMBER OF PRE INJECTION SAMPLE CLEAN FLUSHES 0 99 default 0 This parameter specifies the number of times the syringe is washed with sample This option is used when the solvent used in 4 post injection clean cycle is not compatible with the analysis or when no pre injection solvent clean cycle used If you want solvent plug top of the sampie to compensate for needle dead volume PRE INJECTION SOLVENT CLEAN FLUSHES 0 this parameter must b
106. mpack is not responsible for printing errors and reserves the right to change specifications dexigns and prices without notice amd liability Copyright Ghrempack ntemational Start Configuration See Usersmanual page 2 12 for details Page 1 REFERENCE ADJUST Refer to the users manual 2 10 12 SMPL penetration See usersmanual page 2 10 13 for details Check if the syringe needle is positioned in the middie of the sample cap 7 lt in the middle x 5 7 27 n 7 Y as correct Yes The X as EE example should AN P ee be corrected i i 2mm to the right No Adjust the reference This Y as correction is point again but correct the not easy to adjust 2mm to the right Try to adjust the tray with the four inbus screws i mounted in the bottom of the sampler to page 2 Page 2 From page 1 Check WASH and SOLVENT penetration Check if the syringe needle is positioned in the middle of the wash cap 7 how a 7 lt inthe middie 7 Yes oen Only the Y as position 5 adiustable See drawing in section 1 2 for more details For adjustment the left Cross rail holder should Di 59 of 905 0 54 CHROMPACK Manual
107. mpler 3 7 PROGRAMMING THE RUN CONTROL SAMPLER PARAMETERS If the sampler sampler mode has been set to 51 the first part of Page 8 looks like RUN CONTROL SAMPLER FRST LAST METH 1 105 0 9 0 0 0 8 PRIORITY 9 PL COUNT l0 RESET SELECT LINE 0 0 0 9 0 0 9 0 9 LINE 4 7 FRST LAST METH In these 7 lines vial ranges 1 105 can be coupied with GC methods 1 11 Up to seven ranges can be defined while overlap between the vial ranges is possible vu While entering values for FIRST and LAST vial a check is done for LAST vial z FIRST vial ome Deactivating a vial range can be done by programming zero for FIRST and LAST vial lf FIRST vial 0 while LAST vial gt 0 a message UNDEFINED VIAL RANGE appears when the CP 9001 2 is started If all vial ranges FIRST and LAST are set to zero the sampler GC cannot be started no method is specified with the vial range vials of this range will be processed with the sampler parameters programmed in the active memory of the CP 9001 2 If a sampler GC run is stopped by pressing the STOP RESET key at the keyboard twice or pressing the START RESET button on top of the CP 9001 2 once the sampler continues with the next programmed injection when the CP 9001 2 is restarted by pressing the START key at the keyboard or the START RESET button on top of the GC if the sampler run is stopped before injection the same injection is done at restart
108. n wel nr 3 14 met andere informatie ala dis ik nodig heb 5 dit asn foutje of mis deze biz gawoon voorbaat mijn dank SOR CHER SUPPORT 2 9 D mate ae f 4 _ potduved ANN alr 2201 9 19 Lel paride inf Lace 4 mol 2 13 Ue pod n pet po 02 19 eee 02712 96 09 51 31 118671331 R amp D CP Nederland 4 0027003 31 118671331 SECTION 3 REMOVAL REPLACEMENT amp ADJUSTMENT PROCEDURES CHAPTER CONTENTS 3 2 General procedures for electronic modules 3 3 Adjusting the needle quide 3 4 Exchanging the injection head 3 5 Exchaning the front panel with display and keyboard 3 6 Exchanging the processor board UY 8 7 Exchanging the crossraii 3 8 Software changes 3 9 Standard connection In out connector 3 10 In out connector cabie CP9001 9002 connections 3 11 BCB output connector 3 12 Serial connector RS232 3 12 Options connector 3 13 Penetration depth range for samplers NOTE FOR THE SAMPLER CONFIGURATION PROGRAM SEE THE REFERENCE MANUAL SECTION 2 10 1 505300 REV 1 00 ws uETTMCMPTULPPREREWO TE eee 2 12 96 99 52 4331 118671331 R amp D see CP Nederland dj 003 003 31 118671331 m 3 13 PENETRATION DEPTH RANGE FOR SAMPLERS CP9010 CP9020 25 CP9050 Penetration CP9010 steps CP9020 25 steps CP9050 x0 1mm depth min
109. n port used is increased by one After changing the septum of that injection port the septum counter must be reset to zero i 3 14 CHROMPACK Operation 9050 AUTOMATIC LIQUID SAMPLER SET PL COUNT PROGRAMMED PLUNGER COUNT WARNING LIMIT The programmed vatue is displayed ACT PL COUNT ACTUAL PLUNGER COUNT The number of plunger counts after the last RESET 3 is displayed VIAL ACTIVE VIAL The active vial is displayed INJJVIAL PROGRAMMED INJECTIONS PER VIAL The programmed number of injections per vial is displayed ACT INJ ACTUAL INJECTION The actual injection from the active vial is displayed ACTIVE METHOD The active method used is displayed The STATUS page of the CP 9001 2 gives for the sampler information about the total number of injections to be made the actual injection the active vial and the active GC method STATUS 10 05 READY RUN TIME 0 CYCLES 1 20 lt actual injection total number of injections set actual OVEN 50 50 DET 300 300 INJ 300 300 AUX1 0 0 zz AUXT or AUX2 0 0 zz AUX2 or OCI2 VLV VLV EXT VIAL l zz active ACTIVE METHOD 1 1 lt GC method autoload CHROMPACK 3 15 mee I CP 9050 AUTOMATIC LIQUID SAMPLER Operation 3 9 TEMPERATURE PROGRAMMABLE ON COLUMN INJECTOR SYRINGE seal ee u nur oe time
110. n we start sampling with a needle filled with solvent using pre injection solvent clean flushes see 1 Sampling must then be done with no fill strokes programmed just filling the barrel once to the pl mark 2 The syringe contains now 1 pi solvent 1 ui sample 3 During injection the total amount of sample will be transferred to the injection port while part of the solvent evaporates from the needle 4 After injection stays 0 8 pl we have injected 1 sample 0 2 solvent assuming no mixing of solvent and sample Figure 3 2 A simple sandwich injection MORE ELABORATE SANDWICH INJECTION EU Figure 3 3 A more elaborate sandwich injection further improvement can be made if we separate the sample and the solvent by an air plug Also more solvent can be used as is illustrated here After pre injection solvent clean flushes a solvent plug of 0 5 is taken 1 whereafter an air volume of 0 2 2 Then 1 of sample is taken 3 an extra air volume of 0 8 gi 4 During injection the total amount of sample will be transferred to the injection port 5 0 7 pl 0 5 0 2 of solvent What remains in the needle is 0 8 pi of solvent 3 4 CHROMPACK ere em Operation CP 9050 AUTOMATIC LIQUID SAMPLER 3 2 SYRINGES The CP 9050 sampler uses standard Hamilton 700 series syringes 5 or 10 wl with a needie length of 51 mm an of the needle
111. np MAon SIecker Cehrduse Angl 5 25 4 4x Ceimpkoniakl 25 25 0 SCHOIE 4 Motor 001 8224 Schaltlilze Telton Izcl ation tf Lc hisheckeupplung HS 931 509 Schutzleiter weAbdeckung RS 531 475 001 8080 SCHA 2 Mator 001 8043 10 2 GLY 101212A SKF i SCHOS7 SCH036 SCHOSEC Hub Motor 001 8042 A F hrung SCHO49 7046 SCHOS1 913 2 hi Mzbx amp 2 SCHOSQ B A 27 125 42 001 8046 SCHO60 se KH 1 F M 5 _ PA rrr 71 Y Linearf hr 001 8060 0018031 SEVERRL PRRTS OPTION DOC NR REVISION DATE 754905 01 NAME AM PROJ _ MATERIAL GENERAL TREATMENT ROUGHNESS TOLERANCES UNLESS OTHERWISE STATED REMARKS Y 11 11 88 cu CODE 110 SHEET 1 OF 1 a GYR HERCULESWEG 8 TEL 01180 71000 CHROMPACK THE NETHERLANDS FAX 01180 33118 DIAMOND SHAPED KNURLES 0 8 45 Goole 0 8 23 0 1 0 1 ps 2 5 c 1 DETAIL A SCALE 10 1 3 P 60 7 16UNF20 15 9 E u BURR FREE SEPTUM CAP DOC NR REVISION 3765000 ha FL AMPROJ SCALE 25 1 MATERIAL Al Mg Si F32 GENERAL TREATMENT
112. nsert a vial in position 1 of the tray and insert solvent right and waste left vials on the left hand side of the CP 9050 See Section 2 9 5 for adjusting solvent pickup and wash penetration depth See Section 2 10 11 for adjusting the sample penetration depth The sampie penetration depth depends on the viais used CONFIGURATION SETUP AND ADJUSTMENT PROCEDURES The only way to change the configuration parameters is switching the power of the sampler on while pressing the M key on the control terminal The display shows CONFIGURATION blinking Press the V key to enter this option The display shows of Inj Points With the and 1 keys you can step through the possible values with the gt and Keys you can step through the parameters Set all parameters to tha values given in Section 2 10 CONFIGURATION PARAMETERS Press the C key to leave the CONFIGURATION PARAMETERS menu CONFIGURATION starts blinking again By pressina the C key again the sampler returns to its STANDBY mode showing NOTE Always press the V key to store the CONFIGURATION PARAMETERS If the sampler is Switched off before the V key was pressed the entered parameters will not be stored The sampler is now ready for operation see Section 3 OPERATION 2 10 CHROMPACK Installation CP 9050 AUTOMATIC LIQUID SAMPLER Set value 2 1 LEFT REMOTE 5 7x15 HIGH 2 ON ON OFF 100 150 200 50 100 2 40
113. nserts or adjust to a deeper level if necessary but do not touch the bottom of the vial with the needle tip to avoid bending of the tip Check the syringe needle tip If it is bent tip looks like a hook change the syringe Any restrictions which can easily be caused by a burred or bent needle tip will cause excessive pressure differences that cannot be equalized with normal parameter settings Symptom Results show lower repeatability than normat Use enough POST INJECTION SOLVENT CLEAN FLUSHES to assure a clean syringe This can be very important in case of samples containing high concentration of low volatile components In the worst case the syringe can become blocked without cleaning after injection Use cleaning cycles before injection if you are using a low volatile solvent Check the syringe needle tip if it is bent tip looks like a hook change the syringe Any restrictions which can easily be caused by a burred or bent needle tip will cause excessive pressure differences that cannot be equalized with normal parameter settings Check your method for viscosity delay times see Section 3 6 PROGRAMMING SPECIAL SAMPLER PARAMETERS VISCOSITY Longer delays allow better pressure equilibrium if the sample vial is filled more than 50 a vacuum may be created inside the vial depending on the number of cleaning cycles with sample and injections per sample which leads to poor filling of the syringe If vou are using very low sample via
114. ny kind of electrical damage Instead disconnect the power cord and contact your Chrompack office The supplied power cord must be inserted into a power outlet with a protective earth ground connection When using an extension cord make sure that the cord is also properly grounded Do not change the external or internal grounding connections as this could endanger you and or damage the instrument GHROMPACK Safety information CP 9050 AUTOMATIC LIQUID SAMPLER 7 19 11 12 13 14 15 18 17 18 19 20 CHROMPACK The instrument is properly grounded when shipped You do not need to make any changes to the electrical connections or to the instruments chassis to ensure safe operation When working with this instrument follow the regulations for GLP Good Laboratory Practice Take to wear safety glasses and appropriate clothing not place containers with flammable liquids on this instrument Spillage of the liquid over hot parts may cause fire This instrument may use flammable or explosive gases e g hydrogen under pressure Be sure to be familiarized with and to follow accurately the operation procedures prescribed for those gases before operating the instrument Note that using the Chrompack Hydrogen Safety System will reduce the safety risks when working with hydrogen as the carrier gas Note that considerable amounts of carrier gas and a great part of the sample are releas
115. omponent that is not described in this manuali without the assistance of Chrompack service engineer Unauthorized repairs or modifications wili result in rejection of warranty claims Always disconnect the power cord before attempting any type of maintenance Note that capacitors inside the instrument may still be charged even if the instrument is turned off Use proper tools when working on the instrument to prevent danger for yourself and or damage to the instrument Only use fuses of the type and current rating specified Do not use repaired fuses and do not shortcircuit the fuse holder Damage can result if the instrument is stored under unfavorable conditions for prolonged periods e g subject to heat water etc 505300 REV 1 00 SECTION i 1 1 DOC NO of the parts lists of section 2 REFERENCE DRAWINGS PAGE TITLE DPOC NO REV 1 2 Front view serial 10031 001 1202 1 2 1 3 Rear view serial 10031 001 2202 2 2 1 4 Rear view serial 10129 10300 001 1002A 1 5 Rear view serial H 10070 10128 001 1002 1 6 Front view serial 10001 10069 Q01 1000F 1 7 ALS CP AUTOSAMPLER 220V 001 1202 2 1 8 GRUNDPLATTE BASE BODY COMPLETE 110V 001 9202 1 1 9 GRUNDPLATTE BASE BODY COMPLETE 220V 001 9202 2 1 10 ARM ASSEMBLY 001 9003 1 11 INJECTORKOPF INJECTION HEAD 901 9204 21 12 INJECTION HEAD serial 10031 001 9204 1 13 INJECTION HEAD serial 10070 10128 901 9004 1 14 INJE
116. ose and sample evaporation may occur Be sure the cap is centered otherwise the syringe needle could hit the cap sure the is not tightened too much If so the septum is not flat anymore and the syringe tends to core a curved vial septum and drop small pieces of the material into the sample Solvent and waste vials To fill the solvent vial or empty the waste vial it is required to move the injection head by hand to a place where it does not interfere with puiling the out of the holder Before the next injection cycie the position of the injection head will be automatically reset to the waste position NOTE The septum on the solvent and waste vials is part of an effective syringe needle cleaning concept Not using a septum or not replacing these septa on a regular basis may cause sample cross contamination or even plopping off of the snapcap CHROMPACK 3 5 ure CP 9050 AUTOMATIC LIQUID SAMPLER Operation 3 4 NOTE 1 ACTIVATING THE SAMPLER PROGRAM Page 1 1 COL LIMIT 101 2 3 INJ TEMP 0 4 O0VEN INIT 0 actual 21 OVEN FINAL 9 OVEN RISE 0 INIT 99 STAB TIME l 5 6 7 8 TIME FINAL 0 9 10 CYCLES l ll TX MODE oft 12 SAMPLER 901X on 13 TP OCI 0 51 901 11 94 on SAMPLER 51 In Line 12 one can choose the sampler type and mode The following codes are possible 90 51 10 11 The CP 9010 or CP 905
117. ple Vial position 91 will be used for a priority sample This sample must be analyzed using GC method 2 Program Line 8 with 91 02 note the zero in front of the method number When the running GC cycle comes to an end the priority sample will be analyzed according the parameters of GC method 2 When the priority sample has been analyzed the sampter GC continues where it stopped LINE 9 PL COUNT PLUNGER COUNT WARNING LIMIT Dependent on the conditions used the syringe need to be cleaned or replaced after some time in many cases the number of plunger strokes executed is an important factor The number of plunger strokes is counted by the sampler itself while a warning limit 9800 can be programmed here The value entered will be multiplied by 100 for a warning limit of 9800 one has to enter 98 In case values lt 100 need to be programmed enter the value after a decimal point for warning limit of 50 enter 50 5 for 9 enter 09 1 LINE 10 RESET RESET FUNCTION Q Resets the sampler cycles which means when the CP 9001 2 with sampler activated is started again the sampler starts with the first injection of the first vial in the first vial range programmed It is wise to use RESET 0 before starting a new series of injections to be sure the sampler starts with the first injection of the first vial in the first vial range programmed In many cases the history of the sampler GC combination is not known exactly
118. ringe does not fili properly air bubbles below plunger Try to increase number of filling strokes to work out air bubbles Check the syringe needle tip If it is bent tip looks like a hook change the syringe Any restrictions which can easily be caused by a burred or bent needle tip will cause excessive pressure differences that cannot be equalized with normal parameter settings When using high volatile solvents use PRE INJECTION SAMPLE CLEAN FLUSHES or PRE INJECTION SOLVENT CLEAN FLUSHES if possible with a less voiatile solvent to wet and cool the syringe before sampling as much as possibile Check sample vial penetration depth see Section 2 10 13 if needle tip is below the liquid CHROMPACK 5 5 Iw CP 9050 AUTOMATIC LIQUID SAMPLER Trouble shooting Symptom Results show no or very low detector sianal no peaks A clogged syringe needle might be the reason for very low or even no detector signal Coring of soft septa or picking up sediment on the bottom of the vial have often turned out to be the problem Use enough POST INJECTION SOLVENT CLEAN FLUSHES to assure a clean syringe This can be very important in case of samples containing high concentration of low volatile components In the worst case the syringe can become blocked without cleaning after injection If you are using very low sample volumes check the sample vial penetration depth see Section 2 10 13 Use vials with conical i
119. ropriate clothing Do not place containers with flammable liquids on this instrument Spillage of the iiquid over hot parts may cause fire This instrument may use flammable or explosive gases e g hydrogen under pressure Be sure to be familiarized with and to follow accurately the operation procedures prescribed for those gases before operating the instrument Note that using the Chrompack Hydrogen Safety System will reduce the safety risks when working with hydrogen as the carrier gas Note that considerable amounts of carrier gas and a great part of the sample are released through the split vent If hydrogen is used as the carrier gas or if toxic compounds are analyzed the split vent must be connected via external tubing to a proper fume hood The same appiies for the exhaust of the detector 505300 REV 1 00 eme 0 5 GENERAL SAFETY PRECAUTIONS continued 12 13 14 15 16 17 18 19 20 When measuring gas flow rates through an FID or NPD never measure air and hydrogen together They should be measured separately to minimize explosion hazard Cold compounds such as carbon dioxide liquid nitrogen may cause severe burns Refer to Chrompack manual Cryogenic frostbite Cat no 505079 for detailed information When handling sharp objects such as fused siiica or stainless Steel capillaries or capillary columns traps syringes etc avoid puncture of the skin Never try to repair or replace any c
120. s to control the SPLIT SPLITLESS mode selection The other 5 wires in the cable can also be used for integrated systems start 3C and GC ready Mi gt Splitter valve gt TP OCI valve 2 Max 2Amp Max 505300 REV 1 00 mm o ooa dtes 2 gt Aoc CO m 505300 REV 1 00 am 5 me amet BCB output connector 14 pins T amp B flatcable connector 1 NPN Open Collector a D NPN Open 30 Collector AQ 505300 REV 1 00 400 NPN Open Collector Not connected Not connected Common 5Volt SOMA External Supply 30Volt max Serial connector RS232 9 pins DSUB 2 TXD sending 3 RXD receiving 5 Ground 7 RTS 8 CTS tlo n S CO cto 6 pins flatcable connector This connector is reserved ta STANG instruments options Unauthorized use of this connector may result in serious damage ofthe instrument 505300 REV 1 00 irme PENETRATION DEPTH RANGE FOR SAMPLERS 9010 CP9020 25 CP9050 CP9020 25 steps Penetration 9010 steps CP9050 x0 imm depth mi in max min max min max REMARKS 400 measured at needlee penetrated 1 3 into vial 650 measured when needle nearly touched the bottom of the vial 250 measured at needle just passing the neck of the vial
121. sent NOTE case only one injection port is available the second injection point can be programmed identical to the first ona In this way programming front or rear does not matter the injection is always done in the same injection port Select the injection position to program 0 or 1 with 4 or and press V to enter programming the following display appears A AXIS x 0 1 mm No 0 0410 C L Position in 0 1 mm Injection Point being adjusted Modify the axis position with t keys in a step by step brief action on the key or continuous way key pressed select the other axis Y with lt gt and adjust in the same way AXIS x 0 1 mm No 0 0006 V C L Position in 0 1 mm Injection Point being adjusted Finally select the PENETRATION with lt gt and adjust in the same way Z AXIS x 0 1 mm No 0 0030 C L Position in 0 1 mm Injection Point being adjusted 2 14 CHROMPACK Installation CP 9050 AUTOMATIC LIQUID SAMPLER For programming the penetration depth proceed as follows 1 Move downwards with the 1 key until the bottom of the needle guide lies flat with the upper part of the septum cap for ease of adjustment place a piece of paper on top of the septum cap 2 Note down the display vaiue typical value 800 3 Calculate the display value required for a certain penetration depth by adding the depth of the guidance part of the septum
122. splay of the sampier The only key that stays active only during sampling will be the C key With the C key it is possible to abort the started cycle in the sampling phase of the CP 9050 sampler sampler and GC wiil be stopped Pressing the red START RESET button on top of the CP 9001 2 or pressing the STOP RESET key at the CP 9001 2 keyboard twice has the same effect but these keys will be active ail the time not only in the sampling phase of the CP 9050 sampler In case of TP the dipswitches at position 1 or 2 must be set Then Line 13 shows P Otherwise all dipswitches OFF Line 13 shows optional ae MADRID A mte p Operation 3 5 NOTE NOTE CP 9050 AUTOMATIC LIQUID SAMPLER PROGRAMMING STANDARD SAMPLER PARAMETERS If the sampler sampler mode has been set to 50 51 the first part of Page 4 looks like 901X SAMPLER l INJ VOL 2 INJ VIAL 3 CLEAN SMP 4 FILLSTR 5 gt CLEAN SLV 6 INJ PORT 7 0PTIONS 9 0 7 9 9 11 5 0 INJ VOL 0 5 Values and data ranges shown here assume 5 pi syringe installed programmed during setup see Section 2 10 CONFIGURATION PARAMETERS about programming the syringe size Default values for the parameters and data ranges depend on the syringe size programmed Once activating the CP 9050 sampler by setting Line 12 in Page 1 to 51 shows values and ranges for the syringe size program
123. t be cleaned replaced in case of a SAMPLER ERROR Page 10 Line 4 SAMPL ERR of the CP 9001 2 gives information about the type of error The information is given as AB XY 10 Number of characters received 8 20 Sampler command not accepted This can happen when parameter 5 not within the data range of that parameter e g the GC method was made for 544 syringe iater on a 104 syringe was programmed the CONFIGURATION PARAMETERS AB 40 Run time parameter error SET lt ACT time for DOUBLE or DUAL injection NOT INSTALLED XY 01 Receive buffer full XY 202 No communication with CP 9050 sampler 04 RS232 interface card not present XY 208 Line status error baud rate not correct NOTE Errors AB 10 and XY 01 should normaily not appear Since the code of the last error stays visible till it is cleared it is wise to clear the code Page 10 Line 4 0 before further checking CHROMPACK 9 3 eee CP 9050 AUTOMATIC LIQUID SAMPLER Trouble shooting Ifasampler error code 20 occurs see 9001 2 Page 10 Line 4 it means a sampler command was not accepted by the CP 9050 sampler a parameter is not within the data range of that parameter e g the GC method was made for 5 pi syringe later on 10 syringe was programmed the CONFIGURATION PARAMETERS over all system values in non volatile memory is not After RESET TO DEFAULT se
124. the SAMPLER CONTROL PROGRAM on page 1 of the CP 900x GC by entering code 50 on line 12 The CP 9050 keyboard is not locked anymore now Turn the instrument off and disconnect the power cord Remove the sample tray from the sampler housing Remove the sample tray holders 4 pieces See section 1 DOC NO CRP002 Body assembly item 21 er Remove the top cover by loosening the 8 Phillips headscrews on both sides and on the top Loosen also the 3 Allen head screws that fit into the bottom plate Remove the injection head Refer to page 3 4 Disconnect the crossrail flatcable that is plugged into the processor board Remove the crossrail see drawing Loosen the two Allen head screws of the crossrail leg at the right hand side only Measure the distance between the left crossrail end and the left leg D and between the right crossrail leg and the right end E LLL 1 505300 REV 1 00 3 5 1 3 5 Loosen the Allen head screws at position in order to remove the legs Remove the right hand cover by loosening the 3 screws and the 1 at the backcover Loosen the 3 Phillips screws at the rear of the display A small Screwdriver is required and the 3 Phillips screws at the front It s now possible to remove the keyboard display and the flatcabie connection Proceed in the reverse order to build the sampler back to his
125. the back cover over the electrical terminals mounted with two screws have to be removed The back cover be replaced by an aluminum back cover mounted with two screws The left hand middle and old back cover wili be replaced by one sampler cover over the injector detector flow control and back cover area mounted with two plastic hinges with four screws each NOTE in case of an old CP 9001 holes have to be drilled in the back side of the CP 9001 see Figure 2 4 In that case the hinges must be mounted with M4 bolts and nuts 2 6 CHROMPACK Installation CP 9050 AUTOMATIC LIQUID SAMPLER 2 8 2 9 0 203 234 8 625 2 657 Figure 2 4 Holes to be drilled in the CP 9001 for mounting the sampler cover REPLACING STANDARD SEPTUM CAP S BY SAMPLER SEPTUM CAP S The standard septum caps used for hand injection and 91X 94X samplers need to be replaced by special septum caps which quide the black needle quide of the CP 9050 sampler For packed splitter and or splitless injection ports the one shown in Figure 2 5 will be used The temperature programmed on column injection port with pneumatic head has its own guidance part see Figure 2 6 in Section 2 9 2 ADJUSTING THE Figure 2 5 Septum Cap for Packed INJECTION DEPTHS Splitter Splitless Injectors mm MOUNTING THE CP 9050 SAMPLER With the use of 3 screws supplied the CP 9050 sampler is mounted onto the GC top cover 2 holes are lo
126. the beginning turned to 1 when the needle quide is about 3 mm below the top of the vial and switch back to when the needle quide is about 3 mm above the vial the needle guide shouid rest on sample 2 while pressing downl 2 10 20 RESET TO DEFAULT With this function all changeable parameters are reset to default values All user values are lost BE CAREFUL WHEN USING THIS FUNCTION its only use is to reset all parameters to save values after making changes e g sample penetration or injection depth too deep so the needle may be damaged Use this function if the CP 9050 sampler is reinstalled on another CP 9001 2 GC before setting up new values Resets to default METHODS POSITIONS MOTOR SPEEDS Press V the following message is displayed ARE YOU SURE V CONFIRM V IC Press V to confirm or C to abort WARNING Be careful using this option because you will loose all your programmed parameters 2 11 TABLES OF CONFIGURATION METHOD AND UTILITY PARAMETERS In the next three tables Table and the default values are given for the CONFIGURATION METHOD and UTILITIES Parameters You can use these tables to note down your actual values 2 20 CHROMPACK sem Installation CP 9050 AUTOMATIC LIQUID SAMPLER CONFIGURATION PARAMETERS Table CONFIGURATION PARAMETERS RANGE DEFAULT PROGRAM NB of Inj Points Wash Position Start signal Syringe Volume Tray Selection
127. tion port With t or 4 values can be changed 2 10 16 SYRINGE TEST Vi C This function allows to check if the syringe takes the programmed volume This is done with the plungerspeed mentioned above Press V to enter the programming The following display appears FILLING VOLUME 0 1 uil 1 V IC Adjust the volume with 1 41 1 Press V the plunger is moving up and down and then pulls up the programmed volume 2 Press V again the plunger goes to zero volume 3 Press V same as step 1 4 Press C Quit this parameter At this point it may be necessary to align the zero volume position of the syringe plunger is not going down to zero This can easily be done by unscrewing the little hexagonal nut press down the black plunger holder as far as possible and re tight the little hexagonal nut 2 18 CHROMPACK Installation CP 9050 AUTOMATIC LIQUID SAMPLER 2 10 17 SERIAL BAUDRATE SERIAL BAUDRATE V C Press V to enter the programming The foliowing display appears SERIAL BAUDRATE BAUDS 9600 V C Set the Baudrate to 9600 with t 1 2 10 18 SERIAL LINK TEST IC This parameter can not be entered with V With the Cp 9001 2 the communication from GC to SAMPLER can be checked by programming the sampler mode CP 9001 2 Page 1 Line 12 to 50 or 51 The CP 9001 2 sends the following messages Sampler mode 50 950000 Sampler mode 51 040000 090000 959991
128. us secreevs moveted in tha af the sampler Adjust the reference again bul correct the to lha right to page 2 32 2 505300 REV 1 01 5 3 1 FROM 5 3 1 Check WASH and SOLVENT penetration Check if the syringe needle is positioned in the middle of the wash cap in the middie Yes No Only the Y as position is adjustable See drawing in section 1 2 for more details For adjustment the cross rail holder should adjusted between J 5mm END of configuration 505300 REV 1 01 5 3 2 CHROMPACK Manual Update Distribution Service manual CP 9050 No 041 Instrument 9050 AUTOSAMPLER Date 11 May 1998 Subject Manual update REV 1 13 into REV 1 67 Originator ANALYTIK FP JENA Enclosures pages Author Jan Vos File Service Manual CP 9050 505300 No of pages 54 Dear Colleagues 41 i Remove front page add front page REV 1 67 2 JJ Remove the pages 1 1 until 1 5 5 pages in section 1 and discard add the new pages 3 Remove section 2 completely and discard add new section 2 4 Remove page 3 1 in section 3 add page 3 1 REV 1 01 5 C Remove page 3 14 in section 3 add page 3 13 6 Remove the pages 4 1 until 4 14 14 pages in section 4 and discard add the new pages 7 Remove section 5 completely and discard add new section 5 8 Please insert this page in section 6
129. vement goes strong check if the ann holder is scratching on the rail shift the left armholder picture check by power off the sampler does not into the the keyboard is dented or nas a short contacl loose the screws of the display montage and try it again configurations menu when connecting afier a change of the display keyboard ass y IF the result 15 positiv than put a plastic washer under the board before the serial 9 pol plug fixing of the screws picture D th motor does not stop a sensor does nt work check all connectors if they have a correct contact the roundcable in the end position connectors on Ihe backside of the unit is to fix very correct check specific the y sensor after mainboard change if the index goes into the koppler picture C a repair the motor runs the belt is to tight y direction shift the y motor louder than before x direction shilt the loose pulley z direction shift the z motor the display letters have nol the change of the mainboard or the display turn the little screw on the potentiometer enough contrast Qu mainboard picture mm mi Gm RD mo m arcam wm Gm m roam Gm am o ano m roam Gm Gm Gm Gm CHO NL
130. yringe is cleaned for the next sampling cycle when programmed Pressing the red START RESET button on top of the CP 9001 2 or pressing the STOP RESET key at the CP 9001 2 keyboard twice stops the sampler and CP 9001 2 as well but these keys will be active ail the time not oniy in the sampling phase of the CP 9050 sampler t minute time out If in METHOD programming mode of the sampler no key of the keyboard of the Terminai is pressed within one minute the sampler escapes from programming mode without changing the sampler parameters of that METHOD The sampler returns to STANDBY mode Showing CHROMPACK men Operation NOTE CP 9050 AUTOMATIC LIQUID SAMPLER Resetting to first injection of first vial of first vial range In case a sampier GC run is stopped after one or more injections were done and one wants to start ali over again the CP 9001 2 must be reset LINE 10 RESET 0 otherwise the sampler continues with the next iniection Or just pressing three times ENTER after selecting the specific vial range by selecting LINE X the CP 9001 2 will be reset in the same way as with LINE 10 RESET 0 Cycle counter In case of a sampler there is no need to program the cycle counter Page 1 Line 10 From the defined vial range and the programmed injections per viai the cycles wil be caiculated and displayed the STATUS Page So if the vial range is 1 15 and the injections per have been programmed

Chrompack CP 9050 Liquid sampler manual

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