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G1316A/G1316B SL - Scientific Systems

1. 96 Figure 25 Arrangements of Heater and Cooling Devices G1316B SL G1316C SL Plus If the additional heater and cooling devices are used as shown above the column identification system cannot be used If the column identification system is required fix the heater and cooling devices in the upper or lower locations or fix them right left of the current location The heater and cooling devices are mounted on a carrier that can be fitted to the left and or right heat exchangers 1200 Series TCC Service Manual Maintenance 8 Fixing Heater or Cooling Devices G1316B SL Heat exchanger Carrier for heater or cooler Heater device Screw driver Torx or Posidriv Figure 26 Fixing Heater or Cooling Devices G1316B SL Fixing the Low Dispersion Heat Exchangers G1316C SL Plus For the G1316C SL Plus additional heat exchanger and cooling devices can be installed on the carrier part number G1316 89200 using 3 screws part number 0515 1052 included to part number for carrier as shown in figure below 1200 Series TCC Service Manual 97 8 Maintenance Adding Heater and Cooling Devices G1316B SL G1316C SL Plus Build in heat exchanger Carrier for low dispersion heat exchanger Low dispersion heat exchanger Fitting holder assembly Figure 27 Installing the low dispersion heat exchangers Choose Compatible Fitt
2. ee ESIA aen a ea o Bead a mm 5 _ PE me CAN Bus cable T 2222 Peene SK i ESE Bair ES SSS Mik TESS SSRS 3S L E 4 oE Leo oe j E LAN to LC a g ChemStation location SSS depends on detector g oS i mE Analog detector g 9 T e E signal zsz ft 1 or 2 outputs per SS S8 mn Ec F detector o ggss h Figure 10 Recommended Stack Configuration Rear View 1200 Series TCC Service Manual 37 3 Installing the Column Compartment Installing the Column Compartment Parts required Preparations Description 1 Column compartment 1 Power cord For other cables see text below Locate bench space Provide power connections Unpack the Column compartment Module is partially energized when switched off as long as the power cord is plugged in Risk of stroke and other personal injury Repair work at the module can lead to personal injuries e g shock hazard when the module cover is opened and the instrument is connected to power gt Never perform any adjustment maintenance or repair of the module with the top cover removed and with the power cord plugged in gt The security lever at the power input socket prevents that the module cover is taken off when line power is still connected Never plug the power line back in when cover is removed CAUTION Valve properties are read from the valve head RFID tag during initializatio
3. 1200 Series TCC Service Manual 167 9 Repair Assembling the Main Cover When If cover was broken Tools required None Parts required Part number Description 1 G1316 68713 Plastics kit includes base top left and right The plastics kit contains all parts but it is not assembled CAUTION Wrong assembled In case you insert the left or right side in the opposite position you may not be able to remove the side from the top part gt Take care not to mix up left and right side 168 1200 Series TCC Service Manual Repair Assembling the Main Cover 1 Place the top part on the bench and insert the left and right side into the top part 2 Replace the cover 1200 Series TCC Service Manual 169 9 Repair Installing the Radio Frequency Shield G1316C SL Plus Installing the Radio Frequency Shield G1316C SL Plus When If the Thermostatted Column Compartment SL Plus shall be operated without valve and sliding unit the radio frequency shield is mandatory Parts required Partnumber Description 1 G1316 67002 Valve Cover Kit Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section Removing the Top Cover and Foam on page 110 1 Remove the valve liner 2 Replace the valve liner by a valve cover G1316
4. 1200 Series TCC Service Manual 191 10 Parts and Materials for Maintenance Table 27 G1316C Capillary System Kits Description Part Number Rapid Resolution Selectivity Method Development Kit 5190 1435 Rapid Resolution pH Method Development Kit 5190 1436 1 for capillary kit contents please refer to the Method Development Solution User and Installation Guide G4230 90000 G1316B SL Micro Valve Kit 2 Position 10 Port Table 28 G1316B SL Micro Valve Kit 2PS 10PT Item Description Part Number G1316B SL Micro Valve Kit 2PS 10PT G1316 68745 Column identification tag blank for re ordering use pack of 3 5062 8588 Column clip for re order use is pack of 6 5063 6526 Corrugated tubing to waste re order 5 m 5062 2463 Wrench open end 1 4 5 16 inch 8710 0510 Wrench open end 5 16 3 8 inch 8710 2409 Screwdriver Torx TX8 8710 2509 Screwdriver Hexagonal 2 5 mm 5965 0028 2 Column holders for p LC columns 5001 3702 Column Regeneration Kit for p LC columns see Table 29 on G1316 68721 page 193 Capillary column heat exchanger 90 mm lg 0 17 i d not G1316 87300 assembled contains items 2 3 and 4 Capillary column heat exchanger 115 mm lg 0 17 i d not G1316 87321 assembled contains items 2 3 and 4 Capillary column heat exchanger 170 mm lg 0 17 i d not G1316 87323 assembled contains items 2 3 and 4 192 1200 Series TCC Service Manual Parts and Materials for Maintenance Column Regeneration K
5. 5 16 inch for capillary connections Parts required Part number Description 1 G1316 60007 Heat exchanger assembly left includes ambient temperature sensor 1 G1316 60006 Heat exchanger assembly right Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 1 Remove the Z Panel by opening 3 screws 2 Disconnect the 4 heat exchanger cables from the processor board which are 2 flexible board cables for the column tag reader and heat sensor and 2 power cables each pair red black located below these cables 1200 Series TCC Service Manual 143 9 Repair Removing the Heat Exchanger Assemblies 3 On both sides of the valve actuator there are fixation clips 4 For removing the left heat exchanger view from front which keep the flexible boards of the heat exchanger carefully remove the temperature sensor from the heat assemblies in the correct position Remove the fixation exchanger unit clip for the heat exchanger unit which shall be removed 144 1200 Series TCC Service Manual Repair 9 Installing the Heat Exchanger Assemblies Installing the Heat Exchanger Assemblies G1316A G1316B SL When If the heat exchanger is leaking blocked or does not heat cool or ot
6. 9 Reinstall the foam section the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B SL on page 162 10 Place the column compartment back into stack and reconnect capillaries and the power cable 11 Turn ON the column compartment 122 1200 Series TCC Service Manual Repair 9 Installing a Valve Installing the sliding unit G1316C SL Plus When If a new sliding unit or valve actuator shall be installed Parts required Partnumber Description 1 G1316 60000 Sliding Unit Preparations Make sure that the leak sensor has been installed correctly Installing the leak sensor G1316C SL Plus on page 172 1 Insert the valve liner 2 Insert the sliding unit to the valve liner and push down the sliding unit such that it fits properly to the bottom foam NOTE Before connecting the valve actuator to the main board install the top foam Installing the Top Cover and Foam G1316C SL Plus on page 165 1200 Series TCC Service Manual 123 9 Repair Exchanging the Main Board Exchanging the Main Board G1316A G1316B SL When If board is defective or for repair of other assemblies Tools required Screwdriver Pozidriv 1 PT3 Hexagonal wrench 5 mm Parts required Part number Description 1 G1316 69540 Main board CCM exchange assembly for G1316A G1316B SL for Series 1200 Preparations Turn OFF the column compartment Disconnect the power cable
7. Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 The Agilent 1200 Series G1316A G1316B SL no longer has a GPIB connection 1 Usea5 mm wrench to unscrew the REMOTE connector oe ae ee en Sea eae a GS ee SOSO 39 ZS SS SoS SS _ a fim oo SS SS OS 124 1200 Series TCC Service Manual 2 J2 RS 232C J3 REMOTE J5 25 CAN J7 Power Supply J11 J14 J15 J16 J17 J18 J19 Flexboard right J21 Column Switching Valve Heat Exchanger Assembly left Heat Exchanger Assembly right Fan Assembly right Fan Assembly left Leak Sensor Flexboard left B Battery S Configuration Switch Repair 9 Disconnect all connectors from the processor board J7 f Safety lock Ooo Remove the processor board Place the board on the ESD kit In some cases the RFI spring plate may remain on the interface connectors of the board Carefully remove the spring plate and place it back into its position in the instrument before installing a new board On the new board check the switch setting of address switch S1 see Setting the 8 bit Configuration Switch on page 239 An incorrect switch setting e g TEST BOOT may cause the module to turn in a basic mode yellow or red flashing status light In such
8. Removinga Valve 114 Installing a Valve 119 Exchanging the Main Board 124 Changing the Type and Serial Number 129 Exchanging the Fan 138 Removing the Heat Exchanger Assemblies 140 Installing the Heat Exchanger Assemblies 145 Exchanging the Power Supply 152 Replacing the Leak Sensor or Leak Base G1316A G1316B SL 156 Replacing Status Light Pipe 161 Installing the Foam and the Top Cover 162 Assembling the Main Cover 168 Installing the Radio Frequency Shield G1316C SL Plus 170 Installing the leak sensor G1316C SL Plus 172 Replacing the Door Sensor G1316C SL Plus 174 10 Parts and Materials for Maintenance 177 Valve Options Overview 178 Heater and Cooling Devices for G1316B SL G1316C SLPlus 179 Column Switching Valve 2 Position 6 Port G1316A G1316B SL 181 Column Switching Valve 8 Position 9 Port G1316C SL Plus 183 Micro Column Switching Valve 2 Postion 6 Port G1316A G1316B SL 185 Micro Column Switching Valve 2 Position 10 Port G1316A G1316B SL 186 Accessory Kits 188 Plastic Parts 195 Leak Parts 196 1200 Series TCC Service Manual Contents 11 Parts for Repairs 199 Overview of Main Assemblies 200 Sheet Metal Kit 203 Plastic Parts 205 Foam Parts 207 Power and Status Light Pipes 209 Leak Parts 210 Internal Valve Drive Parts G1316C SL Plus 212 12 Identifying Cables 213 Cable Overview 214 Analog Cables 216 Remote Cables 219 BCD Cables 224 Auxiliary Cable 226 CAN LAN Cables 227 External C
9. on page 174 Valve RFID access failure 2874 The valve tag reader fails reading or writing the RFID tag of the valve head Probable cause 1 Defect in cable connection of valve tag reader to main board 2 Valve head not installed correctly 3 RFID tag defective 4 Valve tag reader is damaged Suggested actions Check cable connection between valve tag reader to main board Review installation of valve head see Installing Valve Heads G1316C SL Plus on page 42 Replace valve head see Table 11 on page 178 Replace Actuator Valve 5067 4106 1200 Series TCC Service Manual 1200 Series TCC Service Manual 7 Test Functions Thermostat Function Test 76 Pressure Test 79 Column Thermostat Temperature Calibration 80 Column Thermostat Temperature Calibration Procedure 82 Column Thermostat Calibration Problems 83 Installing the Temperature Sensor 83 This chapter describes the TCC s built in test functions ee Agilent Technologies 75 7 Test Functions Thermostat Function Test Heater Function Test Description The heater function test is used to evaluate the cooling and heating performance of the two peltier elements When the test is started both heat exchangers are cooled initially to 25 C This temperature is held for 12 seconds and then the setpoint is changed to 20 C The time required to reach 20 C is a measure of the cooling efficiency of the peltier elements At 3 5 minutes the s
10. Operating Altitude Non operating altitude Safety standards IEC CSA UL inches 100 240 VAC 10 50 or 60 Hz 5 320 VA 150 W 512 BTU 0 55 C 32 131 F 40 70 C 4 158 F lt 95 at 25 40 C 77 104 F Up to 2000 m 6500 ft Up to 4600 m 14950 ft Installation Category II Pollution Degree 2 Wide ranging capability Maximum Non condensing For storing the module For indoor use only Research Use Only Not for use in Diagnostic Procedures 1200 Series TCC Service Manual 27 2 Site Requirements and Specifications Performance Specifications Table3 Performance Specifications Thermostatted Column Compartment Type Specification Comments Temperature 10 degrees below ambient to 80 C G1316A range 10 degrees below ambient to 100 C G1316B SL G1316C SL Plus up to 80 C flow rates up to 5 ml min G1316A G1316B SL G1316C SL Plus up to 100 C flow rates up to 2 5 ml min G1316B SL G1316C SL Plus Temperature 0 15 C G1316A stability 0 05 C G1316B SL G1316C SL Plus Temperature 0 8 C accuracy 0 5 C With calibration Column Three 30 cm capacity Warm up 5 minutes from ambient to 40 C cool down time Dead volume Communication s Safety and maintenance 28 10 minutes from 40 20 C 3 pl left heat exchanger 6 ul right heat exchanger Controller area network CAN GPIB RS 232C APG Remote ready start stop and shut down signa
11. These repairs are described in Maintenance on page 85 Exchanging Internal Parts Some repairs may require exchange of defective internal parts Exchange of these parts requires removing the column compartment from the stack removing the covers and disassembling the column compartment The security lever at the power input socket prevents that the column compartment cover is taken off when line power is still connected These repairs are described in Repair on page 107 1200 Series TCC Service Manual Maintenance 8 Warnings and Cautions Module is partially energized when switched off as long as the power cord is plugged in Risk of stroke and other personal injury Repair work at the module can lead to personal injuries e g shock hazard when the module cover is opened and the instrument is connected to power gt Never perform any adjustment maintenance or repair of the module with the top cover removed and with the power cord plugged in gt The security lever at the power input socket prevents that the module cover is taken off when line power is still connected Never plug the power line back in when cover is removed Sharp metal edges Sharp edged parts of the equipment may cause injuries gt To prevent personal injury be careful when getting in contact with sharp metal areas Toxic and hazardous solvents The handling of solvents and reagents can hold health risks gt When working w
12. plate towards the front and remove it switching valve from column compartment G1316A G1316B SL 1200 Series TCC Service Manual 111 9 Repair Removing the Top Cover and Foam 7 For G1316C remove the cables of the valve tag reader valve actuator encoder reader valve actuator drive control and door sensor Valve actuator encoder reader Door sensor neea 8 Remove the top foam Do not connect a power plug to the column compartment after removing the top covers A safety light switch on the main board will turn OFF fan immediately and electronics after 30 seconds to avoid the operation with removed covers An error will be generated status lamp lights red and the logbook will show an error message 112 9 Position of the foam in the safety light switch Be ce a A PENA l PERA EA l BBBr A a D 1200 Series TCC Service Manual Repair roam and er LOV p Removing the Top 10 Position of safety light switch on the main board when removing the foam 113 1200 Series TCC Service Manual 9 Repair Removing a Valve Removing a Valve from the Thermostatted Column Compartment G1316A G1316B SL When If valve failed or bottom foam part has to be removed for other replacements Tools required Screwdriver Pozidriv 1 PT3 Wrench 1 4 5 16 inch for capillary connections Preparations Turn OFF the column com
13. 16 inch Wrench open end 5 16 3 8 inch Part Number G1316 68735 5062 8588 5063 6526 5062 2463 5181 1516 8710 0510 8710 2409 1200 Series TCC Service Manual 189 10 Parts and Materials for Maintenance 190 Table 24 Accessory Kit Standard G1316B SL and G1316C SL Plus Item Description Part Number Screwdriver Torx TX8 8710 2509 Screwdriver Hexagonal 2 5 mm 5965 0028 Capillary column heat exchanger 90 mm lg 0 17 i d not G1316 87300 assembled contains items 2 3 and 4 Capillary column heat exchanger 115 mm lg 0 17 i d not G1316 87321 assembled contains items 2 3 and 4 Capillary column heat exchanger 170 mm lg 0 17 i d not G1316 87323 assembled contains items 2 3 and 4 Ferrule front SST pack of 2 1 Ferrule back SST pack of 2 k Fitting SST pack of 2 R 1 re order 5062 2418 pack of 10 each of fittings front and back ferrule G1316B SL G1316C SL Plus Capillary System Kit G1316B SL G1316C SL Plus Capillary System Kit Table 25 G1316B SL Capillary System Kit G1316 68744 G1316B 060 Item Description Part Number 2 Carriers for Heater or Cooling Devices G1316 83200 E Heater long up 0 12 mm i d 1 6 pl internal volume G1316 80002 j Heater long down 0 12 mm i d 1 6 ul internal volume G1316 80003 E Post column cooler 0 12 mm i d 1 5 ul internal volume G1316 80004 Capillary System Kit see Table 26 on page 191 for details G1316 68716 For items see also Heater and Cooling Dev
14. 2875 During initialization the valve actuator turns until the encoder reads the reference index position An error is generated if the reference index cannot be found within a given time Probable cause Suggested actions 1 Defect in cable connection of valve drive Check cable connection to valve drive control control replace cable 2 Defect in cable connection of valve actuator Check cable connection to valve actuator encoder reader encoder reader replace cable 3 Defect of valve drive or valve actuator Replace Actuator Valve 5067 4106 encoder reader Unknown Unsupported Valve detected 2872 After powering on the RFID tag of the valve head is read out An error is generated if the RFID tag does not contain valid information The RFID can be damaged if the instrument is power cycled during a write access of the tag Probable cause Suggested actions 1 RFID tag contains invalid information Replace valve head see Table 11 on page 178 1200 Series TCC Service Manual 73 6 74 Error Information Door sensor HW failure 2873 This error is generated if a front door is detected while the front door sensor has been disabled during the self test Probable cause 1 Defect in cable connection of door sensor to main board 2 Door sensor defective Suggested actions Check cable connection between door sensor and main board Replace door sensor G1316 81603 see Replacing the Door Sensor G1316C SL Plus
15. 30 Heater and Cooling Devices for G1316B SL 180 1200 Series TCC Service Manual Parts and Materials for Maintenance 10 Column Switching Valve 2 Position 6 Port G1316A G1316B SL Table 14 Column Switching Valve 2PS 6PT for G1316A G1316B SL Item Description Part Number Column switching valve kit includes all parts required for G1353 68700 installation Column switching valve complete assembly 0101 0920 Cover plate when switching valve is not installed G1316 44103 Capillary Kit Column Switching includes two capillaries 0 17mm G1316 68708 i d 180 mm and three capillaries 0 17 mm i d 90 mm G1313 87305 G1316 87300 Rhebuild kit for 7750 030 valve includes 3 groove rotor seal 0101 1258 stator face assy isolation seal instructions 1 Stator screws 1535 4857 2 Stator Head 0100 1850 3 Stator face 0100 1851 4 Stator ring 5 Rotor seal 3 grooves Tefzel 0100 1854 Rotor seal 3 grooves Vespel 0100 1855 Rotor seal 3 grooves PEEK 0100 2233 6 Isolation seal 0100 1852 1200 Series TCC Service Manual 181 10 Parts and Materials for Maintenance Column Switching Valve 2 Position 6 Port G1316A G1316B SL Spring side shows to rear Figure 31 Column Switching Valve Parts 182 1200 Series TCC Service Manual Parts and Materials for Maintenance 10 Column Switching Valve 8 Position 9 Port G1316C SL Plus Column Switching Valve Parts High Pressure G1316C SL Plus Table 15 Valve 8 Postion 9 Port Hig
16. 44123 which fits to the same position and clip it in at its top lt lt FRG 170 1200 Series TCC Service Manual Repair Installing the Radio Frequency Shield G1316C SL Plus 3 Insert the radio frequency shield between the Z panel and valve cover 1200 Series TCC Service Manual 171 9 Repair Installing the leak sensor G1316C SL Plus When Tools required Parts required Preparations 172 This section describes how to install the leak sensor for the Thermostatted Column Compartment SL Plus G1316C SL Plus New modules of the G1316A and G1316B SL versions use the same design For existing G1316A and G1316B SL modules please refer to Replacing the Leak Sensor or Leak Base G1316A G1316B SL on page 156 If leak sensor is defective or leak base is damaged Screwdriver Pozidriv 1 PT3 Screwdriver flat blade Wrench 1 4 inch Hexagonal wrench 3 mm Part number Description 1 5061 3356 Leak sensor assembly 1 G1316 43101 Leak base part of leak panel kit G1316 68700 Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 Remove the sliding unit see Removing the sliding unit G1316C SL Plus on page 117 1200 Series TCC Service Manual Instal
17. 9 Next Steps 8 Reinstall the processor board see Exchanging the Main Board G1316A G1316B SL on page 124 9 Reinstall the fan assemblies see Exchanging the Fan on page 138 10 Reinstall the heat exchanger assemblies see Installing the Heat Exchanger Assemblies G1316A G1316B SL on page 145 11 Replace the foam section the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B SL on page 162 12 Replace column compartment into the stack 13 Reconnect the power cable 14 Turn on the column compartment 1200 Series TCC Service Manual 155 9 Repair Replacing the Leak Sensor or Leak Base G1316A G1316B SL When If leak sensor is defective or leak base is damaged Tools required Screwdriver Pozidriv 1 PT3 Screwdriver flat blade Wrench 1 4 inch Hexagonal wrench 3 mm Parts required Part number Description 1 1 Preparations 156 5061 3356 Leak sensor assembly G1316 43101 Leak base part of leak panel kit G1316 68700 Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 1200 Series TCC Service Manual Repair Replacing the Leak Sensor or Leak Base G1316A G1316B SL 1 Disconnect the leak sensor assembly from the proce
18. Centronics connector on the other end NOT FOR FW UPDATE This kit contains a 9 pin female to 9 pin female Null Modem printer cable and one adapter Use the cable and adapter to connect Agilent Technologies instruments with 9 pin male RS 232 connectors to most PCs or printers 24542U G1530 60600 34398A 5181 1529 34398A 1200 Series TCC Service Manual 229 12 Identifying Cables RS 232 Cables 230 1200 Series TCC Service Manual 1200 Series TCC Service Manual 13 Hardware Information The Electronics 232 Firmware Description 233 Firmware Updates 234 Agilent 1200 Series Interfaces 235 GPIB Interface 236 CAN Interface 236 Remote Interface 236 RS 232C 238 Setting the 8 bit Configuration Switch 239 GPIB Default Addresses 240 Communication Settings for RS 232C Communication 240 Forced Cold Start Settings 242 Stay Resident Settings 243 The Main Power Supply Assembly 244 This chapter describes the detector in more detail on hardware and electronics ee Agilent Technologies 231 13 Hardware Information The Electronics The electronics are comprised of four main components e column compartment main board CCM column identification board CID see Column Identification System on page 13 power supply see The Main Power Supply Assembly on page 244 232 1200 Series TCC Service Manual Hardware Information 13 Firmware Description The firmware of the instrument consists of two in
19. Column Temperature 0 left heater Column Temperature 2 right heater For safety reasons the maximum column heat exchanger temperature is 105 C If an electronic failure occurs which causes the heater to heat continually the current is switched off when the temperature exceeds 105 C and the error message is generated Probable cause Suggested actions 1 Defective heater assembly Exchange the heater assembly 2 Defective TCC board Exchange the TCC board Heatsink Temperature The temperature of the Peltier heatsink has exceeded the maximum limit Heatsink Temperature 0 left heater Heatsink Temperature 2 right heater The maximum temperature of the Peltier heatsink is 70 C If an electronic failure occurs which causes the heatsink to reach 70 C the current is switched OFF and the error message is generated Probable cause Suggested actions 1 Defective heater assembly Exchange the heater assembly 2 Defective TCC board Exchange the TCC board 1200 Series TCC Service Manual Error Information 6 Defective Heater Circuit The electronic circuit for control of the heater assemblies is defective The processor checks the function of the heater circuits continually If a defect is detected in the control circuit the processor switches OFF the heater peltier assemblies and the error message is generated Probable cause Suggested actions 1 Defective TCC board Exchange the TCC board Valve failed to initialize
20. Manual 175 9 Repair Replacing the Door Sensor G1316C SL Plus 176 1200 Series TCC Service Manual 1200 Series TCC Service Manual J 6 ee 10 e Parts and Materials for Maintenance J Valve Options Overview 178 Heater and Cooling Devices for G1316B SL G1316C SL Plus 179 Column Switching Valve 2 Position 6 Port G1316A G1316B SL 181 Column Switching Valve 8 Position 9 Port G1316C SLPlus 183 Micro Column Switching Valve 2 Postion 6 Port G1316A G1316B SL 185 Micro Column Switching Valve 2 Position 10 Port G1316A G1316B SL 186 Accessory Kits 188 G1316A Accessory Kit Standard 188 G1316A Accessory Kit 2PS 10PT modules 189 G1316B SL G1316C SL Plus Accessory Kit Standard 189 G1316B SL G1316C SL Plus Capillary System Kit 190 G1316B SL Micro Valve Kit 2 Position 10 Port 192 Column Regeneration Kit G1316A G1316B SL 193 Accessories G1316C SL Plus 194 Plastic Parts 195 Leak Parts 196 This chapter provides information on parts for maintenance ot Agilent Technologies 177 10 Parts and Materials for Maintenance Valve Options Overview This overview gives a summary of the main parts and assemblies More details are available with each valve option in this chapter Table 10 Valves for G1316A and G1316B SL Module Valve Description Valve Rotor Seal Stator G1316A 055 Column Switching Valve 2 Position 6 Port 0101 0920 0100 1855 Vespel 0100 1851 Face G1316 68700 G1316A G1316B SL on page 181 0100 1
21. Manual 91 8 Maintenance Column identification tag Figure 22 Column Identification Tag for Left Heat Exchanger Column identification tag Figure 23 Column Identification Tag for Right Heat Exchanger 3 For columns with small diameter a cable tie wrap should be used to fix the column identification tag to the column Assure that the tie wrap does not block the front cover 92 1200 Series TCC Service Manual Maintenance 8 Replacing Head Parts of Column Switching Valve G1316A G1316B SL Spring side shows to rear Figure 24 Column Switching Valve Parts When If valve leaks Tools required 1 4 inch wrench 9 64 inch hex key Parts required Description For parts refer to Valve Options Overview on page 178 1 Remove capillaries from ports 1 5 and 6 1200 Series TCC Service Manual 93 8 Maintenance Replacing Head Parts of Column Switching Valve G1316A G1316B SL 2 Loosen each fixing stator screw two turns at a time Remove bolts from head T m AT 3 Remove the stator head and the ceramic stator face NOTE Valve Head 8 Position 9 Port High Pressure part number 5067 4107 has no stator face 4 Remove the stator ring 5 Remove the rotor seal and isolation seal if damaged or contaminated 6 Install the new isolation seal if required Ensure the metal spring inside the ring faces towards the valve body 7 Install the new rotor seal Repl
22. Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section 1 Push the valve head such that it snaps in at its rear position 2 Lift up the sliding unit at the rear 3 Carefully remove the sliding unit from the bottom foam part and pull it out of the valve liner If the thermostatted column compartment shall be operated without valve and sliding unit the opening must be closed using an radio frequency shield and the valve cover in order to avoid radio frequency emission from the module see Installing the Radio Frequency Shield G1316C SL Plus on page 170 1200 Series TCC Service Manual 117 9 Repair Replacing the Valve Actuator G1316 C SL Plus When If the valve actuator shall be replaced Parts required Part number Description 1 5067 4106 Actuator Valve Preparations Remove the sliding unit from the bottom foam part Removing the sliding unit G1316C SL Plus on page 117 1 Slightly expand the metal housing of the sliding unit 1 twist out the valve actuator 2 and lift it out 8 of the sliding unit 118 1200 Series TCC Service Manual Repair 9 Installing a Valve Installing a Valve G1316A G1316B SL When For first time installation or after it was removed Tools required Screwdriver Pozidriv 1 PT3 Wrench 1 4 5 16 inch for capillary connections Preparations Open the column compartment as described in Removing a Val
23. SL Plus Tubing flex polyethylene Leak Funnel 0890 1711 G1316 68722 G1316 67000 1200 Series TCC Service Manual Parts for Repairs 11 Leak Parts Figure 44 Leak Parts G1316A G1316B SL 1200 Series TCC Service Manual 211 11 Parts for Repairs Internal Valve Drive Parts G1316C SL Plus Table 43 Internal Valve Drive Parts G1316C SL Plus Item Description Part Number Actuator Valve Sliding Unit G1316C SL Plus Valve Liner Valve Cover Kit includes following items 5067 4106 G1316 60000 G1316 40501 G1316 67002 1 Valve Cover 2 e Radio Frequency Shield r 2 212 1200 Series TCC Service Manual 1200 Series TCC Service Manual 6 ee 12 e Identifying Cables J Cable Overview 214 Analog Cables 216 Remote Cables 219 BCD Cables 224 Auxiliary Cable 226 CAN LAN Cables 227 External Contact Cable 228 RS 232 Cables 229 This chapter summarizes information on all cables Agg Agilent Technologies 213 12 Identifying Cables Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations Type Description Part Number Analog cables 3390 2 3 integrators 01040 60101 3394 6 integrators 35900 60750 Agilent 35900A A D converter 35900 60750 General purpose spade lugs 01046 60105 Remote cables 3390 integrator 01046 60203 3392 3 integrators 01046 60206 3394 integrato
24. Using cables not supplied by Agilent Technologies can lead to damage of the electronic components or personal injury gt Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations 1200 Series TCC Service Manual 25 2 Site Requirements and Specifications Bench Space The column compartment dimensions and weight see Physical Specifications on page 27 allow to place this module on almost any desk or laboratory bench It needs an additional 2 5 cm 1 0 inches of space on either side and approximately 8 cm 3 1 inches in the rear for the circulation of air and electric connections If the bench should carry a complete Agilent Series system make sure that the bench is designed to carry the weight of all the modules The module should be operated in a horizontal position Environment Your column compartment will work within specifications at ambient temperatures and relative humidity as described in Physical Specifications on page 27 26 1200 Series TCC Service Manual Site Requirements and Specifications 2 Physical Specifications Table2 Physical Specifications Type Specification Comments Weight 10 2 kg 22 5 Ibs Dimensions 410 x 435 x 140 mm 16 1 x 17 x 5 5 width x depth x height Line voltage Line frequency Power consumption Ambient operating temperature Ambient non operating temperature Humidity
25. column should indicate the module you just entered If an other User Interface is also connected start it now 1200 Series TCC Service Manual 133 9 Repair Recover Instructions Overview The following situations may come up where the instrument is no longer usable due to e an incorrect type product number entry after the replacement of a main board of the module e load of wrong firmware based on the wrong type With firmware A 06 02 B 01 02 and above a wrong type cannot be entered The entry is checked against the board revision The wrong type product number could be e incorrect but a valid 1100 1200 series module number e incorrect and invalid 1100 1200 series module number any name Based on above the User Interfaces react differently Table9 Recover From Wrong Type User Interface incorrect but valid type incorrect but valid type incorrect and invalid type Example Conditions correct type G1315B correct type G1315B correct type G1315B entered type G1314B entered type G1314B entered type G1319B plus wrong firmware from G1314B ChemStation shows the incorrect product does not show the module does not show the incorrect Recover with Agilent number NO access to the module is product number Diagnostic Software Interface shows the settings of possible NO access at all to the module Type amp the G1314B Use Recover with Agilent is possible Firmware on Type can be changed via Diagnostic Softw
26. force storage of this set of parameters in non volatile memory Returning the switches 1 and 2 to other positions other than being both up will allow for normal operation Forced cold start erases all methods and data stored in the non volatile memory Except the diagnose and repair log books all methods and data will be erased gt Make sure that all important methods and data are stored before you enforce a cold start 242 If you use the following switch settings and power the instrument up again a forced cold start has been completed Table 53 Forced Cold Start Settings Mode Select 1 2 3 4 5 6 7 8 TEST BOOT h hi jo jo o jo jo li To return to normal operation set switches back to your GPIB or RS 232C configuration settings 1200 Series TCC Service Manual Hardware Information 13 Stay Resident Settings Firmware update procedures may require this mode in case of firmware loading errors Switches 1 and 2 do not force storage of this set of parameters in non volatile memory Returning the switches 1 and 2 to other positions other than being both up will allow for normal operation If you use the following switch settings and power the instrument up again the instrument firmware stays in the resident part that is it is not operable as a column compartment It only uses basic functions of the operating system for example for communication Table 54 Stay Resident Settings Mode Select 1 2 3 4 5 6 7 8 TE
27. main system can be done in the resident system only Update of the resident system can be done in the main system only Main FW update Resident System Main System Resident FW Update Figure 45 Firmware Update Mechanism 1200 Series TCC Service Manual Hardware Information 13 Agilent 1200 Series Interfaces The Agilent 1200 Series modules provide the following interfaces Interface Type Pumps Autosampler DA Detector DA Detector MW VW Detector Thermostatted Vacuum MW Detector Detector RI Detector Column Degasse FL Detector G1315C G1365C Compartment r CAN Yes Yes Yes Yes Yes Yes No LAN on board No No No Yes No No No GPIB Yes Yes Yes No Yes No No RS 232C Yes Yes Yes Yes Yes Yes No Remote Yes Yes Yes Yes Yes Yes Yes Analog Yes No 2x 2x 1x No Yes Interface board Yes Yes Yes No Yes No No LAN BCD Ext 1 The vacuum degasser will have a special connector for specific use For details see description of main board e CAN connectors as interface to other Agilent 1200 Series modules GPIB connector as interface to the Agilent ChemStation e RS 232C as interface to a computer e REMOTE connector as interface to other Agilent products e analog output connector s for signal output and e interface slot for specific interfacing external contacts BCD LAN and so on For identification and location of the connectors see Figure 12 on page 41 Never use cables other than the ones supplied by Agilent Technolo
28. module to module 1 m 5181 1519 Agilent 1200 module to control module G1323 81600 LAN Cables Description Part number Cross over network cable shielded 3 m long for point to 5023 0203 point connection Twisted pair network cable shielded 7 m long for hub 5023 0202 connections 1200 Series TCC Service Manual 227 12 Identifying Cables External Contact Cable 5o c oO 31 10 lt 6 1p SS 11 One end of this cable provides a 15 pin plug to be connected to Agilent 1200 Series module s interface board The other end is for general purpose Agilent 1200 Series Interface Board to general purposes Connector Color Pin Agilent Signal Name G1103 61611 1200 White 1 EXT 1 a Brown 2 EXT 1 x Green 3 EXT 2 Bea Yellow 4 EXT 2 Grey 5 EXT 3 Pink 6 EXT 3 Blue 7 EXT 4 Red 8 EXT 4 Black 9 Not connected Violet 10 Not connected Grey pink 11 Not connected Red blue 12 Not connected White green 13 Not connected Brown green 14 Not connected White yellow 15 Not connected 228 1200 Series TCC Service Manual RS 232 Cables Identifying Cables 12 Description Part number RS 232 cable instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters RS 232 cable kit 9 to 9 pin female and one adapter 9 pin male 25 pin female Suited for instrument to PC Cable Printer Serial amp Parallel is a SUB D 9 pin female vs
29. supply status the upper right indicates the instrument status Status indicator green yellow red Line power switch with green light Figure 18 Location of Status indicators Power Supply Indicator The power supply indicator is integrated into the main power switch When the indicator is illuminated green the power is ON Module Status Indicator The module status indicator indicates one of four possible instrument conditions e When the status indicator is OFF and power switch indicator is on the instrument is in a prerun condition and is ready to begin an analysis 1200 Series TCC Service Manual 57 5 58 Troubleshooting and Diagnostics e A green status indicator indicates the module is performing an analysis run mode e A yellow indicator indicates a not ready condition The module is in a not ready state when it is waiting for a specific condition or action to be completed for example immediately after changing a setpoint or while a self test procedure is running e An error condition is indicated by a red status indicator An error condition indicates the module has detected an internal problem which affects correct operation of the instrument Usually an error condition requires attention for example leak defective internal components The error state is propagated through the system to all connected modules so the error might come from a different module Chec
30. temperature exceeds the acceptable limit for example if the cooling fan of the instrument fails To reset the main power supply to normal operating conditions turn the instrument off wait until it is approximately at ambient temperature and turn the instrument on again The following table gives the specifications of the main power supply Table 55 Power Supply Specifications Standard Maximum power 160 VA 130 W Continuous output Line Input 100 240 volts AC 10 line Wide ranging frequency of 50 60 Hz Pin 1 Power Fail error message Pin 2 AGND Pin3 15 VDC Pin 4 15 VDC Pin 5 PGND Pin 6 PGND Pin 7 24 VDC Pin 8 24 VDC Pin 9 36 VDC not used Pin 10 36 VDC not used Pin 11 DGND Pin 12 5VDC 1200 Series TCC Service Manual 245 13 Hardware Information The Main Power Supply Assembly 246 1200 Series TCC Service Manual 1200 Series TCC Service Manual 14 Appendix Safety Symbols 248 The Waste Electrical and Electronic Equipment Directive 251 Lithium Batteries Information 252 Radio Interference 253 Sound Emission 254 Solvent Information 255 Agilent Technologies on Internet 257 This chapter provides addition information on safety legal and web ee Agilent Technologies 247 14 Appendix Safety Symbols Safety Symbols Table 56 Safety Symbols Symbol Description The apparatus is marked with this symbol when the user should refer to the instruction manual in order to pr
31. top plastic panel together with the Z panel into the guide and press it half way down 146 1200 Series TCC Service Manual Repair 9 Installing the Heat Exchanger Assemblies 5 Press the Z panel together with the top plastic panel 6 Press down completely until it clicks into its holding completely down position Reconnect the heat exchanger cables to the processor board and the grounding connection of the column switching valve 1200 Series TCC Service Manual 147 9 Repair Installing the Heat Exchanger Assemblies 9 Carefully replace the heat exchanger cables into the foam Next Steps channels 10 Reinstall the foam section the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B SL on page 162 11 Replace the column compartment into stack 12 Reconnect capillaries 13 Reconnect the power cable 14 Turn on the column compartment 148 1200 Series TCC Service Manual Repair 9 Installing the Heat Exchanger Assembly G1316C SL Plus When If the heater is leaking blocked or does not heat cool or other assemblies have to be removed Tools required Screwdriver Pozidriv 1 PT3 Wrench 1 4 5 16 inch for capillary connections Parts required Part number Description 1 G1316 60007 Heat exchanger assembly left includes ambient temperature sensor 1 G1316 60006 Heat exchanger assembly right 1 G1316 68712 EPP Foam Part K
32. 41 Foam Parts 1200 Series TCC Service Manual 207 11 Parts for Repairs 208 Table 40 Foam Parts G1316C SL Plus Item Description Part Number EPP Foam Kit G1316A G1316B SL G1316C SL Plus G1316 68712 1 Fixation Clip Kit 5 clips includes following items G1316 67003 Fixation Clip for Heat Exchanger Flex Board Figure 42 Fixation Clip for Heat Exchanger Flex Board 1200 Series TCC Service Manual Power and Status Light Pipes Table 41 Power and Status Light Pipes Parts for Repairs 11 Item Description Part Number Power supply assembly 0950 2528 1 Power light pipe 5041 8382 2 Status light pipe 5041 8384 3 Power switch button 5041 8381 4 Coupler for power supply actuator 5041 8383 Figure 43 Power and Status Light Pipes 1200 Series TCC Service Manual 209 11 Parts for Repairs Leak Parts 210 Table 42 Leak Parts Item Description Part Number 1 Leak sensor 5061 3356 2 O ring for ambient temperature sensor 0400 0002 3 4 Leak Kit includes leak top and leak base 1200 Series G1316 68720 G1316A G1316B SL 5 Leak funnel G1316A G1316B SL 5041 8388 6 Leak funnel holder G1316A G1316B SL G1316 42300 7 Waste assembly includes complete Y tubing assembly with G1316 60002 leak funnel G1316A G1316B SL Waste tubing 1200 mm long part of accessory kit Leak Panel Kit includes following items Leak Panel Top e Leak Panel Base Leak Tube Kit includes following items Funnel Holder G1316C
33. 854 Tefzel 0100 1850 Head 0100 2233 PEEK 0100 1852 Seal G1316A 056 Micro Column Switching Valve 2 Postion 6 0101 1051 0100 2087 Vespel 0101 2089 Port G1316A G1316B SL on page 185 G1316A 057 Micro Column Switching Valve 2 Position 10 0101 1343 0101 1360 0101 1362 G1316 68709 Port G1316A G1316B SL on page 186 G1316B 055 Column Switching Valve 2 Position 6 Port 0101 1420 0101 1409 0101 1417 G1316A G1316B SL on page 181 600 bar G1316B 057 Micro Column Switching Valve 2 Position 10 0101 1419 0101 1415 0101 1421 Port G1316A G1316B SL on page 186 600 bar 1 re build kit 0101 1258 includes 3 groove rotor seal stator face assy isolation seal instructions 2 re build kit 0101 1360 includes PEEK rotor seal PEEK stator face hex key Table 11 Valves for G1316C SL Plus Kit Kit Description Valve Head Rotor Seal Stator G4230A Method Development Valve Kit low 5067 4108 5067 4113 5067 4112 pressure includes 8pos 9port valve G4230B Method Development Valve Kit high 5067 4107 5067 4111 5067 4110 pressure includes 8pos 9port valve l kit with stator face and rotor seal 178 1200 Series TCC Service Manual Parts and Materials for Maintenance 10 Heater and Cooling Devices for G1316B SL G1316C SL Plus The use of these heater and cooling devices is described in Technical Notes or in the Agilent 1200 Series Rapid Resolution LC System 1200 RRLC System manual Table 12 Heat
34. Agilent 1200 Series Thermostatted Column Compartment G1316A G1316B G1316C Service Manual ot Agilent Technologies Notices Agilent Technologies Inc 1995 1996 2008 No part of this manual may be reproduced in any form or by any means including elec tronic storage and retrieval or translation into a foreign language without prior agree ment and written consent from Agilent Technologies Inc as governed by United States and international copyright laws Manual Part Number 61316 90111 Edition 09 2008 Printed in Germany Agilent Technologies Hewlett Packard Strasse 8 76337 Waldbronn Research Use Only Not for use in Diagnostic Procedures Manual Structure The Service Manual G1316 90111 English contains the complete information about the Agilent 1200 Series Thermostatted Column Compartment It is available as Adobe Reader file PDF only Latest versions of the manuals can be obtained from the Agilent web Warranty The material contained in this docu ment is provided as is and is sub ject to being changed without notice in future editions Further to the max imum extent permitted by applicable law Agilent disclaims all warranties either express or implied with regard to this manual and any information contained herein including but not limited to the implied warranties of merchantability and fitness for a par ticular purpose Agilent shall not be liable for errors or for
35. Cleaning should be done with a soft cloth slightly dampened with water or a solution of water and a mild detergent Make sure not to let liquid drip into your module WARNING Liquid dripping into the electronic compartment of your module Liquid in the module electronics can cause shock hazard and damage the module gt Do not use an exessively damp cloth during cleaning gt Drain all solvent lines before opening any fittings 90 1200 Series TCC Service Manual Maintenance 8 Changing Column Identification Tags The column compartment is equipped with an column identification system that stores column specific information Two identification antennas are incorporated in the heat exchanger assemblies Antennas Column identification tag Column clip l y Figure 21 Column ldentification System When If column is used on the opposite heat exchanger or a tag is added to a new column Parts required Partnumber Description 1 5062 8588 Column identification tag pack of 3 1 The identification tag can be easily removed from the column 2 The tag needs to be placed differently depending on whether the column is installed at the left or right heat exchanger see Figure 15 on page 49 and Figure 16 on page 50 The Agilent logo should always be at front When correctly placed on the heat exchanger the distance between tag and antenna is 1 2 mm This is the optimum distance for proper function 1200 Series TCC Service
36. Column 2 0 17 105 1 5021 1816 Column 2 Valve port 8 0 17 105 1 5021 1816 for long column Column 2 Valve port 8 0 17 200 1 5065 9931 for short column Valve port 5 Valve port 10 0 17 105 1 5021 1816 Regeneration pump Valve port 4 0 25 800 1 5065 9930 Valve port 9 Waste 0 6 2000 5062 2463 PTFE Ferrules screws fingertight fittings etc 1 16 fittings and ferrules 2 5062 2418 10 pk fingertight fitting long 1 5062 8541 10 pk fitting screw long 10 5065 4454 10 pk fitting screw extra long 10 5065 9967 10 pk front ferrule 1 5180 4108 10 pk back ferrule 1 5180 4114 10 pk Peek tubing 1 16 0 18 1500 1 0890 1763 Plastic tubing cutter 1 8710 1930 Hex key 3 32 1 8710 2462 Rheotool Socket wrench 2 x 1 4 1 8710 2391 1 ALS Autosampler 2 TCC Thermostatted Column Compartment heat exchanger 3 ul left or 6 ul right 1200 Series TCC Service Manual 187 10 Parts and Materials for Maintenance Accessory Kits The accessory kits for G1316A G1316B SL or G1316C SL Plus contain accessories and tools needed for the installation and maintenance G1316A Accessory Kit Standard Table 22 G1316A Accessory Kit Standard Item Description Part Number G1316A Accessory Kit Standard G1316 68705 Column identification tag blank for re ordering use pack of 3 5062 8588 Column clip for re order use pack of 6 5063 6526 Corrugated tubing to waste re order 5 m 5062 2463 CAN cable 0 5 m 5181 1516 Wrench open en
37. G1316C SL Plus Parts required CAUTION Several optional valve heads are available for the G1316C SL Plus which can be installed and exchanged easily Part number Description 1 5067 4107 8pos 9prt valve head high pressure and or 1 5067 4108 8pos 9prt valve head low pressure Valve Damage Using a low pressure valve on the high pressure side can damage the valve gt When using multiple column compartments as part of a method development solution make sure that the high pressure valve head is connected to the autosampler and the low pressure valve head is connected to the detector gt For details please refer to the Method Development Solution User and Installation Guide part number G4230 90000 CAUTION Column Damage or Bias Measurement Results Switching the valve to a wrong position can damage the column or bias measurement results gt Fitting the lobe to the groove is essential for making sure the valve is switched to the correct position 42 1200 Series TCC Service Manual Installing the Column Compartment 3 Installing Valve Heads G1316C SL Plus 1 Put the valve head onto the valve drive such that the lobe 2 Screw the valve head onto the valve drive using the union fits to the groove nut 4 Push the valve head until it snaps in and stays in the rear position 1200 Series TCC Service Manual 43 3 Installing the Column Compartment Flow Connections of the Column C
38. Increase the timeout threshold value 2 Defective left heater assembly Exchange the heater assembly 3 Defective TCC board Exchange the TCC board Right Temperature Timeout The temperature of the right heat exchanger did not reach the temperature setpoint within the timeout threshold Probable cause Suggested actions 1 Timeout threshold too short Increase the timeout threshold value 2 Defective right heater assembly Exchange the heater assembly 3 Defective TCC board Exchange the TCC board 1200 Series TCC Service Manual 69 6 70 Error Information Defective Temperature Sensor One of the temperature sensors has failed The TCC board monitors the signal from the sensor continually If the signal is missing or out of range the error message is generated Defective Temperature Sensor 0 left column Defective Temperature Sensor 1 left heat sink Defective Temperature Sensor 2 right column Defective Temperature Sensor 3 right heat sink Defective Temperature Sensor 4 ambient correction sensor located on left flex board Probable cause Suggested actions 1 Flex board not connected only if all left or Ensure the flex board is connected correctly right sensor error messages appear simultaneously 2 Defective heater assembly Exchange the heater assembly 3 Defective TCC board Exchange the TCC board Heater Profile Heater Profile 0 left heater Heater Profile 2 right heater The temperature warm
39. L module identifier N serial number embedded in single quotes serial number embedded in single quotes PMP ALS THM TCC VWD DAD MWD FLD RID DAD MWD VWD 130 1200 Series TCC Service Manual Repair 9 The first two characters are letters which should be capitalized The reply line will respond with RA 0000 SER followed by the module serial number you just entered 2 To change the type of the module use the following command print sendmodules Lxxx TYPE XXXXX or print sendmodules Nxxx TYPE XXXXX where xxx is the module type and XXXXxX is the 5 character product number of the module e g G1314B Table8 ChemStation Command Format Type Change Modules with or without optional interface board Modules with LAN on board PRINT SENDMODULES Lxxx TYPE XXXXX PRINT SENDMODULES Nxxx TYPE XXXXX module identifier L module identifier N product number XXXXX embedded in single quotes product number XXXXX embedded in single quotes PMP ALS THM TCC VWD DAD MWD FLD RID DAD MWD VWD Some Agilent 1100 1200 series modules require the correct main board version to match the type for example the SL modules 3 Power cycle the module Then restart the Agilent ChemStation If the serial number you have just entered is different than the original module serial number you will be given the opportunity to edit the configure 1200 access screen during the restart of the Agilent ChemStation 4 After re
40. MD Software can revert to correct product number as described in Recover with Agilent Diagnostic Software Type amp Firmware on page 136 comes up with an error unsupported module G1319B access to the module is possible via Service Mode as described in Recover with Instant Pilot on page 136 shows resident or unsupported module access to the module is possible via Tests as described in Recover with Control Module on page 137 shows the incorrect product number access to the module is possible as described in Recover with Agilent Diagnostic Software Type Only on page 135 Recover with Agilent Diagnostic Software Type Only The Diagnostic Softwares is used in CE mode If no LAN connection is possible use RS 232 The example uses G1315B as correct type 1 Open a connection to the module or via system The module will be listed with the wrong product number type 1200 Series TCC Service Manual 135 9 136 Repair Select Board Check and Change and press Start In the type field enter G1315B and press Apply Close the Agilent Diagnostic Software oF W N After a power cycle the module should show up with the correct product number type in the user interface Recover with Agilent Diagnostic Software Type amp Firmware Agilent Diagnostic Software in CE mode If no LAN connection is possible use RS 232 The example uses G1315B as correct type The module must be c
41. RFI spring bottom G1316 09102 Figure 39 Sheet Metal Kit 1200 Series TCC Service Manual 203 11 Parts for Repairs Table 36 Sheet Metal Kit G1316C SL Plus Item Description Part Number Sheet Metal Kit G1316C SL Plus G1316 68731 204 1200 Series TCC Service Manual Parts for Repairs 11 Plastic Parts Table 37 Plastic Parts G1316A G1316B SL Item Description Part Number 1 Plastic kit includes base sides and top 1200 Series G1316 68713 2 Front cover G1316A 1200 Series G1316 68714 2 Front cover G1316B SL 1200 Series G1316 68724 3 Name plate Agilent 1200 Series 5042 1381 Table 38 Plastic Parts G1316C SL Plus Item Description Part Number Front Cover G1316C SL Plus G1316 68754 Plastik Cover Kit G1316C SL Plus includes following items G1316 68723 Top Cover Kit Left Side Cover G1316C SL Plus Right Side Cover G1316C SL Plus Base Cover G1316C SL Plus Sensor Assy Front Cover G1316 81603 For correct assembling of the top and sides see Assembling the Main Cover on page 168 1200 Series TCC Service Manual 205 11 Parts for Repairs Plastic Parts Figure 40 Plastic Parts 206 1200 Series TCC Service Manual Parts for Repairs 11 Foam Parts Foam Parts Table 39 Foam Parts G1316A G1316B SL Item Description Part Number 1 2 EPP foam kit includes 1 and 2 G1316 68702 1 Top 2 Base NOTE Part numbers printed on the foam parts are not orderable Figure
42. ST BOOT li h jo jo li jo jo jo To return to normal operation set switches back to your GPIB or RS 232C configuration settings 1200 Series TCC Service Manual 243 13 Hardware Information The Main Power Supply Assembly 244 The main power supply comprises a closed assembly and must not be disassembled further for safety reasons In case of a defect the entire power supply needs to be replaced The power supply provides all DC voltages used in the module The line voltage can vary in a range from 100 240 volts AC 10 and needs no manual setting 36V not used line voltage primary ee 24V 4 5A circuits 5V switching regulator 5V 3A linear 15V 3A voltage regulators 15V 3A To disconnect the instrument from line unplug the power cord The power supply still uses some power even if the power switch on the front panel is turned off No accessible hardware fuse is needed because the main power supply is safe against any short circuits or overload conditions on the output lines When overload conditions occur the power supply turns off all output voltages Turning the line power off and on again resets the power supply to normal operation if the cause of the overload condition has been removed 1200 Series TCC Service Manual Hardware Information 13 An over temperature sensor in the main power supply is used to turn off output voltages if the
43. Series TCC Service Manual Test Functions 7 Pressure Test For running a pressure test please refer to the corresponding pump manual The pressure test may be used for testing the tightness of a valve installed in the TCC CAUTION Wrong use of pressure test may damage valve The current implementation of the pressure test automatically uses the maximum pressure generated by the pump used by that system gt Do not use the test for modules having a lower maximum pressure than the pump as this will damage the valve For example do not use 400 bar valve in a TCC in combination with a 600 bar pump 1200 Series TCC Service Manual 79 7 Test Functions Column Thermostat Temperature Calibration 80 Temperature Calibration Principle The actual temperatures of the column heat exchangers left and right depend on the column setpoint temperature For setpoint temperatures above 36 C the heat exchangers are heated to a temperature slightly above the setpoint temperature Conversely for setpoint temperatures below 36 C the heat exchangers are kept at a temperature slightly below the setpoint temperature This fine temperature correction compensates for the small amount of heat exchange through the instrument housing and ensures the column is always kept at the setpoint temperature At 86 C the column setpoint and heat exchanger temperatures are equal temperature cross over point This is the temperature at which a
44. The tests and diagnostic features as provided by the Agilent Lab Advisor Software may differ from the descriptions in this manual For details refer to the Agilent Lab Advisor help files This manual provides lists with the names of Error Messages Not Ready messages and other common issues 1200 Series TCC Service Manual 1200 Series TCC Service Manual 2 Site Requirements and Specifications Site Requirements and Specifications 24 Power Consideration 24 Power Cords 25 Bench Space 26 Environment 26 Physical Specifications 27 Performance Specifications 28 Extended Specifications on G1316B SL G1316C SL Plus 30 gy Agilent Technologies 23 2 Site Requirements and Specifications Site Requirements and Specifications A suitable environment is important to ensure optimal performance of the instrument Power Consideration The module power supply has wideranging capability see Table 2 on page 27 It accepts any line voltage in the range described in the above mentioned table Consequently there is no voltage selector in the rear of the module There are also no externally accessible fuses because automatic electronic fuses are implemented in the power supply WARNING Incorrect line voltage at the instrument Shock hazard or damage of your instrumentation can result if the devices are connected to a line voltage higher than specified gt Connect your instrument to the specified line voltage WARNING Module
45. a BNC connector to be connected to Agilent 1100 1200 Series modules The other end depends on the instrument to which connection is being made Agilent 1100 1200 to 3390 2 3 Integrators Connector Pin Pin Agilent Signal Name 01040 60101 3390 2 3 1100 1200 1 Shield Ground 2 Not connected 7 S 3 Center Signal 6 is 7 RD 4 Connected to pin 6 aA 5 Shield Analog 1 BRN 6 Connected to pin 4 7 Key 8 Not connected 1200 Series TCC Service Manual Agilent 1100 1200 to 3394 6 Integrators Identifying Cables 12 Connector Pin Pin Agilent Signal Name 35900 60750 3394 6 1100 1200 1 Not connected 2 Shield Analog 3 Center Analog Tal oO A0 Agilent 1100 1200 to BNC Connector Connector Pin Pin Agilent Signal Name 8120 1840 BNC 1100 1200 x Al Shield Shield Analog Oa te Center Center Analog 1200 Series TCC Service Manual 217 12 Identifying Cables Agilent 1100 1200 to General Purpose Connector Pin Pin Agilent Signal Name 01046 60105 3394 6 1100 1200 1 Not connected 2 Black Analog oe 3 Red Analog 218 1200 Series TCC Service Manual Identifying Cables 12 Remote Cables O O JNE One end of these cables provides a Agilent Technologies APG Analytical Products Group remote connector to be connected to Agilent 1100 1200 Series modules The other end depend
46. a case turn off the module re set the address switches and turn on the module again Install the new processor board and reconnect the connectors Refit the screws at the REMOTE connectors Reinstall the foam section the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B SL on page 162 Reinstall the column compartment into the stack and reconnect the cables If a new CCM board is installed update the serial number information of the column compartment in the user interface Introduction on page 129 1200 Series TCC Service Manual 125 Repair 10 Check the firmware revision of the module If the firmware revision is older than the current firmware revision of the module update the firmware using the standard firmware update procedure see Replacing the Column Compartment s Firmware on page 100 Exchanging the Main Board G1316C SL Plus When If board is defective or for repair of other assemblies Tools required Screwdriver Pozidriv 1 PT3 Hexagonal wrench 5 mm Parts required Part number Description 1 G1316 61050 Main board CCM for G1316C SL Plus Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 1 Use a5 mm wrench to unscrew the REMOTE
47. a ee ae ae ee eee eee esDC 7c CoCHC h eS APG Remote RS 232C CAN Configuration switch Power G1316B Col Com SL G1316B Serial No Serial No HE Agilent Technologies G CE I M1 8 X nous smeo eam Safety standards configuration switch settings voltage range Agilent Technologies 76337 Waldbronn 108 120 220 280y POWer Consumption Made in Germany 320 VA 50 60 Hz requency Figure 7 Rear View of Oven Electrical Connections and Label 1200 Series TCC Service Manual 19 1 20 Introduction to the Column Compartment Serial Number Information The serial number information on the instrument labels provide the following information CCYWWSSSSS Format CC country of manufacturing DE Germany JP Japan CN China YWW year and week of last major manufacturing change e g 820 could be week 20 of 1998 or 2008 SSSSS real serial number 1200 Series TCC Service Manual Introduction to the Column Compartment 1 Instrument Layout The industrial design of the module incorporates several innovative features It uses Agilent s E PAC concept for the packaging of electronics and mechanical assemblies This concept is based upon the use of expanded polypropylene EPP layers foam plastic spacers in which the mechanical and electronic boards components of the module are placed This pack is then housed in a metal inner cabinet which is enclosed by a plastic external cabinet The advantages of this packag
48. ace the stator ring Ensure the stator ring is flush with the valve body 9 Place the new if required ceramic stator face in place on the stator head Reinstall the stator head 94 1200 Series TCC Service Manual CAUTION Maintenance 8 Valve Head 8 Position 9 Port High Pressure part number 5067 4107 has no stator face 10 Insert the stator screws in the stator head Tighten the screws alternately two turns at a time until the stator head is secure 11 Reconnect the pump capillaries to the valve ports Slide the waste tube into the waste holder in the leak tray Wrong use of pressure test may damage valve The current implementation of the pressure test automatically uses the maximum pressure generated by the pump used by that system gt Do not use the test for modules having a lower maximum pressure than the pump as this will damage the valve For example do not use 400 bar valve in a TCC in combination with a 600 bar pump 12 Perform a pressure tightness test to ensure the valve is pressure tight to 400 bar 1200 Series TCC Service Manual 95 8 Maintenance Adding Heater and Cooling Devices G1316B SL G1316C SL Plus The addtional heater and cooling devices can be arranged in the G1316B SL G1316C SL Plus in various locations depending on the application needs Some examples are shown below Ne ji A j o i
49. ansfer The two connectors for the CAN bus are used for internal Agilent 1200 Series module data transfer and synchronization One analog output provides signals for integrators or data handling systems The REMOTE connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features such as start stop common shut down prepare and so on With the appropriate software the RS 232C connector may be used to control the module from a computer through a RS 232C connection This connector is activated and can be configured with the configuration switch See your software documentation for further information The power input socket accepts a line voltage of 100 240 volts AC 10 with a line frequency of 50 or 60 Hz Maximum power consumption is 220 VA There is no voltage selector on your module because the power supply has wide ranging capability There are no externally accessible fuses because automatic electronic fuses are implemented in the power supply The security lever at the power input socket prevents the module cover from being taken off when line power is still connected Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations 1200 Series TCC Service Manual Introduction to the Column Compartment Electrical Connections Security lever C E m ee a Le m a o e l
50. are Type amp Use Recover with Agilent page 136 command line as described Firmware on page 136 Diagnostic Software Type amp under Recover with Agilent Firmware on page 136 ChemStation on page 136 134 1200 Series TCC Service Manual Table 9 Recover From Wrong Type Repair 9 User Interface incorrect but valid type incorrect but valid type incorrect and invalid type Instant Pilot G4208A Control Module 61323 Agilent Diagnostic Software preferred tool comes up with an error access to the module is possible via Service Mode as described under Recover with Instant Pilot on page 136 comes up with an error NO access to the module is possible Use Recover with Agilent Diagnostic Software Type Only on page 135 shows the incorrect product number access to the module is possible as described in Recover with Agilent Diagnostic Software Type Only on page 135 shows resident module G1314B R NO type change possible Use Recover with Agilent Diagnostic Software Type amp Firmware on page 136 shows resident or unsupported module NO type change possible Use Recover with Agilent Diagnostic Software Type amp Firmware on page 136 shows the incorrect product number access to the module is possible as described in Recover with Agilent Diagnostic Software Type Only on page 135 If wrong firmware has been loaded in addition only the L
51. at it can function simultaneously as an air heater The shape of the heat exchanger surface allows the area around the column to be kept at a similar temperature level as the liquid running through the column This is done by thermal convection and radiation between the heat exchanger fins This design ensures that the column and the solvent flowing through it are almost at the same temperature Actual temperature control is accomplished at the heat exchanger The solvent cools down or heats up on its transfer from the heating block to the column inlet This depends on several factors flow rate setpoint temperature ambient temperature and column dimensions In a flow through temperature regulation system there are necessarily slightly different temperatures at different positions If for example the temperature set by the user is 40 C then the heat exchanger is regulated to a temperature 40 8 C which is different by a certain offset here 0 8 C The solvent temperature at the column entry would be about 39 C The actual temperature displayed on the user interface is always the derived temperature taken at the heat exchanger corrected by the offset explained above Any type of heated column compartment brings one important consequence for column temperature equilibration Before an equilibrium is reached the whole mass of column column packing and solvent volume inside the column has to be brought to the selected temperature T
52. ata Parity Bits Reserved 1 0 Reserved TEST BOOT 1 1 RSVD SYS RSVD RSVD FC Switches 1 and 2 define which set of parameters for example for GPIB RS 232C and so on will be changed Once the change has been completed the instrument must be powered up again in order to store the values in the non volatile memory 1200 Series TCC Service Manual 239 13 Hardware Information Here the parameters are kept independently if you turn the column compartment off and on again They will be kept until the same set of parameters is subsequently changed and power is reset All other previously stored configuration settings are still being kept in non volatile memory In this manner you can store more than one set of parameters for example for GPIB and RS 232C using the same 8 bit configuration switch twice GPIB Default Addresses If you just want to change the GPIB address and need a detailed procedure refer to the Installing Your Agilent ChemStation System handbook Default GPIB address is set to the following addresses Table 48 Default Addresses for Agilent 1200 Series Modules Module Address Binary Address Pump 22 00010110 FLD 23 00010111 VWD 24 00011000 Agilent 8453A 25 00011101 DAD MWD 26 00011010 Column compartment 27 00011011 Autosampler 28 00011100 RID 29 00011101 where 0 means that the switch is down and 1 means that the switch is up Communication Settings for RS 232C Communication The commu
53. ations 27 post column cooling device 30 power settings autoranging 244 power consideration 24 power consumption 27 power cords 25 power supply description 244 pre column heatexchanger 30 radio interference 253 recover wrongtype 134 remote APG interface 236 remote timeout 64 remote cable 214 219 Removing the Top Cover and Foam 110 repairs assembling main cover 168 changing the column 91 cleaning the instrument 90 column switching valve parts 93 correcting leaks 99 exchanging processor board CCM 124 exchanging the fan 138 installing column switching valve 119 installing foam and top cover 162 installing heat exchangers 145 260 internal parts 108 introduction 86 overview 89 removing column switching valve 114 removing heat exchangers 140 removing top cover andfoam 110 replacing leak sensor and leak base 156 replacing status light pipe 161 types simple internal 86 warnings and cautions 86 right fan failed 68 right temperature timeout 69 RS 232 cable 215 RS 232C cable 229 communication settings 240 interface 238 S safety class 249 safety information lithium batteries 252 safety general information 249 standards 27 symbols 248 248 serial number information 20 serial number type using Agilent Diagnostic software 129 using ChemStation 130 using Control Mmodule 132 using Instant Pilot 132 serial number changing 129 setting the addresses 239 setting forced cold start 242 s
54. bient temperature The change in resistance is used by the leak circuit to compensate for ambient temperature changes If the resistance across the sensor increases above the upper limit the error message is generated Probable cause Suggested actions 1 Defective main board Exchange the main board Compensation Sensor Short The ambient compensation sensor NTC on the main board in the module has failed short circuit The resistance across the temperature compensation sensor NTC on the main board is dependent on ambient temperature The change in resistance is used by the leak circuit to compensate for ambient temperature changes If the resistance across the sensor falls below the lower limit the error message is generated Probable cause Suggested actions 1 Defective main board Exchange the main board Left Fan Failed The left cooling fan in the column compartment has failed 1200 Series TCC Service Manual 67 68 Error Information The hall sensor on the fan shaft is used by the TCC board to monitor the fan speed If the fan speed falls below 2 revolutions second for longer than 5 seconds the error message is generated Probable cause Suggested actions 1 Fan cable disconnected Ensure the fan is connected correctly 2 Defective fan Exchange fan 3 Defective TCC board Exchange the TCC board Right Fan Failed The right cooling fan in the column compartment has failed The hall sensor on the fan shaft is us
55. calibrated measuring device can be used to calibrate the column thermostat Temperature temperature at difference C H measuring point Column setpoint temperature Calibration at cross over point 36 C 80 Temperature C Figure 20 1 Point Calibration at the Temperature Cross Over Point 1200 Series TCC Service Manual Test Functions 7 The column thermostat is calibrated correctly when the measured temperature using the external measuring device Column Thermostat Temperature Calibration Procedure on page 82 and the cross over temperature 36 C of both heat exchangers left and right are within a range of 0 5 C 1200 Series TCC Service Manual 81 7 Test Functions Column Thermostat Temperature Calibration Procedure Tools required Parts required 82 Temperature measuring device see note below Description Calibrated temperature measuring device For the measuring and calibration process Agilent Technologies recommends a thermometer with 0 1 C precision Contact the local Agilent Technologies support representative for ordering information The figures in this procedure refer to a specific type of temperature sensor Heraeus Quat340 quartz surface temperature measurement sensor Other sensors may require a different fixing 1 Install the temperature sensor Installing the Temperature Sensor on page 83 2 Select the column compartment temperature calibratio
56. ck into the stack Reconnect the cables Reconnect the capillaries ao oi A amp Turn on the column compartment 1200 Series TCC Service Manual 161 9 Repair Installing the Foam and the Top Cover Installing the Foam and the Top Cover G1316A G1316B SL When After all repairs have been completed Tools required Screwdriver Pozidriv 1 PT3 Preparations The column compartment is open and other procedures have been carried out 1 Route the valve connector through the top foam and 2 Reconnect the valve connector to the main board carefully fit the top foam into the column compartment 162 1200 Series TCC Service Manual Repair 9 Installing the Foam and the Top Cover 3 Make sure that the foam is installed correctly and is located in the safety light switch 4 Position of the foam in the safety light switch 5 Place the top plate on the foam and slide it towards the rear and fix the screws at the rear of the top plate Ensure correct fit with Z plane oss TS wif Bae 1200 Series TCC Service Manual 163 9 Repair 7 Reinstall the cover 8 Close the front panel Next Steps 9 Place the column compartment back into the stack 10 Reconnect the cables 11 Turn on the column compartment 164 1200 Series TCC Service Manual Repair 9 Installing the Top Cover and Foam G1316C SL Plus When After repairs of internal parts have bee
57. connector aSaoqaS aa GSQSaa_aa SSeS S585845 M M M 126 1200 Series TCC Service Manual Repair 9 Main Board 2 Disconnect all connectors from the processor board Power left heat exchanger Power right heat exchanger Valve actuator drive control Valve actuator Power suppl encoder reader pply Door sensor Right fan gt Leak sensor x lt A valve tag reader Left fan 4 Column tag reader Column tag reader right heat exchanger and temperature sensor left heat exchanger KR fe 3 Remove the processor board Place the board on the ESD kit 4 Insome cases the RFI spring plate may remain on the interface connectors of the board Carefully remove the spring plate and place it back into its position in the instrument before installing a new board 5 On the new board check the switch setting of address switch S1 see Setting the 8 bit Configuration Switch on page 239 An incorrect switch setting e g TEST BOOT may cause the module to turn in a basic mode yellow or red flashing status light In such a case turn off the module re set the address switches and turn on the module again Install the new processor board and reconnect the connectors Refit the screws at the REMOTE connectors Reinstall the foam section the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B SL on page 162 9 Reinstall the column compartment into the s
58. d 1 4 5 16 inch 8710 0510 Wrench open end 5 16 3 8 inch 8710 2409 Capillary column heat exchanger 90 mm lg 0 17 i d not G1316 87300 assembled contains items 2 3 and 4 Ferrule front SST pack of 2 1 Ferrule back SST pack of 2 j Fitting SST pack of 2 i 1 re order 5062 2418 pack of 10 each of fittings front and back ferrule 188 1200 Series TCC Service Manual Parts and Materials for Maintenance 10 G1316A Accessory Kit 2PS 10PT modules Table 23 G1316A Accessory Kit 2PS 10PT modules Item Description Part Number G1316A Accessory Kit 2PS 10PT Column identification tag blank for re ordering use pack of 3 Column clip for re order use pack of 6 Corrugated tubing to waste re order 5 m CAN cable 0 5 m Wrench open end 1 4 5 16 inch Wrench open end 5 16 3 8 inch PEEK Capillary 280 mm lg 50 p i d pack of 4 MIC Valve Fitting pack of 2 Column holder for LC columns pack of 2 G1316 68725 5062 8588 5063 6526 5062 2463 5181 1516 8710 0510 8710 2409 G1316 87309 5022 2186 5001 3702 G1316B SL G1316C SL Plus Accessory Kit Standard Table 24 Accessory Kit Standard G1316B SL and G1316C SL Plus Item Description G1316B SL G1316C SL Plus Accessory Kit Standard Column identification tag blank for re ordering use pack of 3 Column clip qty 2 for re order use pack of 6 Corrugated tubing to waste re order 5 m CAN cable 0 5 m Wrench open end 1 4 5
59. d diagnose e maintenance and repair e parts identification e hardware information e safety and related information Agilent Technologies 1995 1996 2008 Printed in Germany 09 2008 G1316 90111 fe Agilent Technologies
60. d on and an entry is written into the instrument logbook This section describes the meaning of error messages and provides information on probable causes and suggested actions how to recover from error conditions 1200 Series TCC Service Manual General Error Messages Error Information 6 General error messages are generic to all Agilent 1200 Series HPLC modules Timeout The timeout threshold was exceeded Probable cause 1 The analysis was completed successfully and the timeout function switched off the module as requested 2 Anot ready condition was present during a sequence or multiple injection run for a period longer than the timeout threshold 1200 Series TCC Service Manual Suggested actions Check the logbook for the occurrence and source of a not ready condition Restart the analysis where required Check the logbook for the occurrence and source of a not ready condition Restart the analysis where required 63 64 Error Information Shut Down An external instrument has generated a shut down signal on the remote line The module continually monitors the remote input connectors for status signals A LOW signal input on pin 4 of the remote connector generates the error message Probable cause 1 Leak detected in another module with a CAN connection to the system 2 Leak detected in an external instrument with a remote connection to the system 3 Shut down in an external instrument
61. ddresses 240 interface 236 1200 Series TCC Service Manual heater profile 70 heaterexchanger pre column 30 heating concept 11 heatsink temperature 72 humidity 27 installation bench space 26 capillaries and waste tubings 46 column switching valve 119 column 45 45 flow connections 44 module 38 power cords 25 temperature sensor 83 unpacking 34 Instant Pilot changing serial number and type 132 recover type 136 instrument layout 21 interfaces APG remote 236 CAN 236 GPIB 236 RS 232C 238 internet 257 introduction concept of heating and cooling 11 system overview 11 L Lab Advisor software 22 60 LAN cable 215 227 eak sensor short 66 eak sensor open 66 eak 65 eaks correcting 99 eft fan failed 67 eft temperature timeout 69 ine frequency 27 ine voltage 27 ithium batteries 252 LMD changing serial number and type 129 recover type and firmware 136 recovery type only 135 M main assemblies 200 non operating altitude 27 non operating temperature 27 0 open cover 68 operating Altitude 27 operating temperature 27 optimization 51 optimizing the performance 52 P parts identification leak panels 196 parts identification column switching valve 203 foams 207 main assemblies 200 plastics 188 205 power and status 209 259 Index sheet metal kit 203 performance Optimization 51 optimizing 52 specifications and features 28 physical specifications 27 physical specific
62. dent on temperature A leak is detected when solvent cools the leak sensor causing the leak sensor current to change within defined limits If the current falls outside the lower limit the error message is generated Probable cause Suggested actions 1 Leak sensor not connected to the main Ensure the leak sensor is connected correctly board 2 Defective leak sensor Exchange the leak sensor 3 Leak sensor incorrectly routed being Exchange the leak sensor pinched by a metal component Leak Sensor Short The leak sensor in the module has failed short circuit The current through the leak sensor is dependent on temperature A leak is detected when solvent cools the leak sensor causing the leak sensor current to change within defined limits If the current increases above the upper limit the error message is generated Probable cause Suggested actions 1 Defective leak sensor Exchange the leak sensor 2 Leak sensor incorrectly routed being Check routing of leak sensor Replacing the pinched by a metal component Leak Sensor or Leak Base G1316A G1316B SL on page 156 1200 Series TCC Service Manual Error Information 6 TCC Error Messages The following errors are TCC specific error messages Compensation Sensor Open The ambient compensation sensor NTC on the main board in the module has failed open circuit The resistance across the temperature compensation sensor NTC on the main board is dependent on am
63. dependent sections e anon instrument specific section called resident system e an instrument specific section called main system Resident System This resident section of the firmware is identical for all Agilent 1200 series modules Its properties are e the complete communication capabilities GPIB CAN LAN and RS 232C e memory management e ability to update the firmware of the main system Main System Its properties are e the complete communication capabilities GPIB CAN LAN and RS 232C memory management e ability to update the firmware of the resident system In addition the main system comprises the instrument functions that are divided into common functions like e run synchronization via APG remote e error handling e diagnostic functions and so on or module specific functions like e internal events such as heater control column identification e and so on 1200 Series TCC Service Manual 233 13 Hardware Information 234 Firmware Updates Firmware updates can be done using your user interface e hand held control module with files from a PC card or e Agilent ChemStation with files from floppy disk The file naming conventions are 1316A_A601_12 dlb xxxx is the product number e g 1316 for the G1316A TCC and vvv is the revision number for example A601 is revision A 06 01 and zz is the build number For instructions refer to your user interface Update of
64. dules This includes tests and calibrations procedures as well as the different injector steps to perform all the maintenance routines Agilent Lab Advisor also allows users to monitor the status of their LC instruments The Early Maintenance Feedback EMF feature helps to carry out preventive maintenance In addition users can generate a status report for each individual LC instrument The tests and diagnostic features as provided by the Agilent Lab Advisor Software may differ from the descriptions in this manual For details refer to the Agilent Lab Advisor help files This manual provides lists with the names of Error Messages Not Ready messages and other common issues 1200 Series TCC Service Manual 1200 Series TCC Service Manual 6 Error Information What Are Error Messages 62 General Error Messages 63 TCC Error Messages 67 This chapter describes the meaning of error messages and provides information on probable causes and suggested actions how to recover from error conditions ot Agilent Technologies 61 6 Error Information What Are Error Messages 62 Error messages are displayed in the user interface when an electronic mechanical or hydraulic flow path failure occurs which requires attention before the analysis can be continued for example repair frit exchange exchange of consumable is necessary In the event of such a failure the red status indicator at the front of the column compartment is switche
65. e oa Ff O N 6 Press the button Send This will give as reply RA 0 TYPE G1315B 7 After a power cycle the module should show up with the correct product number type in the user interface Recover with Control Module The example uses G1315B as correct type 1 Select Tests Generic 2 Press keys m m m dot m This opens hidden functions 3 Select Command In the instruction line enter the command TYPE G1315B This will give as reply RA 0000 TYPE G1315B 5 After a power cycle the module should show up with the correct product number type in the user interface 1200 Series TCC Service Manual 137 9 Repair Exchanging the Fan When Tools required Parts required Preparations CAUTION If the fan is defective or noisy or for repair of other assemblies Screwdriver Pozidriv 1 PT3 Part number Description 1 3160 1017 Fan assembly Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 Incorrect positioning of fan might cause the thermostat to fail Column compartment is not thermostatted correctly Samples can degrade or measurement results can be biased due to wrong temperature gt Make sure the fan is installed in the correct orientation to ensure optimum cooling and operatio
66. e avoided whenever possible When inevitable this has to be carried out by a skilled person who is aware of the hazard involved Do not attempt internal service or adjustment unless another person capable of rendering first aid and resuscitation is present Do not replace components with power cable connected Do not operate the instrument in the presence of flammable gases or fumes Operation of any electrical instrument in such an environment constitutes a definite safety hazard Do not install substitute parts or make any unauthorized modification to the instrument Capacitors inside the instrument may still be charged even though the instrument has been disconnected from its source of supply Dangerous voltages capable of causing serious personal injury are present in this instrument Use extreme caution when handling testing and adjusting When working with solvents please observe appropriate safety procedures e g goggles safety gloves and protective clothing as described in the material handling and safety data sheet by the solvent vendor especially when toxic or hazardous solvents are used 1200 Series TCC Service Manual Appendix 14 The Waste Electrical and Electronic Equipment Directive Abstract The Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC adopted by EU Commission on 13 February 2003 is introducing producer responsibility on all electric and electronic appliances starting with 13 A
67. ed by the TCC board to monitor the fan speed If the fan speed falls below 2 revolutions second for longer than 5 seconds the error message is generated Probable cause Suggested actions 1 Fan cable disconnected Ensure the fan is connected correctly 2 Defective fan Exchange the fan 3 Defective TCC board Exchange the TCC board Open Cover The top foam has been removed The sensor on the TCC board detects when the top foam is in place If the foam is removed the fan is switched and peltier elements are switched OFF and the error message is generated Probable cause Suggested actions 1 The top foam was removed during operation Reinstall the top foam 2 Foam not activating the sensor Exchange the foam 1200 Series TCC Service Manual Error Information 6 Cover Violation The column compartment was switched on with the top cover and foam open The sensor on the CCM board detects if the top foam is in place If the column compartment is switched on with the foam removed the processor switches OFF the peltier elements after a short delay and the error message is generated Probable cause Suggested actions 1 The column compartment was switched on Reinstall the top cover and foam with the top cover and foam removed Left Temperature Timeout The temperature of the left heat exchanger did not reach the temperature setpoint within the timeout threshold Probable cause Suggested actions 1 Timeout threshold too short
68. ed to use the equipment in a manner as specified in this manual General This is a Safety Class I instrument provided with terminal for protective earthing and has been manufactured and tested according to international safety standards Operation Before applying power comply with the installation section Additionally the following must be observed Do not remove instrument covers when operating Before the instrument is switched on all protective earth terminals extension cords auto transformers and devices connected to it must be connected to a protective earth via a ground socket Any interruption of the protective earth grounding will cause a potential shock hazard that could result in serious personal injury Whenever it is likely that the protection has been impaired the instrument must be made inoperative and be secured against any intended operation Make sure that only fuses with the required rated current and of the specified type normal blow time delay and so on are used for replacement The use of repaired fuses and the short circuiting of fuse holders must be avoided 1200 Series TCC Service Manual 249 14 Appendix 250 Some adjustments described in the manual are made with power supplied to the instrument and protective covers removed Energy available at many points may if contacted result in personal injury Any adjustment maintenance and repair of the opened instrument under voltage should b
69. embly on page 244 4 Fan assembly 3160 1017 5 Heatexchanger left 3 ul for G1316A G1316 60007 5 High Temp Heatexchanger left 3 pl for G1316B G1316 60017 6 Heatexchanger right 6 ul for G1316A G1316 60006 6 High Temp Heatexchanger right 6 pl for G1316B G1316 60016 7 Valve optional see Column Switching Valve 2 Position 6 Port G1316A G1316B SL on page 181 or Micro Column Switching Valve 2 Postion 6 Port G1316A G1316B SL on page 185 or Micro Column Switching Valve 2 Position 10 Port G1316A G1316B SL on page 186 8 Leak sensor assembly 5061 3356 9 Leak handling parts See Leak Parts on Cover plate when switching valve is not installed Front cover and plastic parts housing page 210 G1316 44103 See Plastic Parts on page 205 1200 Series TCC Service Manual 201 11 Parts for Repairs Table 34 Overview of Main Assemblies Item Description Part Number Sheet metal parts See Sheet Metal Kit on page 203 Foam parts See Foam Parts on page 207 Screw and Washer Kit Rear Panel includes following items G1316 67004 Screw M4 Washer Hexagonal nut for RS 232 connector 202 1200 Series TCC Service Manual Parts for Repairs 11 Sheet Metal Kit Sheet Metal Kit Table 35 Sheet Metal Kit Parts G1316A G1316B SL Item Description Part Number Sheet metal kit includes items 1 2 and 3 G1316 68701 4 RFI shield G1316 00600 5 RFI spring side G1316 09100 6
70. er and Cooling Devices for G1316B SL G1316C SL Plus Item Description Part Number Heater long up 0 12 mm i d 1 6 pl internal volume G1316 80002 G1316B SL G1316C SL Plus Part of G1316B SL G1316C SL Plus Capillary System Kit on page 190 Heater long down 0 12 mm i d 1 6 pl internal volume G1316 80003 G1316B SL G1316C SL Plus Part of G1316B SL G1316C SL Plus Capillary System Kit on page 190 Post column cooler 0 12 mm i d 1 5 pl internal volume G1316 80004 G1316B SL G1316C SL Plus Part of G1316B SL G1316C SL Plus Capillary System Kit on page 190 Carrier for Heater and Cooler G1316B SL G1316 83200 includes 3 screws SKT HD CAP M3 x 0 5 12 mm long 0515 1052 Part of G1316B SL G1316C SL Plus Capillary System Kit on page 190 1200 Series TCC Service Manual 179 10 Parts and Materials for Maintenance Heater and Cooling Devices for G1316B SL G1316C SL Plus Table 13 Consumables G1316C SL Plus Description Part Number Column Clip Set 8 Colors 5042 9918 Carrier for Heat Exchanger G1316C SL Plus G1316 89200 Fitting Holder Assy includes following items G1316 68706 Fitting Fork Fitting Clip Screws Pack of 4 YY Agilent Technologies 1200 Series aae L shaped pre column heater U shaped Post column cooler Volume 1 6 pl Volume 1 5 ul mounted on carrier mounted on Carrier top for column 1 bottom for column 2 holes to attach carrier Figure
71. etpoint is changed to 30 C and both elements begin heating The time required to reach 30 C is a measure of heating efficiency Heater Function Test Thermostat Function Test Result A typical thermostat function test profile is shown in Figure 19 on page 77 76 1200 Series TCC Service Manual Test Functions 7 Temperature C 304 28 2 4 24 224 20 Right Peltier element Left Peltier element Time minutes Figure 19 Typical Thermostat Function Test Profile Evaluating the Thermostat Function Test During the cooling phase the Peltier elements should cool at a rate of gt 2 C minute During the heating phase the temperature change should be gt 3 C minute Defective thermostat components may cause cooling or heating rates to fall outside these limits 1200 Series TCC Service Manual 71 7 78 Test Functions Function Test Failed Probable Causes Column compartment cover not installed correctly bad insulation Air intake blocked insufficient air flow for cooling Poor peltier efficiency if setpoint temperatures can still be reached and are stable there is no requirement to exchange the heater assembly Defective sensors on flex board Defective heater assembly Suggested Actions V Ensure cover is installed correctly V Ensure sufficient space is available for air circulation see Bench Space on page 26 V Exchange the heater assembly 1200
72. etrachloride with 2 propanol or THF 256 1200 Series TCC Service Manual Appendix 14 Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at http www agilent com Select Products Chemical Analysis It will provide also the latest firmware of the Agilent 1200 Series modules for download 1200 Series TCC Service Manual 257 Index Index A Agilent Diagnostic Software 22 60 Lab Advisor Software 22 60 oninternet 257 algae 255 255 ambient operating temperature 27 ambient non operating temperature 27 analog cable 214 216 auxiliary cable 214 226 battery safety information 252 BCD cable 214 224 bench space 26 C cable analog 214 216 auxiliary 214 226 BCD 214 224 CAN 227 external contact 228 external contacts 215 GPIB 215 LAN 215 227 remote 214 219 RS 232 215 229 cables overview 214 258 calibration temperature 56 80 CAN interface 236 CAN cable 227 changing serial number and type 129 ChemStation changing serial number and type 130 recover type 136 column switching valve optiona description 15 precolumn backflushing 17 column switching valve optiona two column selection 16 column switching valve installing 119 column clip 50 column identification 13 tag 49 column temperature 72 column changing column and tags 91 compensation sensor open 67 compensation sensor short 67 con
73. ety Notices CAUTION A CAUTION notice denotes a hazard It calls attention to an operating procedure practice or the like that if not correctly per formed or adhered to could result in damage to the product or loss of important data Do not proceed beyond a CAUTION notice until the indicated condi tions are fully understood and met A WARNING notice denotes a hazard It calls attention to an operating procedure practice or the like that if not correctly performed or adhered to could result in personal injury or death Do not proceed beyond a WARNING notice until the indi cated conditions are fully under stood and met 1200 Series TCC Service Manual In This Guide In This Guide This manual covers the Agilent 1200 Series Thermostatted Column Compartments TCC e G1316A Agilent 1200 Series TCC e G1316B Agilent 1200 Series TCC SL e G1316C Agilent 1200 Series TCC SL Plus 1 Introduction to the Column Compartment This chapter gives an introduction to the TCC instrument overview and internal connectors 3 Installing the Column Compartment This chapter describes the installation of the Thermostatted Column Compartment 4 How to optimize the Column Compartment This chapter provides information on how to optimize the Thermostatted Column Compartement 5 Troubleshooting and Diagnostics Overview about the troubleshooting and diagnostic features 6 Error Information This chapter describes
74. figuration switch default settings 239 description and factory settings 239 Control Module changing serial number and type 132 recover type 137 cool down time 28 cooling concept 11 cooling device post column 30 cover violation 69 D dead volume 28 defective heater circuit 73 defective temperature sensor 70 delivery checklist 34 Diagnostic software 22 60 dimensions 27 E electrical connections descriptions of 18 electronic waste 251 electronics 232 electrostatic discharge ESD 88 109 environment 26 error messages column temperature 72 compensation sensor open 67 compensation sensor short 67 cover violation 69 defective heater circuit 73 defective temperature sensor 70 heater profile 70 heatsink temperature 72 introduction 62 leak sensor open 66 leak sensor short 66 leak 65 left fan failed 67 1200 Series TCC Service Manual Index left temperature timeout 69 open cover 68 remote timeout 64 right fan failed 68 right temperature timeout 69 shut down 64 timeout 63 valve failed 71 external measuring device information 82 external contact cable 215 228 F features GLP 28 29 instrument layout 21 safety and maintenace 28 firmware main system 233 resident system 233 updates 234 flow cell 255 solvent information 255 forced cold start setting 242 frequency range 27 function test failed 78 result 76 fuses none in the instrument 244 G GLP features 28 GPIB cable 215 default a
75. firmware the following steps have to be performed If new version solves problems of currently installed version or after exchange of the TCC main board CCM the version on board is older than previous installed one LAN RS 232 Firmware Update Tool or Instant Pilot G4208A or Control Module G1323B Description Firmware tools and documentation from Agilent web site Read update documentation provided with the Firmware Update Tool 1 Download the module s firmware the LAN RS 232 FW Update Tool Version 2 10 or above and the documentation from the Agilent web http www chem agilent com scripts cag_firmware asp 2 Load the firmware into the TCC as described in the documentation The G1316B SL requires firmware revision A 06 02 or higher main and resident The G1316C SL Plus requires firmware revision A 06 10 or higher main and resident 1200 Series TCC Service Manual Maintenance 8 Replacing Valve Heads G1316C SL Plus Several optional valve heads are available for the G1316C which can be installed and exchanged easily Parts required Part number Description 1 5067 4107 8pos 9prt valve head high pressure and or 1 5067 4108 8pos 9prt valve head low pressure CAUTION Valve Damage Using a low pressure valve on the high pressure side can damage the valve gt When using multiple column compartments as part of a method development solution make sure that the high pressure valve head is connected to the autosample
76. for proper function The identification tag can be easily removed from the column For columns with small diameter a cable tie wrap should be used to fix the column identification tag to the column Assure that the tie wrap does not block the front cover The tag needs to be placed differently depending on whether the column is installed at the left or right heat exchanger see Figure 15 on page 49 and Figure 16 on page 50 The Agilent logo should always be at front Column identification tag Figure 15 Column ldentification Tag for Left Heat Exchanger 1200 Series TCC Service Manual 49 3 Installing the Column Compartment Column identification tag Figure 16 Column Identification Tag for Right Heat Exchanger Column Clip For better positioning of the column on the heat exchanger a column clip is available see Accessory Kits on page 188 Figure 17 Column Clip part number 5063 6526 pack of 6 50 1200 Series TCC Service Manual 1200 Series TCC Service Manual 000 pe How to optimize the Column Compartment Optimizing the Performance of your Column Compartment 52 Using Additional Heater and Cooling Devices 53 This chapter provides information on how to optimize the Thermostatted Column Compartement Agg Agilent Technologies 51 4 How to optimize the Column Compartment Optimizing the Performance of your Column Compartment 52 For best performance results of the column c
77. gies to ensure proper functionality and compliance with safety or EMC regulations see Cable Overview on page 214 1200 Series TCC Service Manual 235 13 Hardware Information GPIB Interface The GPIB connector is used to connect the module with a computer The address and control switches next to the GPIB connector determine the GPIB address of your module The switches are preset to a default address and recognized by the operating software from Agilent Technologies Table 44 Default Addresses Autosampler 28 Autosampler 28 Pump 22 RID 29 FLD 23 VWD 24 Autosampler HP 1050 11 Agilent 8453A 25 Pump HP 1050 12 DAD MWD 26 VWD HP 1050 10 Column Compartment 27 DAD HP 1050 17 CAN Interface The CAN is an intermodule communication interface It is a 2 wire serial bus system supporting high speed data communication and real time requirement Remote Interface The APG Remote connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down prepare and so on Remote control allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements The subminiature D connector is used The module provides one remote connector which is inputs outputs wired or technique 236 1200 Series TCC Service Manual Hardware Information 13 To provide maximum safety within a distributed ana
78. h Pressure G1316C SL Plus Item Description Part Number Valve Head 8 Position 9 Port High Pressure 5067 4107 1 Stator Screws 1535 4857 2 Stator Head 5067 4110 3 Rotor Seal High Pressure 5067 4111 4 Isolation Seal 0100 1852 Figure 32 Column Switching Valve Parts 5067 4107 1200 Series TCC Service Manual 183 10 Parts and Materials for Maintenance Column Switching Valve Parts 400 bar G1316C SL Plus Table 16 Valve 8 Postion 9 Port 400 bar G1316C SL Plus Item Description Part Number Valve Head 8 Position 9 Port 400 bar 5067 4108 1 Stator Screws 1535 4857 2 Stator Head 5067 4112 3 4 Stator Face Rotor Seal 400 bar 5067 4113 5 Isolation Seal 0100 1852 2 A KF Figure 33 Column Switching Valve Parts 5067 4108 184 1200 Series TCC Service Manual Parts and Materials for Maintenance 10 Micro Column Switching Valve 2 Postion 6 Port G1316A G1316B SL Table 17 Micro Column Switching Valve 2PS 6PT for G1316A G1316B SL 400 bar Item Description Part Number Micro Column Switching Valve 2PS 6PT 400 bar 0101 1051 Stator face 0100 2089 Rotor seal 3 grooves 0100 2087 Table 18 Micro Column Switching Valve 2PS 6PT for G1316B SL 600 bar Item Description Part Number Micro Column Switching Valve 2PS 6PT 600 bar 0101 1420 Stator 600 bar 0101 1417 Rotor seal 3 grooves 600 bar 0101 1409 1200 Series TCC Service Manual 185 10 Parts and Materials for Maintenance Micro Column Sw
79. her assemblies have to be removed Tools required Screwdriver Pozidriv 1 PT3 Wrench 1 4 5 16 inch for capillary connections Parts required Part number Description 1 G1316 60007 Heat exchanger assembly left includes ambient temperature sensor 1 G1316 60006 Heat exchanger assembly right Preparations The heat exchanger s are removed as described in Removing the Heat Exchanger Assemblies G1316A G1316B SL on page 140 CAUTION The flexible cables close to the heat exchanger assemblies may be easily damaged gt Be careful that the flexible cables close to the heat exchanger assemblies are not damaged especially during steps 3 through 6 CAUTION The ambient temperature sensor may get damaged if not installed correctly gt Ensure that the ambient temperature sensor is completely plugged into the rear of the top plastic panel CAUTION New foam parts have been introduced for enhanced performance of the G1316C SL Plus gt However using these foam parts for G1316A or G1316B SL may change thermal properties of these modules and bias measurement results 1200 Series TCC Service Manual 145 Repair Installing the Heat Exchanger Assemblies 1 Replace the leak tubing assembly into its location on leak base Ensure that it keeps in this position during the next steps 2 Replace the heat exchanger assembly A screwdriver might be helpful to insert the silicon isolation 3 Carefully insert the
80. her user interfaces Start the Diagnostic Software 2 Select Tools on the left navigation panel 3 Select in the Tools Selection box Board Check and Change and press the button Start 4 Change the field Type and or Serial as required 1200 Series TCC Service Manual 129 9 Repair Some Agilent 1100 1200 series modules require the correct main board version to match the type for example the SL modules 5 Press the button Apply to complete the action A message The type was changed to XXXXXX Close this application and switch off and on the changed LC module Close the Diagnostic Software Power cycle the module Restart the User Interface Using the Agilent ChemStation Module serial numbers are entered by typing specific commands on the command line at the bottom of the main user interface screen Turn the module on Start the Agilent ChemStation 1 To enter a module serial number type the following command into the command line print sendmodule Lxxx ser YYNNNNNNNN or print sendmodule Nxxx ser YYNNNNNNNN where xxx is the module type YY is country code in capital letters and NNNNNNNN the 8 character serial number of the module in question Table 7 ChemStation Command Format Serial Number Change Modules with or without optional interface board Modules with LAN on board PRINT SENDMODULES Lxxx SER YYNNNNNNNN PRINT SENDMODULES Nxxx SER YYNNNNNNNN module identifier
81. his depends on several factors flow rate setpoint temperature ambient temperature and column dimensions The higher the flow rate the faster the column equilibrates due to thermostatted mobile phase 1200 Series TCC Service Manual 11 1 Introduction to the Column Compartment Column Thermostat Temperature Calibration on page 80 shows a setpoint temperature of 40 C Some time after entering the setpoint the heat exchanger has reached its temperature and the control activity starts The TEMPERATURE NOT READY signal will be cancelled 20 seconds after the sensed temperature was within a range of 0 5 C of the setpoint other values can be set via the user interface However this does not necessarily mean that the column has already reached the correct temperature The equilibration of the column may take longer Stability of the pressure signal is a good indication for equilibrium 45 Heat exchanger temperature 40 35 Column temperature Temperatur C 30 25 0 1 2 3 4 5 6 7 8 9 0 N 2 8 4 6 6 T Time min Figure 1 Equilibration of Heat Exchanger and Column Temperature The temperature calibration and verification is described in Column Thermostat Temperature Calibration on page 80 12 1200 Series TCC Service Manual Introduction to the Column Compartment 1 Column Identification System The Agilent 1200 Series thermostatted column compartment is equipped with a column identification system It a
82. hnologies sales and service office Table 4 Column Compartment Delivery Checklist Description Quantity Thermostatted column compartment 1 Power cable 1 CAN cable 1 Column switching valve optional User Manual 1 Accessory kit see Accessory Kits on 1 page 188 1200 Series TCC Service Manual Installing the Column Compartment 3 Optimizing the Stack Configuration If your column compartment is part of a Agilent 1200 Series system you can ensure optimum performance by installing the following configuration This configuration optimizes the system flow path and ensures minimum delay volume For installations of the G1316C SL Plus as part of the Method Development Solution please refer to the Method Development Solution User and Installation Guide part number G4230 90000 1200 Series TCC Service Manual 35 3 Installing the Column Compartment Solvent cabinet Vacuum degasser Pump Local User Interface Autosampler i Column compartment Detector Figure 9 Recommended Stack Configuration Front View 36 1200 Series TCC Service Manual Installing the Column Compartment 3 AC power a a ecne Remote cable CAN Bus cable to local user interface
83. hut down 64 site requirements environment 26 solvent information 255 solvents 255 sound emission 254 specification physical 27 specifications 28 stack configuration 35 56 57 system overview 11 status indicators T tag installation 49 temperature verification principle 83 temperature calibration description 80 problems 83 procedure 82 temperature verification external measuring device 82 temperature range 28 tests available tests vs interface 59 test thermostat function test failed 78 thermostat function test result 76 thermostat function test 56 timeout 63 troubleshooting available tests vs interface 59 error messages 56 status indicators 56 57 1200 Series TCC Service Manual Index type recover with ChemStation 136 with Control Module 137 with Instant Pilot 136 type and firmware recover with LMD 136 type recover with LMD 135 type changing 129 U unpacking 34 User Interfaces diagnosic tests 59 V valve failed 71 verification temperature 56 voltage range 27 wW warm up time 28 waste electrical and electronic equipment 251 WEEE directive 251 weight 27 1200 Series TCC Service Manual 261 www agilent com In This Book This manual contains technical reference information about the Agilent 1200 Series thermostatted column compartment The manual describes the following e introduction and specifications e installation e using and optimizing e troubleshooting an
84. ices can be installed in any position in the column compartment see Installation of Heater and Cooling Devices G1316B SL on page 47 CE Agilent Technologies 1200 Series L shaped pre column heater Heater long up L shaped pre column heater Heater long down L shaped pre column heater U shaped post column cooler Volume 1 6 pl Volume 1 5 pl mounted on carrier mounted on carrier top for column 1 bottom for column 2 Figure 8 New additional heater and cooling devices The standard column compartment is equipped with a 3 ul and 6 ul heater or cooler Both can be set at the same or different temperature To reduce the delay volume a kit G1316B SL G1316C SL Plus Capillary System Kit on page 190 has been set up for installing a small heaters with 1 6 ul internal delay volume and also a new cooling device with 1 5 ul internal volume is available 30 1200 Series TCC Service Manual Site Requirements and Specifications Extended Specifications on G1316B SL G1316C SL Plus NOTE If the additional heater and cooling devices are used as shown in Figure 8 on page 30 the column identification system cannot be used If the column identification system is required fix the heater and cooling devices in the upper or lower locations or fix them right left of the current location 2 1200 Series TCC Service Manual 31 2 Site Requirements and Specifications Extended Specifications on G1316B SL G1316C SL Plu
85. ices for G1316B SL G1316C SL Plus on page 179 1200 Series TCC Service Manual Table 26 Capillary System Kit G1316 68716 Parts and Materials for Maintenance 10 Item Description Part Number Seat Capillary 100 mm x 0 12 mm 0 8 OD G1367 87303 DAD Heat Exchanger Capillary 310 mm x 0 12 mm G1315 87339 SST Capillary 340 mm x 0 12 mm m m SST Capillary 300 mm x 0 12 mm m m SST Capillary 210 mm x 0 12 mm m m SST Capillary 170 mm x 0 12 mm m m SST Capillary 130 mm x 0 12 mm m f SST Capillary 90 mm x 0 12 mm m f SST Capillary 70 mm x 0 12 mm m f SST Capillary 50 mm x 0 12 mm m f SST Capillary 170 mm x 0 12 mm m f SST Capillary 500 mm x 0 12 mm m m SST Capillary 500 mm x 0 12 mm m m G1316 87319 G1316 87318 G1316 87317 G1316 87316 G1316 87315 G1316 87314 G1316 87313 G1316 87312 G1316 87327 G1316 87309 G1315 87307 G1316C SL Plus Capillary System Kits Table 27 G1316C Capillary System Kits Description Part Number Solvent selection tubing kit 4 solvents 5067 4601 Method Development Capillary Kit low dispersion short column 5067 1595 Method Development Capillary Kit low dispersion long column 5067 1596 Method Development Capillary Kit general purpose 5067 1597 RRHT Selectivity Method Development Kit 2 1 mm ID 5190 1431 RRHT pH Method Development Kit 2 1 mm ID 5190 1432 RRHT Selectivity Method Development Kit 4 6 mm ID 5190 1433 RRHT pH Method Development Kit 4 6 mm ID 5190 1434
86. ies to the column NOTE See Column Switching Valve Optional for G1316A G1316B SL on page 15 on how to connect the column selection valve 1200 Series TCC Service Manual 45 3 Installing the Column Compartment Flow Connec ons of the Column Compartment 6 Ifthe column compartment is not part of a Agilent 1200 7 Route tubings from modules above through the openings Series system or if an Agilent 1200 Series Autosampler is in the funnel holder top and the plastic bottom part located on top connect the corrugated tubing to the Remove small plastic plugs first waste outlet 8 Put the front cover back in place The installation of the column compartment has now been completed NATE Always operated the TCC with the front cover in place for proper thermostatting conditions i and to protect the column area against strong drafts from the ouside 46 1200 Series TCC Service Manual Installing the Column Compartment 3 Installation of Heater and Cooling Devices Installation of Heater and Cooling Devices Installation of Heater and Cooling Devices G1316B SL With the introduction of the 1200 series TCC SL G1316B SL the heater elements were redesigned in order to allow the adding of small heater and cooling devices NOTE Depending on the application these heater and cooling devices can be fixed at various places Information about the usage of these heater and coo
87. ij dit apparaat zijn batterijen geleverd Wanneer deze leeg zijn moet u ze niet weggooien maar inleveren als KCA 1200 Series TCC Service Manual Appendix 14 Radio Interference Cables supplied by Agilent Technoligies are screened to provide opitimized protection against radio interference All cables are in compliance with safety or EMC regulations Test and Measurement If test and measurement equipment is operated with unscreened cables or used for measurements on open set ups the user has to assure that under operating conditions the radio interference limits are still met within the premises 1200 Series TCC Service Manual 253 14 Appendix Sound Emission Manufacturer s Declaration This statement is provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991 This product has a sound pressure emission at the operator position lt 70 dB e Sound Pressure Lp lt 70 dB A e At Operator Position e Normal Operation e According to ISO 7779 1988 EN 27779 1991 Type Test 254 1200 Series TCC Service Manual Appendix 14 Solvent Information Flow Cell To protect optimal functionality of your flow cell e Avoid the use of alkaline solutions pH gt 9 5 which can attack quartz and thus impair the optical properties of the flow cell e Ifthe flow cell is transported while temperatures are below 5 degree C it must be assured that the cell is filled with alcohol e Aque
88. incidental or consequential damages in connection with the furnishing use or perfor mance of this document or of any information contained herein Should Agilent and the user have a separate written agreement with warranty terms covering the material in this document that conflict with these terms the warranty terms in the sep arate agreement shall control Technology Licenses The hardware and or software described in this document are furnished under a license and may be used or copied only in accor dance with the terms of such license Restricted Rights Legend If software is for use in the performance of a U S Government prime contract or subcon tract Software is delivered and licensed as Commercial computer software as defined in DFAR 252 227 7014 June 1995 or as a commercial item as defined in FAR 2 101 a or as Restricted computer soft ware as defined in FAR 52 227 19 June 1987 or any equivalent agency regulation or contract clause Use duplication or dis closure of Software is subject to Agilent Technologies standard commercial license terms and non DOD Departments and Agencies of the U S Government will receive no greater than Restricted Rights as defined in FAR 52 227 19 c 1 2 June 1987 U S Government users will receive no greater than Limited Rights as defined in FAR 52 227 14 June 1987 or DFAR 252 227 7015 b 2 November 1995 as applicable in any technical data Saf
89. ing technology are e virtual elimination of fixing screws bolts or ties reducing the number of components and increasing the speed of assembly disassembly e the plastic layers have air channels molded into them so that cooling air can be guided exactly to the required locations e the plastic layers help cushion the electronic and mechanical parts from physical shock and e the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself 1200 Series TCC Service Manual 21 1 Introduction to the Column Compartment Agilent Lab Advisor Software 22 The Agilent Lab Advisor Software is a standalone product that can be used with or without data system Agilent Lab Advisor helps to manage the lab for high quality chromatographic results and can monitor in real time a single Agilent LC or all the Agilent GCs and LCs configured on the lab intranet Agilent Lab Advisor provides diagnostic capabilities for all Agilent 1200 Series HPLC modules This includes tests and calibrations procedures as well as the different injector steps to perform all the maintenance routines Agilent Lab Advisor also allows users to monitor the status of their LC instruments The Early Maintenance Feedback EMF feature helps to carry out preventive maintenance In addition users can generate a status report for each individual LC instrument
90. inging it to its outer position and unscrew all capillary connections from the valve head 102 1200 Series TCC Service Manual Maintenance 8 Replacing Valve Heads G1316C SL Plus 4 Put the new valve head onto the valve drive such that the 5 Screw the valve head onto the valve drive using the union lobe fits to the groove nut 7 Push the valve head until it snaps in and stays in the rear position 8 Switch on the module 1200 Series TCC Service Manual 103 8 Maintenance Preparing the G1316C SL Plus for Transportation When If the Thermostatted Column Compartment SL Plus G1316C shall be transported Tools required Screwdriver Pozidriv 1 PT3 Parts required Part number Description 1 G1316 67001 Transportation Lock Kit The module has been shipped with transportation locks which must be used for transportation protection A transportation lock kit can be re ordered using 1 Remove the valve head as described in Replacing Valve 2 Replace the valve head by the transportation valve head Heads G1316C SL Plus on page 101 Bring the transportation valve head to the outer position 104 1200 Series TCC Service Manual Maintenance 8 Preparing the G1316C SL Plus for Transportation 3 Use 4 screws M3x8 0515 0897 for fixing the lock plate 4 Use a screw 2680 0128 for fixing the lock plate to the G1316 03701 to the heat exchangers in the outer transportation val
91. ings For the heater device inlet capillary choose fittings which are compatible to your column Swagelock compatible columns 5065 4454 pk of 10 with ferrules A D Fitting screw long Swagelock compatible columns removable 0100 2086 A Jo Nut seal tight Figure 28 Fitting type depends on column type 98 1200 Series TCC Service Manual Maintenance 8 Correcting Leaks When If a leakage has occurred at the heat exchanger or at the capillary connections or at the column switching valve Tools required Tissue pipette Wrench 1 4 5 16 inch for capillary connections Depending on the column position or the use of additional heat exchanger assemblies the view of Figure 29 on page 99 may vary 1 Remove the front cover 2 Use a pipette and tissue to dry the leak sensor area 3 Observe the capillary connections and the column switching valve for leaks and correct if required 4 Re install the front cover Column switching valve Column E Si all mf Leak sensor assembly Waste outlet Figure 29 Possible Leak Areas 1200 Series TCC Service Manual 99 8 Maintenance Replacing the Column Compartment s Firmware When Tools required Parts required Preparations 100 The installation of older firmware might be necessary e to keep all systems on the same validated revision or e if third part control software requires a special version To upgrade downgrade the TCC s
92. is partially energized when switched off as long as the power cord is plugged in Repair work at the module can lead to personal injuries e g shock hazard when the cover is opened and the module is connected to power gt Remove the power cable from the instrument before opening the cover gt Do not connect the power cable to the Instrument while the covers are removed 24 1200 Series TCC Service Manual CAUTION Site Requirements and Specifications 2 Unaccessable power plug In case of emergency it must be possible to disconnect the instrument from the power line at any time gt Make sure the power connector of the instrument can be easily reached and unplugged gt Provide sufficient space behind the power socket of the instrument to unplug the cable Power Cords Different power cords are offered as options with the module The female end of all power cords is identical It plugs into the power input socket at the rear of the module The male end of each power cord is different and designed to match the wall socket of a particular country or region The absence of ground connection and the use of an unspecified power cord can lead to electric shock or short circuit Electric Shock gt Never operate your instrumentation from a power outlet that has no ground connection gt Never use a power cord other than the Agilent Technologies power cord designed for your region Use of unsupplied cables
93. it Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section Removing the Top Cover and Foam on page 110 CAUTION The flexible cables close to the heat exchanger assemblies may be easily damaged gt Be careful that the flexible cables close to the heat exchanger assemblies are not damaged especially during steps 3 through 6 CAUTION The ambient temperature sensor may get damaged if not installed correctly gt Ensure that the ambient temperature sensor is completely plugged into the rear of the top plastic panel CAUTION Bias measurement results Foam parts have been introduced for improving the thermostat performance gt Not using these parts for G1316C SL Plus can reduce thermostat performance and bias measurement results 1200 Series TCC Service Manual 149 Repair Installing the Heat Exchanger Assemblies 1 Small foam part Insert the heat exchanger unit and the small foam part in the corner of the module This foam part is part of the Foam Part Kit G1316 68712 For the left heat exchanger carefully reinstall the temperature sensor from the heat exchanger unit On both sides of the valve actuator fixation clips shall keep the flexible boards of the heat exchanger assemblies in the correct position Instal
94. it G1316A G1316B SL Refer to Figure 34 on page 194 for connection diagram Table 29 Column Regeneration Kit 10 Description where used Part Number Column Regeneration Kit G1316 68721 SST Capillary 700 mm x 0 17 mm 1 32 1 32 column to cell G1312 87304 SST Capillary 100 mm x 0 12 mm 1 32 1 32 SST Capillary 100 mm x 0 12 mm male female 1 32 1 16 SST Capillary 340 mm x 0 12 mm male female 1 32 1 16 SST Capillary 70 mm x 0 12 mm male female 1 32 1 16 pack of 2 SST Capillary 50 mm x 0 12 mm male female SST Capillary 70 mm x 0 12 mm male female SST Capillary 75 mm x 0 12 mm male female 1 32 1 16 Seat Capillary 100 mm x 0 12 mm pack of 2 PEEK fitting special for Chip LC Flexible PEEK Tubing 450 mm x 0 4 mm switching capillary adapter capillary WPS to valve valve to heatexchanger column to cell column to cell valve to detector valve to waste G1316 27301 G1316 87304 G1316 87305 G1316 87306 G1316 87312 G1316 87313 G1316 87326 G1367 87303 G4240 43200 5022 6503 1200 Series TCC Service Manual 193 10 Parts and Materials for Maintenance Accessory Kits To Detector 61367 87303 0 12 x 100 m G1316 87326 0 12 x 78 m male 5022 5503 0 4 x 450 PEEK fm female Waste Heatexch G1316 87306 G1316 80003 0 42 x78 G1316 80002 0 12 x 210 0 12 x 210 G1312 87304 From Col 61316 87305 0 17 x 700 Reg Pump From WPS 0 12 x 340 Figu
95. itching Valve 2 Position 10 Port G1316A G1316B SL Technical details can be found in the Technical Note that is supplied with the kit Table 19 Micro Column Switching Valve 2PS 10PT for G1316A G1316B SL 400 bar Item Description Part Number 2PS 10 PT Valve kit includes all parts required for installation G1316 68709 Rebuild kit includes PEEK rotor seal PEEK stator face hex key 0101 1360 2PS 10 PT valve 0101 1343 Rotor seal Vespel 0101 1361 Stator face 0101 1362 Capillary kit see Table 21 on page 186 G1316 68711 Table 20 Micro Column Switching Valve 2PS 10PT 600 bar for G1316B SL 600 bar Item Description Part Number Column Switching Valve 2PS 10PT for p LC System 600 bar 0101 1419 Stator 600 bar 0101 1421 Rotor seal 5 grooves 600 bar 0101 1415 Table 21 Capillary Kit G1316 68711 From To ID mm Length mm Qty Part number Remark Capillaries ALS Valve port 2 0 17 700 1 5065 9932 186 1200 Series TCC Service Manual Table 21 Capillary Kit G1316 68711 Parts and Materials for Maintenance 10 From To ID mm Length mm Qty Part number Remark Valve port 3 TCC 3 ul In 0 17 105 1 5021 1816 1623 pl Out Column 1 0 17 105 1 5021 1816 Column 1 Valve port 6 0 17 105 1 5021 1816 for long column Column 1 Valve port 6 0 17 200 1 5065 9931 for short column Valve port 7 Detector In 0 17 280 1 5021 1818 Valve port 1 TCC 6 ul In 0 17 105 1 5021 1816 TCC 6 ul Out
96. ith solvents observe appropriate safety procedures for example goggles safety gloves and protective clothing as described in the material handling and safety data sheet supplied by the solvent vendor especially when toxic or hazardous solvents are used 1200 Series TCC Service Manual 87 8 Maintenance CAUTION Electronic boards and components are sensitive to electrostatic discharge ESD ESD can damage electronic boards and components gt In order to prevent damage always use ESD protection when handling electronic boards and components CAUTION Hot heat E S The column compartment has two heat exchanger assemblies that might be hot gt Allow them to cool down before starting repairs 88 1200 Series TCC Service Manual Maintenance 8 Overview of Maintenance The following pages describe maintenance procedures simple repairs that can be done without opening the main cover Table6 Simple Repairs Procedure Typical Frequency Notes Changing Column When column performance or new Identification Tags on page 91 application requires a change Replacing Head Parts of If the valve performance shows Column Switching Valve indication of leakage or wear G1316A G1316B SL on page 93 Correcting Leaks on page 99 Ifa leak has occurred Check for leaks 1200 Series TCC Service Manual 89 8 Maintenance Cleaning the Column Compartment The column compartment case should be kept clean
97. izing the Stack Configuration 35 Installing the Column Compartment 38 Installing Valve Heads G1316C SL Plus 42 Flow Connections of the Column Compartment 44 Installation of Heater and Cooling Devices 47 Placing Columns 49 4 How to optimize the Column Compartment 51 Optimizing the Performance of your Column Compartment 52 Using Additional Heater and Cooling Devices 53 1200 Series TCC Service Manual Contents Troubleshooting and Diagnostics 55 Overview of the Column Department s Indicators and Test Functions 56 Status Indicators 57 Available Tests depending on User Interfaces 59 Agilent Lab Advisor Software 60 Error Information 61 What Are Error Messages 62 General Error Messages 63 TCC Error Messages 67 Test Functions 75 Thermostat Function Test 76 Pressure Test 79 Column Thermostat Temperature Calibration 80 Maintenance 85 Introduction to Maintenance and Repair 86 Warnings and Cautions 87 Overview of Maintenance 89 Cleaning the Column Compartment 90 Changing Column Identification Tags 91 Replacing Head Parts of Column Switching Valve G1316A G1316B SL 93 Adding Heater and Cooling Devices G1316B SL G1316C SL Plus 96 Correcting Leaks 99 Replacing the Column Compartment s Firmware 100 Replacing Valve Heads G1316C SL Plus 101 Preparing the G1316C SL Plus for Transportation 104 1200 Series TCC Service Manual Contents 9 Repair 107 Cautions and Warnings 108 Removing the Top Cover and Foam 110
98. k the error log of your user interface for the originating module For safety reasons an error condition always interrupts the analysis 1200 Series TCC Service Manual Troubleshooting and Diagnostics Available Tests depending on User Interfaces Depending on the used interface the available tests and the screens reports may vary Preferred tool should be the Agilent Lab Advisor Software see Agilent Lab Advisor Software on page 22 Screenshots used in this document are based on the Agilent ChemStation In future the user interface may not show the Diagnostics Tests anymore In this case use the Agilent Lab Monitor Diagnostic LMD Software The Agilent ChemStation may not include any maintenance test functions Table5 Test Functions available vs User Interface TCC Test Agilent ChemStation Instant Pilot G4208A LMD Software Thermostat Function Test Yes No Yes Temperature Calibration Yes Yes Yes l section Maintenance 5 1200 Series TCC Service Manual 59 5 Troubleshooting and Diagnostics Agilent Lab Advisor Software 60 The Agilent Lab Advisor Software is a standalone product that can be used with or without data system Agilent Lab Advisor helps to manage the lab for high quality chromatographic results and can monitor in real time a single Agilent LC or all the Agilent GCs and LCs configured on the lab intranet Agilent Lab Advisor provides diagnostic capabilities for all Agilent 1200 Series HPLC mo
99. l the fixation clip for the heat exchanger unit which has been installed Connect the 4 heat exchanger cables from the processor board which are 2 flexible board cables for the column tag reader and heat sensor and 2 power cables each pair red black located below these cables 150 1200 Series TCC Service Manual Repair Installing the Heat Exchanger Assemblies 5 Install the Z Panel by closing 3 screws 1200 Series TCC Service Manual 151 9 Repair Exchanging the Power Supply When Tools required Parts required Preparations 152 Repair of the power supply assembly always involves exchange of the complete assembly It has no serviceable parts inside If defective Screwdriver Pozidriv 1 PT3 Wrench 1 4 inch Wrench 5 mm and 7 mm Part number Description 1 0950 2528 Power supply Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 Remove the column switching valve if installed see Removing a Valve from the Thermostatted Column Compartment G1316A G1316B SL on page 1140r Removing the sliding unit G1316C SL Plus on page 117 Remove the processor board see Exchanging the Main Board G1316A G1316B SL on page 124 Remove the fan assemblies
100. lary Guide G1316 42303 Figure 37 Capillary Guide 1200 Series TCC Service Manual 197 10 Parts and Materials for Maintenance Leak Parts 198 1200 Series TCC Service Manual 1200 Series TCC Service Manual 6 eece 11 e Parts for Repairs 8 Overview of Main Assemblies 200 Sheet Metal Kit 203 Plastic Parts 205 Foam Parts 207 Power and Status Light Pipes 209 Leak Parts 210 Internal Valve Drive Parts G1316C SL Plus 212 This chapter provides information on parts for repair ee Agilent Technologies 199 iew of Main Assemblies 11 Parts for Repairs Overvi Overview of Main Assemblies Main Assemblies Figure 38 1200 Series TCC Service Manual 200 Table 34 Overview of Main Assemblies Parts for Repairs 11 Item Description Part Number 1 Column compartment main board CCM for G1316A G1316 66530 requires minimum firmware A 05 05 exchange part G1316 69530 1 Column compartment main board CCM for G1316B SL G1316 66540 requires minimum firmware A 06 02 exchange part G1316 69540 1 Column compartment main board CCM for G1316C SL Plus requires minimum G1316 61050 firmware A 06 10 Hexagonal nut for GPIB connector 0380 0643 Hexagonal nut for RS 232 connector 1251 7788 Cable CAN to Agilent 1200 Series modules 0 5 m 5181 1516 Cable CAN to Agilent 1200 Series modules 1 m 5181 1519 3 Power supply assembly additional power and status light parts see The Main 0950 2528 Power Supply Ass
101. ling devices can be found in Technical Notes or in the Agilent 1200 Series Rapid Resolution LC System manual part number G1312 90300 Agilent Technologies 1200 Series holes to attach carrier L shaped pre column heater U shaped post column cooler Volume 1 6 pl Volume 1 5 pl mounted on carrier mounted on carrier top for column 1 bottom for column 2 Figure 13 Installation points for heat exchanger cooling devices NOTE If the additional heat exchanger and cooling devices are used as shown in this figure the column identification system cannot be used If the column identification system is required fix the heater and cooling devices in the upper or lower locations or right left of the current location 1200 Series TCC Service Manual 47 3 48 Installing the Column Compartment Installation of Heater and Cooling Devices G1316C SL Plus For the G1316C SL Plus additional heat exchanger and cooling devices can be installed on the carrier part number G1316 89200 using 3 screws part number 0515 1052 included to part number for carrier as shown in figure below Build in heat exchanger Figure 14 Installing the low dispersion heat exchangers 1200 Series TCC Service Manual Installing the Column Compartment 3 Placing Columns Column ldentification Tag When correctly placed on the heat exchanger the distance between the column identification tag and antenna is 1 2 mm This is the optimum distance
102. ling the leak sensor G131 1 Insert the leak sensor to the hole below the valve liner rear view Leak sensor 2 Insert the leak sensor to the hole below the valve liner front view Leak sensor 3 Route the leak sensor cable below the overhang and through the channel in the bottom foam part Connect the leak sensor to the main board Leak sensor cable To be routed below bottom foam part here 1200 Series TCC Service Manual 173 9 Repair Replacing the Door Sensor G1316C SL Plus When If the door sensor is defective Tools required Screwdriver Pozidriv 1 PT3 Screwdriver flat blade Wrench 1 4 inch Hexagonal wrench 3 mm Parts required Part number Description 1 G1316 81603 Door Sensor Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench 1 Remove the Z Panel and upper leak panel by opening 3 screws 2 Remove the RF shield by carefully pulling down 1 the clips Door sensor 174 1200 Series TCC Service Manual Repair 9 Replacing the Door Sensor G1316C SL Plus 3 Pull the door sensor out of the leak panel ri NOTE For installing a new door sensor route the sensor cable through the leak panel as shown in figure above step 2 clip in the RF shield and fix the panel to the module frame 1200 Series TCC Service
103. llows to read and write column specific information to and from the column identification tag Antennas Column identification tag Column clip l y Figure 2 Column ldentification System Table 1 on page 14 shows the information that can be stored The information fields can be edited via the user interface 1200 Series TCC Service Manual 13 1 Introduction to the Column Compartment Table 1 Column ldentification Module Information Item Example Comment Product number Serial number Batch number Geometry mm Stationary phase Particle size Number of injections Maximum pressure allowed bar Maximum temperature recommended C Maximum pH recommended Column void volume ml 799160D 552 950522 Date of manufacturing 1675 100 x 2 1 ODS Hypersil 10 um 1267 See Note below 400 70 12 The number of injections will be updated each run to create a column lifecycle chistory The user interface allows to edit all information If a column switching valve see Column Switching Valve Optional for G1316A G1316B SL on page 15 is installed in the module the update of the number of injections depends on the position of the column switching valve For example if the left column is selected the right column is not updated and vice versa If no column switching valve is installed both sides are updated at the same time 14 1200 Series TCC Service Manual Introduction to the Column C
104. lor Pin Agilent Signal Name BCD Digit G1351 81600 1200 Green 1 BCD 5 20 Violet 2 BCD 7 80 4 Blue 3 BCD 6 40 m Yellow 4 BCD 4 10 SS Black 5 BCD 0 1 ay Orange 6 BCD 3 8 Red 7 BCD 2 4 Brown 8 BCD 1 2 Gray 9 Digital ground Gray Gray pink 10 BCD 11 800 Red blue 11 BCD 10 400 White green 12 BCD 9 200 Brown green 13 BCD 8 100 notconnected 14 notconnected 15 5V Low 224 1200 Series TCC Service Manual Agilent 1200 to 3396 Integrators Identifying Cables 12 Connector Pin Pin Agilent Signal Name BCD Digit 03396 60560 3392 3 1200 1 1 BCD5 20 2 2 BCD 7 80 8e gt 3 3 BCD 6 40 s B 4 4 BCD 4 10 5 5 BCDO 1 1e 6 6 BCD 3 8 7 7 BCD 2 4 8 8 BCD 1 2 9 9 Digital ground NC 15 5V Low 1200 Series TCC Service Manual 225 12 Identifying Cables Auxiliary Cable 226 Ee 1 One end of this cable provides a modular plug to be connected to the Agilent 1100 Series vacuum degasser The other end is for general purpose Agilent 1100 Series Degasser to general purposes Connector Color Pin Agilent Signal Name G1322 81600 1100 es White 1 Ground Brown 2 Pressure signal Green 3 Yellow 4 Grey 5 DC 5VIN Pink 6 Vent 1200 Series TCC Service Manual Identifying Cables 12 CAN LAN Cables Both ends of this cable provide a modular plug to be connected to Agilent 1200 Series module s CAN or LAN connectors CAN Cables Agilent 1200 module to module 0 5 m 5181 1516 Agilent 1200
105. ls LAN via other 1200 series module Extensive diagnostics error detection and display through control module and Agilent ChemStation leak detection safe leak handling leak output signal for shutdown of pumping system Low voltages in major maintenance areas i d 0 17 mm see Extended Specifications on G1316B SL G1316C SL Plus on page 30 no GPIB on G1316B SL G1316C SL Plus 1200 Series TCC Service Manual Site Requirements and Specifications 2 Table3 Performance Specifications Thermostatted Column Compartment Type Specification Comments GLP features Column identification module for GLP documentation of column type see Column ldentification System on page 13 Housing All materials recyclable All specifications are valid for distilled water at ambient temperature 25 C set point at 40 C and a flow range from 0 2 5 ml min 1200 Series TCC Service Manual 29 2 Site Requirements and Specifications Extended Specifications on G1316B SL G1316 C SL Plus Extended Specifications on G1316B SL G1316C SL Plus The 1200 series G1316B SL G1316C SL Plus thermostatted column compartment is usable from 10 C below ambient up to 80 C for flow ranges up to 5 ml min and up to 100 C for flow ranges up to 2 5 ml min Additional heating and cooling devices are available for the G1316B SL G1316C SL Plus to reduce the risk of additional dispersion at low flow rates see Figure 8 on page 30 These dev
106. lus with high heating and cooling speeds for maximum application flexibility and stability holds up to three 30 cm columns and optimized design gives minimum dead volumes and maximum efficiency two independently programmable heat exchangers contribute volumes of only 3 and 6 ul G1316B SL features additional heating and cooling devices for low flow rates which reduce the risk of additional dispersion G1316B SL and G1316C SL Plus can be supplemented by a kit to install a small heat exchanger with 1 6 ul delay volume to reduce the delay volume In additon a cooling device with 1 5 ul is available electronic column identification module as standard for GLP documentation of column type and major column parameters optional high quality Rheodyne column switching valves with ceramic stator face assemblies for prolonged lifetime For specifications see Performance Specifications on page 28 10 1200 Series TCC Service Manual Introduction to the Column Compartment 1 System Overview The Concept of Heating and Cooling The design of this thermostatted column compartment uses column heating and cooling devices with Peltier elements The solvent entering the column compartment is heated up or cooled down to a settable temperature with two low volume heat exchangers 3 ul on left side 6 ul on right side made of a short piece of capillary 0 17 mm i d leading through a heat exchanger The heat exchanger is designed such th
107. lysis system one line is dedicated to SHUT DOWN the system s critical parts in case any module detects a serious problem To detect whether all participating modules are switched on or properly powered one line is defined to summarize the POWER ON state of all connected modules Control of analysis is maintained by signal readiness READY for next analysis followed by START of run and optional STOP of run triggered on the respective lines In addition PREPARE and START REQUEST may be issued The signal level are defined as e standard TTL levels 0 V is logic true 5 V is false e fan out is 10 e input load is 2 2 kOhm against 5 V and e output are open collector type inputs outputs wired or technique Table 45 Remote Signal Distribution Pin Signal Description 1 DGND Digital ground 2 PREPARE L Request to prepare for analysis for example calibration detector lamp on Receiver is any module performing preanalysis activities 3 START L Request to start run timetable Receiver is any module performing run time controlled activities 4 SHUT DOWN L System has serious problem for example leak stops pump Receiver is any module capable to reduce safety risk 5 Not used 6 POWER ON H All modules connected to system are switched on Receiver is any module relying on operation of others 7 READY H System is ready for next analysis Receiver is any sequence controller 8 STOP L Request to reach system read
108. mperature sensor is required for the temperature calibration and temperature verification procedures The figures below refer to a specific type of temperature sensor Heraeus Quat340 quartz surface temperature measurement sensor Other sensors may require a different fixing 1200 Series TCC Service Manual 83 7 Test Functions Column Thermostat Temperature Calibration 1 Remove the front cover 2 Install the temperature sensor at the measurement position on the left heat exchanger 84 1200 Series TCC Service Manual 1200 Series TCC Service Manual 8 Maintenance Introduction to Maintenance and Repair 86 Warnings and Cautions 87 Overview of Maintenance 89 Cleaning the Column Compartment 90 Changing Column Identification Tags 91 Replacing Head Parts of Column Switching Valve G1316A G1316B SL 93 Adding Heater and Cooling Devices G1316B SL G1316C SL Plus 96 Correcting Leaks 99 Replacing the Column Compartment s Firmware 100 Replacing Valve Heads G1316C SL Plus 101 Preparing the G1316C SL Plus for Transportation 104 This chapter describes the maintenance of the TCC ee Agilent Technologies 85 Introduction to Maintenance and Repair 86 Simple Repairs The column compartment is designed for easy repair The most frequent repairs such as change of column and column switching valve head parts can be done from the front of the column compartment without removing the TCC from the HPLC stack
109. n completed Tools required Screwdriver Pozidriv 1 PT3 Preparations The column compartment is open and other procedures have been completed CAUTION Blocked valve Not bringing the valve head to the outer position will cause the valve to stay permanently in the inner position due to a blockage of the cables gt Move the valve head to the outer position 1 Ifa valve actuator unit is installed route the cables of the 2 Move the valve head to the outer position valve tag reader valve actuator encoder reader and valve actuator drive control through the large central hole of the top foam part 1200 Series TCC Service Manual 165 9 Repair Installing the Foam and the Top Cover 3 Route cables through the top foam part and connect them to the main board Valve actuator encoder reader Door sensor f Valve tag reader Valve actuator drive control 4 Make sure that the foam is installed correctly and is located in the safety light switch 5 Position of the foam in the safety light switch 166 6 Place the top plate on the foam and slide it towards the rear and fix the screws at the rear of the top plate Ensure correct fit with Z plane SES 1200 Series TCC Service Manual Repair 9 8 Reinstall the cover 9 Close the front panel Next Steps 10 Place the column compartment back into the stack 11 Reconnect the cables 12 Turn on the column compartment
110. n mode in the user interface 3 Wait for the temperature to stabilize at the calibration temperature 36 C 4 Measure the temperature of the heat exchanger If the measured temperature deviates by more than 0 5 C from the actual temperature enter the measured value in the measured temperature field for the left heat exchanger 6 Install the sensor at the measurement point on the right heat exchanger Repeat the calibration procedure for the right heat exchanger Limits After calibration the measured temperature and the calibration temperature should be within 0 5 C The maximum deviation which can be adjusted is 1 6 C If the measured value and the calibration value differ by more than 1 6 C this is an indication that a problem exists Column Thermostat Calibration Problems on page 83 1200 Series TCC Service Manual Test Functions 7 Column Thermostat Calibration Problems If the temperature cannot be calibrated check the following e Has the thermostat front cover been closed correctly Is the measuring device functioning correctly and is calibrated according to the manufacturers instructions Hardware Failures Probable hardware failures that can lead to a failed calibration procedure are e Defective or wrongly calibrated measuring device e Defective heater assembly e Defective ambient temperature sensor e Defective CCM board Installing the Temperature Sensor Installation of the te
111. n of the module Valve properties will not be updated if the valve head is replaced while the module is on Selection of valve port positions can fail if the instrument does not know the properties of the installed valve gt Always switch off the instrument when replacing the valve head 38 1200 Series TCC Service Manual Installing the Column Compartment 3 CAUTION The valve actuator contains sensitive optical parts which need to be protected from dust and other pollutions Pollution of these parts can impair the accurate selection of valve ports and therefore bias measurement results gt Always install a valve head for operation and storage For protecting the actuator a dummy valve head part of transportation lock kit part number G1316 67001 can be used instead of a functional valve Do not touch parts inside the actuator If the Thermostatted Column Compartment SL Plus G1316C SL Plus only includes the valve drive option it is shipped with a transportation lock which needs to be removed during installation 1 Remove the 5 screws which hold the lock in position G1316C SL Plus only 2 Remove the dummy valve head by unscrewing the cap nut and removing it from the valve drive G1316C SL Plus only 1200 Series TCC Service Manual 39 3 Installing the Column Compartment 3 Place the column compartment in the stack or on the bench in a horizontal position 4 Ensure the power switch at the front of
112. n of the column compartment 138 1200 Series TCC Service Manual Repair 9 Exchanging the Fan 2 Replace the fan assembly Ensure correct fan orientation A LOQ Y N Y EAT 4 Reconnect the fan assembly to the processor board and check that the cable of the left fan is correctly in the foam channel to assure correct closing of the foam parts 1 Disconnect the fan assembly from the processor board 3 The arrow on the fan should correspond with the direction of air flow which is from the front to the rear of the column compartment 5 Replace the foam part the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B 139 SL on page 162 1200 Series TCC Service Manual 9 Repair Removing the Heat Exchanger Assemblies Removing the Heat Exchanger Assemblies G1316A G1316B SL When If the heater is leaking blocked does not heat cool or if other assemblies have to be removed Tools required Screwdriver Pozidriv 1 PT3 Wrench 1 4 5 16 inch for capillary connections Parts required Part number Description 1 G1316 60007 Heat exchanger assembly left includes ambient temperature sensor 1 G1316 60006 Heat exchanger assembly right Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front c
113. nication protocol used in the column compartment supports only hardware handshake CTS RTR 240 1200 Series TCC Service Manual Hardware Information 13 Switches 1 in down and 2 in up position define that the RS 232C parameters will be changed Once the change has been completed the column instrument must be powered up again in order to store the values in the non volatile memory Table 49 Communication Settings for RS 232C Communication Mode 1 2 3 4 5 6 7 Select RS 232C 0 1 Baudrate Data Bits Parity Use the following tables for selecting the setting which you want to use for RS 232C communication The number 0 means that the switch is down and 1 means that the switch is up Table 50 Baudrate Settings Switches Baud Rate Switches Baud Rate 3 4 5 3 4 5 0 0 0 9600 1 0 0 9600 0 0 1 1200 1 0 1 14400 0 1 0 2400 1 1 0 19200 0 1 1 4800 1 1 1 38400 Table 51 Data Bit Settings Switch 6 Data Word Size 0 7 Bit Communication 1 8 Bit Communication Table 52 Parity Settings Switches Parity 7 8 0 0 No Parity 1200 Series TCC Service Manual 241 13 Hardware Information Table 52 Parity Settings 1 0 Odd Parity 1 1 Even Parity One start bit and one stop bit are always used not selectable Per default the module will turn into 19200 baud 8 data bit with no parity Forced Cold Start Settings CAUTION Switches 1 and 2 do not
114. nostics Overview of the Column Department s Indicators and Test Functions Status Indicators The instrument is provided with two status indicators which indicate the operational state prerun run and error states of the instrument The status indicators provide a quick visual check of the operation of the instrument Error Messages In the event of an electronic mechanical or hydraulic failure the instrument generates an error message in the user interface The following pages describe the meaning of the error messages For each message a short description of the failure a list of probable causes and a list of suggested actions to fix the problem are provided Thermostat Diagnostic Test The thermostat diagnostic test evaluates the heating and cooling efficiency of the two peltier elements Temperature Calibration and Verification The temperature calibration and verification procedure enables the instrument temperature to be measured against an external calibrated measuring device Normally temperature calibration is not required throughout the lifetime of the instrument However in order to comply with local regulatory requirements calibration and verification may be required The following sections describe these functions in detail 56 1200 Series TCC Service Manual Troubleshooting and Diagnostics 5 Status Indicators Two status indicators are located on the front of the module The lower left indicates the power
115. ompartment Use short connection capillaries and place them close to the heat exchanger This will reduce heat dissipation and external band broadening Use the left heat exchanger for small volume columns for example 2 3 mm i d columns at flow rates of less than 200 ul min For even lower band broadening the heat exchanger can be by passed and the column is placed well between the heat exchanger fins Keep the left and right heat exchanger temperature the same unless you do specific applications Assure that the front cover is always closed 1200 Series TCC Service Manual How to optimize the Column Compartment 4 Using Additional Heater and Cooling Devices The optimization installation interconnection and specific settings when using additional heating and cooling devices are described in the Agilent 1200 Series Rapid Resolution LC System manual G1312 90300 1200 Series TCC Service Manual 53 4 How to optimize the Column Compartment Using Additional Heater and Cooling Devices 54 1200 Series TCC Service Manual 1200 Series TCC Service Manual 5 Troubleshooting and Diagnostics Overview of the Column Department s Indicators and Test Functions 56 Status Indicators 57 Power Supply Indicator 57 Module Status Indicator 57 Available Tests depending on User Interfaces 59 Agilent Lab Advisor Software 60 Overview about the troubleshooting and diagnostic features a Agilent Technologies 55 5 Troubleshooting and Diag
116. ompartment Parts required Description Other modules Parts from accessory kit see Accessory Kits on page 188 Two wrenches 1 4 5 16 inch for capillary connections Preparations Install the column compartment WARNING Toxic and hazardous solvents The handling of solvents and reagents can hold health risks gt When working with solvents observe appropriate safety procedures for example goggles safety gloves and protective clothing as described in the material handling and safety data sheet supplied by the solvent vendor especially when toxic or hazardous solvents are used 1 Press release buttons and remove front cover to gain access to heater area 2 The column compartment is equipped with an column identification system that can read column tags Antennas 1200 Series TCC Service Manual Installing the Column Compartment Flow Connections of the Column Compartment 3 NOTE For more information on column identification see Column ldentification System on page 13 NOTE The internal volumes of the heat exchanger assemblies comprise a volume of 3 pl left and 6 pl right The internal capillary diameter is 0 17 mm 3 Place the column on the left heat exchanger assembly and connect the capillaries to the column From autosampler 5 A _y 4 Or place the column on the right heat exchanger assembly and connect the capillar
117. ompartment 1 Column Switching Valve Optional for G1316A G1316B SL Figure 3 Location of Column Switching Valve 1200 Series TCC Service Manual 15 1 16 Introduction to the Column Compartment Two Column Selection The valve can select either column 1 or column 2 The offline column is sealed by connecting head to tail Switching should be done when the flow is off and the pressure is zero Before switching the valve switch off the pump or set the flow to zero Keeping the flow on while the valve is switched can cause exceeding the maximum pressure This will stop method or sequence execution From autosampler Heater assembly 1 Heater assembly 2 To detector Figure 4 Column 1 Active From autosampler Heater assembly 1 Heater assembly 2 Figure 5 Column 2 Active 1200 Series TCC Service Manual Introduction to the Column Compartment 1 Precolumn Back flushing The sample is injected into series connected precolumn and analytical column After the valve has switched the analytical column flow continues in normal direction Only the precolumn is back flushed eluting highly retained peaks directly to the detector From autosampler Heater assembly 1 Heater assembly 2 Analytical Column To detector Figure 6 Precolumn Back flushing 1200 Series TCC Service Manual 17 1 Introduction to the Column Compartment Electrical Connections 18 The CAN bus is a serial bus with high speed data tr
118. on leak base Ensure that it keeps in this position during the next steps 159 9 Repair Replacing the Leak Se nsor or Leak 14 Reinstall the heat exchanger assemblies see Installing 15 Reconnect the leak sensor and heat exchanger cables to the Heat Exchanger Assemblies G1316A G1316B the processor board and place the cables in the foam SL on page 145 channel Next Steps 16 Reinstall the foam section the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B SL on page 162 17 Place the column compartment back into the stack 18 Reconnect the cables 19 Turn on the column compartment 160 1200 Series TCC Service Manual Replacing Status Light Pipe When When part is broken Tools required Screwdriver Pozidriv 1 PT3 Parts required Part number Description 1 5041 8384 Status light pipe Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Repair 9 Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 1 The status light pipe is clipped into the top cover Next Steps 2 Reinstall the foam section the top cover and front cover see Installing the Foam and the Top Cover G1316A G1316B SL on page 162 Place the column compartment ba
119. onfigured to Stay Resident Mode module boots in resident mode flashing status LED 1 Open a connection to the module or via system 2 Select Board Check and Change and press Start 3 In the type field enter G1315B and press Apply 4 After a power cycle the module should show up with the correct product number type in the user interface Load the correct main firmware into the module Turn the module OFF Set module s configuration switch back to normal mode Turn on the module oo N OO If required load final firmware into the module Recover with Agilent ChemStation 1 Use the ChemStation command line to change to TYPE product number as described under Using the Agilent ChemStation on page 130 After power cycle of module the correct TYPE shows up Recover with Instant Pilot USB Flash Drive with file CUSTINST CMD and a PC with USB interface The example uses G1315B as correct type and G1319B as incorrect type 1200 Series TCC Service Manual Repair 9 1 Edit create the file CUSTINST CMD and add the following line XXxxxX Command from USB Type Change TYPE YYYYYY where XXXXX is for example G1319 from the mis typed G1319B and YYYYYY is the correct module type e g G1315B Save and close the file Insert the USB Flash Drive into the Instant Pilot From the Welcome screen enter the Service Mode 7268312 or SERVICE Select the button G1319B wrong module and select XXxxX Command from USB Type Chang
120. ontact Cable 228 RS 232 Cables 229 13 Hardware Information 231 The Electronics 232 Firmware Description 233 Agilent 1200 Series Interfaces 235 Setting the 8 bit Configuration Switch 239 The Main Power Supply Assembly 244 14 Appendix 247 Safety Symbols 248 The Waste Electrical and Electronic Equipment Directive 251 Lithium Batteries Information 252 Radio Interference 253 Sound Emission 254 Solvent Information 255 Agilent Technologies on Internet 257 8 1200 Series TCC Service Manual 1200 Series TCC Service Manual 1 Introduction to the Column Compartment Main Features 10 System Overview 11 Column ldentification System 13 Column Switching Valve Optional for G1316A G1316B SL 15 Electrical Connections 18 Serial Number Information 20 Instrument Layout 21 Agilent Lab Advisor Software 22 This chapter gives an introduction to the TCC instrument overview and internal connectors ee Agilent Technologies 1 Introduction to the Column Compartment Main Features The Agilent 1200 Series thermostatted column compartments are stackable temperature controlled column compartments for LC They are available as standalone modules or as a component of a Agilent 1200 Series system They are used for heating and cooling to meet extreme requirements of retention time reproducibility The main features are Peltier heating and cooling from 10 degrees below ambient up to 80 C G1316A or 100 C G1316B SL G1316C SL P
121. or more of the modules in the system has failed The system processors continually monitor the system configuration If one or more of the modules is no longer recognized as being connected to the system the error message is generated Probable cause Suggested actions 1 CAN cable disconnected Ensure all the CAN cables are connected correctly Ensure all CAN cables are installed correctly 2 Defective CAN cable Exchange the CAN cable 3 Defective main board in a different module Switch off the system Restart the system and determine which module or modules are not recognized by the system Leak A leak was detected in the column compartment module The signals from the two temperature sensors leak sensor and board mounted temperature compensation sensor are used by the leak algorithm to determine whether a leak is present When a leak occurs the leak sensor is cooled by the solvent This changes the resistance of the leak sensor which is sensed by the leak sensor circuit on the TCC board Probable cause Suggested actions 1 Condensation Use a higher temperature setpoint 2 Loose column fittings Ensure all fittings are tight 3 Broken capillary Exchange defective capillaries 4 Leaking column switching valve seal Exchange the valve seal 1200 Series TCC Service Manual 65 66 Error Information Leak Sensor Open The leak sensor in the module has failed open circuit The current through the leak sensor is depen
122. otect risk of harm to the operator and to protect the apparatus against damage Indicates dangerous voltages Indicates a protected ground terminal Indicates eye damage may result from directly viewing the light produced by the deuterium lamp used in this product The apparatus is marked with this symbol when hot surfaces are available and the user should not touch it when heated up A WARNING alerts you to situations that could cause physical injury or death gt Do not proceed beyond a warning until you have fully understood and met the indicated conditions CAUTION i 5e A CAUTION alerts you to situations that could cause loss of data or damage of equipment gt Do not proceed beyond a caution until you have fully understood and met the indicated conditions 248 1200 Series TCC Service Manual Appendix 14 General Safety Information The following general safety precautions must be observed during all phases of operation service and repair of this instrument Failure to comply with these precautions or with specific warnings elsewhere in this manual violates safety standards of design manufacture and intended use of the instrument Agilent Technologies assumes no liability for the customer s failure to comply with these requirements WARNING Ensure the proper usage of the equipment The protection provided by the equipment may be impaired gt The operator of this instrument is advis
123. ous solvents in the flow cell can built up algae Therefore do not leave aqueous solvents sitting in the flow cell Add a small of organic solvents e g acetonitrile or methanol 5 Use of Solvents Observe the following recommendations on the use of solvents e Brown glass ware can avoid growth of algae e Small particles can permanently block capillaries and valves Therefore always filter solvents through 0 4 um filters e Avoid the use of the following steel corrosive solvents Solutions of alkali halides and their respective acids for example lithium iodide potassium chloride and so on High concentrations of inorganic acids like sulfuric acid and nitric acid especially at higher temperatures if your chromatography method allows replace by phosphoric acid or phosphate buffer which are less corrosive against stainless steel Halogenated solvents or mixtures which form radicals and or acids for example 2CHCly O gt 2COCl 2HC1 This reaction in which stainless steel probably acts as a catalyst occurs quickly with dried chloroform if the drying process removes the stabilizing alcohol 1200 Series TCC Service Manual 255 14 Appendix Chromatographic grade ethers which can contain peroxides for example THF dioxane di isopropylether such ethers should be filtered through dry aluminium oxide which adsorbs the peroxides Solvents containing strong complexing agents e g EDTA Mixtures of carbon t
124. over top cover and top foam section see Removing the Top Cover and Foam on page 110 1 Disconnect the heat exchanger cables from the processor board and the grounding connection of the column switching valve 2 Carefully pull out the heater cables out of the foam channels 140 1200 Series TCC Service Manual Repair Removing the Heat Exchanger Assemblies 4 Press against the rear of the Z panel to release the metal plate from the guide and pull it carefully upwards 6 Locate the ambient temperature sensor in the top plastic 3 Unscrew the Z panel 5 Lift the Z panel together with the top plastic panel half way out of the guide f ee INK gt U 141 1200 Series TCC Service Manual 9 Repair Removing the Heat Exchanger Assemblies 7 Carefully remove the ambient temperature sensor 8 Carefully pull out the top plastic panel together with the plugged into the rear of the top plastic panel Z panel completely Vv V4 9 Remove the heat exchanger assembly 10 The repair level of the heat exchanger assemblies is the complete assembly 142 1200 Series TCC Service Manual Repair 9 i emoving the Heat Excnanger Assembies Removing the Heat Exchanger Assemblies G1316C SL Plus When If the heater is leaking blocked does not heat cool or if other assemblies have to be removed Tools required Screwdriver Pozidriv 1 PT3 Wrench 1 4
125. partment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench Remove the front cover top cover and top foam section see Removing the Top Cover and Foam on page 110 1 Disconnect the grounding connection of the valve atthe 2 Unscrew the Z panel Z panel a 114 1200 Series TCC Service Manual Repair 9 Removing a Valve 3 Press against the rear of the Z panel to release the metal plate from the guide and pull it carefully upwards EN 4 Lift the Z panel together with the top plastic panel several centimeters out of the guide then 5 locate the ambient temperature sensor in the top plastic part and push it towards the rear 6 Carefully remove the ambient temperature sensor plugged into the rear of the top plastic panel 1200 Series TCC Service Manual 115 Repair Removing a Valve 8 Remove the Valve from its location 7 Pull the top plastic panel together with the Z panel completely out of the guide IA A NOTE For the installation refer to Installing a Valve G1316A G1316B SL on page 119 1200 Series TCC Service Manual 116 Repair 9 Removing the sliding unit G1316C SL Plus When If valve actuator or sliding unit need to be replaced Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries
126. ponents gt In order to prevent damage always use ESD protection when handling electronic boards and components CAUTION Hot heat ene The column compartment has two heat exchanger assemblies that might be hot gt Allow them to cool down before starting repairs 1200 Series TCC Service Manual 109 9 Repair Removing the Top Cover and Foam When For all repairs inside the column compartment Tools required Screwdriver Pozidriv 1 PT3 Parts required Part number Description G1316 68714 Front cover G1316A G1316 68724 Front cover G1316B SL G1316 68713 G1316 68723 G1316 68702 1 1 1 G1316 68754 1 1 1 1 61316 68712 Front Cover G1316C SL Plus Plastic kit G1316A G1316B SL Plastik Cover Kit G1316C SL Plus Foam parts G1316A G1316B SL Foam parts G1316C SL Plus Preparations Turn OFF the column compartment Disconnect the power cable Disconnect capillaries Remove column compartment from stack and place it on the working bench 1 Press the release buttons and remove the front cover 2 Pull the leak funnel out of the leak funnel holder 110 1200 Series TCC Service Manual Repair 9 Removing the Top Cover and Foam 3 Move the power lock across the power inlet and lift the 4 Lift the cover up and slide it towards the rear clips on the rear of the cover 5 Unscrew the screws at the rear of the top plate slide the 6 If installed disconnect the connector of the column
127. r 01046 60210 3396A Series integrator 03394 60600 3396 Series Il 3395A integrator see details in section Remote Cables on page 219 3396 Series III 3395B integrator 03396 61010 HP 1050 modules HP 1046A FLD 5061 3378 HP 1046A FLD 5061 3378 Agilent 35900A A D converter 5061 3378 HP 1040 diode array detector 01046 60202 HP 1090 liquid chromatographs 01046 60202 Signal distribution module 01046 60202 BCD cables 3396 integrator 03396 60560 General purpose spade Lugs G1351 81600 Auxiliary Agilent 1100 Series vacuum degasser G1322 61600 214 1200 Series TCC Service Manual Identifying Cables 12 Type Description Part Number CAN cables Agilent 1100 1200 module to module 0 5m Ig 5181 1516 Agilent 1100 1200 module to module 1m Ig 5181 1519 External Agilent 1100 1200 Series interface board to general G1103 61611 contacts purpose GPIB cable Agilent 1100 1200 module to ChemStation 1 m 10833A Agilent 1100 1200 module to ChemStation 2 m 10833B RS 232 cable Agilent 1100 1200 module to a computer 34398A This kit contains a 9 pin female to 9 pin female Null Modem printer cable and one adapter LAN cable Twisted pair cross over LAN cable shielded 3m long for 5023 0203 point to point connection Twisted pair cross over LAN cable shielded 7m long for 5023 0202 point to point connection 1200 Series TCC Service Manual 215 12 Identifying Cables Analog Cables 216 One end of these cables provides
128. r and the low pressure valve head is connected to the detector gt For details please refer to the Method Development Solution User and Installation Guide part number G4230 90000 CAUTION Column Damage or Bias Measurement Results Switching the valve to a wrong position can damage the column or bias measurement results gt Fitting the lobe to the groove is essential for making sure the valve is switched to the correct position CAUTION Valve properties are read from the valve head RFID tag during initialization of the module Valve properties will not be updated if the valve head is replaced while the module is on Selection of valve port positions can fail if the instrument does not know the properties of the installed valve gt Always switch off the instrument when replacing the valve head 1200 Series TCC Service Manual 101 Maintenance CAUTION The valve actuator contains sensitive optical parts which need to be protected from dust and other pollutions Pollution of these parts can impair the accurate selection of valve ports and therefore bias measurement results gt Always install a valve head for operation and storage For protecting the actuator a dummy valve head part of transportation lock kit part number G1316 67001 can be used instead of a functional valve Do not touch parts inside the actuator 1 2 Switch off the module 3 Unscrew the valve head Push the valve head for br
129. re 34 Connection Diagram for Column Regeneration Accessories G1316C SL Plus Table 30 Accessories G1316C SL Plus Description Part Number Transportation Lock Kit G1316C SL Plus includes following items G1316 67001 Lock Plate Screw M4 Screw M3x8 pack of 4 Spring Washer Transportation Valve Head 194 1200 Series TCC Service Manual Parts and Materials for Maintenance 10 Plastic Parts Table 31 Plastic Parts Item Description Part Number 2 Front cover G1316A 1200 Series G1316 68714 2 Front cover G1316B SL 1200 Series G1316 68724 2 Front cover G1316C SL Plus 1200 Series G1316 68754 3 Name plate Agilent 1200 Series 5042 8901 Figure 35 Plastic Parts 1200 Series TCC Service Manual 195 10 Parts and Materials for Maintenance Leak Parts Table 32 Leak Parts G1316A G1316B SL Item Description Part Number 1 Leak funnel 5041 8388 2 Leak funnel holder G1316 42300 3 Waste assembly includes complete Y tubing assembly with leak G1316 60002 funnel Corrugated waste tube reorder pack 5m 5062 2463 Figure 36 Leak Parts 196 1200 Series TCC Service Manual Parts and Materials for Maintenance 10 Table 33 Leak Parts G1316C SL Plus Item Desription Part Number Leak Panel Kit includes following items G1316 68722 Leak Panel Top Leak Panel Base Leak Tube Kit includes following items G1316 67000 Funnel Holder G1316C SL Plus Tubing flex polyethylene Leak Funnel 1 Capil
130. s 32 1200 Series TCC Service Manual 1200 Series TCC Service Manual 3 Installing the Column Compartment Unpacking the Column Compartment 34 Delivery Checklist 34 Optimizing the Stack Configuration 35 Installing the Column Compartment 38 Installing Valve Heads G1316C SL Plus 42 Flow Connections of the Column Compartment 44 Installation of Heater and Cooling Devices 47 Placing Columns 49 Column Identification Tag 49 Column Clip 50 This chapter describes the installation of the Thermostatted Column Compartment ee Agilent Technologies 33 3 Installing the Column Compartment Unpacking the Column Compartment CAUTION If the delivery packaging shows signs of external damage please call your Agilent Technologies sales and service office immediately Inform your service representative that the module may have been damaged during shipment Defective on arrival problems If there are signs of damage please do not attempt to install the module Inspection by Agilent is required to evaluate if the instrument is in good condition or damaged gt Notify your Agilent sales and service office about the damage gt An Agilent service representative will inspect the instrument at your site and initiate appropriate actions Delivery Checklist 34 Ensure all parts and materials have been delivered with the module The delivery checklist is shown below Please report missing or damaged parts to your local Agilent Tec
131. s on the instrument to be connected to Agilent 1100 1200 to 3390 Integrators Connector Pin Pin Agilent Signal Name Active 01046 60203 3390 1100 1200 TTL 2 1 White Digital ground NC 2 Brown Prepare run Low 7 3 Gray Start Low a NC 4 Blue Shut down Low j NC 5 Pink Not connected NC 6 Yellow Power on High NC 7 Red Ready High NC 8 Green Stop Low NC 9 Black Start request Low 1200 Series TCC Service Manual 219 12 Identifying Cables Agilent 1100 1200 to 3392 3 Integrators Connector Pin Pin Agilent Signal Name Active 01046 60206 3392 3 1100 1200 TTL 3 1 White Digital ground NC 2 Brown Prepare run Low 11 3 Gray Start Low NC 4 Blue Shut down Low NC 5 Pink Not connected NC 6 Yellow Power on High 9 7 Red Ready High 1 8 Green Stop Low NC 9 Black Start request Low Agilent 1100 1200 to 3394 Integrators Connector Pin Pin Agilent Signal Name Active 01046 60210 3394 1100 1200 TTL 9 1 White Digital ground NC 2 Brown Prepare run Low 3 3 Gray Start Low NC 4 Blue Shut down Low NC 5 Pink Not connected NC 6 Yellow Power on High an 5 14 7 Red Ready High 6 8 Green Stop Low 1 9 Black Start request Low 13 15 Not connected 220 1200 Series TCC Service Manual Identifying Cables 12 START and STOP are connected via diodes to pin 3 of the 3394 connector Agilent 1100 1200 to 3396A In
132. s will display the box labeled Serial Letters and numbers are created using the up and down arrows Into the box labeled Serial enter the 10 character serial number for the module When the 10 character serial number is entered press Enter to highlight the complete serial number Then press Done F6 1200 Series TCC Service Manual Repair 9 6 Turn the module OFF then ON again The Records screen should display the correct serial number for this module 7 Ifa Agilent ChemStation is also connected restart the Agilent ChemStation now as well To change the product number go to the System screen 8 Press Tests F3 and select the module and press Enter 9 While in the Tests screen press m m m dot m 10 From the box now displayed select the Command and press Enter 11 Into the box labeled Nester instruction enter the command TYPE XXXXXX where XXXXXX is embedded in single quotes Letters and numbers are created using the up and down arrows XXXXX is the 5 character product number of the module being changed There must be a space between the word TYPE and the product number Some Agilent 1100 1200 series modules require the correct main board version to match the type for example the SL modules 12 Now press the Execute key Below the box a reply line should then say Reply RA 0000 TYPE XXXXX XXXXX is what you just entered 13 Power cycle the module Turn on should be normal In the Records screen the product
133. see Exchanging the Fan on page 138 Remove the heat exchanger assemblies see Removing the Heat Exchanger Assemblies G1316A G1316B SL on page 140 The leak tubing assembly might fall out of its position 1200 Series TCC Service Manual Repair 9 Exchanging the Power Supply 1 Remove the leak sensor cable out of the foam channel Carefully remove the bottom foam 2 Unscrew the power supply at the rear of the column compartment 2c gt 006 Se ee ee a lo BRS SSS 3 Press down the power switch light pipe to remove it from the coupler Power switch light pipe LM MMMM MMMM MMM MMM LVS VIVID IS IVIL ILS IL IS PUUR 4 Remove the power supply completely Re use the coupler on the new power supply ly ern JON Coupler YYYYYY YY YY yy YUH MUU HHT 1200 Series TCC Service Manual 153 9 Repair Exchanging the Power Supply NOTE The power supply can be replaced entirely if damaged Do not disassemble the power supply it does not contain serviceable parts 5 Insert the power supply into its location and fix it with the screw at the rear panel S852 S255 ocoT ess SS SS SS Co FIC _jo 0 6 Press down and clip in the power switch light pipe into the power supply Power switch light pipe Litt ULL LMM MM MMM LDII IAIA VV AVIV I 154 1200 Series TCC Service Manual Repair
134. ssor board and pull the cable out of the foam channel 2 Remove the column switching valve if installed see Removing a Valve from the Thermostatted Column Compartment G1316A G1316B SL on page 114 or Removing the sliding unit G1316C SL Plus on page 117 Remove the heat exchanger assemblies see Removing the Heat Exchanger Assemblies G1316A G1316B SL on page 140 5 Remove the clips shown from the inside of the column compartment on both sides using a flat screwdriver 1200 Series TCC Service Manual 157 9 Repair ieplacin 6 Remove the leak base from the cabinet by unlocking it 7 Remove the leak sensor assembly from the rear of the with a flat blade on the right and left side of the leak base leak base 8 Replace the leak sensor assembly into the leak base 9 Route the leak sensor cable through the z panel into the left foam channel 158 1200 Series TCC Service Manual Repair 9 Replacing the Leak Sensor or Leak Base G1316A G1316B SL 10 Replace the leak base into the cabinet until it clicks into the cabinet Insert the right side first 11 Position the leak sensor so that it does not touch the bottom of the leak base 12 Replace the clips shown from the inside of the column compartment on both sides using a flat screwdriver 1200 Series TCC Service Manual 13 Place the leak tubing assembly back into its location
135. start the serial number type you have just entered can be seen under the Instrument menu of the main user interface screen 1200 Series TCC Service Manual 131 9 132 Repair Using the Instant Pilot G4208A Connect the Instant Pilot to the module Turn ON the module On the Instant Pilot s Welcome screen press More then select Maintenance Using the up down arrows select the module where you have to change the product number or serial number Press PN SN This will display a screen where you can enter the product number and or serial number Make your changes using the information from the product label of your module Some Agilent 1100 1200 series modules require the correct main board version to match the type for example the SL modules 5 Press OK to highlight the complete command 6 Press Done to transfer the information into the main board s memory Press Cancel to quit the process 7 Power cycle the module The Maintenance screen should display the correct serial number for this module 8 If an other User Interface is also connected restart the User Interface as well Using the Control Module G1323B Connect the control module to the module Turn ON the module On the control module press System F5 then Records F4 Using the up down arrows make sure that the module is highlighted Press FW Update F5 then m This will display a box which says Update Enter Serial 4 Press Enter Thi
136. tack and reconnect the cables If a new CCM board is installed update the serial number information of the column compartment in the user interface Introduction on page 129 1200 Series TCC Service Manual 127 9 Repair 10 Check the firmware revision of the module If the firmware revision is older than the current firmware revision of the module update the firmware using the standard firmware update procedure see Replacing the Column Compartment s Firmware on page 100 128 1200 Series TCC Service Manual Repair 9 Changing the Type and Serial Number Introduction When the main board has to be replaced the new board does not have a serial number For some modules e g pumps or auto samplers the type has to be changed multiple usage boards Use the information from the serial number plate of your module Keep in mind that e the changes become active after a power cycle of the module e the information from the serial number plate of the module is used e the exact type product number is used If the type product number was entered incorrectly the module may become unusable Proceed to Overview on page 134 With firmware A 06 02 B 01 02 and above a wrong type cannot be entered The entry is checked against the board revision Using the Agilent Diagnostic Software The Agilent Diagnostic Software must be configured in Service Mode to have access to the function Board Check and Change Close ot
137. tegrators Connector Pin Pin Agilent Signal Name Active 03394 60600 3394 1100 1200 TTL 9 1 White Digital ground QO NC 2 Brown Prepare run Low 80 15 z e 3 3 Gray Start Low o NC 4 Blue Shut down Low o e o ee NC 5 Pink Not connected 1e NC 6 Yellow Power on High O 5 14 7 Red Ready High 1 8 Green Stop Low NC 9 Black Start request Low 13 15 Not connected Agilent 1100 1200 to 3396 Series II 3395A Integrators Use the cable part number 03394 60600 and cut pin 5 on the integrator side Otherwise the integrator prints START not ready 1200 Series TCC Service Manual 221 12 Identifying Cables Agilent 1100 1200 to 3396 Series III 3395B Integrators Connector Pin Pin Agilent Signal Name Active 03396 61010 33XX 1100 1200 TTL 9 1 White Digital ground QO NC 2 Brown Prepare run Low 80 15 e 3 3 Gray Start Low m o NC 4 Blue Shut down Low o e g a NC 5 Pink Not connected 1e NC 6 Yellow Power on High O 14 7 Red Ready High 4 8 Green Stop Low NC 9 Black Start request Low 13 15 Not connected Agilent 1100 1200 to HP 1050 HP 1046A or Agilent 35900 A D Converters Connector Pin HP Pin Agilent Signal Name Active 5061 3378 1050 1100 1200 TTL 1 White 1 White Digital ground 2 Brown 2 Brown Prepare run Low 3 Gray 3 Gray Start Low Zz 4 Blue 4 Blue Shut down Lo
138. the column compartment is OFF Status indicator green yellow red Line power switch with green light Figure 11 Front View of the Thermostatted Column Compartment 5 Connect the power cable to the power connector at the rear of the column compartment 40 1200 Series TCC Service Manual Installing the Column Compartment 3 Ineta am tho Caliamn Co nartmant Installing the Column Compartment 6 Connect the CAN cable to other Agilent 1200 Series modules 7 If Agilent ChemStation is the controller connect either gt the LAN connection to the LAN interface board in the module or e the GPIB cable to the module Ifa Agilent DAD MWD FLD is in the system the LAN GPIB should be connected to the DAD MWD ELD due to higher data load 8 Connect the APG Remote cable optional for non Agilent 1200 Series instruments 9 Turn ON power by pushing the button at the lower left side of the column compartment The status LED should be green Security lever Configuration switch APG Remote CAN Power RS 232C Figure 12 Rear View of the Thermostatted Column Compartment No The column compartment is turned on when the line power switch is pressed and the green ARAT indicator lamp is illuminated The column compartment is turned off when the line power switch is protruding and the green light is OFF 1200 Series TCC Service Manual 41 3 Installing the Column Compartment Installing Valve Heads
139. the meaning of error messages and provides information on probable causes and suggested actions how to recover from error conditions 7 Test Functions This chapter describes the TCC s built in test functions 1200 Series TCC Service Manual In This Guide 8 Maintenance This chapter describes the maintenance of the TCC 9 Repair This chapter gives instructions on how to repair the TCC 10 Parts and Materials for Maintenance This chapter provides information on parts for maintenance 11 Parts for Repairs This chapter provides information on parts for repair 12 Identifying Cables This chapter summarizes information on all cables 13 Hardware Information This chapter describes the detector in more detail on hardware and electronics 14 Appendix This chapter provides addition information on safety legal and web 4 1200 Series TCC Service Manual Contents Contents 1 Introduction to the Column Compartment 9 Main Features 10 System Overview 11 Column ldentification System 13 Column Switching Valve Optional for G1316A G1316B SL 15 Electrical Connections 18 Instrument Layout 21 Agilent Lab Advisor Software 22 2 Site Requirements and Specifications 23 Site Requirements and Specifications 24 Physical Specifications 27 Performance Specifications 28 Extended Specifications on G1316B SL G1316C SL Plus 30 3 Installing the Column Compartment 33 Unpacking the Column Compartment 34 Optim
140. ugust 2005 This product complies with the WEEE Directive 2002 96 EC marking requirements The affixed label indicates that you must not discard this electrical electronic product in domestic household waste Product Category With reference to the equipment types in the WEEE Directive Annex I this product is classed as a Monitoring and Control Instrumentation product Do not dispose off in domestic household waste To return unwanted products contact your local Agilent office or see mma agilent com for more information 1200 Series TCC Service Manual 251 14 Appendix Lithium Batteries Information Lithium batteries may not be disposed off into the domestic waste Transportation of discharged Lithium batteries through carriers regulated by IATA ICAO ADR RID IMDG is not allowed Danger of explosion if battery is incorrectly replaced gt Discharged Lithium batteries shall be disposed off locally according to national waste disposal regulations for batteries gt Replace only with the same or equivalent type recommended by the equipment manufacturer Lithiumbatteri Eksplosionsfare ved fejlagtig h ndtering Udskiftning ma kun ske med batteri af samme fabrikat og type gt Lever det brugte batteri tilbage til leverand ren Lithiumbatteri Eksplosionsfare Ved udskiftning benyttes kun batteri som anbefalt av apparatfabrikanten gt Brukt batteri returneres appararleverandoren 252 B
141. up or cooling profile of the heater is incorrect When the temperature setpoint is changed the heater begins heating or cooling the column heat exchanger During this time the processor monitors the temperature change and checks if the temperature profile is changing in the correct direction If the temperature is not changing as expected the error message is generated 1200 Series TCC Service Manual Error Information 6 Probable cause Suggested actions 1 Defective heater assembly Exchange the heater assembly 2 Defective TCC board Exchange the TCC board Valve Failed Valve Failed 0 failed to switch to the position where ports 1 and 2 are connected Valve Failed 1 failed to switch to the position where ports 1 and 6 are connected The column switching valve failed to switch The switching of the column switching valve is monitored by two micro switches on the valve assembly The switches detect the successful completion of the valve movement within a predefined time window If the valve fails to reach the end point or fails to reach the end point within the time window the error message is generated Probable cause Suggested actions 1 Defective column switching valve Exchange the column switching valve 2 Defective TCC board Exchange the TCC board 1200 Series TCC Service Manual 71 6 72 Error Information Column Temperature The temperature of the column heat exchanger has exceeded the maximum limit
142. ve from the Thermostatted Column Compartment G1316A G1316B SL on page 114 CAUTION The flexible cables close to the heat exchanger assemblies may be easily damaged gt Be careful that the flexible cables close to the heat exchanger assemblies are not damaged especially during steps 3 through 6 The ambient temperature sensor may be damaged if incorrectly installed CAUTION gt Ensure that the ambient temperature sensor is completely plugged into the rear of the top plastic panel 1200 Series TCC Service Manual 119 Repair a Valve 4 Carefully plug the ambient temperature sensor into the rear of the top plastic panel Vv 1200 Series TCC Service Manual Installing 1 If no column valve is installed remove the RFl shield and 2 Replace the valve into its location the plastic cover no longer used 3 Carefully insert the top plastic panel together with the Z panel into the guide and press it half way down 120 Repair Installing a Valve 6 Press down completely until it clicks into its holding position A W ZS f J f j Ve 8 Reconnect the grounding connection of the valve at the Z panel completely down 5 Press the Z panel together with the Top Plastic Panel M vie Dr WIG TL iD THI wil 7 Fix the Z panel with the two screws 121 1200 Series TCC Service Manual 9 Repair Next Steps
143. ve head G1316 40002 in the central positions of the plate position of the plate 1200 Series TCC Service Manual 105 8 Maintenance Preparing the G1316C SL Plus for Transportation 106 1200 Series TCC Service Manual 1200 Series TCC Service Manual 9 Repair Cautions and Warnings 108 Removing the Top Cover and Foam 110 Removinga Valve 114 Installing a Valve 119 Exchanging the Main Board 124 Changing the Type and Serial Number 129 Recover Instructions 134 Exchanging the Fan 138 Removing the Heat Exchanger Assemblies 140 Installing the Heat Exchanger Assemblies 145 Exchanging the Power Supply 152 Replacing the Leak Sensor or Leak Base G1316A G1316B SL 156 Replacing Status Light Pipe 161 Installing the Foam and the Top Cover 162 Assembling the Main Cover 168 Installing the Radio Frequency Shield G1316C SL Plus 170 Installing the leak sensor G1316C SL Plus 172 Replacing the Door Sensor G1316C SL Plus 174 This chapter gives instructions on how to repair the TCC ott Agilent Technologies 107 9 Repair Cautions and Warnings Sharp metal edges Sharp edged parts of the equipment may cause injuries gt To prevent personal injury be careful when getting in contact with sharp metal areas When opening capillary or tube fittings solvents may leak out The handling of toxic and hazardous solvents and reagents can hold health risks gt Please observe appropriate safety procedures for e
144. w 5 Pink 5 Pink Not connected 6 Yellow 6 Yellow Power on High 7 Red 7 Red Ready High 8 Green 8 Green Stop Low 9 Black 9 Black Start request Low 222 1200 Series TCC Service Manual Agilent 1100 1200 to HP 1090 LC or Signal Distribution Module Identifying Cables 12 Connector Pin HP Pin Agilent Signal Name Active 01046 60202 1090 1100 1200 TTL 1 1 White Digital ground NC 2 Brown Prepare run Low 8 7 4 3 Gray Start Low 6 E a 7 4 Blue Shut down Low 8 5 Pink Not connected 1 NC 6 Yellow Power on High 3 7 Red Ready High 6 8 Green Stop Low NC 9 Black Start request Low Agilent 1100 1200 to General Purpose Connector Pin Pin Agilent Signal Name Active 01046 60201 Universal 1100 1200 TTL 1 White Digital ground A Q 1 2 B oo Brown Prepare run Low oo es 29 key 3 Gray Start Low oo o0 a 4 Blue Shut down Low z 5 Pink Not connected oo rm 6 Yellow Power on High S O Re 7 Red Ready High 8 Green Stop Low 9 Black Start request Low 1200 Series TCC Service Manual 223 12 Identifying Cables BCD Cables One end of these cables provides a 15 pin BCD connector to be connected to the Agilent 1200 Series modules The other end depends on the instrument to be connected to Agilent 1200 to General Purpose Connector Wire Co
145. with a remote connection to the system 4 The degasser failed to generate sufficient vacuum for solvent degassing Remote Timeout Suggested actions Fix the leak in the external instrument before restarting the module Fix the leak in the external instrument before restarting the module Check external instruments for a shut down condition Check the vacuum degasser for an error condition Refer to the Service Manual for the Agilent 1200 Series vacuum degasser A not ready condition is still present on the remote input When an analysis is started the system expects all not ready conditions e g a not ready condition during detector balance to switch to run conditions within one minute of starting the analysis If a not ready condition is still present on the remote line after one minute the error message is generated Probable cause 1 Not ready condition in one of the instruments connected to the remote line 2 Defective remote cable 3 Defective components in the instrument showing the not ready condition Suggested actions Ensure the instrument showing the not ready condition is installed correctly and is set up correctly for analysis Exchange the remote cable Check the instrument for defects refer to the instrument s reference documentation 1200 Series TCC Service Manual Error Information 6 Synchronization Lost During an analysis the internal synchronization or communication between one
146. xample goggles safety gloves and protective clothing as described in the material handling and safety data sheet supplied by the solvent vendor especially when toxic or hazardous solvents are used Module is partially energized when switched off as long as the power cord is plugged in Risk of stroke and other personal injury Repair work at the module can lead to personal injuries e g shock hazard when the module cover is opened and the instrument is connected to power gt Never perform any adjustment maintenance or repair of the module with the top cover removed and with the power cord plugged in gt The security lever at the power input socket prevents that the module cover is taken off when line power is still connected Never plug the power line back in when cover is removed 108 1200 Series TCC Service Manual Repair 9 The electronics of the column compartment will not allow operation of the module when the top cover and the top foam are removed A safety light switch on the main board will inhibit the operation of the fans immediately Voltages for the other electronic components will be turned off after 30 seconds The status lamp will light red and an error will be logged into the logbook of the user interface Always operate the column compartment with the top covers in place CAUTION Electronic boards and components are sensitive to electrostatic discharge ESD ESD can damage electronic boards and com
147. y state as soon as possible for example stop run abort or finish and stop injection Receiver is any module performing run time controlled activities 9 START REQUEST L Request to start injection cycle for example by start key on any module Receiver is the autosampler 1200 Series TCC Service Manual 237 13 Hardware Information RS 232C The RS 232C connector is used to control the column module from a computer through RS 232C connection using the appropriate software This connector can be configured with the configuration switch module next to the GPIB connector The RS 232C is designed as DCE data communication equipment with a 9 pin male SUB D type connector The pins are defined as Table 46 RS 232C Connection Table Pin Direction Function 1 In DCD 2 In RxD 3 Out TxD 4 Out DTR 5 Ground 6 In DSR 7 Out RTS 8 In CTS 9 In RI Instrument 1 1 2 2 3 3 4 4 5 5 6 6 7 7 8 8 9 9 DB9 DB9 Female Female 238 1200 Series TCC Service Manual Hardware Information 13 Setting the 8 bit Configuration Switch The 8 bit configuration switch is located next to the GPIB connector Switch settings provide configuration parameters for GPIB address serial communication protocol and instrument specific initialization procedures Factory setting is shown for column compartment Table 47 8 bit Configuration Switch Mode Select 1 2 3 4 5 6 7 8 GPIB 0 0 GPIB Address RS 232C 0 1 Baudrate D

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