アミノ分析キット EZ:FAAST (P.517-521)
Contents
1. 20 100mL 0 6 1 5mL GC Zebron AAA GC 10mx0 25mm GC MS CD TM EZ faast Phenomenex sa A 6 NN 1 kr Saag SW EC 45 Zebron GC Rak 04484 KTC es 0 6mL SPE 1 2 1 8 F NE kkkksik _2. EZ FAAST Phenomenex EZ faast GCMS QP2010 000 EZ faast 7 7 0 R C 1 mp eS cat Rc 2HCI CO OR NH 9 Y GC GC MS 1 GC M5
3. 1 40 45 5 33 n GCMSsolution AART dt Nn ct 1 0_ TE on i dae aa emer oo i as NGevelpe EZssatdsrhetwei UL EH E lo sn auc a fa jer 5 5 IL ni ER PTaagt de ata Noee zesat erhatvei 1 1 15 45 50 en F 33 Cl3C33 GLC Shimadzu GLC Ltd EZ FAAST Phenomenex GC 05 1 Amino Acid Analysis AAA Kit 4
4. EZ FAAST Phenomenex 7 0 0 EZ faast EZ faast GC MS LC MS GC FID GC MS LC MS 0000000 90 0000000W0 0000000 0
5. E faast 2 LOD nmolmL S N 3 1 1 7 Chemical Name Abbreviation FID Alanine ALA 1 0 1 B Alanine B ALA Alliin a c Aminoadipic acid AAA 1 0 2 1 2 1 4 Aminobenzoic acid PABA SPE a Aminobutyric acid ABA 1 0 2 NN ES SE 4 TH a y Amino n butyric acid GABA e Aminopimelic acid APA 0 47 0 4 acid A 5 ua Aspartame Aspartic acid ASP 0 87 0 1 Bicin Carboxymethyl cysteine Chloro phenylalanine C PHE Cystathionine CTH 4 10 3 2 4 93 Cysteine CYS gt Cystine C C 4 10 2 4 Diamino n butyric acid DABA SPE Diaminopimelic DAPA 3 4 Dihydroxyphenylalanine DOPA Dopamine_ DA c 1 Ethionine ETH C
6. P N CGO 7169 EZ faast GC GC MS ZB AAA 10m 0 25mm I D 00G 4402 BO EZ faast LC MS EZ faast 4u AAA MS 250 x 2 0 mm 00G 4402 YO EZ faast LC MS EZ faast 4u AAA MS 250 x 3 0 mm AGO 7184 GC SD1 2 3 2mL Vial X AGO 7269 GC SD1 2 3 2mL Vial X ALO 7500 LC MS SD1 2 3 mL Vial ALO 7501 LC MS SD1 2 3 mL Vial WEB GC MS https solutions shimadzu co jp glc
7. 9 ns _ A BE 1 5mL SPE G EZ faast 0 SPE 384 EZ faast P N KGO 7165 GC FID 79 500 KGO 7166 GC MS 985 700 KGO 7167 GC FID 95 700 KGO 7168 GC MS 311 900 KHO 7337 LC MS 250X 0mm 308 700 KHO 7338 LC MS 250X3 0mm 308 700 KHO 7339 LC MS 250X 0mm 324 900 KHO 7340 LC MS 250X3 0mm 324 900
8. Or galanine a gt 0 2 gt UtaITIC CI 3 Glutamine GLN 8 10 o Glycine GLY 2 0 1 Glycine glycine dipeptide GLY GLY Glycine proline dipeptide GPR 1 5 Histamine HA J 5 4 6 Histidine HIS 1 0 2 Be MS Ee Homocystine HC CH Homophenylalanine HPHE Homoserine HSER a 2 1 1 4 Hydroxyproline 4HYP 2 0 2 lsoleucine ILE 0 65 0 2 allo lsoleucine alLE 0 65 0 1 Leucine LEU 0 65 0 1 Lysine LYS 1 0 2 Lysine alanine dipeptide LYS ALA Methionine MET 0 87 0 2 Methionine Sulfone Methionine Sulfoxide 0 7 GC FID 3 Methyl cysteine Naphthyl alanine GC FID 3 Nitrotyrosine Norleucine NLE NPD G C MS GC MS Norvaline NORV LC MS Ornithine ORN 1 0 2 nenyialaning HE 0 47 0 2 eny ycine hd LC IMS Pipecolic Acid HPRO Proline PRO 1 0 1 Proline hydroxyproline dipeptide PHP 0 87 10 Sarcosine SAR 1 0
9. 1 Seleno Cystine Se C C Seleno Methionine Se MET Serine SER 2 0 2 Serotonin SRO Theanine THE Thioproline TPR 0 43 0 1 Threonine THR 2 0 2 Threonine aspartic acid dipeptide THR ASP Tryptophan TRP 0 43 0 1 Tyramine Tyrosine TYR 0 4 0 2 Valine VAL 0 6 0 2 or or OO o 1 0000000W 0000000W 0000000 H 60 https solutions shimadzu co jp glc 05 GC EZ FAAST Phenomenex EZ faast 88 IS S00nmol ml EZ faast GC FID EV a10 000 5 H Instrument himadzn C 3010 Column FEB AAA 0 35mm x 10m Cen temp BOC 207C min 320 C Tatal Time 12min Injector Split 1 0 He SOcmvs Const velociry 2380 Detector FID 320 Sampnlelnjectaoinsize 2 0pL Preparetion size TOOpL EZ faast GC FID Instrument Shimadzu GC 2010 Column ZB AAA 0 25mm x 10m Oven temp 80 C 20 C min 320 C Total Time 12min j Spl
10. it 120 He SOcm s Const velociry at 280 C Detector FID at 320 C SampleInjectoin size 2 0uL Preparetion size 100uL EZ faast 3 TIS G00nmol ml EZ faast GC MS dt NN TIC x1 Q00 Q001 a RE nwn THAN TO me 95 mm li gt EZaast 3 ln Temp 0 TC EE TT ST 3 8 ha Pha 1 1 1 8 gy 5 i 8 amp lnrerfaceTemp 0 se lon Source Temp 200 1 1ViLIi OR 93 I 3 GLC Shimadzu GLC Ltd EZ FAAST Phenomenex GC 005 EE GCCopilgryColumm TIC Medgl CM SP 75 x1 Q00 0001 Warkstation GCMSsnlution Ver2 5 Cnlumm BAA TO mS mm LD wn EzZiaast ln Termp 5 0 Column Temp 110 I Oman 30 min 320 Ominy Cartief Gas He Fnwr control Mode Pressune Es InjecHiam Miethod 5P pt ah HE M5 InerfaCeTenmh 0 uk MW mk LU LU eeei Ian Saurce Temp 300 i j 10 15 20 25 30 35 40 45 50 55 60 6 5 i PKU 8 LZHI II Phe 1768 6 nmol ml caum ZB MMA 10mx0 25mmlD Rag
11. t GC Injectign volume 1ul Injection Temp i250 Cokumn Termp 110C Ermin 30C min MC Camier Gas He Split 1 M5 lnterface Temp 280C jam Souree Temp 00 TIC A0002 0 RE pee Scanrange imgi45 450 Phe 90 4 nmogl ml 1 50 i 5 I C lt ML Mi UL WAM _ wy 9 HP 10 0 x1 000 0001 1 CMSP2O1 4 5 Workststign GCMSsalutian Ver3 5 BAAA TO mS mwm Hi 4 0 East 1 GC 1 Tam 0 Ln CnlumnTamp 110 Inmmn 0 rmin 0 TT 320 mnl Carrier Gas He 1 5 Flow Control Mode Pressune amp Pressure 15 kPa lnpection Method p split Fatio 15 1 0 gE i 250 1 i Ion Saumre Temp 200 EW H Scan Range mgi45 450 mm LM Scanlniewl 15sec https solutions shimadzu co jp glc 05 GC
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