InertSustain C18
Contents
1. MPa InertSustain C18 InertSustain C18 A BB 1 1 AUML Time mn 0 50 100 150 200 250 300 h 0 2 4 6 8 10 Time min Conditions Column InertSustain C18 5um 250x 4 6 mm ID Eluent CHsCN 25 mM KHLPO pH 7 0 KsHPO4 40 60 v v Flow Rate 1 0 mL mn Col Temp 40 C Detection UV 220 nm Sample 1 Dextromethorphan Conditions Column size 5 um 250 x 4 6 mm ID lt E CHs0H Hz0 A B C D E F G HowRee 10mL7mn ODS ODS ODS ODS ODS ODS ODS Col Temp 40 C InertSustain C18 1009 pH mm 2 1 3 0 4 mm Cat No Ca2. FAX 03 5323 6622 FAX 06 6357 4580 FAX 045 985 7901 FAX 024 536 1518 FAX 029 858 3780 FAX 043 248 2485 FAX 048 667 1656 FAX 052 931 1814 FAX 082 233 1110 FAX 092 291 2552 FAX 04 2934 2128 FAX 04 2934 3361 FAX 024 534 2139 TM 1693 1130 6 22 1 30F TEL 03 5323 661 1 http www gls co jD E mailiinfo gls co jp FAX 03 5323 6622 20110111AB10T
3. 5 mm 2 1 3 0 4 0 4 6 20 MPa System LC800 HPLC system 5020 07411 5020 07421 5020 07431 5020 07441 44 000 0 TRAP 9 00e5 Colum 1 C18 3 um 150 x 2 1 mmID 5020 07412 5020 07422 5020 07432 5020 07442 44 000 Eluent A 0 1 HCOOH In CHiCN 8 00e5 B 0 1 HCOOH in Hz0 5020 07413 5020 07423 5020 07433 5020 07443 50 000 700s5 owle 504m7Wn 2 5020 07414 5020 07424 5020 07434 5020 07444 50 000 _ 600e5 RN 5020 07415 5020 07425 5020 07435 5020 07445 55 000 SS Injection Vol 2 uL 2 500 Sample Q1703 01 03 5020 07416 5020 07426 5020 07436 5020 07446 65 000 a 4 00e5 1 Sulpilide i 2 Mil Maprotiline 3 0e5 Te20dhe 372 176 11 Ee 278 233 mm 2 1 3 0 4 6 4 Amoxapine 314 271 12 Trimmipramine 295 100 2 0085 5 Doxepn 0 Dl 1 4 HP mm Cat No Cat No Cat No Sertralin 100e5 7 Flvoxamne 319771 15 Compemne 615 86 a 30 5020 14411 5020 14421 5020 14441 55 000 0 00 8 Imipramine 281 86 each 100 ng mL Ne 50 5020 14412 5020 14422 5020 14442 55 000 Time min 75 5020 14413 5020 14423 5020 14443 60 000 14 MM 100 5020 14414 5020 14424 5020 14444 60 000 7 1 Sy gt eb 7 i a 150 5020 14415 5020 14425 5020 14445 65 000
4. le 4 pH InertSustain C18 2nd Stage pH1 10 InertSustain C18 ES pH 0DS 3rd Stage
5. pH InertSustain C18 0DS InertSustain C18 Column size 5 um 150 x 4 6 mm 1D Eluent 50 mM Triethylamine pH10 0 CHs0H 70 30 v v Flow Rate 1 0 ml min Col Temp 50 C Eluent CHsCN Hz0 65 35 v v Flow Rate 1 0 mL min Col Temp 40 C Detection UV 254 nm Sample Naphthalene InertSustain C18 2 7 1 3 4 56 0 10 Time mn 20 30 Column InertSustain C18 5 um 250 x 4 6 mm ID Eluent CHsOH Hz0 80 20 v v Sample Flow Rate 0 3 mL mn 1 Uracil 2 Caffeine 3 Phenol Col Temp 40 C 4 Butylbenzene 5 0 Terphenyl Detection UV 254 nm 6 Amylbenzene 7 Iriphenylene InertSustain C18 ES
6. 0DS InertSustain C18 0DS InertSustain C18 I 2 TnertSustain C18 Conditions 5 7 T Col Size 3 0x2 1D kHzPO lo 7 0 KaHPO4 30 70 v v 2 1 fwRte 02mL7mN oo Detection
7. a ET rs rs 5 7 mm 1 0 1 5 3 13 4 8 mm Cat No Cat No 15 30 5020 14201 5020 14211 46 000 1 6 UC 50 5020 14202 5020 14212 46 000 a 75 5020 14203 5020 14213 55 000 100 5020 14204 5020 14214 55 000 5 um 150 5020 14205 5020 14215 58 000 0 2 4 6 8 10 0 M 0 0 250 5020 14206 5020 14216 66 000 Time min imelmin Conditions Conditions NR mm 2 1 3 0 4 0 4 6 Syst 6L 7400 HPLC Syst Syst LC800 HPLC syst 9 i InertSustain C18 5 um 150 x 4 6 mm ID nm InertSustain C18 5 um 250 x 4 6 mm I D mm Cat No Cat No Cat No Cat No Eluent A CHsCN Eluent A Hz0 HCOOH 90 10 a ven a ven A 77 30 5020 07311 5020 07321 5020 07331 5020 07341 40 000 A B 40 60 v v A B 93 7 35 min 75 25 10 mm 35 65 1 min 0 100 4 min 0 100 v v 50 5020 07312 5020 07322 5020 07332 5020 07342 40 000 Flow Hate 2 mL min Flow Rate 1 0 mL min Col Temp 40 C Col Temp 30 C 75 5020 07313 5020 07323 5020 07333 5020 07343 45 000 Detection UV 254 nm Detection VS535 nm Iiection VoL 20 ul Ilection Vol 10 ul 100 5020 07314 5020 07324 5020 07334 5020 07344 45 000 Sample Sample Bilberry powder 1 25 mg mL 1 Glycyrrhizic acid dipotassium salt 250 mg L 1 Delphinidin 3 0 galactoside 9 Peonidin 3 0 galactoside 150 5020 07315 5020 07325 5020 07335 5020 07345 50 000 2 Propyl p hydroxybenzoate
8. 5020 14255 5020 14265 5020 14275 E 2 3 Um 5 um 5020 19300 5020 19299 34 000 5020 19400 5020 19399 34 000 5020 19200 5020 19199 30 000 5020 19100 5020 19099 30 000 5020 19600 5020 19599 39 000 5020 19500 5020 19499 39 000 Cat No 62 000 5020 07356 77 000 75 000 5020 07366 88 000 132 000 5020 14256 154 000 190 000 5020 14266 220 000 260 000 5020 14276 300 000 HPLC 5 um mm X mm 6 0 Xx 50 7 6 X 50 10X50 14X50 20X50 Cat N0 5020 07357 5020 07367 5020 14257 5020 14267 5020 14277 33 000 44 000 66 000 83 000 100 000 G AT a 2 TEL 03 5323 661 1 TEL 06 6357 5060 TEL 045 985 7900 TEL 024 533 2244 TEL 029 858 3700 TEL 043 248 2441 TEL 048 667 1611 TEL 052 931 1761 TEL 082 233 TEL 092 291 1101 5200 TEL 04 2934 2121 TEL 04 2934 1100 TEL 024 533 2244
9. 50 mg L 2 Delphinidin 3 0 glucoside 10 Petunidin 3 0 arabinoside 3 Cyamidin 3 0 galactoside 11 Peonidin 3 0 glucoside 250 5020 07316 5020 07326 5020 07336 5020 07346 60 000 4 Delphinidin 3 0 arabinoside 12 Malvidin 3 0 galactoside 5 Cyanidin 3 0 gl id 13 Peonidin 3 0 arabinosid gt gt 6 Petunidin 3 0 9alctoside 14 Malvidin 3 0 glucoside 7 Cyanidin 3 0 grabinoside 15 Malvidin 3 0 arabinoside 8 Petunidin 3 0 glucoside mm mm 1 0 1 0 9 2 1 5 10 2 1 3 0 3 0 4 0 4 6 4 0 2 1 3 0 3 0 20 4 0 4 6 4 0 30 MPa HPLC 5 um mm mm 6 7 6 10 14 20 Cat No 5020 07352 5020 07362 5020 14252 5020 14262 5020 14272 E 2 3 Um 5 um 5020 19250 5020 19249 5020 19350 5020 19349 5020 19150 5020 19149 5020 19050 5020 19049 5020 19550 5020 19549 5020 19450 5020 19449 Cat No 50 000 5020 07354 60 000 5020 07364 85 000 5020 14254 100 000 5020 14264 130 000 5020 14274 62 000 65 000 110 000 160 000 230 000 Cat No 5020 07355 5020 07365
10. HPLC InertSustain C18 hl riPnrs EO InertSustain C18 Inertsil TnertSustain 2um 3um 5 um 350m2g 14 100A 0 nm USP L1 0 85 mL g pH 1 10 In er 1t Sustain ly InertSustain C18 Inert RE SBE Cust ES D 5 i 0DS f 1st Stage 2 ES a
11. UV 230 nm 1 Uracil 4 Berberine chloride 2 Pyridine 5 Dextromethorphan 4 3 Pheno InertSustanC18 ES 5 a 3 a em Column A Column B 4 5 8 Time min Time min Time min Time min lt InertSustain C18 COON Column Size 3 um 150 x 2 1 mm D FCF Eluent CHsCN 0 1 HsPOz 25 75 v v Sample Col Temp 4 Phenol Flow Rate 1 R EN 0 a Blue FCF 5 Detection i i nm Salicylic acid InertSustain C18 Time mm 5 FCF 2 Column A Column B Column C Column D 10 10 10 10 Time min Time min Time min Time min ES HPLC
12. t No 0 0 2 um 30 5020 14351 5020 14361 62 000 2 a 50 5020 14352 5020 14362 62 000 I 4065 80 MPa 75 5020 14353 5020 14363 68 000 3 085 3065 100 5020 14354 5020 14364 68 000 2 0e5 2 0e5 150 5020 14355 5020 14365 78 000 1 0e5 2 1 0e5 mm 1 0 1 5 10 20 30 40 10 20 30 40 mm 1 0 1 RO H 2 5 2 0 1 A i H20 pH 9 5 SS NN NM AAM UM 30 5020 14301 5020 14311 51 000 Conditions Sample Conditions System GL 7400 HPLC system i Ce mg System 0 system 50 9020 14302 9020 14312 51 000 Col InertSustain C18 5 um 250 x 4 6 D lartaric 8CI mg 4000 0 TRAP i 10 MM NAAHPO 0HZB PO a ON a i i Column InertSustain C18 3 um 75 x 2 1 mm 75 5020 14303 5020 14313 60 000 Flow R 1 0 mL mi VIaIOTIC 8CI mg Eluent 1 CH3CN 0 1 HCOOH in Hz0 pH 2 5 10 90 ol Temp 40 MO i i 2 CHsCN 0 1 WI 28 in Hz0O pH95l 30 70 v v 100 5020 14304 59020 14314 60 000 D UV 210 Acetic 8CI mg Flow Rat 0 3 mL mi OO 10 a 7 Fumalic acid 10mg U Cu Tein 40 C Sample 3 um 150 5020 14305 9020 14315 65 000 8 Succinic acid 1000 mg L Detection LC MS M6S ESI Positive MAM 1 Ranitidine 100 ng mL 01 315 2 03 315 0 250 5020 14306 5020 14316 75 000 9 Acrylic acld 100 mg L Injection Vol 5 ul 2 Sulpide 100 ng mL 01 342 2 03 112 2 4
13. wa 3rdIStade 1St Stage Es oe EE EE 4 1 a a 2 dd a 0 A NE 7 2 9 mm ON I gt 6 o FS J o 1st Stage Evolutionally Surfaced Silica ES 0DS ES ES
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