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Agilent J&W - アジレント・テクノロジー株式会社

Contents

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6. www agil
7. GC
8. GC 1 4 1 2
9. www agilent com chem jp 141 2 142
10. GC 8 16 10 15 cm
11. www agilent com chem jp
12. 10b DB 1 15 m x 0 25 mm 0 25 nm 30 cm sec 60 C 1 20 C min 60 180 C Time min www agilent com chem jp GC 50 C
13. pH 0 5 1
14. GC C DB 1ms 100 60 340 360 PCB HP 1ms 100 60 325 350 PCB
15. www agilent com chem jp Agilent Ultimate www agilent com chem jp 24 1 25 30 2 10 15
16. www agilent com chem jp GC
17. 0 5 m GC 5182 9765
18. 0120 477 111 www agllentcom chem jp FA0 Ti MI e web Agilent e
19. 7
20. GC GC MS ECD TCD
21. 9 2 k 2 k k 5 5 10 10 k
22. GC 0 18 0 32 mm 0 45 0 53 mm
23. 1 2 30 C 10 C 1 DB 1 15 m x 0 25 mm 0 25 nm 30 cm sec Ca a Cs 60 C 1 20 C min 60 180 C Cs C 1 n Cig 174 2 n Cij 196 3 n
24. 13a 5 C min 13b oo cw hm 6 8 10 Time min 0 2 4 6 8 10 12 14 Time min www agilent com chem jp GC
25. GC
26. HCI HS0 HN0J HPO Cr0 KOH Na0H NH OH
27. OH NH SH 1
28. 1 3 14 50
29. PLOT PLOT 0 25 0 53 mm GC MS PLOT HP PLOT Molesieve 5A 35 C HP PLOT AL0 KCI KCI
30. 8 1 DB _WAX DB WAXet mm mL DB FFAP HP Innowax 0 18 0 2 3 4 025 45 8
31. Agilent BT0 Agilent 5975C GC MSD Ar www adilent com chem jp DB 1ms 100 DB 1 So GC MS CH 100 100 S N AS 340 360 C
32. 5 www agilent com chem jp 1 1 0 18 0 32 mm 0 18 0 25 um 0 45 0 53 mm 0 8 1 5 um
33. 1 1 GC 40 50 C 8 2 GC 3 4 5 2 5 2
34. 10 www agilent com chem jp GC
35. 2 2
36. www agilent com chem jp 2 GC 5 15 m x 0 25 mm 0 25 nm Ci C5 50 Phenyl DB 17 mn cm DB 17 DB 17 50 DB 1
37. ON 10 FID NPD ECD ITCD www agilent com chem jp 139 140 1 20 C 2
38. MSD 280 C 45 180 m z 100 ppm Accustandard M REF M REF X a 1 0 3 13B1 2 4 115 6 5 125 7 6 1 1 1 143a 5 7 12 i 8 22 8 9 1 1 1 2 134a 10 40 11 1 1 2 2 134 8 19 12 12B1 6 13 1 1 152a 18 24 14 1 2 1 1 2 2 114 14 15 2 1 1 1 2 124 16 1 1 1 142b 6 17 21 5 18 11 19 160 20 20 1 6 21 1 1 1 141b 22 2 2 1 1 1 123
39. 10a 10a DB 1 15 m x 0 25 mm 0 25 nm 30 cm sec 100 C Cu Cs En 0 10 20 30 40 50 Time min www agilent com chem jp 155 156 10b GC
40. www agilent com chem jp 9 DB 1 30 m x 0 32 mm 38 cm sec 100 C 0 25 um Time min 1 24 59 2 3 1 00 um 0 5 10 15 20 25 Time min 1
41. www agilentcom chem jp GC SAA GC 1 10 20 GC 400 450 C
42. N e g N m
43. J amp W GC 0C GC MS
44. EN14105 ASTM D6584 EN14105 ASTM D6584 B100 400 C 160 BD65 5 5m x 0 53 mm www agilent com chem jp EN14103 FAME EN14103 B100 EN14110 EN14110 B100 GC
45. Rtx 65TG BPX50 CP TAP CB DB 17ht mm m um C 0 25 15 0 15 40 340 365 122 1811 0 25 30 0 15 40 340 365 122 1831 0 32 15 0 15 40 340 365 123 1811 0 32 30 0 15 40 340 365 123 1831 0 32 60 0 15 40 340 365 123 1861 www agilent com chem jp 119 120 DB EUPAH PAH EU 16 PAH Agilent J amp W DB EUPAH GC EU PAH EU PAH QC bjk
46. www agilent com chem jp 89 Agilent 8 90 DB 1 mm m um C 0 05 10 0 05 60 325 350 126 1012 0 05 10 0 20 60 325 350 126 1013 0 10 5 0 12 60 325 350 127 100A 0 10 10 0 10 60 325 350 127 1012 0 10 10 0 40 60 325 350 127 1013 0 10 20 0 10 60 325 350 127 1022 0 10 20 0 40 60 325 350 127 1023 0 10 40 0 20 60 325 350 127 1046 0 10 40 0 40 60 325 350 127 1043 0 15 10 1 20 60 325 350 12A 1015 0 18 10 0 18 60 325 350 121 1012 0 18 10 0 18 60 325 350 121 1012E 0 18 10 0 20 60 325 350 121 101A 0 18 10 0 40 60 325 350 121 1013 0 18 10 0 40 60 325 350 121 1013E 0 18 20 0 18 60 325 350 121 1022 0 18 20 0 18 60 325 350 121 1022E 0 18 20 0 40 60 325 350 121 1023 0 18 40 0 40 60 325 350 121 1043 0 18 40 0 40 60 325 350 121 1043E 0 20 12 0 33 60 325 350 128 1012 0 20 25 0 33 60 325
47. QC www agilent com chem jp GC GC mm m hm C DB 1 0 18 10 0 18 60 325 350 121 1012 DB 1 0 18 10 0 20 60 325 350 121 101A DB 1 0 18 10 0 40 60 325 350 121 1013 DB 1 0 18 20 0 18 60 325 350 121 1022 DB 1 0 18 20 0 40 60 325 350 121 1023 DB 1 0 18 40 0 40 60 325 350 121 1043 HP 1 0 18 20 0 18 60 325 350 19091Z 577 DB 1ms 0 18 20 0 18 60 340 360 121 0122 HP 1ms 0 18 20 0 18 60 325 350 19091S 677 DB 5 0 18 10 0 18 60 325 350 121 5012 DB 5 0 18 10 0 40 60 325 350 121 5013 DB 5 0 18 20 0 18 60 325 350 121 5022 D
48. PLOT DB 2887 100 ASTM D2887 lt HP 1 Petrocol EX2887 MXT2887 MXT 1 Rtx 2887 DB 2887 mm m um C 0 53 10 3 00 60 350 125 2814 DB HT SimDis 100 430 C C6 C100 430 C Petrocol EX2887 CP SimDist Ultimetal MXT 2887 Rtx 2887 AC Controls High Temp Sim Dist AT 2887 DB HT SimDis mm m um C 0 53 5 0 15 60 400 43
49. 0 53 mm amp 0 53 mm di 3 N 2 1 41 1 2 1 3 8 3 Rs 0 84 R 1 16 R 1 68 2 29 min 4 82 min 8 73 min 1 1 2 9
50. 2 2 www agilent com chem jp GC 2 0 1 10 0 um 0 05 0 53 mm
51. 4 mm 0 10 12500 0 18 6 600 0 20 5 940 0 25 4 750 0 32 3 710 0 45 2 640 0 53 2 240 k 5 20 5 N m 4 2 1 41 2 1 2 1 3 7 2
52. 3 5 20 mL min 150 www agilent com chem jp
53. k 0 tp t a AM 0 2a 2b 100 n CH 1200 1478 n C n C n C GC www agilent com chem jp log VR x log VR I 100y 100 z y 8 RE 08 RQ log tr x log w
54. 1 2 www agilent com chem jp 145 430 3000 GC GC IN He
55. 1 6
56. 1 2 24 MS TCD ECD 0 5 1
57. 2 2 2 1 2 1 1 2 3 1 2 2 5 1 1 RN OT Son OND OT mh NO Na NI PSLNo DE 1 ppm GS GasPro 113 4332 30 m x 0 32 mm OI Analytical 1 COS 60 C 255 2 H5S 10 C min 60 250 C 3 Propyl 0IAnalical CS 198 5 1 5 Methyl mercaptan 200 pL 6 Ehylmercaptan 0OIAnalytical Model 538
58. 20 30 C 2 5 15a b 15a DB 1 15 m x 0 25 mm 0 25 nm 30 cm sec 10 C min 40 70 C 70 C 3 10 C min 70 120 C 1 3 2 2 3 4 1 3 5 1 4 6 12 7 8 9 8
59. 99 995 99 995 H 0 1 ppm 0 0 5 ppm 1 0 5 m i 15 cm 6 4 5 cm www agilent com chem jp
60. Stx 1ht DB 1ht mm m hm C 0 25 15 0 10 60 400 122 1111 0 25 30 0 10 60 400 122 1131 0 32 15 0 10 60 400 123 1111 0 32 30 0 10 60 400 123 1131 118 DB 5ht 5 400 C HT5 Stx 5ht VF 5ht DB 5ht mm m um C 0 25 15 0 10 60 400 122 5711 0 25 30 0 10 60 400 122 5731 0 32 15 0 10 60 400 123 5711 032 30 0 10 60 400 123 5731 www agilent com chem jp DB 17ht 50 365 C
61. 103 1 4 d4 IS 104 1 4 101 102 105 100 103 104 106 1 2 98 99N 195 107 80 82 108 1 2 3 96 97 109 77 78 110 111 1 2 4 90 91 112 96 87 113 94 98 114 1 2 3 95 79 84 85 92 8 3 189 UU 6 0 _ 7 0 8 0 me min GCEV003 www agilent com chem jp 53 EPA T0 15 1 npbV DB 5ms Entech Instruments 123 5563 60 m x 0 32 mm 1 00 nm 1 1 5 mL min 1 30 41 35 C 50 4 50 6 C min 35 140 C 0 o H o 4 150 C mn 140 220 C 7 220 C 3 0 8 1 3 39
62. USP Phase G16 HP 20M SUPELCOWAX 10 CP WAX 52 CB SUPEROXIL CB WAX Stabilwax BP 20 007 CW Carbowax DB WAXetr ZB WAX HP INNOWax mm m mm C 0 18 20 0 18 40 260 270 19091N 577 0 20 25 0 20 40 260 270 19091N 102 0 20 25 0 40 40 260 270 19091N 202 0 20 50 0 20 40 260 270 19091N 105 0 20 50 0 40 40 260 270 19091N 205 0 25 4 0 25 40 260 270 19091N 130 0 25 5 0 15 40 260 270 19091N 030 0 25 15 0 25 40 260 270 19091N 131 0 25 15 0 50 40 260 270 19091N 231 0 25 30 0 15 40 260 270 19091N 033 0 25 30 0 25 40 260 270 19091N 133 0 25 30 0 50 40 260 270 19091N 233 0 25 60 0 15 40 260 270 19091N 036 0 25 60 0 25 40 260 270 19091N 136 0 25 60 0 50 40 260 270 19091N 236 0 32 15 0 25 40 260 270 19091N 111 0 32 30 0 15 40 260 270 19091N 013 0 32 30 0 25 40 260 270 19091N 113 0 32 30 0 50 40 260 270 19091N 213 0 32 60 0 25 40 260 270 19091N 116 0 32 60 0 50 40 260 270 19091N 216 0 53 15 1 00 40 240 250 19095N 121 0 53 30 1 00 40 240 250 19095N 123 0 53 60 1 00 40 240 250 19095N 126 www agilent com chem jp DB FFAP
63. C C HP PLOT AL0 S C C GS Alumina C C HP PLOT 0 C C C C0 C0 HP PLOTU HP PLOT 0 GS 0 C C
64. PAH S N DB EUPAH mm m um C 0 18 20 0 14 40 320 340 121 9627 0 25 60 0 25 40 320 340 122 9612 0 32 15 0 25 40 320 340 123 9612 www agilent com chem jp Agilent J amp W S N DB 1701P HP PAS1701 ECD SPB 1701
65. 1 3 1 2 7 2 0 25 mm 0 32 mm 1 7 0 18 mm GC 15 m x 0 32 mm GC MS 7 DB 624 30 m 1 1 3
66. 5 GC 1 2
67. PLOT 1 0 GS 0 CP PoraPLOT Q CP PoraPLOT 0 HT Rt QPLOT Supel0 PLOT GS 0 HP PLOT 0 mm m hm C 0 32 15 20 00 60 270 290 19091P 003 0 32 30 20 00 60 270 290 19091P 004 0 53 40 00 60 270 290 19095P 003 0 53 30 40 00 60 270 290 19095P 004 HP PLOT 0 C C CO C0 PoraPlot U RTU PLOT HP PLOT U mm m nm C 0 32 30 10 00 60 190 19091P U04 0 53 15 20 00 60 190 19095P U03 0 53 30 20
68. 0 5 1 152 www agilent com chem jp Nl N NUM I NM MO MM li UM MMMMY Ill GC
69. e 60 90 0 amp A www adilent com chem jp j t ec www agilent com chem jp 0120 477 111
70. 5 C min 15 C min 1 2 14 14 DB 1 15 m x 0 25 mm 0 25 pm 1 30 cm sec 3 40 C 2 5 C min 40 70 C SE 0 15 C min 70 130 C IEEE 5 1 4 8s 6 12 7 8 9 3 2 7 3 4 5 0 2 4 6 8 10 12 Time min www agilent com chem jp 10 C min 50 100 C 100 C 3 10 C mn 100 300 C
71. 1 CO C0 GC MS PLOT CP Silica PLOT GS GasPro mm m C 0 32 5 80 260 300 113 4302 0 32 15 80 260 300 113 4312 0 32 30 80 260 300 113 4332 0 32 60 80 260 300 113 4362 www agilent com chem jp 133 134 GS CarbonPLOT 360 C Carbopack CLOT Carboxen 1006 PLOT CP CarboPLOT P7 GS CarbonPLOT mm m um C 0 32 15 1 50 0 360 113 3112 0 32 30 1 50 0 360 113 3132 0 32 30 3 00 0 360 113 3133 0 32 60 1 50 0 360 113 3162 0 53 15 3 00 0 360 115 3113 0 53 30 3 00 0 360 115 3133 www agilent com chem jp HP PLOT Molesieve PLOT 0 N C0 CH 5 5A
72. TMS 5 DB 121 5023 20 m x 0 18 mm 0 40 nm 11 mm 5183 4759 39 cm sec 100 C 1 i 900 10 C min 100 240 C 5183 4711 250 C 18740 20885 1 100 10 23 26s 42 HP FID 300 C 5181 1267 30 mL min 2 ng L 1 i 4 6 7 8 9 13 1 2 3 3 5 12 4 0 i 5 14 16 6 7 8 9 15 10 3 4 MDAJ 11 34 12 4
73. 0 32 mm 0 53 mm Rtx BAC1 RocBAC2 DB ALC1 DB ALC2 mm m um C DB ALC1 0 32 30 1 80 20 260 280 123 9134 OS di wv agilent com chem jp DB ALC1 0 53 30 3 00 20 260 280 125 9134 Ss DB ALC2 0 32 30 1 20 20 260 280 123 9234 DB ALC2 0 53 30 2 00 20 260 280 125 9234 HP Fast USP Phase G43 2 5 MDL 2 DB 624 PE 624 007 624 007 502 CP 624 ZB 624 HP Fast mm m hm C 0 53 30 1 00 20 260 19095V 420 www agilent com chem jp 127 PLOT PLOT
74. 1
75. AL0 KCI Al0 Na S0 Rt Alumina PLOT Alumina PLOT 50 GC Alumina 200 C 7 GS Alumina mm m C 0 53 30 60 200 115 3532 0 53 50 60 200 115 3552 www agilent com chem jp 132 HP PLOT Al 0 M GS Alumina C C GS Alumina HP PLOT AL0 M mm m um C 0 32 50 8 00 60 200 19091P M15 0 53 30 15 00 60 200 19095P M23 0 53 50 15 00 60 200 19095P M25 www agilent com chem jp GS GasPro PLOT
76. www agilent com chem jp
77. Te 60 400 ASTM D6584 60 400 EN14105 40 260 270 EN14103 FAME FAME 20 260 280 EN14110 HP GC 6 20 260 DB 624 PE 624 007 624 94 007 502 CP 624 ZB 624 DB ALC1 20 260 280 Rtx BAC1 Htx BAC2 DB ALC2 20 260 280 Rtx BAC1 Htx BAC2 HP 60 270 290 ASTM
78. 6 mm 0 10 0 4 0 18 0 4 0 20 0 4 0 25 0 4 0 32 0 5 0 45 0 8 0 53 0 8 138 GC 2 GC
79. 2 3 www agilent com chem jp
80. USP Phase G3 HP 50 Rtx 50 CP Sil 24 CB 007 17 MPS 50 HP 17 SP 2250 SPB 50 ZB 50 AT 50 DB 17 mm m um C 0 05 10 0 10 40 280 300 126 1713 0 10 10 0 10 40 280 300 127 1712 0 10 10 0 20 40 280 300 127 1713 0 10 20 0 10 40 280 300 22 2 0 18 20 0 18 40 280 300 121 1722 0 18 20 0 30 40 280 300 121 1723 0 25 15 0 15 40 280 300 122 1711 0 25 15 0 25 40 280 300 122 1712 0 25 15 0 50 40 280 300 122 1713 0 25 30 0 15 40 280 300 122 1731 0 25 30 0 25 40 280 300 122 1732 0 25 30 0 50 40 280 300 122 1733 0 25 60 0 25 40 280 300 122 1762 0 32 15 0 15 40 280 300 123 1711 0 32 15 0 25 40 280 300 123 1712 0 32 15 0 50 40 280 300 123 1713 0 32 30 0 15 40 280 300 123 1731 0 32 30 0 25 40 280 300 123 1732 0 32 30 0 50 40 280 300 123 1733 0 32 60 0 25 40 280 300 123 1762 0 53 5 2 00 40 280 300 125 1704 0 53 15 0 25 40 260 280 125 1711 0 53 15 0 50 40 260 280 125 1717 www agilent com chem jp DB 17 mm m um C 058 15 1 00 40 260 280 MI 0 53 15 1 50 40 260 280 2 0 53 30 0 25 40 260 280 25 0 53 30 0 50 40 260 280 M5
81. H H_ H UTE UTE 85 100 60 80 R 2 2 o a
82. GC 0 e
83. 4 14 2 4 15 m x 0 25 mm 0 25 nm Ci Vg 0 2 4 6 8 10 12 14 16 www agilent com chem jp DB 1 Pn RAoN DB 1
84. A 1 1 gq 2 3 6 4 3 5 6 8 9 eg p 1 8 cs trans yp trans 3 4 trans trans cs cis eg g trans d 31 8 10 12 14 16 18 20 22 24 26 28 Time min to A DD np he ho DB 1 20 m x 0 1 8mm x 0 18 hm NO 3 CO B 9 21 NS 0 0d Co 4 Time min SPEARMINT www agilent com chem jp 61 62 DB 1ms 122 0132UI 30 m x 0
85. 3 0 1 2 3 4 5 6 7 Time min 12aJ 50 C GC 35 C
86. FAME www agilent com chem jp 39 40 Agilent DB 5ms 122 5532UI 30 m x 0 25 mm 0 25 nm 38 cm s 250 C 1 4 mL mn 65 C 900 mL min 2 0 75 mL min PRD FHD 325 C 450 mL min 40 mL min Pbonb U 45 mL min
87. bm 2 7 11 UI MM TT 1 AM 4 GC
88. DB 5ms 5 95 60 325 350 HP 5ms 5 95 60 325 350 HP 1ms DB 100 60 325 350 BP 1 SPB 1 CP Sil 5 Rtx 1ms HP 1 DB 1 PCB 1 0V 1 SE 30 007 1 ZB 1 HP 5ms DB 5 HP 5 5 95 60 325 350 SPB 5 XTI 5 Mtx 5 FAME CP Sil 8CB SE 54 Rb5 BPX 5 MDN 5 Rtx 5ms BP 5 ZB 5 DB 5ms 5 95 60 325 350 Rix 5ms Rtx 5Sil MS Rxi 5ms FAME
89. HCI NH OH HCI NH OH 1 www agilent com chem jp 0 5 1
90. J UU UU J 11 12 13 14 15 16 17 Time min a ONDO PhON rw CED CN 4 9 Po DB 5ms 122 5532 30 mx 0 25 mm 0 25 pm 11 mm 5183 4759 31 cm sec 50 C 4 mm G1544 80730 50 C 05 18740 20885 25 C min 50 150 C 10 L KJ 23 26s 42 HP 5181 1267 10 C min 150 325 C 250 C 6 19 100 1 30 27 48 MSD 300 C 6 m z 40 380 1 2 3 49 71 4 1 5 5 20 26 6
91. 28 ND OT 0 LR 20 2425 27 26 18 30 31 35 33 36 oo 5 19 29 DB XLB g 4 4 DDE 4 4 DDD 4 4 DDT cls trans 10 12 14 16 18 20 22 24 Time min GCEPO05 7 5 cm PO AD Nm CE 21 35 46 10 12 14 16 18 20 22 24 Time min GCEPOO6 www agilent com chem jp EPA 8151A 3 5 DB 35ms 123 3832 30 m x 0 32 mm 0 25 pm 45 cm sec 50 C 0 5 25 C min 50 100 C 12 C min 100 320 C 320 C 2 250 C 30 IECD 350 C
92. 6 2 7 2 www agilent com chem jp 1 2
93. GC 20 www agilent com chem jp GC 164
94. 0 32 67 0 45 78 20 psi 1 mL min 0 53 10 12 0 53 mm 1 mL min 20 psi 9 5 10
95. PEG PLOT Agilent GC Agilent
96. b kj a cd cd 1 2 3 cd ah DB EUPAH EU PAHs www agilent com chem jp CLP 0 18 mm GC CLP 22 CLP 16 7 3 56 DB XLB GC
97. www agilent com chem jp 147
98. GC ee e e ee www agilentcom chem jp 76 www agilent com chem jp GC mm m hm C DB 1ms 0 18 20 0 18 60 325 350 121 0122Ul 0 25 15 0 25 60 325 350 122 0112UI 0 25 30 0 25 60 325 350 122 0132UI 0 25 60 0 25 60 325 350 122 0162UI 0 32 15 0 25 60 325 350 123 0112UI 0 32 30 0 25 60 325 350 123 0132Ul HP 1ms 0 18 20 0 18 60 325 350 19091S 677UI 0 25 15 0 25 60 325 350 19091S 931UI 0 25 30 0 25 60 325 350 19091S 933UI 0 25 30 0 50 60 325 350 19091S 633UI 0 25 30 1 00 60 325 350 19091S 733UI 0 32 15 0 25 60 325 350 9091S 911UI 0 32 25 0 52 60 325 350 19091S 612UI 0 32 30 0 25 60 325 350 19091S 913UI 0 32 30 1 00 60 325 350 9091S 713UI DB 5ms 0 18 20 0 18 60 325 350 121 5522UI 0 18 20 0 36 60 325 350 121 5523UI 0 25 15 0 25 60 325 350 122 5512UI 0 25 15 1 00
99. 6 1 15 m x 0 25 mm 0 25 nm 2 2 2 3 5 2 4 Cig DB 225 5 Polar 6 Ci2 DB 1 Non polar 0 2 4 6 8 10 12 14 16 0 2 4 6 8 10 12 14 16 DB 225 DB 225 DB 1 www agilent com chem jp 17 PLOT PLOT 35 C
100. DBVRX 30mx0 32 mm 1 8 pm 123 1534 D 5399 GC DB 2887 125 2814 30 mx 0 32 mm 1 8 um D 5441 GC MTBD HP PONA 50mx020mm 0 5um 19091S 001 DB Petro 100mx0 25mm 0 5 um 122 10A6 D 5442 GC DB 1 25mx0 32 mm 0 25 nm 123 1022 DB 5 15mx0 25 mm 0 25 nm 122 5012 D 5475 GC HP 5ms 30 m x 0 25 mm 0 25 pm 19091S 433 DB 1701P 30mx0 25mm 0 25 pm 122 7732 DBXLB 30mx0 25 mm 0 25 pm 122 1232 DB 35ms 30mx0 25 mm 0 25 nm 122 3832 D 5480 GC DB PS1 15mx0 53 mm 0 15 nm 145 1011 D 5501 GC HP 1 190917 530 100 mx 0 25 mm 0 5 um D 5507 GC HP PLOTO 15mx053mm 40nm 19095P 003 HP PLOTU 30mx0 53 mm 20 um 19095P U04 D 5508
101. 2 1 m p U S EPA 2 1 1 2 2 o PID ELCD GC MS 83 106 VOCOL NON PAKD Rtx Volatiles PE Volatiles 007 624 HP 624 CP 624 Rtx VRX Rtx VGC DB VRX mm m hm C 0 18 20 1 00 10 260 121 1524 0 18 40 1 00 10 260 121 1544 0 25 30 1 40 10 260 122 1534 0 25 60 1 40 10 260 122 1564 0 32 30 1 80 10 260 123 1534 0 32 60 1 80 10 260 123 1564 0 45 30 2 55 10 260 124 1534 0 45 75 2 55 10 260 124 1574 www agilent com chem jp 125 Agifmmt Technoiegtes 7683 Series PP DB 624 U S EPA 502 2 EPA 501 3 502 2 503 1 524 2 601 602 8010 8015 8020 8240 8260
102. DB 5ms mm m mm C 0 18 20 0 18 60 325 350 121 5522 0 18 20 0 36 60 325 350 121 5523 0 18 40 0 18 60 325 350 121 5542 0 20 12 0 33 60 325 350 128 5512 0 20 25 0 33 60 325 350 128 5522 0 20 50 089 60 325 350 128 5552 0 25 15 0 10 60 325 350 22 5511 0 25 15 0 25 60 325 350 22 5512 0 25 15 0 50 60 325 350 22 5516 0 25 15 1 00 60 325 350 22 5513 0 25 25 0 25 60 325 350 22 5522 0 25 25 0 40 60 325 350 22 552A 0 25 30 0 10 60 325 350 22 5531 0 25 30 0 25 60 325 350 22 5532 0 25 30 0 50 60 325 350 22 5536 0 25 30 1 00 60 325 350 22 5533 0 25 50 0 25 60 325 350 22 5552 0 25 60 0 10 60 325 350 22 5561 0 25 60 0 25 60 325 350 22 5562 0 25 60 1 00 60 325 350 22 5563 www agilent com chem jp 83 DB 5ms mm m um C 0 32 15 0 10 60 325 350 123 5511 0 32 15 0 25 60 325 350 123 5512 0 32 15 1 00 60 325 350 123 5513 0 32 25 0 52 60 325 350 123 5526 0 32 30 0 10 60 325 350 123 5531 0 32 30 0 25 60 325 350 123 5532 0 32 30 0 50 60 325 350 123 5536 0 32 30 1 00 60 325 350 123 5533 0 32 60 0 10 60 325 350 123 5561 0 32 60 0 25 60 325 350 123 5562 0 32 60 0 50 60 325 350 123 5566 0 32 60 1 00 60 325 350
103. GC GC GC 1 1 GC 150 250 C Agilent ChemStaton
104. GC GC J amp W Scientific 2000 HP DB 40 Agilent J amp W GC Agilent J amp W GC Agilent J amp W GC Agilent J amp W GC
105. 4 5 6 NPD 7 DB 1 DB 5 DB 1701 DB 17 DB WAX 8 PLOT
106. 3 50 60 173 1 2 30 C
107. 60 C 240 250 C 0 53 mm 230 240 C 0V351 USP Phase G35 HP FFAP GC Stabilwax DA DB FFAP Nukol 007 FFAP BP21 CP WAX 58 FFAP CB AT 1000 0V351 CP FFAP CB HP FFAP mm m hm C 0 20 25 0 30 60 240 250 19091F 102 0 20 50 0 30 60 240 250 19091F 105 0 25 30 0 25 60 240 250 19091F 433 0 32 25 0 50 60 240 250 19091F 112 0 32 30 0 25 60 240 250 19091F 413 0 32 50 0 50 60 240 250 19091F 115 0 53 10 1 00 60 240 19095F 121 0 53 15 1 00 60 240 19095F 120 0 53 30 1 00 60 240 19095F 123 www agilent com chem jp 113 CAM HP Basicwax Stabilwax DB Carbowax Amine CAM
108. EPA PA _ Agilent 501 amp ELCD DB VRX 30 mx 0 45 mm 2 55 Im 124 1534 ECD DB 624 30 m x 0 45 mm 2 55 hm 124 1334 502 2 8021 8 amp PID DBVRX 75 mx 0 45 mm 2 55 hm 124 1574 VOC CLP ELCD DB 624 75 mx 0 45 mm 2 55 Im 124 1374 601 8010 amp PID DB VRX 75 mx 0 45 mm 2 55 Im 124 1574 ELCD DB 624 75 m x 0 45 mm 2 55 hm 124 1374 503 1 602 amp PD DBVRX 30 m x 0 45 mm 2 55 hm 124 1534 8020 DB 624 30 m x 0 45 mm 2 55 Im 124 1334 MSD 524 2 624 amp MSD DB VRX 60 mx 0 25 mm 1 40 hm 122 1564
109. 1 PEG HP 88 C 18 1 2 mL min CU 120 C 1 10 C min 175 C 10 a 5 C min 210 C 5 5 C min 230 C 5 trans 11 1 FID 250 C 16 17 18 19 20 Time min www agilent com chem jp 2
110. Agilent J amp W GC MS Agilent J amp W
111. Ar 0 GS Molesieve HP PLOT Molesieve HP PLOT Molesieve 200 C 7 HP PLOT Molesieve mm m nm C 0 32 30 12 00 60 300 19091P MS4 0 32 15 25 00 60 300 9091P MS7 0 32 30 25 00 60 300 19091P MS8 0 53 15 25 00 60 300 9095P MS5 0 53 30 25 00 60 300 9095P MS6 0 53 15 50 00 60 300 9095P MS9 0 53 30 50 00 60 300 9095P MS0 www agilent com chem jp 135 HP PLOT 0 Porapak 0 Porapak N PLOT C C C C0 00
112. www agilent com chem jp 157 12b c 12d 5 12a DB 1 15 m x 0 32 mm 0 25 nm 30 cm sec 10 C min 40 130 C 1 3 2 2 3 4 1 3 5 1 4 6 12 7 8 9 8 3
113. DBWAX 60mx0 32mm 0 25um 123 7062 HP 1 50mx0 32 mm 0 52 pm 190917 115 D 3797 GC o HP INNOWax 60 mx0 32 mm 0 5 bm 19091N 216 D 3798 GC p HP INNOWax 60mx0 32 mm 0 5 bm 19091N 216 D 3871 DBVRX 124 1574 75mx0 45 mm 2 55 um D 3893 GC DBVRX 124 1534 30 mx 0 45 mm 2 55 um D 3973 DB VRX 124 1534 30 mx 0 45 mm 2 55 bm 32 www agilent com chem jp ASTM D 4415 DB FFAP 23 3232 30 m x 0 32 mm 0 25 um D 4424 GC HP PLOT AI203S 50mx0 53 mm 15 um 19095P S25 D 4443 GC DB VRX 124 1534
114. Time min GCEs004 1544 80730 4 mm G 10 23 26s 42 HP 5181 1267 DB XLB lon 485 70 485 40 to 486 40 PBDE 105D 122 1231 nd Tetra BDE 30 m x 0 25 mm 0 10 um 0 100 ppb each 0 38 cm sec 100 C 1 2 mL min E 10 00 11 00 2 00 13 00 100 C 1 20 C min 100 C 340 C lon 563 60 563 30 to 564 30 PBDE 105 D 340 C 12 00 x xxx x Penta BDE s ML Oppbeach AA Agilent 5973 MSD 325 CC EI SIM 231 8 248 0 327 9 398 6 400 5 405 8 845 7 563 6 643 5 721 4 799 3 lon 643 50 643 50 to 644 20 PBDE105D 05 HL Hexa BDE 500 200 ppb each 10 00 11 00 2 00 13 00 2 wwwagilent com chem jp 8 0 AO 5
115. 10 C 10 C min 30 11 11 DB 1 15 m x 0 25 mm 0 25 nm 30 cm sec 10 C min 50 130 C 1 3 8 2 2 1p3 3 4 13 1 4 7 8 9 12
116. 40 250 C 0V 351 USP Phase G35 DB FFAP GC Stabilwax DA HP FFAP Nukol 007 FFAP BP21 CP Wax 58 FFAP CB AT 1000 OV 351 CP FFAP CB DB FFAP mm m um C 0 25 15 0 25 40 250 122 3212 0 25 30 0 25 40 250 122 3232 0 25 30 0 50 40 250 122 3233 0 25 60 0 25 40 250 122 3262 0 25 60 0 50 40 250 122 3263 0 32 15 0 25 40 250 123 3212 0 32 25 0 50 40 250 123 3223 0 32 30 0 25 40 250 123 3232 0 32 30 0 50 40 250 123 3233 0 32 30 1 00 40 250 123 3234 0 32 50 0 50 40 250 123 3253 0 32 60 0 25 40 250 123 3262 0 32 60 0 50 40 250 123 3263 0 32 60 1 00 40 250 123 3264 0 45 30 0 85 40 250 124 3232 0 53 10 1 00 40 250 125 32H2 0 53 15 0 50 40 250 125 3217 0 53 15 1 00 40 250 125 3212 0 53 30 0 25 40 250 125 3231 0 53 30 0 50 40 250 125 3237 0 53 30 1 00 40 250 125 3232 0 53 30 1 50 40 250 125 3233 0 53 60 1 00 40 250 125 3262 112 www agilent com chem jp HP FFAP
117. DB WAX www agilent com chem jp 3 Non Polarity DB 1 DB 5 DBXUB HP 1 HP 5 DB 1ms DB 5ms HP 1ms HP 5ms DB 2887 HP 5ms DB Petro Semivol DBPONA DB 5 625 DB HT Sim Dis DBN DB 1ht Ultra 2 Ula 1 HP PASS DB EVDX k 5 3
118. Rxi 5Sil MS VF 5ms PTE 5 CP Sil 8 CB Low Bleed MS BPX 5 AT 5ms ZB 5ms SLB 5ms Equity 5 DB 1301 6 0 20 280 300 Rtx 1301 PE 1301 VF 1301ms VOC 94 DB 35 HP 35 ClP 35 65 40 300 320 Rtx 35 SPB 35 AT 35 Sup Herb MDN 35 BPX 35 DB 35ms CIP 35 65 50 340 360 Rtx 35 Rtx 35ms VF 35ms SPB 35 Al 35 Sup Herb MDN 35 BPX 35 DB 1701 DB 1701P TMS 14 20 280 300 SPB 1701 CP Sil 19 CB Htx 86 1701 CB 1701 0V 1701 007 1701 BPX10 www agilent com chem jp 27 GC C HP 50 DB 17
119. DA 4 1 1 2 1 30 3 n 275 4 4 5 5 n 25 6 7 1 2 22 5 8 8 n 1 9 1 20 10 3 11 n 17 5 15 12 5 DB 5ms 10 I I 2 4 6 8 10 Time min US EPA 8270 US EPA 8270 8 DB 5ms 122 5532UI 30 m x 0 25 mm 0 25 nm 30 cm s 40 C 1 100 C 15 C mim 10 C 210 C 1 5 C mn 310 C 8 260 C 53 7 mL min 50 mL min 0 5 80 mL min
120. K r B 3P 2d r Im d hml 8 9 K k Cs K CM K kB k _ C 2d cy 9 8
121. GC HP PLOT 0 19095P Q04 30mx0 53 mm 40 pm D 5580 GC DB 1 125 1035 p m C9 30 mx0 53 mm 5 00 nm D 5599 GC DB 5 122 5032 30 mx 0 25 mm 0 25 um D 5623 GC HP 1 190917 613 30 mx 0 32 mm 4 00 bm D 5713 GC DB Petro 128 1056 50 mx0 20 mm 0 5 bm 34 www agilent com chem jp ASTM D 5739
122. USP Phase G5 SP 2330 Rbc2330 007 23 AFSiar BPX 70 SP 2340 VF 23ms SEE DB 23 mm m um C 20 020 40 250 260 121 2323 0 15 025 40 250 260 122 2312 025 30 015 40 250 260 122 2331 2 30 025 40 250 260 122 2332 9 60 015 40 250 260 122 2361 025 60 025 40 250 260 122 2362 0 30 025 40 250 260 123 2332 0 32 60 0 25 40 250 260 123 2362 0 15 050 40 230 240 125 2312 053 30 050 40 230 240 125 2332 www agilent com chem jp 105 HP 88 88 oa 250 260 C FAMEs DB 23 CP Sil 88 SP 2560 SP 2340 SP 2330 BPX 70 BPX 90 HP 88 HP 88 mm m um C 0 25 100 0 20 0 250 260 112 88A7 0 25 60 0 20 0 250 260 112 6867 0 25 30 0 20 0 250 260 112 8837 106 www agilent com chem jp
123. 60 300 None HP PLOT AO KCI KCI 60 200 CP Al0 KCI PLOT Rt Alumina PLOT Alumina PLOT Al203 KCI gt C C HP PLOT Al0 S 60 200 CP Al20 PLOT Na S0 gt CI Ci GS Alumina 60 200 AO KCIL Al203 NazS04 Rt Alumina PLOT Alumina PLOT gt CI 6 HP PLOT 0 60 270 290 CP PoraPLOT 0 CP PoraPLOT CO0 C0 Q HT REOPLOT SupelQ PLOT GS 0 HP PLOTU CC C0 60 190 PoraPlot U RTU PLOT CO Ci Ci C0 gt
124. IS 3 IS 1 2 1 2 3 SS 3 1 2 3 VOC EPA 8260 DB VRX 1
125. 50 tans 9 27 35 43 www agilent com chem jp 45 EPA 508 1 DB 35ms DB 35ms 123 3832 30 m x 0 32 mm 0 25 pm DB XLB 11 mm 5183 4759 123 1236 30 mx0 32 mm 0 50 nm 4 mm 61544 80730 75 C 0 5 10 C min 75 300 C 300 C 2 250 C 30 LECD 350 C 30 mL min 1 50 pg a BHC y BHC 8 BHC BHC DCPA 44
126. DB 17 HP 50 G19 25 25 DB 225 DB 225ms 620 380 420 DB WAX 625 TPA Carbowax 20 M DB FFAP HP FFAP 627 5 95 DB 5 HP 5 HP 5ms DB 5ms 628 25 75 DB 35 HP 35 DB 35ms G32 20 80 DB 35 HP 35 DB 35ms 635 DB FFAP HP FFAP G36 1 5 DB 5 HP 5 HP 5ms DB 5ms 638 Phase G1 DB 1 HP 1 HP 1ms DB 1ms G39 1 500 DB WAX G41 10 DB 5 HP 5 HP 5ms DB 5ms 642 35 65 DB 35 HP 35 DB 35ms G43 6 94 DB 624 DB 1301 G45 HP
127. 93 27 2 6 5 MelonalTM 57 94 28 cis 58 95 29 59 8g 96 30 trans 60 97 61 98 5 62 99 8 63 100 7 64 101 T 1 19 20 45 46 102 2 2778 100 103 5 104 5 bill 4 105 ass ae 5 106 67 92 9 1 69 N 781 8 102 99 101 0 54 155 103 104105 NN Nl 6 1 0 10 20 4 60 70 80 90 100 105 Tme mi GCFF004 www agilent com chem jp
128. G2589 20045 A 1 4 00 8 00 12 00 16 00 20 00 24 00 Time min GCHE001 EPA 8270 5 ng mL DB 5 625 30 m x 0 25 mm 0 5 um B 1 1 1 4 00 6 00 8 00 10 00 12 00 14 00 16 00 Time min GCHE002 EPA 8270 5 ng mL DB 5 625 20 m x 0 18 mm 0 36 um www agilent com chem jp 1 EPA 8081A DB 35ms 122 3832 30 m x 0 25 mm 0 25 pm 35 cm sec 50 C 50 C 1 25 C mn 50 100 C 35 39 5 C min 100 300 C 3 0 2 an 300 C 5 jm 250 C 1 2 7 2 6 30 TT NN MSD 300 C 4 3 m z 50 500 be
129. gg 34 tert 74 1 2 Eee 35 75 11 mm 36 5 76 11 12 5183 4759 37 77 1 38 d4 IS 78 1 5 mm 18740 39 79 80200 40 12 80 18740 20885 83 trans 84 1 3 2 85 86 1 1 2 2 87 o 5975 88 12 3 89 cs 90 4 IS 49 91 92 93 94 43 44 95 41 42 45 96 97 98 ter 99 124 61 62 100 sec 101 1 3 102
130. mm m hm C 0 20 12 0 33 60 325 350 19091B 101 0 20 25 0 11 60 325 350 19091B 002 0 20 25 0 33 60 325 350 19091B 102 0 20 50 0 11 60 325 350 19091B 005 0 20 50 0 33 60 325 350 19091B 105 0 32 25 0 17 60 325 350 19091B 012 0 32 25 0 52 60 325 350 19091B 112 0 32 50 0 17 60 325 350 19091B 015 0 32 50 0 52 60 325 350 19091B 115 35 HP 35 USP Phase G42 Rtx 35 SPB 35 AT 35 Sup Herb HP 35 BPX 35 DB 35 mm m um C 0 25 30 0 25 40 300 320 122 1932 0 25 60 0 25 40 300 320 122 1962 0 32 30 0 25 40 300 320 123 1932 0 32 30 0 50 40 300 320 123 1933 0 53 15 1 00 40 280 300 125 1912 0 53 30 0 50 40 280 300 125 1937 0 53 30 1 00 40 280 300 125 1932 www agilent com chem jp CH CaHs T0 S 50 CisHs 50 100 DB 17 50 HP 50
131. 121 1222 20 x 0 18 0 18 a 1 H 77 3 cm s 120 C 260 120 C 0 49 9060 59 4 C min 120 C 160 C rm 23 7 C min 160 C 260 C 1 35 6 C min 260 C 300 C 1 69 220 C 90 35psi 0 5 400000 6 25 99 mL min 2 3mUmin 050 1 00 1 50 2 00 2 50 3 00 3 50 4 00 450 5 00 550 6 00 6 50 7 00 2 mm Time min E06 EECD 320 C Ar CH4 P5 1 TCMX 60 mL min 2 a BHC 1 44 DDE 05 LL 50 ppb 3 BHC A 14 4 BHC 5 BHC 15 44 DDD 6 16 7 17 4 4 DDT NNN 8 Ye 9 gt 20 10 S 21 4 22 DCB DB XLB 0 32 mm 123 1232 30 m x 0 32 mm 0 25 hm 1 9e 08 He 38 cm s 120 C 90 16e 08 3
132. 5183 4759 1 5 mm 18740 80200 18740 20885 Julie Kancler Brian Wallace Teledyne 1 1 2 18 3 19 4 2 20 5 21 6 22 7 2 2 tert 23 8 MTBE 24 9 25 10 1 26 11 DMI 27 12 2 MEK 28 13 29 14 2 30 15 31 16 32 33 9 8 16 19 14 35 1 3 1 15 iM MI 10 1 17 2 2 5 5 0 7 5 10 0 12 5 Time min 1 2 1 2 2 MIBK 2 1 NN DMF mjp 0o DMSO0 NN N 1 3 2 DMI 33 GCLS028
133. www agllent com chem jp www agilent com chem jp 51 52 GC MS EPA DB VRX 122 1564 60 m x 0 25 mm 1 40 pm 30 cm sec 45 C 11 mm 5183 4759 45 C 10 1 5 mm 18740 12 C min 45 190 C 80200 190 C 2 5188 5367 6 C min 190 225 C 225 C 1 amp 0 A 4560 61 62 68 63 40 mL mn 11 Tenaxz 175 C 220 C 0 6 110 C 30 mL mn MSD 235 C 35 260 m z m z 44 2 pg6 5 29 36 i 46 27 3 1615 a 2 2 234 7 11a8 2 113 5 6 jp 9 I 1 1 1 0 5 10 15 Time min GCEV001 DB 624 122 1364 60 m x 0 25 mm 1 4 nm 11 mm 31 cm sec 40 C 2IG0M0
134. 50 50 40 280 300 Rtx 50 CP Sil 19 CB BPX 50 SP 2250 DB 17ms 50 50 40 320 340 HP 50 Rtx 50 VF 17ms 007 17 SP 2250 SPB 50 BPX 50 SPB 17 AT 50 DB 200 35 30 300 320 Rtx 200 VF 200ms 65 DB 210 EPA 8140 50 45 240 260 SP 2401 609 50 DB 225ms DB 225 FAME 50 40 220 240 SP 2330 CP Sil 43 CB OV Na 50 225 Rtx 225 BP 225 007 225 HP INNOWax 40 260 270 HP 20M SUPELCOWAX 10 CP WAX 52 CB SUPEROXIL CB WAX Stabilwax BP 20 007 CW Carbowax DB WAXetr ZB WAX DB WAX 0U 20 250 260 HP 20M SUPELCOWAX 10 CP WAX 52 CB SUPEROXI CB WAX Stabilwax BP 20 007 CW Carbowax HP INNO
135. 65 n 22 2 44 d10 66 Agilent HP 5ms DB 5ms EPA 8270 0 5 bm HP 5ms 30 m x 0 25 mm 0 25 Im 19091S 433 PAHs DB 5ms 20 mx 0 18 mm x 0 18 nm 121 5522 www agilent com chem jp b k EPA 525 2 DB 5ms 122 5532 30 m x 0 25 mm 0 25 nm
136. CP ALO KCI PLOT Rt Alumina PLOT Alumina PLOT AL0 KCI GS Alumina KCI mm m C 0 53 30 60 200 115 3332 0 53 50 60 200 115 3352 HP PLOT AL0 S Ci Cs GS Alumina HP PLOT AL0 S mm m hm C 0 25 30 5 00 60 200 19091P S33 0 32 25 8 00 60 200 19091P S12 0 32 50 8 00 60 200 19091P S15 0 53 15 15 00 60 200 19095P S21 0 53 30 15 00 60 200 19095P S23 0 53 50 15 00 60 200 19095P S25 www agilent com chem jp GS Alumina C C C C
137. 25 cm s 200 C 0 25 20 mL min 1 2 1 1 1 1 m 0 32 mm SE Mii B 160 2855 5 5 33 C 14 5 C min 33 C 60 C 5 6 15 C min 275 C 20 7 G2397A LECD 300 C oe N 30 mL min MD 2 N 20 10 1 1 2 Hz 11 6003 a 12 500 13 4 16 18 14 1 2 400 5 11 19 15 2 6 9 12 16 1 1 1 2 300 3 8 10 13 17 17 14 15 18 2003 19 1 2 3 2 20 1 2 3 100 T T T jj T T T T T T T T T T T T T T T tf T tf T 10 15 20 25 30 min Hz 300
138. 40 C 0 001 70 C 80 C 90 C 3 10 min 0 20 mn 0 20 min 0 05 mn 0 1 0 2 mn 1 0 mL 1 2 3 4 5 6 2 6 05 10 15 20 25 30 Time min www agilent com chem jp GCLS024 Time mim 2 0 25 3 0 GCLS023 1 5 11 mm 5183 4759 1 5 mm 18740 80200 18740 20885 Methanol Acetaldehyde Ethanol lsopropanol Acetone 1 Propanol 73 DMI DB 624 123 1364 60 m x 0 32 mm 1 80 pm 17C mn 50 60 C 9 2 C min 60 115 C 35 C mn 115 220 C 220 C 6 Platen 140 C 250 C 2 mL 250 C 1 18 FID 270 C 5 000 ppm 11 mm
139. 75 Agilent J amp W GC SN 0 18 mm Agilent J amp W GC GC Agilent J amp W LTM Agilent J amp W LTM
140. 5 10 40 50 C 2 3 C min 1 4 GC GC 2 4 cm GC
141. HP 624 USP Phase G43 AT 624 Rtx 624 PE 624 007 624 007 502 CP 624 ZB 624 VF 624ms DB 624 mm m hm C 0 18 20 1 00 20 280 121 1324 0 20 25 20 260 128 1324 0 25 30 1 40 20 260 122 1334 0 25 60 1 40 20 260 122 1364 0 32 30 1 80 20 260 123 1334 0 32 60 1 80 20 260 123 1364 0 45 30 2 55 20 260 124 1334 0 45 75 2 55 20 260 124 1374 0 53 30 3 00 20 260 125 1334 0 53 60 3 00 20 260 125 1364 0 53 75 3 00 20 260 125 1374 GC DB ALC1 DB ALC2 GC
142. 7 1 50 2 1 50 1 50 t 1 ts 1 tt 2 PS wi 1 hh 1 2 w 2 w 1 3 t bl vb 2 www agilent com chem jp 9 B B 8 9
143. Time min 12b DB 1 15 m x 0 32 mm 0 25 nm 30 cm sec 6 50 C 2 10 C min 50 130 C 1 3 0 2 2 3 4 1 3 5 1 4 6 12 7 8 9 3 0 2 4 6 8 Time min 158 www agilent com chem jp GC 12c DB 1 15 m x 0 32 mm 0 25 nm 30 cm sec 50 C 4 10 C min 50 130 C 6 7 1 3 23 5 2 2 3 4 1 3 5 1 4 6 1 2 7 8 9 3 0 2 4 6 8 10 Time min 12d DB 1 15 m x 0 32 mm 0 25 nm
144. 60 1 19 59 Agilent 5975 MSD 200 C 20 1 60 6 21 61 cis 1 3 35 260 m z 200 C 22 trans 12 62 3 25 sec 23 MTBE 63 gt 1F0 9 24 1 64 150 C 25 65 tans 1 3 5mL 26 2 66 1 1 2 4 27 67 d8 IS 0 ppb E 68 20 ppb 29 69 1 3 ie 100 30 70 ie 100 800 ppb 32 22 72 28 29 33 73 3
145. HP 1301 HP 1701 Rtx 1301 PE 1301 VF 1301ms SPB 1701 CP Sil 19 CB Rix 1701 BP 10 OV 1701 007 1701 ZB 1701 VF 1701ms DB 1301 mm m um C 0 25 30 0 25 20 280 300 122 1332 0 25 30 1 00 20 280 300 122 1333 0 25 60 0 25 20 280 300 122 1362 0 25 60 1 00 20 280 300 122 1363 0 32 30 0 25 20 280 300 123 1332 0 32 30 1 00 20 280 300 123 1333 0 32 60 1 00 20 280 300 123 1363 0 53 15 1 00 20 260 280 125 1312 0 53 30 1 00 20 260 280 125 1332 0 53 30 1 50 20 260 280 125 1333 DB 1701 mm m hm C 0 10 20 0 10 20 280 300 27 0722 0 10 20 0 40 20 280 300 127 0723 0 18 10 0 40 20 280 300 121 0713 0 25 15 0 25 20 280 300 22 0712 0 25 15 1 00 20 280 300 122 0713 0 25 30 0 15 20 280 300 122 0731 0 25 30 0 25 20 280 300 22 0732 0 25 30 1 00 20 280 300 122 0733 0 25 60 0 15 20 280 300 22 0761 0 25 60 0 25 20 280 300 22 0762 0 25 60 0 50 20 280 300 122 0766 0 25 60 1 00 20 280 300 22 0763 102 www agilent com chem jp DB 1701 mm m hm
146. NIN lt 0 www agilent com chem jp GC 250 C 150 200 C 275 300 C 250 C 250 C 250 C 1 HL 1 1 HL 1 50 0 5 GC
147. PEG PEG H0 9 PEG DB WAX DB WaxFF Carbowax 20M 0 10 mm GC DB WAXetr HP INNOWex MS
148. DB FFAP HP FFAP CAM 108 DB WAX DB WaxFF PEG USP Phase G16 20 C PEG HP WAX DB WaxFF DB Wax HP 20M SUPELCOWAX 10 CP WAX 52 CB SUPEROX CB WAX Stabilwax BP 20 007 CW Carbowax HP INNOWax Rtx WAX ZB WAX VF WAXms DB WAX DB WaxFF mm m um C DB WAX 0 05 10 0 05 20 250 260 126 7012 0 05 10 0 10 20 240 250 126 7013 0 10 10 0 10 20 250 260 127 7012 0 10 10 0 20 20 240 250 127 7013 0 10 20 0 10 20 250 260 127 7022 0 10 20 0 20 20 240 250 127 7023 0 18 10 0 18 20 250 260 121 7012 0 18 20 0 18 20 250 260 121 7022 0 18 20 0 30 20 240 250 121 7023 0 18 40
149. 41 11 1 121 1524 2 42 1 20 m x 0 18 mm 1 00 nm 3 43 I 55 cm sec 1 5 mL min 5 45 1 1 6 46 1 7 47 45 C 3 20 C min 190 225 C 8 48 2 9 49 36 C min 45 190 C 225 C 05 10 50 tet amp lekmar 3100 250 C 1 11 51 5 11 260 C 10 1 Vocarb 3000 100 C 14 11 54 12 245 C 15 tert 55 16 56 150 C 17 57 2 Ee 18 58 1 4
150. GC MS ms Agilent J amp W ms GC 2 2
151. HP 225 SP 2330 CP Sil 43 CB Rtx 225 BP 225 0V 225 007 225 Al 225 DB 225ms mm m nm C 0 25 15 0 25 40 240 122 2912 0 25 30 0 25 40 240 122 2932 0 25 60 0 25 40 240 122 2962 0 32 30 0 25 40 240 123 2932 2 DB 1 100 USP Phase G2 HP 1 Ultra 1 SPB 1 CP Sil 5 CB Low Bleed MS Rtx 1 BP 1 OV 1 OV 101 007 1 MS SP 2100 SE 30 CP Sil 5 CB MS ZB 1 AT 1 MDN 1 ZB 1
152. 4 2 4 6 4 D10 D12 33 b k D12 US EPA 551 1 A HP 1ms a 19091S 733UI 30 m x 0 25 mm 1 00 hm 11 mm 5183 4759 B DB 1301 122 1333 4 mm G1544 80700 30 m x 0 25 mm 1 00 mm 5 23 26s 42 HP Agilent 7890A GC 5181 1273 Agilent 7683B 5 0 5181 1273 0 5
153. 8081A Accustandard Inc 35 bg mL 1 0 Po 1 1 2 3 2 4 3 SS 5 10 15 25 30 35 40 3 Tme rin i 4 1 2 S 2 17 BHC 26 gt 3 44 6 35 44 SS 7 18 BHC 27 36 45 8 2 SS 19 28 gt 37 46 9 nm 8S 2 29 tans 38 47 10 g m 2 79 30 a 39 pp DDD 0 11 22 31 40 Il 49 cis 12 A 23 32 41 pp DDT 50 trans 13 B 24 33 pp DDE 42
154. GC Agilent J amp W GC Agilent J amp W 92
155. C 0 32 15 0 25 20 280 300 123 0712 0 32 15 1 00 20 280 300 123 0713 0 32 30 0 15 20 280 300 123 0731 0 32 30 0 25 20 280 300 123 0732 0 32 30 1 00 20 280 300 123 0733 0 32 50 1 00 20 280 300 123 0753 0 32 60 0 25 20 280 300 123 0762 0 32 60 1 00 20 280 300 123 0763 0 53 15 1 00 20 260 280 125 0712 0 53 30 0 25 20 260 280 25 0731 0 53 30 0 50 20 260 280 125 0737 0 53 30 1 00 20 260 280 125 0732 0 53 30 50 20 260 280 25 0733 0 53 60 1 00 20 260 280 125 0762 DB 225 CN 50 6 FAMEs CH Il HP 225 0 0 USP Phase G7 ch ym CH 50 SP 2330 CP Sil 43 CB Rtx 225 BP 225 0V 225 007 225 AT 225 DB 225 mm m um C 0 10 20 0 10 40 220 240 127 2222 0 18 20 0 20 40 220 240 121 2223 0 25 15 0 25 40 220 240 122 2212 0 25 30 0 15 40 220 240 122 2231 0 25 30 0 25 40 220 240 122 2232 0 32 30 0 25 40 220 240 123 2232 0 53 15 1 00 40 200 220 125 22
156. GC MS 0 25 mm 5 5 ng nm mm 0 18 0 20 0 25 0 32 0 53 0 10 20 35 25 50 35 75 50 100 025 35 75 50 100 75 125 100 250 050 75 150 100 200 125 250 250 500 100 150 250 200 300 250 500 500 1000 300 400 600 500 800 1000 2000 5 00 1000 1500 1200 2000 2000 3000 1 www agilent com chem jp lt a pgilent a a5I15 lo OO VON espelGrer Ferru e NoK fts CO 0 149850 shom MP 23 dein US N Yan 09 22 8 DB 624 15 m x 0 53
157. HP INNOWax 1 1 19091N 133 2 2 30 m x 0 25 mm 0 25 pm 3 3 4 4 30 cm sec 5 ie 5 0 9 mL min 6 6 80 C 1 7 eg 7 5 C min 80 250 C 8 18 250 C 2 9 9 1 250 C 10 nm 20 1 MSD 280 C 415 17 11 mm 5183 4759 19 5183 4647 18740 20885 0 5 30 5 23 26s 42 HP 5181 1273 6 Time min GCFFO06 HPChiral 6 1 1 2 19091G B233 2 30 m x 0 25 mm 0 25 pm 3 B 39 cm sec
158. 32 cm sec 45 C 45 C 1 30 C min 45 130 C 130 C 3 12 C min 130 180 C 7 C min 180 2407C 12 C min 240 325 C 325 C 5 300 C 1 0 6 19 MSD 325 C m z 45 450 Accustandard 525 2 M 525 2 SV_ASL M 525 2 FS ASL M 525 2 CP ASL M 525 2 NP1 ASL M 525 2 NP2 ASLI 2 ng uL 5 ng uL IS SS 11 mm 5183 4759 4 mm G1544 80730 10 23 26s 42 HP 5181 1267 100 115 49 71 116 118 I 6 7 8 9 10 I 11 12 13 14 15 16 Time min GCES016 Agilent GC
159. 45 78 110 17 g 46 79 111 18 47 80 1 112 19 48 81 2 113 20 49 82 pg 114 1 21 3 55 51 4 83 115 22 52 85 97 116 23 8 53 88 24 54 89 117 25 56 90 118 T 26 57 91 119 lt cis 58 5 _
160. 59 93 BR trans 94 5 121 95 cis 122 3 6 123 67 68 124 D amp 125 1 6 126 7 127 10 5 12 30 2 5 20 26 14 24 9 54 lp 377 18 77 89 18 35 141 3 73 100 117 1 33 101 21 6L621 71 4 91 111 123 4 63 88 102 ii Mi 99 103 118 127 8 4 58 108 120 70 105 125 0 5 10 15 20 25 30 35 40 45 50 Time min GCFFOO3 www agilent com chem jp 63 64 Il Carl Frey Analytical Service Dragoco DB WAX 122 7032 Kevin Myung Flavor and Research Bush Boake Allen Inc 30 m x 0 25 mm 0 25 nm 25 cm sec 150 C 45 C 2 3 C min 45 250 C 11 mm 5183 4759 250 C
161. 80 260 300 CP Silica PLOT SF6 80 C GS OxyPLOT 350 CP LowOX GS CarbonPLOT Ci 55 C0 0 360 Carbopack CLOT Carboxen C 0 1006 PLOT CP CarboPLOT P7 www agilent com chem jp 29 GC C DB EUPAH EC 40 320 340 DB 624 6 20 260 AT 624 Rtx 624 PE 624 007 EPA 502 2 94 624 007 502 CP 624 ZB 624 gt VF 624ms DB VRX MSD ELCD PID 10 260 VOCOL NON PAKD Rtx Volatiles PE Volatiles 007 624 HP 624 CP 624 Rtx VRX Rtx VGC DB 35ms CLP 35
162. 8240 8260 DB 624 60 m x 0 25 mm 1 4 hm 122 1364 VOC CVS HPVOC 60 m x0 20 mm 1 10 pm 19091R 306 MSD 524 2 624 amp MSD DB VRX 20 mx 0 18 mm 1 00 hm 121 1524 8240 8260 DB 624 20 m x 0 18 mm 1 00 um 121 1324 VOC CLPVOCs EDB DBCP 504 1 8011 ECD DB VRX 30 m x 0 45 mm 2 55 hm 124 1534 DB 624 30 mx 0 45 mm 2 55 hm 124 1334 603 8015 amp FID DB VRX 30 mx 0 45 mm 2 55 Im 124 1534 1 1 2 0 09 NPD DB 624 30 m x 0 45 mm 2 55 hm 124 1334 _ 525 625 MSD HP 5ms 30 m x 0 25 mm 0 50 hm 19091S 133 8270 SPE 528 604 ECD DB 5ms 30 mx 0 25 mm 0 25 hm 122 5532 8040 8041 FID DB XLB 30 m
163. DB 1 123 106E 60 m x 0 32 mm 0 50 bm D 3257 GC DB 624 125 1334 30 m x 0 53 mm 3 nm D 3329 GC DBWAX 30 mx0 45 mm 0 85 um 124 7032 DB 624 30mx045mm 255 pm 124 1334 D 3432 GC HP 1ms 30 m x 0 32 mm 1 00 pm 19091S 713 D 3447 DB 624 125 1334 30 m x 0 53 mm 3 nm D 3545 GC DB 624 125 1334 30 m x 0 53 mm 3 nm D 3687 DB WAX 30mx0 45 mm 0 85 bm 124 7032 DB WAX 30 mx0 45 mm 0 85 nm 124 7032 D 3695 GC DB WAX 124 7032 30 mx 0 45 mm 0 85 pm D 3710 GC DB 2887 125 2814 10mx0 53 mm 3 um D 3760 GC
164. Entech 7100 2 84 GC MS 6890 5973N 11 109 OO 29 180 m z 06 min 13 58 33 280 m z 6 30 min 14 29 lt 15 45 _ 70 eV _ 16 1 B1 400 mL 112 1 2 2 10 10 ppbV 19 76 50 ppbV 20 ppbV 9 8 20 ppbV 30 ppbV trans 1 2 22 tert MTBE 73 30 ppbV 23 63 24 43 25 2 MEK 72 26 n 57 29 27 cis 1 2 96 28 43 29 5 128 4 5 30 83 31 42 32 1 1 1 97 33 12 62 34 78 17 35 17 36 56 40 37 1 4
165. 40 C 1 11 mm 5183 4759 5 C min 40 290 C 250 C 5183 4647 1 50 18740 20885 MSD 300 C gt 5L 23 26s 42 HP 5181 1273 EE 1 20 1 u 1 28 p 60 96 2 2 3 29 61 3 30 p 62 97 trans 4 2 3 31 1 8 63 98 n
166. 65 50 340 360 Rtx 35 Rtx 35ms VF 35ms PCB 508 1 SPB 35 AT 35 Sup Herb MDN 35 BPX 35 HP 5ms DB 5 HP 5 EPA 8270 5 95 60 325 350 SPB 5 XTI 5 Mtx 5 CP Sil 8CB SE 54 HRtx 5 BPX 5 MDN 5 Htx 5ms DB XLB PCB 209 30 340 360 Rtx XLB MDN 12 CLP PCB 508 1 DB TPH LUFT 10 290 ee DB MTBE MTBE 35 260 280 0 30 www adilentcom chem jp GC
167. 10 7 psig mm m 0 18 0 2 0 25 0 32 0 45 0 53 10 5 10 12 10 15 15 8 12 5 10 1 2 20 10 20 25 20 30 30 15 25 10 20 3 5 2 4 40 20 40 50 40 60 60 30 45 20 30 6 10 4 8 75 8 14 5 10 105 7 15 www agilent com chem jp
168. 7 8 6 9 6 10 a aa www agilent com chem jp DB ALC 1 125 9134 30 m x 0 53 mm 3 00 pm 80 cm sec 40 C 40 C 250 C 1 10 FID 300 C 23 mL min 11 mm 5183 4759 1 5 mm 18740 80200 18740 20885 Il 1 Methanol 2 Acetaldehyde 3 REhanal 4 lsopropanol 5 Acetone 6 1 Propanol 1 0 DB ALC 2 250 C 125 9134 1 10 30 m x 0 53 mm 3 00 nm FID 300 C 80 cm sec 40 C 23 ml min 0 1
169. HP 5ms 30 m x 0 25 mm 0 50 hm 19091S 133 FID DB 5ms 30 mx 0 53 mm 1 50 pm 125 5532 SFE DB 608 30 mx 0 53 mm 0 50 um 125 6837 610 8100 FID DB 5ms 30 m x 0 25 mm 0 25 hm 122 5532 PAHs DB 5ms 30 mx 0 32 mm 0 25 um 123 5532 SFE DB 1ms 30 mx 025 mm 0 25 um 122 0132 612 8120 ECD DB 5ms 30 m x 0 32 mm 0 50 hm 123 5536 8121 HP 5ms 30 mx 0 32 mm 0 50 hm 19091S 113 SPE DB 1 30 m x0 32 mm 0 50 hm 123 103E 551 551 1A ECD DB 5ms 30 mx 0 25 mm 1 00 hm 122 5533 DB 1 30 m x 0 25 mm 1 00 Im 122 1033 552 552 1 ECD DB 35ms 30 mx 0 32 mm 0 25 hm 123 3832 552 2 DB XLB 30 m x 0 32 mm 0 50 hm 123 1236 PCB 508 1 608 ECD DB 35ms 30 mx 0 32 mm 0 25 Im 123 3832 PCB 8081A 8082 DB XLB 30 m x 0 32 mm 0 50 hm 123 1236 CLP 515 615 ECD DB 35ms
170. 11 1 4 33 2 55 n 77 bl 12 34 56 78 k 13 1 2 35 2 4 6 57 2 4 6 79 a 14 2 36 2 4 5 58 4 80 d12 15 2 37 2 59 81 1 2 3 cd 16 4 38 2 60 82 ah 17 n n 39 2 61 d10 83 gh 18 40 62 19 d5 41 26 63 20 42 64 21 43 3
171. 153 30 cm sec 25 cm sec 35 cm sec 40 cm sec 30 35 cm sec 60 cm
172. 2 1 4 0 Rs 087 Rs 1 N 107 250 0 53 mm 1 D 3 0 pm 0 32 mm I D 1 8 hm www agilent com chem jp amp 0 45 mm 0 53 mm
173. RPB 30 m x 0 45 mm 2 55 pm D 4735 GC DB FFAP 24 3232 30 mx 0 45 mm 0 85 nm D 4773 100 2000 D 4864 GC DB WAX 24 7032 30 m x 0 45 mm 0 85 nm D 4947 DB 5 30mx0 53 mm 1 50 um 125 5032 DB 608 30mx0 53 mm 0 83 nm 125 1730 D 4961 DB FFAP 30mx0 45 mm 0 85 nm 24 32
174. 0 18 10 0 18 60 325 350 121 5012 0 18 10 0 18 60 325 350 121 5012E 0 18 10 0 40 60 325 350 121 5013 0 18 20 0 18 60 325 350 121 5022 0 18 20 0 18 60 325 350 121 5022E 0 18 20 0 40 60 325 350 121 5023 0 18 20 0 40 60 325 350 121 5023E 0 18 40 0 18 60 325 350 121 5042 0 20 12 0 33 60 325 350 128 5012 0 20 15 0 20 60 325 350 128 50H7 0 20 25 0 33 60 325 350 128 5022 0 20 50 0 33 60 325 350 128 5052 0 25 15 0 10 60 325 350 122 5011 0 25 15 0 25 60 325 350 122 5012 0 25 15 0 50 60 325 350 122 501E 0 25 15 1 00 60 325 350 122 5013 0 25 25 0 25 60 325 350 122 5022 0 25 30 0 10 60 325 350 122 5031 0 25 30 0 25 60 325 350 122 5032 0 25 30 0 50 60 325 350 122 503E 0 25 30 1 00 60 325 350 122 5033 0 25 50 0 25 60 325 350 122 5052 0 25 60 0 10 60 325 350 122 5061 0 25 60 0 25 60 325 350 122 5062 0 25 60 0 50 60 325 350 122 506E 0 25 60 1 00 60 325 350 122 5063 0 32 15 0 10 60 325 350 123 5011 0 32 15 0 25 60 325 350 123 5012 0 32 15 1 00 60 325 350 123 5013 0 32 25 0 17 60 325 350 123 502D 0 32 25 0 25 60 325 350 123 5022 0 32 25 0 52 60 325 350 123 5026 0 32 25 1 05 60 325 350 123 502F 0 32 30 0 10 60 325 350 123 5031 0 32 30 0 25 60 325 350 123 5032 0 32 30 0 50 60 325 350 123 503E 0 32 30 1 00 60 325 350 123 5033 0 32 30 1 50 60 325 350 123 503B 0 32 50 0 25 60 325 350 123 5052 0 32 50 0 52 60 325 350 123 5056 0 32 50 1 0
175. 1 5 mm 45 C 3 18740 80200 8 C min 45 90 C 5188 5367 90 C 4 6 C min 90 200 C 0 01A_4560 NNN amp 40 mL min 11 0 5 Tenaxz 175 220 C 0 6 110 C 8 30 mL min MSD 235 C 35 260 m z m z 44 63 64 33 34 0 60 60 20 21 22 le HL 32 30 3 9 1110 18 2 55 Nl Me lse 1 7 43 5 6 44 1 I 0 5 10 15 20 Time min GCEV002 www agilent com chem jp Ta HITV U tert 1 2
176. C16 C18 cis trans 270 C 50 1 230 C 3 n 1 21 19 Bij 1617 20 18 22 23 24 25 FID 280 C 28 29 2627 303132 334 3 9 41 2 4 6 8 10 12 14 Time min 16 18 20 22 24 26 28 GCFF027 11 mm 5183 4759 5183 4647 18740 20885 5 E 23 26s 42 HP 5181 1273 www agilent com chem jp Ri SO OD Oe 0 po RRRCLRRLRRRRRRRRNRNNYN NN NN NN OPCo RN eb Pt ND A ON pe ba C6 0 C7 0 C8 0 C9 0 C10 0 C11 0 C12 0 BHT C13 0 C14 0 C14 1n5 C15 0 C16 0 C16 1n7 trans C16 1n7 cis C17 0 C17 1 C18 0 C18 1n9 trans C18 1n9 cis C18 1n7 C18 2n6 C18 3n6 C18 3n3 C18 2 d9 11 C18 2 d10 12 C20 0 C20 1n9 C20 2n6 C20 3n6 C20 4n6 C20 3n3 C20 5n3 C22 0 C22 1n9 C22 2n6 C22 4n6 C22 5n3 C24 0 C22 6n3 C24 1n9 DB 624 125 1334 1 Methanol 30 m x 0 53 mm 3 hm 2 Ethanol 3 lsopropanol
177. mm m um C ASTM 0 32 15 01 60 400 123 BD11 D6584 EN14105 0 32 10 0 1 60 400 123 BDO1 0 32 30 0 25 40 260 270 1909BD 113 EN14103 FAME 0 32 30 1 8 20 260 280 123 BD34 EN14110 MSTFA 10 x 1 mL 5190 1407 ASTM D6584 N N D6584 5190 1408 1 mL x 5 2 x 5 mL E14105 4 x 1 mL 5190 1409 4 x 3 x 1 mL 5190 1410 116 www agilent com chem jp DB 1ht 100 400 C
178. 1 4 TCD 200 C 200 ppmV 200 ppmV C0 250 ppmV N 0 56 N2 CO 2 N20 CH4 wi 2 2 2 4 2 6 2 8 3 3 2 3 4 3 6 3 8 Time min GCEA006 0 M2 N20 CH4 CO 2 4 6 8 10 Time min GCEA007 N2 H20 CH4 CO N20 1 1 5 2 2 3 35 4 4 5 Time min GCEA008 www agilent com chem jp GC LH HH HP INN0Wax 19091N 216 60 m x 0 32 mm 0 5 nm 20 psi 75 C 10 min 3 C min 100 C 0 mm 10 C min 145 C 0 min 250 C 100 1 FD 250 C 10 mL HP INNOWax 19091N 577 20 m x 0 18 mm 0 18 pm 33 ps 70 C 3 min 45 C min 145 C 1 min 250 C 100 1 600 1 FD 250 C
179. 2 DB 5ms A 1 Medazepam 10 lemazepam 15 Nitrazepam 122 5532UI p 2 Halazepam 11 FIunitrazepam 16 Chlordiazepoxide 30 m x 0 25 mm 0 25 nm 9 0 3 Oxazepam 12 Bromazepam 17 Clonazepam 53 cm sec 4 lorazepam 13 Prazepam 18 Demoxepam 1 6 11 mn 5 Diazepam 14 Lormetazepam 19 Estazolam 60mLmm 16 2402 PMP am 60 mL min 2 4 50 9 BB ohanan 13 170 C 3 2 min 9 0xazopam 24 7 C min 170 250 C 5 3 min 7 18 6 C min 250 280 C 4 0 min 6 5 8 50 0 C min 280 325 C 4 min 19 50 a 280 C 4 i 20 psi 0 38 min 50 mL min 0 40 min a ml G1544 80730 FID 350 C 20 1 TIL 5 10 ppm a 10 7 8 9 10 11 12 13 14 15 16 Time min NO GC
180. C0 C0 GS GasPro Ci Ci C0 SF 80 C GS CarbonPLOT C C 00 00 GS 0xyPLOT 1400 C C 128 www agilent com chem jp GS 0xyPLOT C C ASTM CP LowOX GS 0xyPLOT mm m C 0 53 10 350 115 4912 HP PLOT AL0 KCI
181. 30 cm sec 4 terLButanol 40 C 5 2 Propen 1 ol allyl alcohol 40 C 5 6 1 Propanol 10 C min 45 260 C 4 ia i propargyl alcohol 260 C 3 sec Butano aw 0 C 9 2 Methyl 3 buten 2 ol 10 lsobutanol a a 11 2 Methoxyethanol methyl Cellosolve ia EE 12 3 Buten 1 ol 30 mL min 13 2 MethyL2 butanol tert amyl alcohol O CS 0 01 0 05 1 14 1 Butanol 3CS 22 29 30 37 39 4142 43 49 50 52 44 46 51 0 5 10 15 20 Time min GCICO01 11 mm 5183 4759 5183 4647 18740 20885 5 23 26s 42 HP 5181 1273 www agilent com chem jp 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 2 Buten 1 ol crotyl alcohol Ethylene glycol 1 Penten 3 ol 2 Pentanol Glycidol 3 Pentanol 2 Ethoxyethanol Cellosolve Propylene glycol 3 Methyl 1 butanol isoamyl alcohol 2 Methyl 1 butanol active amyl alcohol 4 Methyl 2
182. ColumB 500 100 6 4 3003 2 3 2003 6 T T T T T T T T T T T T T T T T T T T T T 10 15 20 25 30 min EPA_551 1 EPA 551 1 HP 1ms HP 1ms EPA 551 www agilent com chem jp 41 42 15 1 EU PAHs DB EUPAH 121 9627 20 m x 0 18 mm 0 14 nm 11 mm 5183 4759 Agilent 6890N 5975B MSD Agilent 7683B 5 0 5181 1273 0 5 LL 4 mm G1544 80700 75 L min 5 pL 23 26s 42 HP 1 0 mL min
183. tw 1 1 k 1 1 k 6 k 3 2
184. NN J amp W GC uaaatttetattnttttaeaneeea 1 5 es 2 2 EEOE To oO D8 39 SNoadaaiseeccaamaaaseaateeceeceenaasas aa a kb Raa ii cc LL 75 6 EE 76 GC GC MS TUT NS Die PEG 137 cc lt gt FO 053 E 157 Agilent J amp W GC
185. 2 6 1S J 65 C 1 7 1 5 C min 65 170 C 8 N 250 C 9 1S 2R 5S 30 1 10 1R 2S 5R FID 300 C 2 1 lt 025 ng uL 5 10 15 20 Time min GCFF008 Cyclodex R 2 112 2532 5 1 H 30 m x 0 25 mm 0 25 nm 2 3 55 cm sec 4 J 105 C 1 250 C 1 100 FID 300 C 30 mL min 1 Mg L 1 lt 13 min _ GCFF009 www agilent com chem jp 65 FAME I DB 23 122 2362 60 m x 0 25 mm 0 25 pm Steve Watkins Jeremy Ching FAME Analytics http www fameanalytics com 43 cm sec 130 C 1 0 6 5 C min 130 170 C 2 75 C 170 215 C 215 C 12 40 C min 215 230 C
186. 5 32 64 99 6 33 2 6 5 66 100 7 3 34 67 1 101 8 2 35 68 102 9 37 69 103 y 0 38 70 2 104 11 39 71 105 12 41 cis 72 106 13 42 trans 73 107 2 14 43 74 108 15 44 76 109 1 16
187. HP 1 190912 115 50 m x 0 32 mm 0 52 bm E 1863 GC DB WAXetr 60mx0 32 mm 1 00 um 123 7364 E 202 DB 624 25 1334 30 mx 0 53 mm 3 nm E 475 GC ter HP 5 19095J 623 30 mx 0 53 mm 5 00 bm www agilent com chem jp 35 EPA EPA GC
188. PLOT 35 C PLOT GS Alumna CC GS Alumina KCI HP PLOT 0 C C C GS Alumina HP PLOT 0 C HP PLOT 0 H
189. 2uLx10 50 ng uL 50 C 1 10 C min 50 180 C 5 C mn 180 230 C 11 mm 5183 4759 10 C min 230 320 C 320 C 2 4 mm 5181 3316 10 23 26s 42 HP 5181 1267 1 Monuron 19 Propanil 2 Diuron 20 Ametryne 1112 13 3 PTE 21 Prometryne 4 Dichlobenil 22 Simetryn 5 Vernolate 23 Metribuzin 6 Pebulate 24 lerbutryn 27 7 Molinate 25 Metolachlor 8 Sulfallate 26 Bromacil 20 23 9 Atraton 27 Dacthal 10 Prometon 28 Diphenamid 11 Arazne 29 Butachlor 36 12 Propazine 30 Napropamide 13 Simazine 31 Carboxin 18 19 14 Terbuthylazine 32 Tricyclazole 15 Pronamide 33 Norflurazon 16 Secbumeton 34 Hexazinone 4 24 17 Terbacil 35 Difolotan 8 Alachlor 36 Flurdone 17 25 30 35 36 Time min GCEP019 ECD PBDE DB XLB 72 cm sec 100 C 4 0 mL mn 15 m x 0 18 mm ID 0 07 hm Te 2 NSIM Agilent Technologies 100 C 05 8 30 C min 100 300 C 1 22 4 BDE BDE 17 300 C 5 2 244 BDE BDE 28 250 C 3
190. 50 pg 4 2 4 MCPP MCPA 4 4 S 2 4 D 2 4 5 TP 2 4 5 T 2 4 DB DCPA aci EPC SS OO m 1 30 mL mn lt 11 00 11 mm 5183 4759 4 mm 5181 3316 10 23 26s 42 HP 5181 1267 4 6 8 10 12 14 16 Time min GCEP017 www agilent com chem jp 47 DB XLB 250 C 30 30 m x 0 25 mm 0 25 pm MSD 300 C m z 50 400 32 cm sec 50 C
191. Cy 216 4 n Cn 234 5 n C14 253 6 n Cg 268 Time min 7 n Ci 287 2 DB 1 30 m x 0 25 mm 0 25 pm 3 3 4 C 1 111 100 Methyl 2 157 3 182 4 Ci 174 5 219 0 2 4 6 8 10 12 14 16 6 C12 216 www agilent com chem jp 13 3 HP 88 30 m x 0 25 mm 1 D 0 25 nm FAME
192. GC MS DB 5 30mx0 25 mm 0 25 um 22 5032 E DBTPH 30mx0 32 mm 0 25 um 23 1632 D 5769 GC MS HP 1 190912 236 60 mx 0 25 mm 1 00 pm D 5790 GC MS DBVRX 60mx0 25 mm 1 40 bm 122 1564 DBVRX 20mx0 18 mm 1 00 pm 21 1524 DB 624 60mx0 25 mm 1 4 um 22 1364 DB 624 20mx0 18 mm 1 00 bm 121 1324 D 5812 GC HP 5ms 30 mx 0 25 mm 0 25 bm 9091S 433 DB 1701P 30mx0 25mm 0 25 nm 122 7732 DB XLB 30mx0 25 mm 0 25 um 122 1232 DB 35ms 30mx0 25 mm 0 25 bm 22 3832 D 5917 GC HP INNOWax 19091N 116 60 mx 0 32 mm 0 25 um D 5974 GC DB 23 22 2362 60 mx 0 25 mm 0 25 bm D 5986 GC FTIR HP 1 9095Z 626 C8
193. HP 1ms Rtx 1ms Rxi 1ms VF 1ms CP Sil 5 CB Low Bleed MS MDN 1 AT 1 ZB 1ms Equity 1 DB 1ms mm m im C 0 10 10 0 10 60 340 360 27 0112 0 10 10 0 40 60 340 360 27 0113 0 10 20 0 10 60 340 360 27 0122 0 10 20 0 40 60 340 360 27 0123 0 18 20 0 18 60 340 360 121 0122 0 20 12 0 33 60 340 350 28 0112 0 20 25 0 33 60 340 350 28 0122 0 25 15 0 25 60 340 360 122 0112 0 25 30 0 10 60 340 360 122 0131 0 25 30 0 25 60 340 360 122 0132 0 25 60 0 25 60 340 360 122 0162 0 32 15 0 25 60 340 360 123 0112 0 32 30 0 10 60 340 360 123 0131 0 32 30 0 25 60 340 360 123 0132 0 32 60 0 25 60 340 360 123 0162 www agilent com chem jp 81 HP 1ms GH 100 HP 1 CH _ 100 lt S N DB 1ms Rtx 1ms Rxi 1ms VF 1ms CP Sil 5 CB Low Bleed MS MDN 1 AT 1 ZB 1ms Equity 1 HP 1ms mm m nm C 0 18 20 0 18 60 325 350 1909
194. 14 25 34 43 KN 8 Accustandard Inc 11 mm 5183 4759 4 mm 5181 3316 25 Science Park New Haven CT 06511 800 442 5290 10 23 26s 42 HP 5181 1267 Il EPA 8081A SS IS DB 5ms 250 C 122 5532 30 30 m x 0 25 mm 0 25 pm MSD 300 C 35 cm sec 50 C m z 50 500
195. x y x y z x z z y 2 t 1 100 EE RO y thc Ry 2b o 2 3 a 1 2 k 0 1 1 k 2 3 N 4 2 N N 5 545 ji h w 4 www agilent com chem jp 7
196. 120C 1 7 ero 25 C min 120 C 160 C 1 8 ln 9 10 C min 160 C 260 C tu 145 18 15 C min 260 C 300 C 4 mn st 19 220 C tu 35 psi 1 15 5e 07 20 de 07 ECD 320 C 3e 07 ArCH4 P5 ni 2 60 mL min 200 400 600 800 1000 1200 1400 16 00 2uL 50 ppb www agilent com chem jp Time min GCHE007 43 0 25 mm 0 18 mm 32 0 18 mm 77 A DB 5 625 122 5632 30 m x 0 25 mm 0 50 pm B DB 5 625 121 5622 20 m x 0 18 mm 0 36 nm He 1 1 mL min 40 C 1 320 C 25 C mn 4 80 300 C 0 5 OuickSwap 5 0 psi 80 0 psi 1 0 psi Agilent 5975C MSD 6 mm
197. IS 114 38 2 2 4 57 8 39 n 41 1 d 44 45 40 130 1 32 9 41 1 2 63 18 19 25 36 42 1 4 88 30 41 43 83 3 16 23 24 2 27 44 4 2 MIBK 43 20 2 45 cis 1 3 75 57 1 46 rans 1 3 75 8 14 33 47 91 1 ho 5 48 1 1 2 97 15 31 49 2 43 50 129 42 51 166 52 1 2 107 ee 2 4 7 1 5 6 9 10 11 12 13 14 5 91 me min 56 m 91 p 53 62 71 58 104 59 o 91 60 73 6 61 1 1 22 83 6 62 4 95 63 4 05 657 sg 64 1 3 5 105 65 1 2 4 05 31 5 66 1 3 146 67 91 68 1 4 146 69 1 2 146 70 1 2 4 80 71 225 4 15 16
198. 0 2 10 i E 1 5 PAT 26 200 5 150 4 5 23 27 6 25 0 1 7 9 102 13145 16 19 21 22 50 0 T 1 I I T I I 2 5 5 0 7 5 100 12 5 150 17 5 20 0 22 5 Time min 1 Heptane 10 Ehylbenzene 19 tButylbenzene 2 Cyclohexane 11 p Xylene 20 s Butylbenzene 3 Octane 12 m Xylene 21 Styrene 4 0nane 13 Cumene 22 Tridecane 5 Benzene 14 Dodecane 23 1 3 Diethylbenzene 6 Decane 15 o Xylene 24 1 2 Diethylbenzene 7 Toluene 16 Propylbenzene 25 n Butylbenzene 8 1 4 Dioxan 17 p Ethyltoluene 26 a Methylstyrene 9 Undecane 18 m Ethyltoluene 27 Phenylacetylene DA 225 200 2 175 3 4 24 150 23 125 5 6 25 27 100 9 1 16 18 20 75 7 10 12 13 1415 50 25 8 0 T T 0 0 5 1 0 15 2 0 2 5 3 0 3 5 4 0 4 5 Time min www agilent com chem jp GCHE003 57 HP PLOT 0 19095P 004 30 m
199. 2 5 STP 13 14 3 4 lt 14 min gt MDE Eve 15 GCLS004 16 www agilent com chem jp 71 72 DB 35ms 122 3832 dis IL 11 mm 5183 4759 31 cm sec 50 C 4 mm 5181 3316 50 C 05 18740 20885 25 C min 50 150 C 10 L 23 26s 42 HP 5181 1267 10 C min 150 300 C 250 C 0 30 1 MSD 280 C 7 m z 40 270 46 11 9 8 3 8 12 14 5 3 16
200. 3 Time min 15b DB 1 15 m x 0 25 mm 0 25 nm 1 9 30 cm sec 3 5 C min 40 60 C 60 C 3 5 C min 60 120 C 1 3 4 2 2 3 4 1 3 5 1 4 6 12 7 8 9 3 Time min 162 www agilent com chem jp
201. KCI C C ASTM KCI CP AL0 KCI PLOT Rt Alumina PLOT Alumina PLOT AL0 KCI HP PLOT AL0 KCI mm m um C 0 25 30 5 00 60 200 19091P K33 0 32 50 8 00 60 200 19091P K15 0 53 30 15 00 60 200 19095P K23 0 53 50 15 00 60 200 19095P K25 Deans www agilent com chem jp 130 GS Alumina KCI KCI
202. hm C 0 18 20 0 18 60 325 350 121 5621 0 18 20 0 36 60 325 350 121 5622 0 25 30 025 60 325 350 122 5631 025 30 050 60 325 350 122 5632 0 25 30 1 00 60 325 350 122 5633 0 25 60 0 25 60 325 350 122 5661 0 32 30 025 60 325 350 123 5631 0 32 30 050 60 325 350 123 5632 www agilent com chem jp Agilent J amp W DB VRX U S EPA 502 2 524 2 8260 0 45 mm 0 53 mm GC 6 30 0 18 mm 8
203. 00 60 190 19095P U04 www agilent com chem jp Agilent J amp W GC
204. 123 5563 0 53 15 1 50 60 300 320 125 5512 0 53 30 0 50 60 300 320 125 5537 0 53 30 1 00 60 300 320 125 553J 0 53 30 1 50 60 300 320 125 5532 HP 5ms 5 HP 5 GC MS S N USP Phase G27 DB 5ms Rtx 5MS Rtx 5 Amine PTE 5 CP Sil 8 CB Low Bleed MS BPX 5 ZB 5ms Equity 5 www agilent com chem jp HP 5ms mm m hm C 0 18 20 0 18 60 325 350 9091S 577 0 20 0 33 60 325 350 19091S 101 0 20 25 0 33 60 325 350 19091S 102 0 20 50 0 33 60 325 350 19091S 105 0 25 15 0 10 60 325 350 9091S 331 0 25 15 0 25 60 325 350 19091S 431 0 25 15 1 00 60 325 350 9091S 231 0 25 30 0 10 60 325 350 9091S 333 0 25 30 0 25 60 325 350 19091S 433 0 25 30 0 50 60 325 350 9091S 133 0 25 30 1 00 60 325 350 19091S 233 0 25 60 0 10 60 325 350 19091S 336 0 25 60 0 25 60 325 350 9091S 436 0 32 5 0 52 60 325 350 19091S 112 0 32 3
205. 17 18 19 20 21 22 23 24 25 26 27 28 Ti 54 me min GCEA002 www agilent com chem jp 11 mm 1 5183 4759 1 5 mm 18740 80200 18740 20885 C C GS GasPro 113 4362 60 mx0 32 mm 11 mm 5183 4759 CE NN 4 mm Ge 5181 3316 40 C 2 10 C min 40 120 C 18740 20885 120C 3min 23 26s 42 HP 5181 1267 10 C min 120 200 C 250 C 0 20
206. 1737 0 53 30 1 00 40 260 280 MM 32 0 53 30 1 50 40 260 280 2 SS 0 53 60 1 00 40 260 280 125 1762 HP 50 50 DB 17 USP Phase G3 DB 17 Rtx 50 CP Sil 24 CB 007 17 MPS 50 SP 2250 SPB 50 ZB 50 AT 50 HP 50 mm m hm C 0 18 20 0 18 40 280 300 9091L 577 0 20 12 0 31 40 280 300 19091L 101 0 25 5 0 15 40 280 300 9091L 330 0 25 15 0 25 40 280 300 9091L 431 0 25 30 0 15 40 280 300 9091L 333 0 25 30 0 25 40 280 300 9091L 433 0 25 30 0 50 40 280 300 9091L 133 0 32 15 0 50 40 280 300 19091L 111 0 32 30 0 25 40 280 300 19091L 413 0 32 30 0 50 40 280 300 19091L 113 0 32 60 0 25 40 280 300 19091L 416 0 53 15 1 00 40 260 280 19095L 021 0 53 30 0 50 40 260 280 19095L 523 0 53 30 1 00 40 260 280 19095L 023 www agilent com chem jp 101 DB 1301 DB 1701 DB 1301 6 DB 1301 SP Phase G43 DB 1701 14
207. 2 12 p 42 76 13 43 77 14 44 78 15 45 1 79 16 46 80 17 1 8 47 8g 81 18 3 5 5 46 2 83 19 3 49 4 84 n 20 2 50 85 21 51 86 22 52 87 23 p 53 90 24 54 91 25 55 92 26 56 gw
208. 2 15 meters 30 meters 60 meters www agilent com chem jp 1 3 1 2 8 3
209. 2 3 4 6 BDE BDE 71 28 Ns 4 2 2 4 4 BDE BDE 47 _ 201 5 23 4 4 BDE BDE 66 ECD 300 C 6 2 2 4 4 6 BDE BDE 100 2 5 mg ml 7 22 4 4 5 BDE BDE 99 1 8 22 3 4 4 BDE BDE 85 1 9 2 2 4 4 5 6 BDE BDE 154 10 2 2 4 4 5 5 BDE BDE 153 2 45 7 11 2 2 3 4 4 5 BDE BDE 138 3 6 12 2 2 3 4 4 5 6 BDE BDE 183 1 13 23 3 4 4 5 6 BDE BDE 190 BB 14 BDE BDE 209 12 5 mg mL BDE 209 PBDE Accustandard Inc New Haven CT I 0 2 4 6 8 10 12 Time min GCES003 48 www agilent com chem jp 1016 1268 1221 DB XLB 121 1232 30 m x 0 18 mm 0 18 nm 37 cm sec 150 C 100 C 1 1 2 C min 100 265 C 250 C MSD 340 C SIM 1 12 5 ppm 1 1 11 mm 5183 4759 0 4 30 0 0 90 0 10 110 120
210. 2607280 19095Z 421 Was 15 5 00 60 2607280 19095Z 621 0 30 088 60 300 320 19095Z 023 053 30 150 60 300 320 19095Z 323 6 30 265 60 2607280 19095Z 123 8 30 300 60 260 280 19095Z 423 053 30 500 602607280 190957 623 053 60 500 60 2607280 190957 626 dt CH LM 5 CHL se GH USP Phase G27 HP 5 Ultra 2 SPB 5 CP Sil 8 CB Rtx 5 BP 5 OV 5 007 2 MPS 5 SE 52 SE 54 XTI 5 PTE 5 HP 5MS ZB 5 Al 5 MDN 5 ZB 5 DB 5 mm m hm C 0 10 10 0 10 60 325 350 127 5012 0 10 10 0 17 60 325 350 127 501E 0 10 10 0 33 60 325 350 127 501N 0 10 10 0 40 60 325 350 127 5013 0 10 20 0 10 60 325 350 127 5022 0 10 20 0 40 60 325 350 127 5023 0 15 10 1 20 60 300 320 12A 5015 94 www agilent com chem jp DB 5 mm m hm C
211. 26s 42 HP 5181 1267 77 79 3 80 1 2 81 83 LN 4 14 16 18 20 22 24 Time min is 1 nm 23 2 4 45 67 2 24 46 2 4 68 d 14 3 2 25 2 47 4 69 4 d5 26 2 4 48 70 5 27 1 2 4 49 24 71 33 6 28 d8 50 72 a 7 2 29 51 4 73 d12 8 2 30 4 52 74 9 3 31 53 4 75 2 10 1 4 d4 32 4 3 54 4 6 2 76 n
212. 30 cm sec 8 40 C 2 10 C min 40 130 C 3 2 3 4 2 4 6 8 10 3 Time min MP N NN NN 13a DB 1 15 m x 0 25 mm 0 25 um 30 cm sec 5 C min 50 120 C 1 3 2 2 3 4 13 5 1 4 6 12 7 8 9 3 13b DB 1 15 m x 0 25 mm 0 25 nm 30 cm sec 40 C 2 3 2 1 3 1 4 1 2 3 COJPOSRIKODKCm J 63 3 160 5 C min 40 120 C
213. 30 m x 0 32 mm 0 25 Im 123 3832 8150 8151 DB XLB 30 mx 0 32 mm 0 50 hm 123 1236 N P 507 614 NPD DB 35ms 30 m x 0 25 mm 0 25 um 122 3832 619 622 ELCD DB 5ms 30 m x 0 25 mm 0 25 um 122 5532 8140 8141A FPD MSD MSD DB XLB 30 mx 0 18 mm 0 18 hm 121 1232 PBC DB XLB 60 mx 0 25 mm 0 25 um 122 1262 www agilent com chem jp 37 USP GC USP Agilent 61 HP 1 DB 1 HP 1ms DB 1ms 62 HP 1 DB 1 HP 1ms DB 1ms 63 50 50 DB 17 HP 50 65 3 DB 23 G6 DB 200 DB 210 67 50 3 50 DB 225 DB 225ms G14 DB WAX G15 3 000 3 700 DB WAX G16 15 000 DB WAX 617 75 25
214. 34 250 C 5183 4647 1 50 18740 20885 MSD 250 C 5 23 26s 42 HP 5181 1273 1 20 1 HL 1 31 p 65 2 32 66 3 33 cis 67 4 2 3 34 68 5 35 69 6 36 trans 70 7 oe 37 71 6 38 72 9 2 3 39 gw 73 1 10 40 74 1 11 41 75
215. 5 10 Tme imi 15 23 1 1 2 1 2 2 113 24 12 1 1 2 2 114B2 GC PAL 500 IV www agilent com chem jp 55 HP PLOT 0 19095P 004 30 m x 0 53 mm 40 00 nm 5 psi 8 mL min 35 C 250 1 3 TCD 200 C 200 ppmV 200 ppmV CO 250 ppmV N 0 N 0 ll HP PLOT 19095P MS6 30 m x 0 53 mm 25 00 nm 6 psi 10 mL min 50 C 5 min 25 C min 200 C 250 14 TCD 250 C 200 ppmV 200 ppmV CO 250 ppmV N 0 N 0 I GS CarbonPLOT 113 3133 30 m x 0 32 mm 3 00 nm 12 psi 3 mL min 35 C 250
216. 50 C 1 8081A Accustandard Inc 25 C mn 50 100 C 35 ug mL 1 0 5 C min 100 300 C 300 C 5 a 16 1 1 2 3 1 2 4 3 SS 1 3 sl Lz 2 3 gt 5 4 1 2 IS 7 5 10 3 6 2 7 50 2 SS m SS a 2 5 me min ll A 20 28 gt 36 44 SS 3 B 21 6 BHC 29 trans 37 45 4 22 30 ao 38 46 5 go BHC 23 31 39 pp DDD 47 6 IS 24 32 40 Il 48 7 yrBHC 25 33 pp DDE 41 pp DDT 49 cis 9 EPL 26 34 42
217. CAM mm m hm C 0 25 15 0 25 60 220 240 12 2112 0 25 30 0 25 60 220 240 112 2132 0 25 30 0 50 60 220 240 12 2133 0 25 60 0 25 60 220 240 12 2162 0 32 30 0 25 60 220 240 113 2132 0 32 30 0 50 60 220 240 113 2133 0 53 30 1 00 60 200 220 15 2132 Agilent GC Agilent GC Agilent J amp W GC ASTM CEN
218. CP Sil 19CB Rtx 1701 BP 10 CB 1701 OV 1701 007 1701 DB 1701P mm m nm C 0 25 30 0 25 20 280 300 122 7732 0 32 25 0 25 20 280 300 123 7722 032 30 0 25 20 280 300 123 7732 0 53 30 1 00 20 260 280 125 7732 www agilent com chem jp 121 PCB U S EPA 608 508 8080 HP 608 SPB 608 NON PAKD Pesticide 007 608 DB 608 mm m mm C 0 18 20 0 18 40 280 300 121 6822 0 25 30 0 25 40 280 300 122 6832 0 32 30 0 50 40 280 300 123 1730 0 45 30 0 70 40 260 280 124 1730 0 53 15 0 83 40 260 280 125 1710 0 53 30 050 40 260 280 125 6837 0 53 30 0 83 40 260 280 125 1730 wwwr agilent com chem jp www agilent com chem jp
219. D 1945 GC HP PLOT MoleSieve 15mx0 53 mm 50 nm 19095P MS9 HP PLOTO 15mx0 53 mm 40 bm 19095P 003 D 1946 GC HP PLOT MoleSieve 15mx0 53 mm 50 nm 19095P MS9 HP PLOTO 15mx0 53 mm 40 bm 19095P 003 D 1983 DB WAX 122 7032 30 mx 0 25 mm 0 25 nm D 2163 GC LP HP PLOT AO KCI 30 mx0 53 mm 15 nm 19095P K23 HP_PLOT AO S 30m x0 53 mm 15 pm 19095P 823 D 2268 GC n DB 122 106E 60 mx 0 25 mm 0 50 pm D 2306 GC C8 HP INNOW8x 19091N 136 60 mx 0 25 mm 0 25 um D 2426 GC DB 125 1035 30 mx 0 53 mm 5 00 bm D 2427 GC C2 C5 DB 1 30mx0 53 mm 5 00 um 125 1035 GS Alumina 30mx0 53mm 115 3532 D 2504 GC C2 HP PLOT MoleSieve 19095P MS0
220. PLOT U G46 14 86 DB 1701 38 www agilent com chem jp GC 40
221. mm 3 0 nm 30 mx 0 53 mm 3 0 pm 30 m x 0 53 mm 3 0 pm 1 0 18 0 25 mm 0 18 mm GC MS 0 32 mm gt 2 pL 0 25 mm 0 45 mm amp
222. x 0 25 mm 0 25 um 122 1232 DB 5ms 30 m x 0 53 mm 1 50 hm 125 5532 DB 608 30 m x 0 53 mm 0 50 hm 125 6837 506 606 ECD DB 5ms 30 mx 0 25 mm 0 25 hm 122 5532 8060 8061 FID DB 5ms 30 mx 0 53 mm 1 50 hm 125 5532 SPE DB 608 30 m x 0 53 mm 0 50 hm 125 6837 36 EPA PA Agilent 605 ECD DB 5ms 30 m x 0 25 mm 0 25 Im 122 5532 DB 5ms 30 m x 0 53 mm 1 50 um 125 5532 DB 608 30 mx 0 53 mm 0 50 pm 125 6837 607 8070 NPD DB 5ms 30 m x 0 25 mm 0 25 um 122 5532 SPE DB 5ms 30 m x 0 53 mm 1 50 pm 125 5532 609 8090 ECD
223. 0 60 325 350 123 5053 0 32 60 0 25 60 325 350 123 5062 0 32 60 1 00 60 325 350 123 5063 5 www agilent com chem jp 95 DB 5 mm m mm C 0 45 15 1 27 60 300 320 124 5012 0 45 30 0 42 60 300 320 124 5037 0 45 30 1 27 60 300 320 124 5032 0 53 10 2 65 60 260 280 125 50HB 0 53 15 0 25 60 300 320 125 501K 0 53 15 050 60 300 320 125 5017 0 53 15 1 00 60 300 320 125 501J 0 53 15 1 50 60 300 320 125 5012 0 53 25 5 00 60 260 280 125 5025 0 53 30 0 25 60 300 320 125 503K 0 53 30 0 50 60 300 320 125 5037 0 53 30 0 88 60 300 320 125 503D 0 53 30 1 00 60 300 320 125 503J 0 53 30 1 50 60 300 320 125 5032 0 53 30 2 65 60 260 280 125 503B 0 53 30 3 00 60 260 280 125 5034 0 53 30 5 00 60 260 280 125 5035 0 53 60 1 50 60 300 320 125 5062 0 53 60 5 00 60 260 280 125 5065 HP 5 5 USP Phase G27 DB 5 Ultra 2 SPB 5 CP Sil 8 CB Rtx 5 BP 5 OV 5 007 2 MPS 5 SE 52 SE 54 XTI 5 PTE 5 HP 5MS ZB 5 Al 5 MDN 5 Z
224. 0 0 10 60 325 350 19091S 313 0 32 30 0 25 60 325 350 19091S 413 0 32 30 0 50 60 325 350 19091S 113 0 32 30 1 00 60 325 350 19091S 213 0 32 60 0 25 60 325 350 19091S 416 DB XLB 340 360 C PCB PAHs GC MS MSD DB XLB MS PCB Frame G Analytical Chemistry News amp Features Aug 1 1997 468A 475Aj Rtx XLB MDN 12 www agilent com chem jp 85 DB XLB mm m hm C 0 18 20 0 18 30 340 360 121 1222 0 18 30 0 18 30 340 360 121 1232 0 20 12 0 33 30 340 360 128 1212 0 20 25 0 33 30 340 360 128 1222 0 25 15 0 10 3
225. 0 145 1001 www agilent com chem jp 123 GC DB 5 625 5 EPA 625 1625 8270 CLP EPA 2 4 N XTI 5 Roc5 PTE 5 BPX5 DB 5 625 mm m
226. 0 18 20 250 260 121 7042 0 18 40 0 30 20 240 250 121 7043 0 20 25 0 20 20 250 260 128 7022 0 20 30 0 20 20 250 260 128 7032 0 20 50 0 20 20 250 260 128 7052 www agilent com chem jp DB WAX DB WaxFF mm m mm C 0 25 15 0 25 20 250 260 122 7012 0 25 15 0 50 20 240 250 122 7013 0 25 30 0 15 20 250 260 122 7031 0 25 30 0 25 20 250 260 122 7032 0 25 30 0 50 20 240 250 122 7033 0 25 60 0 15 20 250 260 122 7061 0 25 60 0 25 20 250 260 122 7062 0 25 60 0 50 20 240 250 122 7063 0 32 15 0 25 20 250 260 123 7012 0 32 a 0 50 20 240 250 123 7013 0 32 30 0 15 20 250 260 123 7031 0 32 30 0 25 20 250 260 123 7032 0 32 30 0 50 20 240 250 123 7033 0 32 60 0 25 20 250 260 123 7062 0 32 60 0 50 20 240 250 123 7063 0 45 30 0 85 20 230 240 124 7032 0 53 15 0 50 20 230 240 125 7017 0 53 1 00 20 230 240 125 7012 0 53 30 0 25 20 230 240 125 7031 0 53 30 0 50 20 230 240 125 7037 0 53 30 1 00 20 230 240 125 7032 0 53 60 1 00 20 230 240 125 7062 DB WaxFF 0 10 20 0 20 20 240 250 127 7023FF Agilent Agilent GC www agilent com chem jp www agilent c
227. 0 2 5 mL min 5181 1273 1 0 1 7 mL min 325 C 0 8 60 mL min 45 C 0 8 45 C mn 45 200 C 2 5 C mn 200 C 225 C 3 C min 225 266 C 5 C mn 266 300 C 10 C min 300 320 C 320 C 45 MSD 300 C 180 C 330 C m z 50 550 1 c Agilent J amp W DB EUPAH 2 a 3 cd 14000 4 00 5 5 12000 65 b Rs24 7 ki 1 6 10000 9 a 9000 1 2 3 cd 8000 a h 7000 gh 6000 la 5000 ae al 4000 ah 3000 2000 1000 0 T T Tj T TT TT 10 00 15 00 20 00 25 00 30 00 35 00 40 00 Time EU_PAHs 15 1 EU PAHs DB EUPAH
228. 0 340 360 122 1211 0 25 15 0 25 30 340 360 122 1212 0 25 30 0 10 30 340 360 122 1231 0 25 30 0 25 30 340 360 122 1232 0 25 30 0 50 30 340 360 122 1236 0 25 30 1 00 30 340 360 122 1233 0 25 60 0 25 30 340 360 122 1262 0 32 30 0 25 30 340 360 123 1232 0 32 30 0 50 30 340 360 123 1236 0 32 60 0 25 30 340 360 123 1262 0 53 15 1 50 30 320 340 125 1212 0 53 30 1 50 30 320 340 125 1232 DB 35ms CH CHi CH 35 0 si 1 0 CHi OH GC MS 340 360 C 1 4 bis HP35ms USP Phase G42 Rtx 35 Rtx 35ms VF 35ms SPB 35 Al 35 Sup Herb MDN 35 BPX 35 86 www agilent com chem jp DB 35ms mm m nm C 0 18 20 0 18 50 340 360 21 3822 0 20 15 0 33 50 340 360 28 3812 0 20 25 0 33 50 340 360 128 3822 0 25 15 0 25 50 340 360 22 3812 0 25 30 0 15 50 340 360 22 3831 0 25 30 0 25 50 340 360 22 3832 0 25 60 0 25 50
229. 0 PFPD i 7 Thiophene 1 ppm 0 8 Dimethyl sulfide 9 2 Propanethiol 2 5 10 34 10 1 Propanethiol 11 2 Methyl2 propanethigl 12 12 2 Methyl 1 propanethiol 13 1 Methyl 1 propnaethiol 3 14 1 Butanethiol 2 4 6 8 10 12 14 16 18 Time min DB Petro 122 10A6 1 Methane 18 p Xylene 2 n Butane 19 o Xylene NSIM pm 3 lsopentane 20 n Nonane 25 6 cm sec 4 n Pentane 21 lsopropylbenzene 5 n Hexane 22 Propylbenzene 0 C 15 6 Methylcyclopentane 23 1 2 4 Trimethylbenzene 1 2C mnm 0 50 C 7 Benzene 24 lsobutylbenzene 2cC mm 50 130 C 8 Cyclohexane 25 sec Butylbenzene UI CN 9 lsooctane 26 n Decane 4C mn 130 180 C 10 n Heptane 27 1 2 3 Timethylbenzene 180 C 20 11 Toluene 28 Butylbenzene 200 C 5 1 1 3 2 MethyIheptane 1 2 4 5 letramethylbenzene ia i OD 14 4 Methylheptane 31 Naphthalene 9 15 n Octane 32 Dodecane 16 Ehylbenzene 33 Tridecane 30 mL min 17 m Xylene I 12 78 18 87 17 18 2 34 5 6 7 10 11 12 16 19 23 24 25 26 8 27 22 9 28 29 31 15 33 14 2071 32 130 min GCPE032 www agilent com chem j
230. 0 pg mL 1 Phenol 2 2 Chlorophenol 3 2 Nitrophenol 4 2 4 Dimethylphenol 5 2 4 Dichlorophenol 6 4 Chloro 3 methylphenol 7 2 4 6 Irinitrophenol 8 2 4 Dinitrophenol 9 4 Nitrophenol 10 2 Methyl 4 6 dinitrophenol 11 Pentachlorophenol 11 mm 4 mm G 18740 10 4 10 1 7 16 www agilent com chem jp 1 544 80730 5183 4759 20885 23 26s 42 HP 5181 1267 23 24 69 GS GasPro 113 4332 30 m x 0 32 mm 53 cm sec 25 C 3 10 C min 25 200 C 200 C 200 C 1 50 TCD 250 C 50 LL 11 mm 5183 4759 1 5 mm 18740 80200 18740 20885 Time min www agilent com chem jp 13 GCIC058 C0 SF COS HS
231. 032 0 53 30 2 65 60 260 280 125 103B 0 53 30 3 00 60 260 280 125 1034 0 53 30 5 00 60 260 280 125 1035 0 53 50 5 00 60 260 280 125 1055 0 53 60 1 00 60 300 320 125 106J 0 53 60 1 50 60 300 320 125 1062 0 53 60 3 00 60 260 280 125 1064 0 53 60 5 00 60 260 280 125 1065 0 53 105 5 00 60 260 280 125 10B5 HP 1 100 lt C5 USP Phase G2 DB 1 Ultra 1 SPB 1 CP Sil 5 CB Rtx 1 BP 1 OV 1 OV 101 007 1 MS SP 2100 SE 30 CP Sil 5 CB MS ZB 1 AT 1 MDN 1 ZB 1 www agilent com chem jp HP 1 mm m hm C 0 18 20 0 18 60 325 350 190912 577 0 20 12 0 33 60 325 350 19091 60312 0 20 17 0 11 60 325 350 190912 008 0 20 25 0 11 60 325 350 19091Z 002 0 20 25 0 33 60 325 350 19091Z 102 0 20 25 0 50 60 325 350 19091Z 202 0 20 50 0 11 60 325 350 19091Z 005 0 20 50 0 33 60 325 350 19091Z 105 0 20 50 0 50 60 325 350 1
232. 12 0 53 30 0 50 40 200 220 125 2237 0 53 30 1 00 40 200 220 125 2232 www agilent com chem jp 103 DB 200 35 1 300 320 C DB 1701 DB 17 CH ln ECD USP Phase G6 Rtx 200 VF 200ms DB 200 mm m um C 0 25 30 0 25 30 3007320 122 2032 0 25 30 0 50 30 300 320 122 2033 0 32 30 0 25 30 300 320 123 2032 0 32 30 0 50 30 300 320 123 2033 0 53 30 1 00 30 280 300 125 2032 104 www agilent com chem jp DB 23 50 CH FAMEs S HP 23
233. 1S 677 0 20 25 0 33 60 325 350 19091S 602 0 25 15 0 25 60 325 350 19091S 931 0 25 30 0 10 60 325 350 19091S 833 0 25 30 0 25 60 325 350 19091S 933 0 25 30 0 50 60 325 350 19091S 633 0 25 30 1 00 60 325 350 19091S 733 0 25 60 0 25 60 325 350 19091S 936 0 32 15 0 25 60 325 350 19091S 911 0 32 25 0 52 60 325 350 19091S 612 0 32 30 0 25 60 325 350 19091S 913 0 32 30 1 00 60 325 350 19091S 713 0 32 60 025 60 325 350 19091S 916 82 www agilent com chem jp DB 5ms 5 F CH CH GC MS CO CC S N 1 4 b MSD HP 5TA USP Phase G27 Rtx 5ms Rtx 5Sil MS Rxi 5ms Rxi 5Sil MS VF 5ms PTE 5 CP Sil 8 CB Low Bleed MS BPX 5 Al 5ms ZB 5ms SLB 5ms Equity 5
234. 2 14 16 Time min GCIC041 31 cm sec 50 C 5 10 C min 50 160 C 250 C 1 100 FID 300 C 30 mL min 0 5 pg uL 0 5 1 14 tert 2 15 sec 3 16 4 17 1 3 5 p 18 1 4 6 m 19 n 7 o 20 1 2 6 21 13 9 22 1 4 10 n 23 2 11 2 24 3 12 3 25 4 13 4 HP 5ms 19091S 433 30 m x 0 25 mm 0 25 pm 33 cm sec 35 C 5 8 C mn 35 220 C 250 C FID 300 C 1 2
235. 25 mm 0 25 nm Agilent 7890A 5975B MSD 6890N FI Agilent 7683B 5 0 pL 5188 5246 1 0 40 cm s MSD 35 cm s FID 200 1 62 C 12 5 3 C min 62 92 C 5 C min 92 165 C 100 C min 165 310 C 310 C 2 5 MSD 300 C 180 C 280 C m z 45 550 11 mm 5183 4759 6576 MS 5188 5 23 26s 42 HP 5181 1273 1 og 19 2 20 3 1 3 21 cis 4 3 22 5 23 6 3 24 7 o 25 6 26 9 D 27 0 g
236. 3 0 53 30 1 50 60 300 320 9095J 323 0 53 30 2 65 60 260 280 9095J 123 0 53 30 5 00 60 260 280 9095J 623 www agilent com chem jp J 97 98 Ultra 1 100 HP 1 DB 1 HP 1 SPB 1 CP Sil 5 CB Rtx 1 BP 1 007 1 MS Ultra 1 mm m um C 0 20 12 0 33 60 325 350 19091A 101 0 20 25 0 11 60 325 350 19091A 002 0 20 25 0 33 60 325 350 19091A 102 0 20 50 0 11 60 325 350 19091A 005 0 20 50 0 33 60 325 350 19091A 105 0 32 5 0 17 60 325 350 19091A 012 0 32 25 0 52 60 325 350 19091A 112 0 32 50 0 17 60 325 350 19091A 015 0 32 50 0 52 60 325 350 19091A 115 Ultra 2 5 HP 5 DB 5 HP 5 SPB 5 CP Sil 8 CB Rtx 5 BP 5 CB 5 007 5 2B 5 www agilent com chem jp Ultra 2
237. 3 0 MSD 300 C 180 C 290 C m z 50 550 1 0 5 5 nu 4 mm G1544 80700 0 5 23 5188 5246 6 2 16 17 ONDON PR 10 00 15 00 20 00 25 00 Time min 30 00 www agilent com chem jp EPA8270 2 4 DB 5ms DB5msPeaks N g 1 4 D4 1 4 D8 D10 2 4
238. 32 GC HP PLOTO 15mx0 53 mm 40 um 19095P 003 D 4983 GC HP 5ms 30 m x 0 32 mm 1 00 nm 19091S 213 I CAM 30mx0 53 mm 1 pm 15 2132 D 5008 GC 2 HP 1 15mx0 53 mm 5 00 um 19095Z 621 HP INNOWax 30 mx0 32 mm 0 25 pm 9091N 113 D 5060 GC HP INNOW8x 9091N 216 60 mx 0 32 mm 0 5 pm D 5075 DB 5 30mx0 53 mm 1 50 bm 125 5032 DB 5 30mx0 32 mm 1 00 um 123 5033 D 5134 GC n HP PONA 9091S 001 50 m x 0 20 mm 0 5 um D 5135 GC HP INNOWax 9091N 216 60 m x 0 32 mm 0 5 um D 5175 GC DB 1 30mx0 32 mm 1 00 nm 23 1033 DB 608 30mx0 32 mm 0 5 um 123 1730 DB XLB 30mx0 25mm 0 25 um 22 1232 D 5303 GC G
239. 340 360 22 3862 0 32 0 25 50 340 360 23 3812 0 32 30 0 25 50 340 360 123 3832 0 53 30 0 50 50 320 340 25 3837 0 53 30 1 00 50 320 340 25 3832 DB 17ms 50 320 340 C GC MS CIP HP 50 Rtx 50 VF 17ms 007 17 SP 2250 SPB 50 BPX 50 SPB 17 AT 50 DB 17ms mm m mm C 0 18 20 0 18 40 320 340 21 4722 0 25 15 0 15 40 320 340 22 4711 0 25 0 25 40 320 340 122 4712 0 25 30 0 15 40 320 340 122 4731 0 25 30 0 25 40 320 340 22 4732 0 25 60 0 25 40 320 340 122 4762 0 32 15 0 25 40 320 340 23 4712 032 30 025 40 320 340 23 4732 www agilent com chem jp 87 DB 225ms 50 FAME USP Phase G7
240. 350 128 1022 0 20 50 0 33 60 325 350 128 1052 0 25 15 0 10 60 325 350 122 1011 0 25 15 0 25 60 325 350 122 1012 0 25 15 1 00 60 325 350 122 1013 0 25 25 0 25 60 325 350 122 1022 0 25 30 0 10 60 325 350 122 1031 0 25 30 0 25 60 325 350 122 1032 0 25 30 0 50 60 325 350 122 103E 0 25 30 1 00 60 325 350 122 1033 0 25 50 0 25 60 325 350 122 1052 0 25 60 0 10 60 325 350 122 1061 0 25 60 0 25 60 325 350 122 1062 0 25 60 0 50 60 325 350 122 106E 0 25 60 1 00 60 325 350 122 1063 0 25 100 0 50 60 325 350 122 10AE 0 25 150 1 00 60 325 350 122 10G3 5 www agilent com chem jp DB 1 mm m hm C 0 32 15 0 10 60 325 350 23 1011 0 32 15 0 25 60 325 350 23 1012 0 32 15 1 00 60 325 350 23 1013 0 32 15 3 00 60 280 300 23 1014 0 32 15 5 00 60 2807300 23 1015 0 32 25 0 12 60 325 350 23 1027 0 32 25 0 25 60 325 350 23 1022 0 32 25 0 52 60 325 350 23 1026 0 32 25 1 05 60 325 350 23 102F 0 32 30 0 10 60 325 350 23 1031 0 32 30 0 25 60 325 350 23 1032 0 32 30 0 50 60 325 350 123 103E 0 32 30 1 00 60 325 350 23 1033 0 32 30 1 50 60 300 320 123 103B 0 32 30 3 00 60 280 300 23 1034 0 32 30 5 00 60 280 300 23 1035 0 32 50 0 2
241. 5 k H H 5 mm IN N 5 www agilent com chem jp UTE CE 6 Ha UTE x 100 Heoretical 6 H
242. 5 60 325 350 23 1052 0 32 50 0 52 60 325 350 23 1056 0 32 50 1 05 60 325 350 123 105F 0 32 50 1 20 60 325 350 123 105C 0 32 50 5 00 60 280 300 23 1055 0 32 60 0 10 60 325 350 23 1061 0 32 60 0 25 60 325 350 23 1062 0 32 60 0 50 60 325 350 123 106E 0 32 60 1 00 60 325 350 23 1063 0 32 60 1 50 60 300 320 123 106B 0 32 60 2 00 60 280 300 123 106G 0 32 60 3 00 60 280 300 23 1064 0 32 60 5 00 60 280 300 23 1065 0 45 30 2 60 325 350 124 1032 0 45 30 2 55 60 260 280 124 1034 0 53 5 2 65 60 325 350 125 100B 0 53 5 5 00 60 325 350 25 1005 0 53 7 5 1 50 60 325 350 25 1002 0 53 10 2 65 60 260 280 25 10HB 0 53 10 5 00 60 260 280 125 10H5 0 53 15 0 15 60 340 360 25 1011 0 53 15 0 25 60 320 340 25 101K 0 53 15 0 50 60 300 320 25 1017 0 53 15 1 00 60 300 320 125 101J www agilent com chem jp 91 QI CH 100 92 DB 1 mm m hm C 0 53 15 1 50 60 300 320 125 1012 0 53 15 3 00 60 260 280 125 1014 0 53 15 5 00 60 260 280 125 1015 0 53 25 1 00 60 300 320 125 102J 0 53 25 5 00 60 260 280 125 1025 0 53 30 0 10 60 340 360 125 1039 0 53 30 0 25 60 320 340 125 103K 0 53 30 0 50 60 300 320 125 1037 0 53 30 1 00 60 300 320 125 103J 0 53 30 1 50 60 300 320 125 1
243. 60 325 350 122 5513UI 0 25 25 0 25 60 325 350 122 5522UI 0 25 30 0 25 60 325 350 122 5532UI 0 25 30 0 50 60 325 350 122 5536UI 0 25 30 1 00 60 325 350 122 5533UI 0 25 50 0 25 60 325 350 122 5552UI 0 25 60 0 25 60 325 350 122 5562UI 0 25 60 1 00 60 325 350 122 5563UI 0 32 30 0 25 60 325 350 123 5532UI 0 32 30 0 50 60 325 350 123 5536UI 0 32 30 00 60 325 350 123 5533UI 0 32 60 1 00 60 325 350 123 5563UI HP 5ms 0 18 20 0 18 60 325 350 9091S 577U 0 25 15 0 25 60 325 350 19091S 431UI 0 25 30 0 25 60 325 350 19091S 433UI 0 25 30 0 50 60 325 350 19091S 133UI 0 25 30 1 00 60 325 350 19091S 233UI 0 25 60 0 25 60 325 350 19091S 436UI 0 32 30 0 25 60 325 350 9091S 413UI 0 32 30 1 00 60 325 350 19091S 213UI www agilent com chem jp 77 Agilent J amp W GC GC GC MS He H 20 Agilent Agilent J amp W
244. 9091Z 205 0 25 15 0 10 60 325 350 9091Z 331 0 25 15 0 25 60 325 350 9091Z 431 0 25 15 1 00 60 325 350 9091Z 231 0 25 30 0 10 60 325 350 9091Z 333 0 25 30 0 25 60 325 350 9091Z 433 0 25 30 1 00 60 325 350 9091Z 233 0 25 60 0 25 60 325 350 9091Z 436 0 25 60 1 00 60 325 350 9091Z 236 0 25 100 0 50 60 325 350 9091Z 530 0 32 15 0 25 60 325 350 19091Z 411 0 32 15 1 00 60 325 350 19091Z 211 0 32 25 0 17 60 325 350 19091Z 012 0 32 25 0 52 60 325 350 19091Z 112 0 32 25 1 05 60 325 350 19091Z 212 0 32 30 0 10 60 325 350 190912 313 0 32 30 0 25 60 325 350 19091Z 413 0 32 30 1 00 60 325 350 19091Z 213 0 32 30 3 00 60 260 280 19091Z 513 0 32 30 4 00 60 260 280 19091Z 613 0 32 30 5 00 60 260 280 19091Z 713 0 32 50 0 17 60 325 350 19091Z 015 0 32 50 0 52 60 325 350 190912 115 0 32 50 1 05 60 325 350 190912 215 0 32 60 0 25 60 325 350 19091Z 416 0 32 60 1 00 60 325 350 19091Z 216 0 32 60 5 00 60 260 280 19091Z 716 0 53 5 0 15 60 320 400 19095Z 220 0 53 5 0 88 60 320 400 19095Z 020 0 53 5 2 65 60 260 280 19095S 100 0 53 7 5 5 00 60 260 280 19095Z 627 www agilent com chem jp 93 HP 1 mm m um C 053 10 088 60 300 320 19095Z 021 053 10 265 60 2607280 190957 121 9 15 0 15 60 320 400 19095Z 221 9 15 1 50 60 300 320 19095Z 321 053 15 300 60
245. 989 0094EN 250 pnb in 10 00 11 00 2 00 13 00 GCES014 www agilent com chem jp 49 50 EPA 8270 HP 5ms 40 C 1 0 mn 19091S 133 15 C min 40 100 C 30 m x 0 25 mm 0 50 pm 20 C min 100 240 C 0 0 1 2 mmn UP 99mLmin 2 0 mL min ND 0 35 20 mL min 0 35 min 30 mL min 10 mLmn 1 2 mL min NN 35 500 m z 3 25 sec 50 ng 1 75 62 67 45 i 11 mm 68 69 74 5183 4759 4 mm 5181 3316 10 1 23
246. B 5 96 www agilent com chem jp HP 5 mm m hm C 0 18 20 0 18 60 325 350 19091J 577 0 20 12 0 33 60 325 350 19091J 101 0 20 25 0 11 60 325 350 19091J 002 0 20 25 0 33 60 325 350 19091J 102 0 20 25 0 50 60 325 350 19091J 202 0 20 50 0 11 60 325 350 19091J 005 0 20 50 0 33 60 325 350 19091J 105 0 20 50 0 50 60 325 350 19091J 205 0 25 5 0 10 60 325 350 9091J 330 0 25 15 0 25 60 325 350 9091J 431 0 25 15 1 00 60 325 350 9091J 231 0 25 30 0 10 60 325 350 9091J 333 0 25 30 0 25 60 325 350 9091J 433 0 25 30 1 00 60 325 350 9091J 233 0 25 60 0 25 60 325 350 9091J 436 0 25 60 1 00 60 325 350 9091J 236 0 32 15 0 25 60 325 350 19091J 411 0 32 25 0 17 60 325 350 19091J 012 0 32 25 0 52 60 325 350 19091J 112 0 32 25 1 05 60 325 350 19091J 212 0 32 30 0 10 60 325 350 19091J 313 0 32 30 0 25 60 325 350 19091J 413 0 32 30 0 50 60 325 350 19091J 113 0 32 30 1 00 60 325 350 19091J 213 0 32 50 0 17 60 325 350 19091J 015 0 32 50 0 52 60 325 350 19091J 115 0 32 50 1 05 60 325 350 19091J 215 0 32 60 0 25 60 325 350 19091J 416 0 32 60 1 00 60 325 350 19091J 216 0 53 10 2 65 60 260 280 9095J 121 0 53 15 1 50 60 300 320 9095J 321 0 53 15 5 00 60 260 280 9095J 621 0 53 30 0 88 60 300 320 9095J 02
247. B 5 0 18 20 0 40 60 325 350 121 5023 DB 5 0 18 40 0 18 60 325 350 121 5042 HP 5 0 18 20 0 18 60 325 350 19091J 577 DB 5ms 0 18 20 0 18 60 325 350 121 5522 DB 5ms 0 18 20 0 36 60 325 350 121 5523 DB 5ms 0 18 40 0 18 60 325 350 121 5542 HP 5ms 0 18 20 0 18 60 325 350 19091S 577 DB XLB 0 18 20 0 18 30 340 360 121 1222 DB XLB 0 18 30 0 18 30 340 360 121 1232 DB 35ms 0 18 20 0 18 50 340 360 121 3822 DB 17 0 18 20 0 18 40 280 300 121 1722 DB 17 0 18 20 0 30 40 280 300 121 1723 DB 17ms 0 18 20 0 18 40 320 340 121 4722 HP 50 0 18 20 0 18 40 280 300 19091L 577 DB 23 0 18 20 0 20 40 250 260 121 2323 DB 225 0 18 20 0 20 40 220 240 121 2223 DB 624 0 18 20 1 00 20 280 121 1324 DB 1301 0 18 10 0 40 20 280 300 121 1313 DB 1701 0 18 10 0 40 20 280 300 121 0713 DB 1701 0 18 20 0 18 20 280 300 121 0722 DB WAX 0 18 10 0 18 20 250 260 121 7012 DB WAX 0 18 20 0 18 20 250 260 121 7022 DB WAX 0 18 40 0 18 20 250 260 121 7042 DB WAX 0 18 40 0 30 20 240 250 121 7043 HP INNOWax 0 18 20 0 18 40 260 270 19091N 577 DB 5 625 0 18 20 0 18 60 325 350 121 5621 DB 5 625 0 18 20 0 36 60 325 350 121 5622 DB VRX 0 18 20 1 00 10 260 121 1524 DB VRX 0 18 40 1 00 10 260 121 1544 DB 608 0 18 20 0 18 40 280 300 121 6822 www agilent com chem jp 79 GC MS
248. C12 60 mx0 53 mm 5 00 um D 6144 GC g HP 1 19091Z 236 60 mx 0 25 mm 1 00 bm D 6159 GC HP PLOTAI203 KCI 50mx0 53 mm 15 nm 9095P K25 GS Alumina 115 3552 50 m x 0 53 mm DB 1 50mx0 53 mm 125 1035 D 6160 GC PCB HP 5ms 30 m x 0 32 mm 0 25 nm 9091S 413 DB XLB 30mx0 25 mm 0 25 um 122 1232 D 6352 GC 174 700 C DB HT SimDis 45 1001 5 m x 0 53 mm 0 15 um D 6417 GC DB HT SimDis 145 1001 5 m x 0 53 mm 0 15 um D 2360 GC HP INNOWax 19091N 116 60 mx 0 32 mm 0 25 nm E 1616 GC
249. O 30 mx 0 53 mm 50 pm www agilent com chem jp 31 ASTM D 2505 GC GS GasPro 113 4362 60 mx 0 32 mm D 2593 GC GS Alumina 115 3532 30 m x 0 53 mm D 2712 GC GS Alumina 115 3552 50 m x 0 53 mm D 2804 GC DB WAX 30mx0 45 mm 0 85 nm 124 7032 DB 210 15 mx 0 53 mm 1 pm 125 0212 D 2887 GC DB 2887 125 2814 10 m x 0 53 mm 3 nm ExtendedD GC HP 1 10mx0 53 mm 0 88 um 19095Z 021 288 C60 HP1 5mx053 mm 0 88 pm 19095Z 020 D 3054 GC
250. P PLOT Molesieve GS GasPro PLOT GC GasPro Primary Selectivity Interactions in PLOT Phases Dispersive Shape Size yw lonic Surface Zeolites Alumina Al20 GS 0xyPLOT Dispersive Shape Size cy lonic Surface Bonded Graphitized Carbon Porous Polymers Bonded Silica Molecular Sieves PLOT Column Examples Zeolite Molesieve HP PLOT Molesieve Graphitzed Bonded Carbon GS CarbonPLOT Porous Ploymers HP PLOT 0 HP PLOTU Bonded Silica GS GasPro Alumina Al203 GS Alumina GS Alumina KCIL HP PLOT Al0 KCI HP PLOT Al203 S HP PLOT Al0 MY Proprietary Phase GS OxyPLOT 1 DB 1 DB 5 2 ms 3
251. Pentachloroethane 26 1 2 Dibromo 3 chloropropane DBCP 27 Hexachloroethane 28 Hexachlorocyclopentadiene 68 2 3 11 mm 5183 4759 5183 4711 18740 20885 23 26s 42 HP 5181 1267 10 10 19 1 16 18 12 1 20 21 15 27 26 22 10 15 Time min www agilent com chem jp 20 25 GCIC034 DB 200 122 2032 30 m x 0 25 mm 0 25 pm 11 mm 1 5183 4759 10 5183 4711 18740 20885 23 26s 42 HP 5181 1267 34 131 15 5 yl 22 20 2 6 7 1718 23 24 25 _MLL UL 2 4 6 8 10 1
252. S GasPro 113 4332 30 mx 0 32 mm HP PLOTO 30mx0 53 mm 40 bm 19095P 004 D 5307 GC HP 1 19095Z 627 7 5 mx 0 53 mm 5 00 bm www agilent com chem jp 33 ASTM D 5310 GC HP 5ms 30 mx 0 25 mm 0 25 nm 19091S 433 DB 225ms 30mx0 25mm 025Hm 122 2932 D 5316 GC 1 2 HP 1ms 30 mx0 32 mm 1 00 um 19091S 713 1 2 3 DB 624 30mx0 45 mm 2 55 pm 124 1334 D 5317 GC HP 5ms 30 m x 0 25 mm 0 25 pm 19091S 433 DB 1701P 30mx0 25mm 0 25nm 122 7732 DBXLB 30mx0 25 mm 0 25 pm 122 1232 DB 35ms 30mx0 25 mm 0 25 pm 122 3832 D 5320 DB 1 30mx0 53 mm 3 00 bm 125 1034 1 1
253. Wax Rtx WAX ZB WAX VF WAXms CAM 60 220 240 Stabilwax DB Carbowax Amine HP FFAP DB FFAP 40 250 0V351 SP 1000 Sitabilwax FN WU DA 007 FFAP Nukol DB 23 FAME cis trans 50 50 40 250 260 SP 2330 Rtx 2330 007 23 AT Silar BPX 70 SP 2340 VF 23ms CycloSil 8 DB 1701 30 35 260 280 LIPODEX C RLZ DEXm B DEX 28 2 0 3 HOHe 110 8 DEX 120 HP 30 240 250 LIPODEX C Rt DEXm DEX NPD p 110 DEX 120 28 www agilent com chem jp GC C PLOT HP PLOT Molesieve 35 C 5A
254. ent com chem jp t Agilent 7890A PP GC W www agilent com chem GC7890Ajp es cw W SN W Te tj
255. om chem jp 109 DB WAXetr PEG etr Extended Temperature Range USP Phase G16 HP 20M SUPELCOWAX 10 CP WAX 52 CB SUPEROX IL CB WAX Stabilwax BP 20 007 CW Carbowax HP INNOWax ZB WAX DB WAXetr mm m hm C 0 20 25 0 40 30 250 260 128 7323 0 25 30 0 25 30 260 280 122 7332 0 25 30 0 50 30 250 260 122 7333 0 25 60 0 25 30 260 300 122 7362 0 25 60 0 50 30 250 260 122 7363 0 32 15 0 25 30 260 280 123 7312 0 32 15 1 00 30 250 260 123 7314 0 32 30 0 25 30 260 280 23 7332 0 32 30 0 50 30 250 260 123 7333 0 32 30 1 00 30 250 260 123 7334 0 32 50 00 30 250 260 23 7354 0 32 60 0 25 30 260 280 123 7362 0 32 60 0 50 30 250 260 23 7363 0 32 60 00 30 250 260 23 7364 0 53 15 1 00 30 240 260 125 7312 0 53 15 2 00 50 230 250 125 7314 0 53 30 1 00 30 240 260 125 7332 0 53 30 1 50 30 230 240 125 7333 0 53 30 2 00 50 230 250 125 7334 0 53 60 1 00 30 240 260 125 7362 110 www agilent com chem jp HP INNOWax PEG PEG
256. p 59 n DB HT SimDis 145 1001 5 m x 0 53 mm 0 15 nm 18 mL min 35 C 10 C min 30 430 C OPTIC PTV 2 C sec 55 450 C FID 450 C 15 mL min CS 2 n 0 5 10 ll 16 20 50 40 60 32 70 24 28 30 I I 5 10 15 I I 20 25 30 35 40 45 Time min GCPE038 61 A DB 1 A 25 cm sec 40 C 122 1032 B 47 cm sec 40 C 30 m x 0 25 mm 0 25 hm A 40 C 1 5 C min 290 C B DB 1 B 40 C 0 38 13 C min 290 C 13 09 121 1022 250 C 40 1 1 20 m x 0 18 mm 0 18 pm DB 1 30 m x 0 25 mm 0 25 hm
257. p trans 28 1 cis 29 g 2 gf 30 pe 3 1 31 D 4 32 5 33 6 34 7 4 35 gw 8 a LAVOIL Agilent J amp W DB 1ms 30 mx 0 25 mm x 0 25 pm GC 122 0132UI GC MS www agilent com chem jp DB 1 Dragoco Carl Frey Bush Boake Allen Inc 122 1032 Kevin Myung 30 m x 0 25 mm 0 25 pm 25 cm sec 150 C
258. pentanol 1 Pentanol 2 Penten 1 ol 3 Methy 2 buten 1 ol Cyclopentanol 3 Hexanol 2 Hexanol 4 Hydroxy 4 methy 2 pentanone Furfuyl alcohol cls 3 Hexen 1 ol 1 Hexanol cls 2 Hexen 1 ol Cyclohexanol 3 Heptanol 2 Heptanol 2 Butoxyethanol butyl Cellosolve cls 4 Hepten 1 ol trans 2 Hepten 1 ol 1 Heptanol Benzyl alcohol 2 EthyI 1 hexanol a Methylphenyl alcohol Octanol Nonanol 2 Phenoxyethanol a Ethylphenethyl alcohol b Ethylphenethyl alcohol Decanol 67 DB 624 123 1334 30 m x 0 32 mm 1 80 nm 35 cm sec 35 C 5 10 C min 35 245 C 250 C 1 100 FID 300 C 30 mL min Pentane lodomethane 1 1 Dichloroethene 1 1 2 Trichlorotrifluoroethane Freon 113 3 Chloropropene allyl chloride Methylene chloride 1 1 Dichloroethane Chloroform 1 1 1 Trichloroethane 1 Chlorobutane Carbon tetrachloride 1 2 Dichloroethane 1 2 Dichloropropane cis 1 2 Dichloropropene trans 1 2 Dichloropropene 1 1 2 Trichloroethane 1 1 1 2 Tetrachloroethane 1 2 Dibromoethane EDB 1 Chlorohexane trans 1 4 Dichloro 2 butene OS Sd HE pe Pr Sa a oeo 21 lodoform 22 Hexachlorobutadiene 23 1 2 3 Trichloropropane 24 1 1 2 2 Tetrachloroethane 25
259. sec 50 cm sec 70 cm sec 80 cm sec 60 70 cm sec lt 2 cm sec 3 4 cm sec
260. x 0 53 mm 40 00 nm 9 0 psi 60 C 60 C 5 20 C min 60 200 C 200 C 1 250 C 100 mL min 0 25 cc TCD 250 C 11 mm 5183 4759 1 5 mm 18740 80200 18740 20885 COS H 0 So oo TR oN Me0H i C tC n C cis C 16 17 MN Time min 18 DB 1 123 1035 30 m x 0 32 mm 5 00 nm 23 cm sec 50 C H S 50 C 4 20 C min 50 120 C 120 C 4 25 C min 120 220 C 220 C 2 5 200 C 1 10 PFPD 0I Analyticall 220 C 3 ppmV OD 600 LL 12 6 15 23 16 20 3 910 19 5 7 8 11 17 21 4 12 14 18 9 24 13 2 4 6 8 10 12 14 16 Time min www agilent com chem jp GCPEO17 C n C 10 12 GCPEO14 nr vnN oS 5 Air Toxics Ltd Folsom CA

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