MonoTrap(溶媒抽出用)カタログPDF
Contents
1. SS lt DSC18 RSC18 RSC18 TD us vl Monolithic Material Sorptive Extraction2. TM 163 1130 6 22 1 30F TEL 03 5323 661 1 FAX 03 5323 6622 http www gls co jp E mail info gls co jp 20130329KHST
3. MMSE Start Up KIT for SE 20 5 40 55 000 MMSE Start Up KIT for TD OPTICLINEX 10 5 3 60 000 MMSE Start Up KIT for TD T DexATD TD 20 10 5 3 60 000 J _ sl RSC18 TD RGC18 TD RGPS TD RSC18 MT Holder 5 MTStand 1 MT ExtractCupwith Clean Pin Hole Septum 200 pL Vial 20 mL 5 with Vial 40 mL MonoTrap TD Liner for OPTIC LINEX MonoTrap TD Liner for Dex ATD TD 20 MT Holder 5 1050 79003 9 000 MonoTrap TD Liner for OPTIC LINEX 1 1003 75001 MT Stand 1 1050 79004 7 000 MonoTrap TD Liner for T Dex ATD TD 20 Clean Pin Hole Septum with Vial 200 nuL GC GC IMS InertCap Pure WAX WAX InertCap Pure WAX
4. System GC MS Column InertCap Pure VVAX 0 25 mm D x30m df 0 25 um Col Temp 40 5 min hold 5 C min 250 C Carrier Gas He 1 mL min Injection Split 1 20 250 C Detection MS Scan 35 600 m z Sample Size 1 0 pL 5 1 Cycloisosativene 2 00 2 8I9 TP 8 2 O Cubebene 3 Sativen 1 75 4 Sativen 5 8 Elemene 1 50 6 Yy Muurolene 7 Eudesma 4 14 11 diene 1 25 8 8 Chamigrene 10 9 Muurolene 1 00 4 10 0 Cadinene 16 11 Calamenene 0 75 4 1 12 9 Calacorene 4 13 Cinnamaldehyde 0 50 9 12 15 17 14 3 Methy 7 8 dihydroquinolin 5 6H one _ 3 8 18 15 Cedr8 ene 16 Murolan 3 9 1 diene 10 peroxy 25 I wr 17 Cadinol 18 Cadalene EL IE a a 19 Coumarin 10 0 15 0 20 0 25 0 30 0 35 0 40 0 Timein 3 4 5 0 4 5 4 0 3 5 3 0 2 5 2 0 1 5 1 0 0 5 0 0 3 12 75 g 10 mL 1 MonoTrap 200 uL
5. MonoTrap RCC 18 NN 25 g 100 mL 60 C 3 I 60 3 5 500 LL OS IR 5 System GC FPD GC FPD Column InertCap AQUATIC 0 25 mm 1 D x 60 m df 1 00 um x100 000 Col Temp 40C 5 min hold 6 min 220 10 min holg Carrier Gas He 1 mL min 1 75 Injection Split 1 50 1 Dimethyl trisulfide 220 1 50 1 S Detection FPD 9 NN SampleSize 1 0u 1 25 1 09 Dimethyl disulfide 975 SR 0 50 60 C 7 0 25 4 60 C 3 0 00 CN OA 10 0 12 5 15 0 17 5 20 0 22 5 25 0 27 5 30 0 32 5 UNO 12 13 20 3
6. MonoTrap RGC18TD 3 50 3 25 3 00 3 2 75 4 2 50 3 2 25 3 2 00 3 1 75 3 1 50 4 1 25 4 1 00 3 0 75 3 0 50 3 0 25 4 1 0 00 I 1 1 I 1 1 I 25 0 30 0 Time min 10 0 15 0 20 0 1 1 1 35 0 40 0 System Column Col TemDp Carrier Gas Desorb Temp Time Flow SDIit Cryo Trapping Injection TemDp Detection GC MS Thermal Desorption T Dex I InertCap Pure VWVAX 0 25 mml D x30m df 0 25 um 40 C 5 min hold 4 C min 250 C He 1 mL min constant flow 200 C 5 min 2 mL min Splitless 160 C 0 MS Scan 40 600 m z 1 6 MethyH5 hepten 2 one 2 trans Geranylacetone 3 Megastigmatrienone 4 Megastigmatrienone 3 4 Monolithic Material Sorptive Extraction MonoTrap RGC18 TD
7. PDMS PolydimethyIl Siloxane ODS C18 MonoTrap S DCC18 RCC18 RGC18 TD PDMS Polydimethyl Siloxane RGPS TD MonoTrap MonoTrap ODS DCC18 ODS DSC18
8. MonoTrap RGPS TD 6 5g 40 mL System GC MS Thermal Desorption T Dex HL Column InertCap Pure VVAX 0 32 ImmLD X60m df 0 50 um 40 C 30 Col Temp 40C 3 min hold 6 C min 250 C 30 min hold Carrier Gas He 1 mL min constant flow Desorb Temp 250C TD GC MS Time 5 min Flow 7 ml min Split Splitless Cryo Trapping 150C Injection Temp 250 C Detection MS Scan 28 5 600 m z x10 000 000 3 00 2 75 2 50 2 25 2 00 1 75 1 50 MonoTrap RGPS TD 1 25 1 00 3 PDMS A 0 50 0 25 a 0 00 9 55 92455SR5SEE2EER2EERE 8 PDMS B 5 0 7 5 10 0 12 5 15 0 17 5 20 0 22 5 25 0 27 5 30 0 MonoTrap RGPS TD Time min PDMS B 10 mm MonoTrap DCC18 1 mm 50 1050 72101 20 000 MonoTrap RCC18 M MA 50 1050 72201 20 000 MonoTrap DSC
9. 5 g 15 mL 60 System 30 Column Col TemDp Carrier Gas 1000 UL Injection 5 Detection GC MS InertCap Pure VVAX 0 25 mm D x30m df 0 25 um 40C 5 min hold 4 C min 250 C He 1 mL min SDlitless 250 C MS Scan 40 600 m z Sample Size 1 0 uL 100 uL x1 000 000 1 50 TIC 1 25 1 00 17 20 1 Methylpyrazine 11 2 Acetylfuran 2 3 Dimethylpyrazine 12 Benzaldehyde 0 75 4 EthyIpyrazine 13 2 FormyH5 methylfuran 1 5 6 Methy 5 hepten 2 one 14 MethyI 2 furoate 0 50 6 2 Ethy 6 methylpyrazine 15 2 Furanmethanol 2 5 gt 7 Trimethylpyrazine 16 Dimethoxybenzene 25 4 18 19 8 Furfural 17 Irimethoxybenzene 0 6 7 9 Acetol acetate 18 Pyrrole 2 aldehyde 10 2 4 Heptadien 1 al 19 Coumaran 0 00 TFTTUTTTTTTUTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTI 20 Caffeine 10 0 15 0 20 0 25 0 30 0 35 0 40 0 45 0 50 0 55 0 Time min 2 3 10 11 200 puL MonoTrap RCC18
10. MonoTrap iso 260 prog 260 1010 68142 61 000 0 25 iso 260 prog 260 1010 68162 109 000 iso 260 prog 260 1010 68262 120 000 is0 240 prog 240 1010 68425 43 000 1 00 iso 240 prog 240 1010 68445 77 000 iso 260 prog 260 1010 68242 67 000 30 InertCap 5 MonoTrap http Www gls co jp technique technical_note index html Contents me mo es wm m s ee se s em ww s eee sw po em w ee ee nm ee
11. MonoTrap GQ 2013 4 hl ciences Monolrap onolithic Material Sorptive Extraction ww mn I la aa 8 gt ip Based on monolithic technology Merck KGaA Dermstadt Germany MonoTrap Monolithic Material Sorptive Extraction MMSE MonoTrap MMSE
12. MonoTrap RGC18 TD OPV 277 10 g 40 mL MS 1 9 OPV277 60 C 1 System GC MS Thermal Desorption T Dex I Column InertCap Pure VVAX GC MS 0 25 mml D x 60m df 0 25 um TD GC MS O ctooooo 19 13 min Col Temp 40 5 min hold 6 min 250 1 5 TIC Carrier Gas He 1 mL min constant flow 14 1070010 00 0 1 2 10 DesorbTemp 200 6 N 07 Time 5 min 96 Flow 1 mL min 03 Split Split 1 2 Desorb 10 mL min Split 20 mL min nw 3 Cryo Trapping 150 CO 18 25 18 50 18 75 19 ie 1 20 00 20 25 20 50 20 75 Injection Temp 250 0 x100 000 Detection MS Scan 28 8 600
13. 5 MonoTrap RCC18 System GC MS Column InertCap AOUATIC 0 25 mmID X60m df 1 00 um Col Tembp 40 C 5 min hold 4 C min 220 C Carrier Gas He 1 mL min Injection Split 1 50 220 6 Detection MS Scan 30 600 m z Sample Size 1 0 LL 1 2 Methylpentane 16 Ethylbenzene 2 3 Methylpentane 17 Mm p Xylene 3 Hexane 18 o Xylene x1 000 000 4 Methylcyclopentane 19 Propy benzene 5 2 MethyIhexane 20 Ethy methyl benzene 6 2 3 Dimethylpentane 21 Irimethy benzene 7 3 MethyIhexane 22 Ethy methyl benzene 8 Irimethylpentane 23 Trimethyl benzene 9 Heptane 24 Propy toluene 10 Benzene 25 Cymene 11 ITrimethylpentane 26 Indane 12 Irimethylpentane 27 Cymene 13 2 MethyIheptane 28 1 Ethy 3 5 dimethyIbenzene 14 Toluene 29 Naphthalene 29 15 2 Methyloctane 30 1 MethyInaphthalene 30 10 0 15 0 20 0 25 0 30 0 35 0 40 0 45 0 50 0 Time min 8 11 12 20 22 21 23
14. 30 System GC MS Column InertCap Pure VVAX 0 25 ImmlD 2 30m df 0 25 um Col Temp 40 C 5 min hold 6 min 250 C 5 min hold Carrier Gas He 95 kPa Injection SDlitless 250 C Detection MS Scan 55 400 m z Sample Size 1 0 pL 32 33 15 0 17 5 Time min 20 0 22 5 25 0 27 5 T O00 NO RO MN 10 12 13 14 15 16 17 2 2 6 Trimethyl 6 vinyltetrahydropyran Ethy 2 hydroxy 18 19 30 Benzaldehyde 3 Ethy 4 methylpentanol lsoamy l acetate 20 2 Bornene Limonene 21 n Propyl propionate 1 Pentanol 22 Ethyl d 2 hydroxycaproate Ethy hexanoate 23 8 Cyclocitral Maleic anhydride 24 Ethy decanoate 3 IMethylpentanol 25 D Galactopyranose 1 1 Dimethoxy 2 propanol methyl glycoside Ethy 2 hexenoate 26 Diethy succinate 1 Hexanol 27 3 Methylthio 1 propanol C S 3 Hexen 1 Ol 28 1 5 8 Trimethy Nonanal 1 2 dihydronaphthalene CS 2 Hexen 1 Ol 29 Hexanoic acid Benzy Alcohol 3 methyIDutanoate 31 Phenylethy Alcohol Ethyl octanoate 32 Diethyl d malate Furfural 33 Octanoic Acid 2 Ethy 1 hexanol Monolithic Material So
15. DCC18 MonoTrap DCC18 DSC18 44 mL Limonene Caprylic acid Indole 2 6 Dimethylpyrazine Methylpyrazine MonoTrap DCC18 MonoTrap DSC18 MonoTrap a MT Stand MT Holder MonoTrap S 2 MT Holder 1 DA MonoTrap
16. 10 9 System GC MS Thermal Desorption T Dex I Column InertCap Pure VWVAX 0 25 mm D x 60m df 0 25um Col Temp 40 C 5 min hold 6 min 250 C GO 230 Carrier Gas He 1 mL min constant flow DesorbTemDp 200 C Time 5 min Flow 1 mL min Split Splitless Cryo Trapping 150 C Injection Temp 250 CO Detection MS Scan 28 5 600 m z 50 x1 000 000 1 Methanethiol 19 2 Nonanone TG 2 Ethyl Acetate 20 2 5 Dimethy 3 ethylpyrazine 4 5 3 2 Butanone 21 Benzaldehyde 40 5 4 2 methyIbutanal 22 lsobutyric acid 5 3 methyIbutanal 23 2 Undecanone 3 5 6 1 Propanol 24 Butanoic acid 24 7 Toluene 25 2 Furanmethanol 3 0 8 Dimethyl disulfide 26 Acetamide 25 4 9 Hexanal 27 2 Tetradecanol 4 10 2 Pentenal 28 2 Iridecanone 2 0 11 3 Penten 2 one 29 Hexanoic acid 1 5 12 2 Heptanone 30 Dimethyl sulfone 29 2429 13 D Limonene 31 0 Octalactone 1 0 3 1 14 16 18 28 33 14 Acetoin 32 2 Pentadecanone 17 22 27 15 Acetol 33 Octanoic acId 0 5 6 9 11 13 19 19PO 21 2 dp 26 30 a 32 16 Dimethylpyrazine 34 0 Decalactone 0 0 8 ec cscsioeissn a 1 Dimethylpyrazine 35 Decanoic acid 5 0 10 0 15 0 20 0 25 0 30 0 35 0 TO NCVERZIe Time min 16 18
17. Cat No 8500 50000 Cat No 8500 50001 EYELA NTS 4000B nn 230DESESA 2 6 MS CM MonoTrap Disk MT Extract Cup MonoTrap MT Extract Cup 5 Rod GC MMSE5 E Monolithic Material Sorptive Extraction MlonoTrap MonoTrap DCC1
18. GC MS x1 000 000 40 0 29 30 MonoTrap DCC18 MonoTrap Indole Lo ML 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 20 0 45 0 System Column Col TemDp Carrier Gas Injection Detection Sample Size 0 N00 RO MN 50 0 GC MS InertCap Pure VVAX 0 25 mmlD X30m df 0 25 um 40 C 5min hold 4 min 250 C 5 min hold He 120 kPa Splitless 0 5 min 250 C MS Scan 40 350 m 2 1 0 pL c sS Ocimene Linalool Caryophyllene Benzoic acid methyl ester C Farnesene Benzy Alcohol Indole Benzy Benzoate MonoTrap DCC18 60 C
19. PTFE MonoTrap RGPS TD TD GC MS x1 000 000 70 A TIC 5 3 7 6 0 5 0 4 0 8 3 0 9 12 13 2 0 6 11 2 10 1 0 1 4 1 1 1 1 1 20 30 40 50 60 70 Time min 1 60 C 90 TD GC MS x1 000 000 MonoTrap RGPS TD PTFE System GC MS Thermal Desorption T Dex HI Column InertCap Pure VVAX 0 25 mmlD X60m df 0 25 um Col Temp 35 C 5 min hold 4 min 250 C Carrier Gas He 1 mL min constant flow Desorb TemDp 250 C Time 5 min Flow 5 mL min SDIit SDlitless Cryo Trapping 150 C Injection TemDp 250 C Detection MS Scan 28 8 600 m z 1 D Limonene 2 6 IMethy 5 hepten 2 one 3 Nonanal 4 Linalool 5 Octadecane 6 Hexanoic acid 7 Dinonyl sebacate 8 Phenoxyethyl alcohol 9 Octanal 2 phenyImethylene 10 1 Octadecanol 11 Benzy Benzoate Tetradecanolc acid Sdualane
20. Based on monolithic technology Merck KGaA Darmstadt Germany Merck KGaA MonoTrap 150 m g C18 I ops C18 MonoTrap MonoTrap GC GC MS
21. 25 27 Monolithic Material Sorptive Extraction MonoTrap RCC18 1 2 10 o System GC MS NY Column InertCap Pure VVAX 0 25 mm D x30m df 0 25 um Col Temp 40C 5 min hold 4 C min 250 C Carrier Gas He 1 mL min gt Injection SDlitless a 500 uL D 6 5 250 C Detection MS Scan 35 500 m z Sample Size 1 0 LL IM 1 000 000 0000000 0 7 0 1 lsopropenyl 6 5 4 8 4 methylbenzene Indene 6 0 3 5 5 I 5 5 3 5 0 3 J 5 0 3 4 5 3 x 4 5 3 NN 4 0 3 Nu 4 0 3 5 3 5 4 3 0 3 0 3 a 1 2 0 3 2 0 1 0 1 5 4 0 5 1 0 4 0 5 _ 16 0 16 5 170 17 5 18 0 18 5 19 0 195 20 0 20 5 0 0 3 Time min 10 0 15 0 20 0 25 0 30 0 35 0 40 0 45 0 50 0 Time min
22. 18 50 1050 71101 20 000 MonoTrap RSC18 50 1050 71201 20 000 MonoTrap RGC18 TD 30 1050 73201 25 000 30 1050 74202 25 000 1 1 mm 2 MonoTrap 2 MonoTrap RSC18 TD 10 mm 2 9 mm 2 MonoTrap RGPS TD 10 mm MonoTrap MOonolrap Rllellc1glrp D R C G S C18 ODS C18 PS PDMS PolydimethyIl Siloxane TD Monolithic Material Sorptive Extraction MonoTrap
23. 8 log P MonoTrap 2 6 140 r MonoTrap 2 200 ug mL in Methanol 120 100 3 80 25 UL 60 159 NaC 20 mL 40 20 0 logP 60 30 60 30 MonoTrap DCC18 PDMS A 90 rpm A 200 LL 200 LL Ml A Lia 2 6 Dimethylpyrazine 1 nuL 1 uL Cineol 2 74 107 0 I gt 97 0 MonoTrap
24. hold 4 C min 250 Carrier Gas He 1 mL min constant flow Desorb TemDp 250 C Time 10 min Flow 1 mL min Split Split 1 20 split flow 20 mL min Detection MS Scan 28 8 600 m z 6 5 x1 000 000 TIC 6 0 13 17 1 lsoamyl acetate 12 p Menthan 2 one 2 lsopentanol 13 Linalool 9 5 1 3 Ethy hexanoate 14 Terpineol 5 4 Hexyl acetate 15 Geranyl acetate 5 Hexeny acetate 16 Damascenone 4 5 6 Hexenyl acetate 17 y Decalactone 4 0 7 Hexanol 18 0 Decalactone 5 8 3 Hexenol 19 6 Penty 5 6 dihydro 2H pyran 2 one 3 5 9 2 Hexenol 20 O Undecalactone 3 0 7 10 Furfural 21 y Dodecalactone 11 Benzaldehyde 22 0 Dodecalactone 2 5 20 20 1 21 1 5 6 12 16 2 2 3 10 1 15 HH9 1 0 0 5 5 0 10 0 15 0 20 0 25 0 30 0 35 0 40 0 45 0 Time min 10 0 15 0 8 5 3 1000 uL 100 LL 4 5 6 25 0 30 0 35 0 Time min 20 mL 60C 30 300 LL 5
25. m z 5 0 1 MS 19 10 min 4 0 S 3 5 1 MR 3 01 ee RS 0 a 3 x 1 bP 0 i 2 0 4 30 i kc 1 5 1 01 0 0 4 15 0 17 5 20 0 22 5 25 0 27 5 30 0 32 5 35 0 37 5 40 0 42 5 14 hl rimrPs http Www gls cO jD MonoTrap InertCap iL Tciences TEL 03 5323 661 1 TEL 06 6357 5060 TEL 045 985 7900 TEL 024 534 2191 TEL 029 858 3700 TEL 048 667 161 1 TEL 043 248 2441 TEL 052 931 1761 TEL 082 233 1101 TEL 092 738 6633 TEL 04 2934 2121 TEL 024 533 2244 FAX 03 5323 6622 FAX 06 6357 4580 FAX 045 985 7901 FAX 024 536 1518 FAX 029 858 3780 FAX 048 667 1656 FAX 043 248 2485 FAX 052 931 1814 FAX 082 233 FAX 092 738 1110 6636 FAX 04 2934 2128 FAX 024 534 2139 _ Q
26. rptive Extraction MonoTrap DCC 18 2 System Column Col Temp Carrier Gas Injection 12 1000 LL 5 Detection Sample size GC MS InertCap Pure VVAX 0 25 mm 1D X 30m df 0 25 um 40C 5min holg 4 min 250 5 min holg He 95 kPa Split 1 10 250 C MS Scan 25 450 m z 1 0 UL uL x1 000 000 275 3 2 50 3 2 25 3 4 A gt 1 50 4 1 25 3 3 Octanone 1 00 3 Dimethyl trisulfide 0 75 3 0 25 3 ll L 1 Octen 3 0l 000 3 2 B 0 25 10 0 15 0 20 0 25 0 30 0 35 0 40 0 45 0 50 0 55 0 Time min MonoTrap DCC18 MonoTrap
27. ww nm RCC18 SE TD RGC18 TD TD SE TD Monolithic Material Sorptive Extraction MonoTrap RGPS TD 3 0 g 40 mL System GC MS Thermal Desorption OPTIC 4 60 10 Column InertCap Pure WAX 0 25 mml D x 60m df 0 25 um Col Tembp 40 C 3 min hold 5 C min 250 Carrier Gas He 1 mL min constant flow TD GC MS Desorb TemDp 250 C Time 10 min Flow 1 mL min 400 x10 000 000 Split Split 1 20 split flow 20 mL min Ne TIC 18 Cryo Trapping 150 Injection Temp 250C 3 50 Detection MS Scan 28 8 600 m z 3 25 3 00 4 2 75 4 1 Pyridine 13 Irimethylpyrazine 250 4 2 Pyrazine 14 Acetylfuran 1 1 3 Methylpyrazine 15 Furfuryl acetate 2 25 3 4 3 Hydroxy 2 butanone 16 2 Formyl 5 methylfuran 2 00 5 1 Hydroxy 2 propanone 17 2 Formy 1 methylp
28. yrrole 1 75 E 3 15 6 Dimethylpyrazine 18 2 Furanmethanol 1 50 9 7 Dimethylpyrazine 19 1 Acetyl 1 4 dihydropyridine 1 8 Ethylpyrazine 20 1 Furfurylpyrrole 1 25 3 7 9 Dimethylpyrazine 21 Guaiacol 1 00 4 6 12 16 10 1 Hydroxy 2 butanone 22 Maltol 0 75 ho 11 Ethylmethylpyrazine 23 1H Pyrrole 2 carboxaldehyde 1 2 11 4d 14 12 EthyImethylpyrazine 24 2 Methoxy 4 vinylphenol 0 50 3 ll 9 2 23 24 0 25 3 20 6 7 9 11 12 0 00 EE 90 NL WM 0 4 IT 10 0 12 5 15 0 17 5 20 0 22 5 25 0 27 5 30 0 32 5 35 0 37 5 40 0 Time min MonoTrap RGPS TD 30 mL 40 mL 36 C 10 160 rpm System GC MS Thermal Desorption OPTIC 4 Column InertCap Pure VVAX 0 25ITmimnlD 30m df 0 25 um Col Temp 40 C 5 min
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