Analytical Circle No.55 （2009.12）
Contents
1. FASTKIT FASTKIT FASTKIT FASTKIT 10ppm 5ppm 10ppm 5ppm 10ppm 5ppm 10ppm 5ppm BB Fe F FASTKIT 50ng mL 5ppm Step 1 12. 5ng 50 10mL A B 8096 1 308 34201 304 34203 50 300 83091 25 45 000 G Y Wako Analytical Circle No 55 4105 5 5 I Luminescence Technology EL 4053 gt LT I229C 20770 LT 223C PI0004 Ea C H Br N S C H Br N S C H Br Br gt Br 27 2 2 Br S A S Br N N 1g 20 100 288071 87 4 S 189367 54 2
3. LC MS 16 Analytical Circle No 55 303 08241 No mm um 303 83721 80511 4 0x10 32 000 300 83731 80522 4 6 x 50 3 1 150 000 307 83741 80524 4 6 x 150 180 000 304 83751 80525 l 46 x 250 195 000 301 83761 80594 2 1 x 150 180 000 308 83771 80595 2 1 x 250 195 000 309 88821 81511 40 10 32 000 306 88831 81522 4 6 x 50 3 1 150 000 303 88841 81524 4 6 x 150 180 000 309 88941 l 46 x 250 195 000 300 88851 81
4. 1 ODS HG RS AR AR 2 5 4 6mmx150mm Wakosil N T C18 HPLC I
5. GC BPX90 0 25 0 25mm 100m 200 C 2min 25 C min gt 260 36min He 1 0m9 min 90 096 85 096 98 0 98 0 CAS No 24305 63 3 CAS No 51554 07 5 CAS No 7501 44 2 CAS No 556 52 5 C H 0 336 51 C H 0 334 49 0 312 49 C H 0 74 08 O 10 No ceGC 071 05711 20 000 078 05721
6. 5mL 1 5 2 PEEK 1mL Mini Column Cellufine GH 25 5mL NaCI 0 6 90 80 0 5 70 Column Minr Column Cellufine GH 25 5mL 04 Sample Lysozyme 10mg m 0 5mol L NaCI Injection 1mL SS 0 3 99 2 Buffer 10mM phosphate buffer pH7 2 40 Flow rate 1mL min 9 lt 02 30 3 20 0 1 10 0 0 0 2 4 7 9 elution min No 633 16721 19845 15 Mini Column Cellufine Sulfate 5mL 29 500 20115 Mini Column Cellufine ET clean S 5mL 22 500 639 19515 19515 Mini Column Cellufine Phosphate 5mL 21 500 635 16781
7. MSDS Material Safety Data Sheet MSDS SDS Safety Data Sheet 1 435 1 354 2 81 562 1 462 2 100 1 2 2
8. 8 p35 36 Cm DMonofunctional 18 Wakosil II 5618 HG 1 5C18AR Wakosi H 5C18 RS 5618 HG Wakosil I 5C18 AR 1 5C18 RS 1 3 5 2 7 6 5 1 5 4 3 _ lt 1 gt 2 3 Eluent CH OH CH CN 25 75 v Eluent CH OH 0 196H PO 5mM 1 Hexanesulfonic Acid Sodium Salt Flow Rate 1 0ml min at 40 Detection UV 280nm ow Rate 1 UmI min Detection UV 210nm Sample 1 Vitamin K 2 Vitamin 3 Vitamin D 4 Vitamin 6 Vitamin Sample 1 Vitamin 2 Nicotinic Acid 3 Nicotinamide 4 Vitamin 5 Caffeine 6 Vitamin 7 Vitamin H 8 Vitamin C18H37 Si Wakosil I 5C18 HG Wakosil I 5C18 AR Wakosil H 5C18 RS 51 18 37 2 4 O OH 3 Eluent CH CN 50mM S _ 1 Triethylamine 5 lt i H PO 10 90 v v 3 4 C18H37 6 Flow Rate 1 0ml min Detection UV 210nm O N Sample 1 Scopolamine HBr 2 Atropine sulfate
9. IAC mir E IAFLAKING B1 B2 G1 G2 5ng 1896 10mL B1 B2 G1 G2 8096 M1 M1 5ng 189 10mL 809 29 AFLAKING
10. japonica Thunberg Caprifoliaceae 7 305 HOOC pH HPLC Conditions gt O Column Wakopak Navi C18 5 4 6mm x 150mm O OH Eluent CH CN 0 1vol HCOOH 10 90 Flow rate 1 0 m9 min at 40 Detection UV 325nm Ne Injection vol 0 4mg m9 500 ES C H O II Sample Chlorogenic Acid 354 31 0 10 20 min H OF x 039 20331 Perilla frutescens Britton var acuta Kudo Perilla frutescens Britton var crispa Decaisne OCH H CO lt HPLC Conditions gt Column Wakosil I 5C18 RS 4 6mm x 150mm CH 3 Eluent CH CN H O 35 65 OCH H Flow rate 1 0 m8 min at 30 Detection UV 230nm CAS No 2883 98 9 Injection vol 0 2mg m
11. 303 08241 No _ He mm 305 88781 47811 40 10 32 000 302 88791 47822 4 6 x 50 150 000 305 88801 mm t 7 upas 46 x 150 180 000 302 88811 47894 2 1 x 150 180 000 301 34551 19811 4 0x10 32 000 308 34561 19822 4 6 x 50 3 1 150 000 305 34571 19824 Di S DOS O 4 6 x 150 180 000 302 34581 19894 2 1 x 150 180 000 307 88621 20811 4 0x10 32 000 304 88631 20822 G 4 6 x 50 150 000 301 88641 20824 4 6 x 150 180 000 308 88651 20894 2 1 x 150 3 1 180 000 309 88701 42811 40 10 32 000 306 88711 42822 4 6 x 50 150 000 303 88721 mam 46 x 150 180 000 300 88731 42894 2 1 x 150 180 000 306 39481 14811 40 10 32 000 303 39491 14822 4 6 x 50 3 1 150 000 306 39501 14824 AE 4 6 x 150
12. NGo ACS EBDE 175S 175 50 g m ACS BDE 183S BDE 183 50g m9 557 85241 BDE 183 CS BDE 183 50g m B PFOS kas No 1763 23 1 No 512 2883 AoS PFOS 001S 1004 g m 515 28821 ACS PFOS OOIN 6 600 ao No 7126 579 38271 A C CAS No 608 93 5 2 J OO 509 45761 A 011 100mg 3 600 583 81461 muran m
13. SGE 2010 3 31 GCT A HPI 2 http www wako chem cojp siyaku info chromato article SGE htm Wako Analytical Circle No 55 SQ AB O z8 9 i 27 K 4 S S 4 rt O 28 Cellufine Mini Column 5mL 1ml 5m9
14. 4 0x10 3 3 32 000 300 88591 20522 4 6 x 50 150 000 303 88601 20524 4 6 x 150 180 000 301 88881 20525 R 46 x250 195 000 300 88611 20594 2 1 x150 180 000 308 88891 20595 2 1 x 250 195 000 305 88661 42511 4 0x10 3 3 32 000 302 88671 42522 4 6 x 50 150 000 309 88681 42524 4 6 x 150 180 000 301 88901 1 46 x250 195 000 306 88691 42594 2 1 x 150 180 000 308 88911 42595 2 1 x 250 195 000 304 39421 14511 4 0x10 3 3 32 000 301 39431 14522 4 6 x 50 150 000 308 39441 14524 4 6 x 150 180 000 305 39451 14525 EE 777752 46 x 250 195 000 302 39461 14594 2 1 x 150 180 000 309 39471 14595 2 1 x 250 195 000 307 88501 17511 4 0x10 3 3 32 000 304 88511 17522 4 6 x 50 150 000 301 88521 17524 4 6 x 150 180 000 307 88861 I 46 x 250 195 000 308 88531 17594 2 1 x 150 180 000 304 88871 17595 2 1 x 250 195 000
15. 50mm 150mm 250mm 4 6x50mm 4 6x150mm 4 6x250mm CHIRALPAK IA IB IC CHIRALPAK AY H AD H AS H CHIRALCEL OZ H OD H OJ H CHIRALPAKY AY RH AD RH AS RH CHIRALCEL Y OZ RH OD RH OJ RH 3 m 5 m IL C MS LC MS 2 1mm
16. 8310 K KA u 8331 Veratox for DON 5 5 59 000 8332 Veratox for DON HS 25 250ppb 59 000 8333 Veratox DST 0 25 5 0ppm 59 000 Fumonisin L _ Agri Screen for Fumonisin Veratox for Fumonisin 1 8835 Veratox for Fumonisin 5 10 0 5 59 000 8832 Veratox for Fumonisin HS High Sensitivity 50 600ppb 59 000 Ochratoxin Veratox for Ochratoxin 2 25ppb T 2 Toxin Veratox for T 2 Toxin 25 250ppb Zearalenone Veratox for Zearalenone 25 500ppb Histamine 9505 Veratox for Histamine 2 5 5 0ppm 45 000 9506 1 Vetoxr Hetanine Ta Pa LEE 2550mm 456 270 000 9510 13 400 Neogen http wwwneogen com U MX Analytical Circle No 55
17. Step 2 ee 100L Step 3 Step 4 15 Z 2 150L FASTKIT BR 32 000 300 88231 307 868241 304 88251 301 8826 1 308 88271 3059 88281 32 000 32 000 32 000 G KY Wako Analytical Circle No 55 4105 5 5 gt f aflatoxin 2 5 i RE 24
18. 3 MSDS 21 10 1 PRTR 22 23 HP http www prtrnite gojp index html MSDS HP http www siyaku com MSDS MSDS 15 4 1 2 2 57 2 19 2 No5 4 Pre PRTR IN IHPRTR No 12 H21930 SS PRTR
19. 540 8605 1 2 FAX 06 6233 3409 E mail analyti wako chem coJp Q amp A No 54 57 10 s 29
20. ProteCo G C18 HQ203 HQ 303 200A 300A Chromatograpnic condions MW5000 200A 200m g 100m2 g Tempemum 6 2 5 60 mnute Detecton 210m mi RA WW 5 BSA 250120 ProteCol G C18 HQ305 GLT CI8HQ Sum 300A 4 6mm x 250mm 66 100 250122 ProteCol G C18 HQ305 C18 HQ 46mmx150mm 61 900 250125 ProteCol G C18 HQ305 C18 HQ 2 1mm x 250mm 66 100 250127 ProteCol G C18 HQ305 C18 HQ 2 1mm x 150mm 61 900 250130 ProteCol G C18 HQ303 C18 HQ 2 1mm x 150mm 66 100 250132 ProteCol G C18 HQ303 C18 HQ 2 1mm x100mm 61 900 250150 ProteCol G C18 HQ203 C18 HQ 2 1mm x 150mm 66 100 250152 ProteCo _G C18 HQ203 C18 HQ 2 1mm x 100mm 61 900 G OK SGE
21. 1 N hydroxypyridine 2 LC ProteCol P PEEKsil 20 amp 9 ProteColTM P C18 HQ column PEEKsiIW tubing Fe ProteColTM P C18 HQ column Steel tubing SeE Analytical Science A B PEEK C PEEK D E F Sl rt O 26 N hydroxypyridine 2 RR 1 PEEK ProteCol M P C18 ProteCol P C18 HQ 8 75 27
22. 90 0 20 000 075 05731 New 2 85 096 100mg 20 000 072 05741 98 09 20 000 079 05751 New 98 0 10000 m mm B JE 054596 forte BPX90 New 195 000 15 80721 K S 33 6 Wako Analytical Circle No 55 TRM Traceable Reference Material Wako NMIJ SI TRM SI The International System of Units NMIJ NMIJ
23. TRM 019 22311 Asulam Reference Material New 6 000 018 22261 Atrazine Reference Material Traceable Reference Material 8 500 028 16331 25000 020 16271 6 000 025 16341 Bethrodine Reference Material Traceable Reference Material 10 000 022 1635 10 000 027 1628 7 000 037 20871 Chloroneb Reference Material Traceable Reference Material 15 000 030 21081 25000 049 3088 1000 049 30641 DEP Reference Material Traceable Reference Material 12 000 045 3086 20000 042 30871 15 000 052 07841 Echlomezol Reference Material Traceable Reference Material 12 000 058 07821 13 000 059 0785 16 000 05407801 Ethofenprox Reference Material Traceable Reference Material 5 000 065 05311 6 000 091 05671 8 000 094 05661 Isoprothiolane Reference Material Traceable Reference Material 6 000 134 15961 11 000 136 1602 15 000 133 16031 Mefenacet Reference Material New Traceable Reference Material 12 000 137 1595 8 000 135 15991 10 000 13216001 Metalaxyl Reference Material New Traceable Reference Material 100mg 9 000 139 1601 15 000 164 2379 6 000 164 23811 Pendimethalin Reference Material Traceable Reference Material 13 000 161 23821 20000 165 23461 13 000 162 23611 Propyzamide Reference Material Traceable Reference Material 12 000 168 23831 6 000 198 15281 Simetryn Reference Material 7 000 201 17501 Thiophanate Reference Material Traceable Reference
24. 5 13 2 03 3270 8243 551180 092 622 1005 Z 082 285 6381 O 052 772 0788 20045 476 2061 029 858 2278 2 022 222 3072 00 e 011 271 0285 0120 052 099 0120 052 806 eWako Chemicals USA Inc eWako Chemicals GmbH Neuss gt z lt gt e es http www wakousa com http www wako chemicals de Head Office Richmond VA Tel 49 2131 311 0 Tel 1 804 714 1920 5502 amp SEE SSE Tel 1 949 679 1700 Boston Sales Tel 1 617 354 6772 URL http www wako chem co jp 09Z12 8 o1DN E mail analyti wako chem co jp
25. Column Wakopak Navi C18 5 4 6mm x 150mm Eluent CH CN H O 65 35 Flow rate 1 0 m0 min at 40 di H Detection UV 285nm 4 133 04 0 s Injection vol 1 0mg m soln 1000 O C H O Sample L Asarinin Standard 35435 0 10 20 min 017 22091 L Asarinin Standard 9896up HPLC LIZ 333 4 Wako Analytical Circle No 55 Q amp A 39 Wakopak ODS ODS Wakopak C18 ODS ODS ODS 1 2 2 3
26. J 6 Nonane 35000 OIL 4982 556 85211 511 66021 525 80261 148 900 ClL BDE 99 CS BDE 47 Nonane 50ggm ACS BDE 099S BDE 47 lsooctane 50ggm img EO 4983 Cu BDE 47 None 50ggme 12me _ 214 500 P 1528 10X Cyclohexanone 1000 g mg 3 00 _ iowg 237 500 No 23 502 96301 28 500 585 70291 cl PBB 153 CS 2 2 4 4 5 5 34 100 506 96321 B 155S 2 2 4 4 6 6 9 000 509 96311 ACS 155 22 4466 5mg 19 500 570 69951 PBB 157 CS 3 23 3 44 5 37 500 571 39831 495 000 503 96331 1695 3 3 4 4 5 5 9 000 02572 BJ y BHC y HCH CAS 58 89 9 No j man 029 05773 WAKO _ Tolene 1Ozgme imex5 8600 3 400 6 700 025 05731 WAKO 20 5200 AcS P 059N i
27. YC PRTR 22 21 G HM Analytical Circle No 54 2009 9 p 1 p 22 PDF P 1 7 Treceabl 1 22 4 22222 Wako Analytical Circle No 55 FAX E mail FAX 10 3 000 22 1 31
28. 1 900 6 500 1 900 7 500 2 400 2 150 1 600 4 900 1 150 5 100 1 650 4 500 1 900 12 000 1 500 6 800 1 900 13 600 1 500 6 500 1 900 7 500 2 200 14 000 18 200 15 000 1 950 1 900 7 500 2 100 12 000 1 900 2 000 5 600 32 100 19 000 1 700 6 500 2 200 14 000 lt BN HP 1 450 1 500 6 500 1 600 G OK FASTKIT FASTKIT NIPPONHAM FASTKIT FASTKIT 1 4 000
29. ProteCol W P C18 HPH125 column ProteCol P C18 HPH125 k 4 ProteCol P C18 HPH125 column pH 9 15 40 C 3000 1000 Effect of pH on different paramrters of monomeric Silica Silica Normalised Symmetry Factor 1000 1500 2000 2500 3000 3500 Column Volumes at pH9 15 40 PH9 15 250110 ProteCol P C18 HPH125 PEEK lined C18HPH 5um 120A 4 6mmx250mm 250112 ProteCol P C18 HPH125 lined C18HPH 46mm x 150mm 250115 ProteCol P C18 HPH125 PEEK lined C18HPH 2 1mm x 250mm 250117 ProteColW P C18 HPH125 PEEK lined C18HPH 2 1mm x 150mm 0 200 amp 300
30. M Nos a ase 29 000 RIV 4 299 33403 12g 25mQ 100 290 33411 SP L 39 000 29633413 31g 70m me 297 33421 NH M 20 40 000 New 293 33423 14g 25m9 s 294 33431 NH L g 70 000 New 290 33433 342 70 0 i TLC NH 60F 0 75mm 20 x 20cm 10 58 000 NH 60F 0 5mm 20 x 20cm 10 35 000 NH 60F 0 25mm 60F 0 25mm 100 145 08721 149 08621 146 08631 143 08641 164 08531 FM 5 10 10 6 000 193 08381 10 2 700 197 08384 70 100 21 000 199 08383 20 x 20cm 25 15 000 190 08391 10 3 000 194 08394 70FM 100 22 500 196 08393 20 x 20cm 25 17 200 193 08401 10 2 800 193 08406 5 10 200 23 100 UR
31. 6 016 17671 Aflatoxin 2 01017691 Aflatoxin 02 150 02111 Ochratoxin 2 Aflatoxins Mixture Solution 1 1 01 2 0g m 2 G1 G2 in Acetonitrile B2 G2 40 5 Aflatoxins Mixture Solution 2 1 2 01 02 in Acetonitrile 025 0 014 21141 011 21151 Fumonisins Mixture Solution ENo 013 21091 45 000 016 21101 45 000 013 21111 5my 45 000 010 21121 45 000 017 21131 Aflatoxin M1 Solution in Acetnitrile 0 5 5mg 52 000 060 04901 57 000 067 04911 64 000 159 02701 5my 59 000 205 16801 75 000 267 0191 15000 U MX AFLAKING 0CHRAKING HORIBAAcvancedTechno QAC
32. lt J Ll Xy gt a 20 11 21 21 10 1 PRTR MSDS SDS 2 1 PRTR 2 MSDS
33. 30K n kos kasi 250 2 200 01mg m2 BSA 500 0 O WOO NS 0 di 450 5 000 x g 8 100 20 50 0 9 0 2 4 6 8 10 14 20 24 30 100 1 0 PES DNA RNA HPLC WM 50 500L 36 7 00901 OD010C33 24 10 000 361 00921 OD010C34 10K 100 34 000 363 06461 OD010C35 500 148 000 360 06611 OD100C33 24 10 000 367 06621 OD100C34 100K 100 34 000 369 08901 OD100C35 500 148 000 G OK Wako Analytical Circle No 55 2 9 rt O 26
34. NALYTICAL http www wako chem co jp 4 2 Lock Silica Gel SP 2 Pre Luer Lock 2 9 72 7 Z L O Q amp A 39 3 m SGE HPLC ProtoCol D O Cellfine Mini Column 5mL PALL N 33 6 TRM Traceable Reference Material POPs COP4 D FASTKIT D Neogen Agri Screen aflatoxin gt B AFLAKING OCHRAKING Luminescence Technology W 43 gt LaboLock O Wako Presep Lock Silica Gel SP Presep
35. FeliCa SONY 49 LahpkLook Series Chemical Design 2 EyeD USB RF ID FiliCa 38 000 G M 540 8605 1 2 2 06 6203 1788 55118 103 0023
36. SEP 24 0 1 aga 1 k Blue Es 1 NA 1 1 wa PSI HH Aflatoxin Veratox for Aflatoxin S NEDBEN Agri Screen Neogen CD ELISAs ELISA lt e x x 20ppb 5 Total aflatoxins B1 B2 G1 G2 Agri Screen for Aflatoxin Veratox for Aflatoxin HS High Sensitivity Veratox for Aflatoxin AST Aflatoxin Single Test 5 150ppb 55523EERIROERIIKP DON Vomitoxin
37. http www siyaku com 17 Wako Analytical Circle No 55 _ tT Siyaku Com s PC LaboLock SCITEC SSE 2010 4 ss gt PC JS Es ma 8 7 LaboLock C SecukeyLock PC C 3CH 12CH RF ID p FJ SC 3M KB 12 LAN RF ID 1 Felica card
38. 197 08404 100 21 000 199 08403 20 x 20cm 25 13 200 195 12871 70PF 0 75mm 20 x 20cm 10 15 000 233 00533 FM 20 x 20cm 20 15 500 K IS 8 1 5 GC 2 6 3 7 Appendix 4 HPLC CHROMATOGRAPHY http wako chem cojp siyaku catalog htm O Y Wako Wako Analytical Circle No 55 Wako 405 5 4 LL S t O 26 Wako 4
39. Luer Lock NH Silica Gel SP NH Silica Gel SP 5 2 E Presep NH2 L _ Silica Gel SP Presep NH LC Conditions LC Conditions Column Silica Gel SP Type L Column NH Type L Eluent Ethyl Acetate 90 10 v v Eluent Hexane Ethyl Acetate 90 10 v v Flow 20mL min at ambient Flow 20mL min at ambient Detection UV254nm Detection UV254nm Sample Toluene 0 1g mL in Eluent Sample Toluene 0 1g mL in Eluent Dibutyl Phthalate 0 1g mL in E
40. 4d NY gt s 0 5 5m m 5 2 5
41. 637 16741 19900 55 Mini Column Cellufine Pheny 5mL 28 200 636 16711 19805 55 Mini Column Cellufine A 500 5mL 27 500 639 16701 19800 55 Mini Column Cellufine 500 5mL 27 500 1mL G OK Analytical Circle No 55 WPES 0 WPES amp 1 5 a i 500 100 490 PES 400 30K 80 3 3 Ei 300
42. O Si C18H37 3 Brucine IS 9 Wakosil 5C18 HG Wakosi 5C18 AR Wakosi 5C18 RS 5 Eluent CH CN H 0 60 40 v Y Flow Rate 1 0 at 30 Detection UV 254nm 1 ODS Sample 1 Uracil 2 Benzene 3 Naphthalene 4 Biphenyl 5 Phenanthrene 6 Fluoranthene 7 Pyrene 8 Chrysene 9 HP http wako chem cojp siyaku info chromato article hplc_cat htm Wako Analytical Circle No 55 2 z8 9 gt lt J Ll y s SB rt O 26 89 Wako GC GC BPX90 98 0 CAS No 5431 33 4 C iH 0 338 52 BPX90
43. 0 0 19 SP Lavebder Oil Oil of Lavender L10 lt SPE Lemon Oil Oil of Lemon LE108 2 2 138 16042 25m9 132 16045 Macadamia Nut New d O Tocopherol about 0 02 5000 13615982 m 25 130 15985 Meadowfoam Seed Oi New 9 Tocopherol about 0 02 5000 150 00276 Qi 500m0 152 01892 156 01895 Orange Oil 500m0 MPB 999 20541 Origanum Oil Oil of Origanum from Thymus capitatus 155997 2 SPE 500 27655 Pam Oi Oil of Pan 8 188 02372 182 02375 Rapeseed Oil New ons 183 02322 187 02325 Rose Hips Oil Ascorbyl Dipalmitate about 0 002 i 195 15372 Pe 199 i5375 Ol New 192 15382 8 196 15395 Sesame Onon New 192 15262 sa 196 15265 SunHower Seed 0i New 9d 9 Tocopherol about 0 02 500 7 333 10 Wako Analytical Circle No 55
44. 1 N hydroxypyridine 2 Stainless steel column Steel tubing ProteCol P NIST SRM870 method ProteCol P C18 HQ105 005 2 2 ProteCol P C18 HQ105 NIST SRM870 method ODS Silanol Activity tailing factor amitriptyline ProteCoITM P 2 NIST SRM870 method C18 www usp org USPNE columns html Gs 25 250100 ProteCol _p C18 HQ105 PEEK lined C18 HQ 46mmx
45. 10 3400 635 05811 NMIJCRM4203 a 14 160 579 3573 CLM 1282 12 1004 g m 122 500 CDLM 624 12 100 4 g m 148 800 333 8 Wako Analytical Circle No 55 llo 5124 amp HCH CAS 319 84 6 025 05753 WAKO _ Tolene 10gg m 10 000 6 200 9 500 021 05711 WAKO 20 _ 50 PON 620 575 35711 CLM 2482 12 o None 1ooggme 12me 108400 5 BHC HCH 8 CAS No 319 85 7 No F E Acs P 0S 100 g m0 6 200 Acs P 011S 10X 000xgmt 1 0 9500 028 05721 WAKO iss 5 500 P 011N 10mg 6 200 572 35721 6 Nome zxizw No s 17 ooo 50 g m 25200 5659 85201 COIL 153 05 153 35 000 526 80311 214 500 5 5zgme 2526 579 99831 BE U 131400
46. 180 000 303 39511 14894 2 1 x 150 180 000 305 88541 17811 4 0x10 32 000 302 88551 17822 4 6 x 50 150 000 309 88561 17824 mD 4 6 x 150 180 000 306 88571 17894 2 1 x 150 180 000 G OK Wako Analytical Circle No 55 17 J SS nu ProteCol HPLC ProteCol HPLC Columns ProteCol HPLC Columns proteColm P PreteColm G PEEK PEEKWined Glass lned PEEK 6 0 PEEK lt 8 6 rR pa a PEEK ProteCol P amp ProteCol G
47. 250mm 65000 250102 ProteCol M P C18 HQ105 PEEK lined C18 HQ 46mmx150mm 59 300 250105 ProteCol _p C18 HQ105 PEEK lined C18 HQ 2 1mm x 250 56 700 250107 ProteCol M P C18 HQ105 PEEK lined C18 HQ 2 1mm x 150mm 52 600 250200 ProteCol _p C18 HQ103 PEEK lined C18 HQ 2 1mm x 150mm 59 200 250202 ProteCol M P C18 HQ103 lined C18 HQ 2 1mm x 100 59 000 15 Analytical Circle No 55 HPH pH pH ProteCol P C18 HPH125 lt lt pH r pH8 DIOmOLDOSYIC monomeric PEEK Attack 1111115 pH9 cross linked cross linked 3
48. 5 3 14 Wako Analytical Circle No 55 LT 1222C Cz H4 Br 2 198964 46 4 1g 33 100 LT I234C 07 C H B O 35 d 196207 58 6 1g 48 800 1237 891182 24 4 1g 79 600 LT 240C PI0014 C JH B O Si x 958293 23 7 1g 106 300 LT I243C 5 5 478404 10 3 lg 88 300 1g 52 700 17 12246 _ PI0006 y O gt 188200 93 3 1g 35 600 C H Br O 55 357219 41 1 1g 51 100 C gt e 1g 82 100 LT 1241C BIOS Le RE 1g 108 500 Kisa 1244 C H Br S 25 136 2 2 Br S S 365547 21 3 ig 90 800 ig 33 100 LT I233C C H B O lt 254755 24 3 lig 48 800 LT 236C PI0010 i 852138 90 0 1g 79 600 LT I239C C H B O Si O J 852138 91 1 ig 106 300 17 12426 PI0016 C H Br S 00 528570 55 0 1g 88 300 S S i wis WZ i 188690 66 6 lig 88 300 LT 249C 10023 ig 88 300 LT 256C 10030 5 Br 1098102 93 2 1g 9 600 COOC12H25 LT 260C 0034 H Br N S CeH1s N S 180729 93 5 _ 1g Y84000 LT 1264C 0038 09 s Z Br Br C 1g 101 800 LT I267C PI0041 CG H Br N 7 ig 82 100 LT 270C PI0044 C u
49. 594 2 1 x 150 180 000 306 88951 81595 2 1 x 250 195 000 306 83831 83511 40 10 32 000 305 83781 83522 4 6 x 50 3 1 150 000 302 83791 83524 4 6 x 150 180 000 305 83801 83525 T 46 x 250 195 000 302 83811 83594 2 1 x 150 180 000 309 83821 83595 2 1 x 250 195 000 303 08241 mm m 307 88741 47511 3 32 000 304 88751 47522 4 6 x 50 150 000 301 88761 47524 4 6 x 150 180 000 305 88921 4525 Khi K 46 x250 195 000 308 88771 47594 2 1 x 150 180 000 302 88931 47595 2 1 x 250 195 000 303 34491 19511 4 0x10 3 3 32 000 306 34501 19522 4 6 x 50 150 000 303 34511 19524 4 6 x 150 180 000 300 34521 SE Ziz 46 x250 195 000 307 34531 19594 2 1 x 150 180 000 304 34541 19595 2 1 x 250 195 000 303 88581 20511
50. 9 soIn 1009 Sample E Asarone Standard L j j j 208 25 0 20 40 60 80 100 min 011 22011 Asarone Standard 9896up HPLC Atractylodes lancea De Candolle Atractylodes chinensis Koidzumi Compositae HPLC Conditions gt Column Wakopak Wakosil I 5C18 RS 4 6mm x 150mm Eluent H O 55 H PO 1 CH CN 33 67 Flowrate 0 8 m0 min at 40 Detection UV 336nm Injection vol 0 02mg m amp CH OH soln 200 Sample Atractylodin Standard H CAS No 55290 63 6 CH O L j j j j 18222 0 5 10 15 20 25 30 35 mm 011 21531 Atractylodin Standard 9896up HPLC As asarum sieboldii F Maekawa 5 471 HPLC Conditions gt
51. H Br S as Br S 2 1g 84 000 LT I250C 10024 CaHsBrSSi S p 7 7 i 1089687 05 7 1g 90 800 LT I257G PI0031 H B N O 2 eL O N O 958261 51 3 1g 106 300 J LT I261C PI0035 C H Br N S CeH13 Br S Y S Br 853722 91 5 CeH1s 1g 106 300 LT I265C 10039 mw 274 N ig 79 600 LT 1268C 10042 CO er N 0 gt 1g 106 300 LT I271C 0045 05 O N Br S 2 S 1g 990 800 N O LT 254C 0028 09 O Br Br 1g 99 800 S O LT 259C PI0033 CaoH Br N O S re p es 1000623 95 9 _ 2 5 1g 101 800 LT 263C 0037 0 5 w 5 Ye S 359017 65 5 1g 101 800 a LT I266C P10040 C H4iBrsN 2 955964 73 5 1g 79 600 LT I269C 10043 C H B NO N O o 1g 108 500 LT I272G 10046 CaoH aBr N O0 S O Br S 1057401 13 4 N 1g wa00 Wako Analytical Circle No 55
52. Material 100mg 20 000 204 17471 Thiuram Reference Material New 5 000 225 01751 Vinclozolin Reference Material New 14 000 NMIJ http www02 wako chem cojp siyaku trm index asp KJIS Wako Analytical Circle No 55 7 POPs C L POPs Persistent Organic Pollutants ES EZ 0 9 1 POPs 4 COP4 POPs A
53. amaman mamanman maman 8 43 800 U TN Wako Analytical Circle No 55 gt S rt O 26 SF gt 2 019 22372 6 013 22375 Almond Oil New d 9 Tocopherol about 0 02 500 0 010 22302 7142922305 Avocado Oi New 9 9 Tocopherol about 0 02 500 0 032 01602 036 01605 Cedar 036 03562 030 03565 Clove Oil 032 20902 s 25g 036 20905 Coconut Oil New 16 48 03217016 500 037 21172 w 031 21175 Oil New 5o0mg 25g 058 06162 s 052 06165 Eucalyptus Oil 500mg 067 03492 s 061 03495 Fennel Oil 500m0 079 05572 073 05575 Grape Seed Oil 107 00122 101 00125 Jojoba Oil 117 00802 N d O Tocopherol about 0 04 111 00805 Kukui Nut Oil W Ascorbyl Dipalmitate about 0 005 50
54. luent Pyridine 0 1g mL in Eluent Diethyl Phthalate 0 1g mL in Eluent Sample load 1 0 mL Sample load 1 0 mL lle s 2 0 5 10 Retention Time NH 60F TLC Presep Column Luer Lock L Eluent n Hexane IPA 90 10 v v Flow rate 20mL min Hexane IPA 90 10 v v Detection 230nm Sample 2 4 6 Trimethylpyridine 2 Sample 24 6 Trimethylpyridine 2 0g Rf 4 Dimethylaminopyridine 0 5g in 10mL Eluent 4 Dimethylaminopyridine Sample load 1 0mL 1 0mL sample loop 333 2 Wako Analytical Circle No 55 SP NH 40 64 m 38 63 5 7nm 5 5 7 5nm 0 65 0 85mL g 0 6 0 8mL g 450 500 2 410 510mg pH 5 5 7 5 85 115 No _ 293 33401 SP
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