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Ivium Compactstat 取扱説明書

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Contents

1. on off Method
2. N F B N 26 S4 Method F B Q H Q H
3. Model 65 7 Time domain Frequency domain Time domain Pitting Index Frequency domain FFT MEM
4. XY Z Autoscale Scale O WORD EXCEL WMF
5. 32 5 StandardMode CyclicVoltammetry CurrentAveraging True Linear Scan CurrentAveraging
6. vertex ReverseScan CV ResultGraph E_start Pause Resume DynamicVertexes 1 max Lmin
7. 2 Acquisition Period AC 2 Result optimalisation
8. IR feedback Compensation 0 2V 1mA 2k l end I Frequencies 255 I Frequencies Amplitude 0 1mV 1V I Frequencies Frequencies each decade 1 I Frequencies End 10 Hz 2MHz 83 9 Method Frequencies Manual override I Frequencies Start Ilevels I pretreatment 1 scanrate 1 scanrate I start I vertex 1 1 vertex2 Levels Levelslindex time N samples N scans Mode Phase sensitive Phase sensitive phase Potential range Pretreatment
9. 10 Hz 2MHz 0 255 5 IviumSoft Lpretreatment Method Extra View scanrate Istep Istart Ivertex1 Lvertex2 I start 2 Lstart Ivertex1 Lvertex2 I start 0 255 levellindex Stan
10. 2 C 4 2 3 W Method Method Start Abort File Save dgata IviumStat CompactStat 4mm 6 Gnd W W2 C R S
11. Lstep Lstep scanrate Standard 2m HiSpeed Method LinearSweep Standard 30 LinearSweep LSV Method 5 mu 1 Value Mode Standard HiSpeed Title E start 10 9227V E end 10 9226V DynamicVertexes On Off
12. DISCONNECT EMO S 1 DISCONNECT LCD 37 9
13. Data Options Data Option Analoglnputs Plot title Analoginputs 81 S9 Method Data Option Analoglnputs Axis title AnalogInputs Data Option AnalogInputs Transform AnaloglInputs Data Option AnalogInputs Transform Parameters Analognputs Data Option Ecorrections Convert Reference Electrode potentials actuare RE Data Option Ecorrections Convert Reference Electrode potentials Base RE Data Option Ecorrections Offset potential Data Option Electrode Electrode properties Area
14. Pulse time Pulse amplitude E start E step Scanrate ElectroAnalysis Differential Pulse Method Value Title E start 10 9226V E end 10 9226V Pulse time 0 0001 0 4s Pulse amplitude 1 100mV E step 0 125 1000mV Scanrate 0 00001 1000V s CurrentRange 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment 7 5 Data Options
15. Tools Pulse Generator Connect Off Cell Estat4 4 Cell Estat2 2 W C 1k Estat 1kQ 100kQ Estat 100kQ 10MG Estat 10MQ R RO Estat 100Q 1gF 1kQ Dam FDigm2z Head 17 S3 Direct Cellstat4 4 CellIstat2 2 W O dummy lstat
16. 2 Fourier Linear PotentialSweep 50 60Hz Low pass filter Band reject filter 64 7 Linear Sweep Analysis Corrosion analysis Defined constants Linea
17. Connect CompactStat USB DLL lviumStat CompactStat IviumSoft IviumSoft VB Delphi C 79 S9 Method S9 Method 2nd Harmonic Amplitude Transients Mixed Mode
18. CyclicVoltammetry TrueLinear E_step E_step Scanrate 2m HiSpeed CyclicVoltammetry Galvanostatic I_start Vertex 1 Vertex 1 Vertex 2 Vertex 2 Istart 1 1 step Istep Scanrat
19. W S R C 4 2 5 W2 PC Windows XP Windows2000 USB IviumStat 2 USB USB A B PC ON OFF
20. Peakfind automatic Scan 1 Current 1 H H H B HH U 2 HH Potential V advanced 70 7 Peakfind advanced Peakfind advanced 5 Search Peaks Baseline subtract Automatic peak find HeScale Copy graph Copy peaks Search parameters automatic peakfind 3 Scan 1 Construct from whole peak Find method 1st derivative Height mode proportional Minimum height 0 015 Width made absolute Minimum width 0 025 Sensitivity 5 pnts Smoothing 5 points Manual peak addition Add marked peak mark CV reverse scan Clear markers Peak results 0 630 4 0055819E 01 0 105 1 7272627E 02 6B 9090509E 01 2 0729050E 00 0 175 1 2444854E 4 9779458E 00 6 5146951E 00 0 335 8 05931
21. Il conol 0050A for 30 s or unti E gt 3 50V far 10s 0 050 4 for 30 s or until E lt D 100Y 50mA 30 3 5V 2 10 OCP 50mA 30 0 1V 10 OCP Tiereers ChroneAimpsiomsiy CheonoPolerbomehy Med Mcds Elochochemicol Ncise F EloxtoAnches Resistance s Oo v Potential 40 5 MixedMode 1F 2 O 1kHz Cs Transients MixedMode Method Value Title Stages 255 OCP P 39 40 Cycles 0 65535
22. True Linear Scan CurrentAveraging LinearSweep Current Aberaging Hispeed LinearSweep rueLinear E_step E_step Scanrate 2m HiSpeed LinearSweep TrueLinear DynamicVertexes LinearSweep Galvanostatic
23. leve 1 86 Thresholds E max Thresholds E min Title Vertex 1 Vertex 2 S9 Method LinearSweep GalVanostatic ChronoPotentiometry LinearSweep Galvanostatic ChoronoPotentiometry E stat Vertex1 Vertex2 E_start 2 E_start Vertex1 Vertex2 E_start
24. HI LO Ivium LoadMethod MethodFile Method Mthod imf idf ids Mthod imf i ExecuteMethod Savedatafile 1 idf ids OverwritelfExist 1
25. Show Left Right 3 IviumStat Control File Options Tools Help About Connect 1m amp Advanced jil SigView Direct Method Fesuk graph Result data D iviumstat manual TEST3 Scale Analyss lt Edit lt LinearSweep 9 Standard In TEST3 no a CurrentAveraging TrueLinear 1 HEwclicVoltammelry Transienls Value Analog inpuls none AutoCA Of Apply wit OCP nf IR feedback nf BiStat On E offset Current Range 10u amp CR min 10ua CR max 10u amp Mode Scanning Delete Cellaftermeas Of 1 Delele al Pretreatment 0 _ leve M 8 3 1 0B 8 ne Data Options Automatic save Start Scan completed Save data WE2 Current Save dataset Data appear Potential 16 3 Direct S 3 Direct Direct Direct Fc 8 oo Method Current range onnecF Cioma E ll BiStatd lt
26. 6 4mm C W 1kQ S W R 100M C W2 100k C GND Test 2 Test1 1 TEST1 imf File Load method Start 14 2 CompactStatPlus
27. P 57 AUX S10 AutoCR Current Range Max Min 44 5 ElectroAnalysis Square Wave 1 forward backword forward backward Forward backward forward backward Pulse amplitude
28. n idf ids S4 Method Olay na labels A scan 1 scan 2 sCaI PP Ml Save data Save dataset Delete Delete al Data appear Data appearance channel list Option Data appearance Copy overlay list Load Overlay Dataset Delete Delete all
29. TESTCELL1 D9 Ivium Dummycell 1 4mm Gnd W W2 W2 C R S 10 2 Method Method Start Abort File Save dgata Gnd W W2 C R S under test
30. 4 12 2 CWriitrl File Options Toos Help Abouk come ei Et EYWB Direct Melhod Resuk graph Hesuk data D Myiumstakmanualhcy50Hmy Scale gt Analysis Edit LinearSweep Scan Olay CyclicVoltammetry Fe in KNO3 nelabes gt Standard Current amp veraging scan 1 cv500my TrueLinear Transients Made Standard Title Fe inKN 3 E start nnnnn V Vertex 1 03nn V Vertes 2 000 V E step 5 my N scans 4 cls Save data Scanrate 05 V s Save dataset Current Range AutoCR Cell after meas Pretreatment _ levels 2 on AUX wy 1 Data appear Potential Y Start 100 pnts Scan completed Delete Delete all File load save Options Tools Help About
31. MEM MEM FFT FFT MEM 5 DC Subtract baseline DC Elcctrochcmical Noisc Analysis Time damain analysis Frequenoy doman anaysis Baseine remove Daa nA Noise transients Potential Soment anakgs Inose lt Eroise Pp Filirn de Secment g Potential 66 7 Ivium Technologies Electroch ermical Noisc Analysis Tire domain analysis Fcqucny doman anclysls Baseine remove Daa 10loglI
32. IviumStat CompactStat IVIUM TECHNOLOGIES 2007 11 20 Ver 1 6 S 1 S 2 IviumSoft IviumStat CompactStat S 3 Direct 1 1 2 3 BiStat S 4 Method Direct SigView File Option Tools Help Methog Method Result graph Result data S5 LinearSweep Standard LinearSweep CurrentAveraging LinearSweep TrueLinear LinearSweep Galvanostatic LinearSweep LSV Method CyclicVoltammetry Standard CyclicVoltammetry CurrentAveraging CyclicVoltammetry TrueLinear NO Q OT 10 11 13 14 14 14 15 16 17 18 19 20 20 21 21 2
33. B C IviumSoft EviumStat Iviumdrivers D E USB Windows S1 USB Universal Serial Bus Ilvium Dvice
34. E_start Estep Scanrate Estep E _end Pulse time E end E step E start E step Scanrate ElectroAnalysis Normal Pulse Voltammetry Method Value Title E start 10 9226V E end 10 9226V Pulse time 0 0001s 0 4s E step 0 125 1000mV Scanrate 0 00001 1000V s Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5
35. IlviumStat ijpt B07003 ipt 10nA Fail Pulse generator amp 4 EEEIEEDEDEIGD 10 650m eh 100 HLVekage 10 vy Direct ed 100 a 0 VM Pulse generator Apply
36. Method Direct Method Aborr method 2 3 Load data idf Load Scan Oley Load data Save data idf Load dataset ids
37. lviumStat Control Fle Options Tools Help Abouk cs lee eo Diect Melhod D Myiumstatmanualhchronpulsen LinearSweep Standard CurrenAveragin TrueLinear Cyclicyolkammetry Standard Paes Mode Standard rme liEsm E start nnnnn V E end 10000 V E step 5 my Scanrate D005 v s Equilibration time Os Current Hanae 1m amp Fiter automatic Stability automatic Connect to dummy 1 Analog inputs none AutoCR of Apply wt OCP nf ethod Riesult graph Result data l Il2p ma TEST 1 T 06 Potential scanlaml no labels 2 scan 1 Save dala Save dataset Delete Delete all Data appear 201 pnts Scan completed Test2 TESTCELL1 TEST2 imf File Load method Start lviumStat Control File Options
38. Level Level Stage Properties Until An1 gt On value Level Level Stage Properties Until An1 lt On value Level Level Stage Properties Until dAn1 dt gt On value Level Level Stage Properties Until dAn1 dt lt On value Level Level Stage Properties Until dE dt gt On value Level Level Stage Properties Until dE dt lt On value Level
39. Current Stripping Stripping currert Current stripping On Cycles Standard level 1 65535 0 ChronoAmperometry Chrono Potentiometry standard MixedMode Abort Cycles Cycles separate Thresholds Cycles separate On time 0 Off
40. save fitresult load Zplot files Zplot save a Zplot files Zplot Edit copy graph copy simulated Options fitting options Optimize _Error weight equal for each bpoint propotional to absolute impeadance propotional to value Allow negative values R C etc 68 7 R C W
41. S10 AutoCR Current Range Max Min S5 Transients ChronoPotentiometry CIWWJirl Fle Qptions Took Help Abouk Connect lt 1ua Basc lt sigvew Dect Mehod Resuk gaph Resut data D Wiumslatwmanualcp1 scae Anapss E amp LnearSweep Scanlawl CyclcVoammety Multicycle CP no labels Transients ElectoAnalysis Yscan 1 cycle 1 I Impedance Cycles separate Of Thresholds an E max 0300 V E mn 0200 V Imlerval time 001 Cunent Range 1uA Potential range 4V IPretreatment 0 _ levets AUX dgW Potential Example of ChronoPotentiometry with 2 levels and 4 cycles and dnamic levelswitching at 0 9 Vok and 0 2 Vok 255 10
42. Basic Advanced Basic Mode Advanced Mode Advanced Mode SigView 4 dummy1 1kQ dummy2 100kQ dummy3 10MQ dummy4 100 1k 1F Method Direct 2 Test 1 TESTCELL1
43. occasion flyers E step Scanrate 1 E end Amplitude istep Frequency E start E step Scanrate ElectroAnalysis AC Voltammetry Method Value Title E start 10 9226V E end 10 9226V E step 0 125 1000mV Scanrate 0 00001 1000V s Amplitude 0 05 1000mV AC Frequency 10 lt 20000000Hz Phase sensitive On Off On Off RMS Phase 0 180 C Current Range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 5
44. Automatic save filename Automatic save on completion On Automatic save save every X BiStat W2 80 S9 Method BiStat CR min BiStat CR max BiStat Current range WE2 CRmin lt gt CR max BiStat E offset W2 2V BiStat mode Standard Scanning Standard WE2 R Scanning W2 WE W2 W1 x un
45. S10 AutoCR Current Range Max Min ElectroAnalysis AC Voltammetry AC AC AC RMS AC 1 1 AC
46. Plus Plus 12V Plus CompactStatPlus US USB 2 BiStat 2 s2 Mtnod 1 3 Method IviumStat IviumSoft CompactStat IviumSoft P 10 Connect CompactStat Connect
47. Interval time 0 00001 2 5s Current Range 10nA 10A 1 Potential Range 1mV 10V IPretreatment Leve 1 5 5 14294901760s Data Options P 57 Data reduction On Off On Off Aerage every 1 65535 AUX 10 38 5 Transients MixedMode MixedMode OCP DC OCP
48. PC USB CompactStat AC IviumSoft USB 1 IviumSoft CD ROM 2 CD ROM setup exe 1 CompactStat USB CompactStat 2 USB 2 IviumStat USB 3 A
49. CompactStat USB PC USB connect IviumStat POWER CEL OFF PC connect Tool Restore Device 3 Restore factory setting Restore factory firmware Restore previous firmware
50. Apply wrt OCP E start wrt OCP On E start OCP Off E start Apply wrt OCP monitor interval OCP Apply wrt OCP monitor time OCP OCP Apply wrt OCP Record real E On Off OCP Apply wrt OCP Vtx End wrt OCP On Verex E_end OOP Off AutoCR 100 Current Range AutoCR Max range AutoCR Min Range AutoCR Max range AutoCR Min range Automatic save
51. Q wl o X Ain ocp pre Q Ain ocp OCP pre pretereatment Q X Scale Autoscale Scale X axis ScaleY axis Scale Z axis 3D 2 Edit Smooth Savitzky Golay Analysis Eauivalent circuit Corrosion rate Peakfind automatic
52. L ClearGraph Loop 32 Loop Loopend Loop Loopend Loop LoopCycles SetMuxTolndex Loopend Loop Loopend 60 6 DirectCommand SetMuxChannel DigOuts Digout2 1 HI
53. DualCR On Off 2 On Off AutoCR Max Min SwichFreq Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 5 1 4294901760s AUX 10 AutoCR Current Range Max Min 55 5 Impedance CurrentScan Istart lstep lend Inpedance Constat V P50
54. OCP OCP Autoscale Graph options Data appearance 0 ScaleXaxis Autoscale Graph options Data appearance Scale X axis LC ScaleYaxis Scale Z axis Scale Z axis 3D 2 Print graph Copy graph Printgraph Windows Setphase
55. W S R C W2 2 R S W C W galvanostatic C W potententiostatic R W C amp W 2 4 0 2 1A 200 mV 4
56. Direct 5 LoadBatch SaveBatch DeleteLine Line anie DAvumseNBschFiexpachmurg InsertLine Line Melhod alder TE Line Datafolder D wwiumstaNBatchFiles Test Loop Methodfile dd line Delete ine Insert ine Test Line Popeees NO Line 1 Loadkiethod hethodfile testmusx1 gt LoopCycless2 Start Line 3 ExeculekMelhad Savedatafile tmux Line 4 LoopEnd Line 5 Empty AbortLine Line Line AbortBatch Line Set Line 2 properties LoopCycles SethlusTolndes Y On 2 Line1 testmux1 Method Start bort line Abort batch set Abotine _Abotbah Line2 2
57. Filter Stability Z1 Z2 kohm 0 8_ 0 6_ 0 4 0 2_ 0 0_ 2l Phi Rs Cs Rs Cs Z 2Z Z Z 3D Y Y Y Y 3D Impedance 00 2ZA kahm 51 NN 5 Impedance Constant E Method Value Title
58. Par CDC Fixed Value Error Unit Calc Calc Startvalue The Fit range start end Simulate Execute
59. Scan P 23 28 Start Abort P 19 File save data 2 save data P 19 CompactStat AC DC DC USB CompactStat PC USB lviumSoft CompactStat
60. Analoglnputs Plot title Axis title Transform Ecoorrections Offset Potential Convert Reference Electrode potentials Electrode awwae am awma7 am amae am Hg Hg2CI2 sat KCI Ag AgCl sat KCI NN 5 Advanced Method Value Equilibration time 1 65535s E start Filter Automatic 1M 100k 10k 1k 10 Hz X Y Stability Hispeed Standard High stability Connect to Cel 4EL Cel 2EL Dummy1 Dummy2 Dummy
61. Close Stop viumSoft Help menu Contents Topic search Help on help Method IL Start gt 0 Cell after meas ON Pretreatment OCP Open Cell Potentia OCP Advanced Apply wrt OCP ON Equilibration time gt 0O E_start Advanced Eauilibration time
62. 100kHz 1MHz 100kHz 10kHz 1kHz 10Hz Edoubler IviumStat20V 20V 2 5A 20V 0 66mV HiMux 8ch 2V 1 V s 10000V s LSV CV 4mm x 32 dd BNC 8 8 x 2 0V IMP 10 Q LinScan 2V 1uV s 10000V s LSV CV Plus CompactStat 20V 250mA 20V 0 66mV re NN 100mA 89
63. Tools menu Device maintenance Verify S N Verify Fimware Set Configration BiStat Code Calibration Manual contol Upgrade firmware p 77 20 S4 Method Upload file Restore device Performance test 1 ASCTI
64. CurrentScan 29 5 LinearSweep Standard E_step E_step Scanrate Standard 2m HiSpeed Scanrate Estep 100 000 Hispeed DynamicVertexes AutoCR LinearSweep CurrentAveraging LinearSweep Standard
65. Q CPE L T 0O G Gerisher del del Accept CDC Apply CDC
66. Amplitude I step Frequency I start Start End I step Scanrate Impedance CurrentScan Method Value Title I start 10 9226V I end 10 9226V I step 0 125 1000mV IFrequencies AC P 50 Current Range 1pA 10A Cell after meas On Off On Off E standby 10 9226V IPretreatment Leve 1 5 5 1 4294901760s AUX 10 56 Data Option 5
67. Rs Z1 Cs 1 2 7 frequency Z2 10Hz 2MHz 0 2 2 5 ElectroAnalysis AC Detection Method Value Title E start 10 9226V Interval time 0 002 2 5s Run time 2s 2000000000s Amplitude 0 05 1000mV AC Frequency 10 20000000Hz Current Range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 5 1 4294901760s Data Options 7 P 57 AUX 10 48 5 mu 1 ElectroAnalysis Normal Pulse Voltammetry
68. IR SIgView Direct Fescale Dptions Copy We ge black left blue right Direct 1 7 FS E FS nn 0 2 0 4 tim amp ng 1 D Freq 1000 Hz lgain 32 Filter 1 CR 1ma Egain 54 Cauplin 1 18 S4 Method SsS4 Method File menu Method Start Method
69. P 57 Data reduction On Off On Off Aerage every 1 65535 AUX 8 10 42 5 mu 1 1 ElectroAnalysis Amperometric Detection ElectroAnalysis Amperometric Detection Method Value Title E start 10 9226V Interval time 0 002 2 5s N samples 5 2048pnts Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E stand
70. USB PC USB 500 mA CompactStat 10 mA 2 500 mA PC IviumSoft CompactStat 8 amp 1 LED 50 mA 1 USB USB 2 500 mA USB CompactStat
71. 12nV 10V 0 05fA 5A 4nV 4V 0 05fA 30mA gt 100GQ 8pF E 10pA M in8 out2 0 4V 16bit in2 out3 0 5V A C 10 Hz 2MHz 0 5V X Y 4V EE ei OO 6VA USB 1 1 20 WxDxH 260 x 330 x 120 mm 120 x 260 x 25 mm 4 0kg 0 6kg PC WindowsXP Vista or 2000 USB 88 S10 Bistat W2 W2 RE W2 W 30mA W 2V 2 0V 0 0625mV se 25 1pA 10mA 11 2 4 0 076 0 0000023 0 15fA 2 W
72. LED P 10 Method LinearSweep Impedance Method P 19 58 4 Method 5 6 7 8 9 Method Basic Advanced Method P 19 58 W W2 S R C GND P 11 12 Method Start l P 19 Result graph Result data Result data Refresh
73. Max Min 52 5 Impedance Constant I Constant E DC amp AC Inpedance Constat V P50 Impedance Constant Method Value Title I start 10 9226V IFrequencies AC P 50 Current Range 1pA 10A Cell after meas On Off On Off E standby 10 9226V IPretreatment Leve 1 5 5
74. 2 Exponential exponent 1 6 3 2 CV Search Peaks Baseline subtract Peak search Fescale Copy qranh Io Fe in KNO3 0 2 In Potential Set markers with Left Mouse button and press sublract baseline when ready Baseline type Marked baseline properties lt palunomial marked exponential marked automatic calculate Sublract baseline automalic Calculate Baselin undo subtraction Figure 2 baseline determination of CV forward scan CV CV reverse scan 74 7 Search Peaks Baseline sublract Feak search Hescale copy araph Fe in KNO3 6 4 0 2 0 0 0 2 Potential V Set markers with Left Mouse button and nress subtract baseline when ready Baseline pe Marked baseline properties ial
75. Cell Bistat4 4 W2 Cell Bistat2 W C W2 Stability hispeed standard high Filter 1MHz 100kHz 10kHz 1kHz 10Hz Apply BiStat AC Extern analog input 8 analog output 2 digital output 3 digital input 2 iRcomp
76. Manual peak addition 72 7 Add marked peak 2 3 3 2 Cyclic Voltammetry CV reverse scan Baseline subtraction Baseline subtract
77. GND 11 2 2 e W S C R 2 EL W S C R W C 4 EL 3 W S C R 2 4 W C R S
78. 2 HiMux 15 IviumStat CompactStat 32 BNC HiMux HiMux HiMux HiMux 1 F 3 M HiMux3 Plus Plus 15 CompactStat
79. Edit frequenciess Frequencies Start End Frequencies each decade 1 Applyl Frequency scan Start End Amplitude Mnual override 50 Edit frequencies Frequencies Frequency scan Start End Amplitude 10 1 2 Frequencies each decade 2 apply 2nnnn H 1 0 Manual nyerride ea 20000 00 EE55 57 10 00 2214 23 10 00 735 78 245 17 1000 1000 1 58 10 00 27 14 10 00 9 03 10 00 301 10 00 1 00 Advanced
80. 005mV 1000mV Impedance Frequencies 0 0001mV 1000mV Analog inputs 8ch 2ch ch1 ch2 4 ch ch1 amp ch2 ch3 amp ch4 8ch Extra View Apply wrt OCP Open Cell Potential Method C OCP OCP E_start Apply wrt OCP E start wrt OCP On Extra View OCP
81. 1 4294901760s AUX 10 53 5 Impedance PotentialScan Constant E DC E start Frequencies start end Estep stat end E end idf iids Inpedance Constat V P50 Z1 Z2 Y1 Y2 etc Escan CsvsE I E end 2 vsE Amplitude ZsE Y vsE E step Frequency 0 MM 3 Start End Mo
82. HiSpeed Title Levels 255 Cycles 0 65535 Cycles seprate On Off Interval time 0 00001 2 5s Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 5 1 4294901760s Data Options P 57 Data reduction On Off On Off Average every 1 65535 AUX
83. S10 AutoCR Current Range Max Min hey 5 Transients ChronoAmperometry 255 10 4x10 2m 2m HiSpeed 8192 Data reduction average
84. Stop 69 7 Accept Cancel o IviumSoft peak finding Analysis Peakfind automatic Peakfind advanced Automatic Advanced Advanced
85. 255 65535 1xS OCP lt 5mS 2mS 0 2S Stages E applied E control I applied control Duration Record ac Until E gt OCP Until E OCP Until I
86. CompactStat 5V USB USB PC USB A B 37 ON LED PC LED CELL LED LED 9 CompactStat USB DC USB
87. Line3 method tmux Line4 62 7 5 Idens Current density Method Data Option Data Option Apply to selected data Idens
88. Save dataset Save data 19 S4 Method Options menu Options OSettings 60Hz 60Hz XR 20V mode lviumStatXR Edoubler Edoubler 2007 11 CompactStatPlus CompactStatPlus AC input AC input viumBoost40A 20A 40A 20A FRA settingsheet FRA Stabilisation period AC
89. 21 S4 Method LSV CV Method Method a im Method Direct Ee Le Method Equilibration time 0s Current Range 1m amp Filer 10kHz Stability high stability Connectto Cel4EL lt Oo PU Method a i Compensation 100 0 Ohm BiStat On E offset 0250 V Current Range 1ma CR min 1ma Method Frelrealment 0 _ levels Dala Options Automatic save Y On flename databackup save evety 3600 s on completon Dff
90. On Off I max 40A 1 min 40A E step 0 125 1000mV Scanrate 0 00001 1000V s Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 5 1 lt 4294901760s Data Options P 57 AUX S10 AutoCR Current Range Max Min 31 E
91. 57 Advance Method 58 BiStat 59 6 Batch 60 S 7 S8 automatic advanced DLL S 9 Method S 10 63 63 63 64 65 66 68 70 7 1 76 78 78 79 79 80 88 89 8 amp 1 S 1 IviumSo t IviumSoft 1 CompactStat IviumStat PC
92. CompactStat Connect IviumSoft CompactStat CompactStat LED IjviumStat iviumStat PC USB USB IiviumSoff Connect IviumSofft IviumStat DISCONNECT 1 2 3
93. LO ValueText Incremental Method table II true viumSoft BatchEditor
94. Tools Device mentenance Calibrate measurement offset Calibrate applied offset Restore factory options PC PC USB Tool Device Mentenance Met
95. E step Equilibration time E_start Start E_start Equilibration time Filter 1MHz 100kHz 10kHz 1kHz 10Hz Basic X Y DO Method Method Frequencies 255 Frequencies Amplitude 0 1mV 1V Frequencies Frequencies each decade 1
96. Search Peaks Baseline subtract Feak search Fescale Copy qranh 0 4 Potential Set markers with Left Mouse button and press subtract baseline when ready Baseline type Marked baseline properties lt polynomial marked order i WAY exponential marked I CVrevesescan automaticcalculate subtract baseline Cautomatic C3 ETC9 clearmakers undo subtraction example of baseline subtraction with a bth order polynomial subtract baseline 73 7 2 Polynomial 1
97. on O1 NM 1 CyclicVoltammetry Standard E_start Vertex 1 Vertex 1 Vertex 2 Vertex 2 E_begin 1 E _step E_step Scanrate Standard 2m HiSpeed Fe in KNO3 Ss 20_ 4 NN 10 6 0_ 0 10 8 2 cg HiSpeed 32 000 ReverseScan
98. 4x10 2m 2m HiSpeed 8192 E max E min level level level level1 2 4 0 9V 0 2V 3 3D lviumStat Control Fle Options Tools Help abouk Comect IIl Ilov Ext 1uA Em gt sigviewl Diect Method Result graph Hesuk data
99. Frequencies DC DC PC ImpedanceConstant 1
100. Level Stage Properties Until dI dt gt On value Level Level Stage Properties Until dI dt lt On value Level Level Stage Properties Until Ifraction gt Level Level Stage Properties Until Ql gt Level Thresholds Level LinearSweep Galvanostatic ChronoPotentiometry E max E min
101. BatchMode BatchEditor LoadBatch SaveBatch Batch File Method Methodfolder Datafolder methodfile imf Methodfolder Datafolder 61 S6 BatchCommand Line BatchParameter BatchCommand AgdLine
102. Save dataset ids Loadmethod imf Save method imf Export data as ASCI Import data as ASCII Result data Export Copy all to Clipboard P 28 IviumSoft Cyclic Voltammetry
103. Frequencies End 10Hz 2MHz Frequencies Manual override Frequencies Start 10 Hz 2MHz Frequency Transients Mixed Mode 10 2MHz Impedance Frequencies 1 4MHz Ifraction mixed mode Econtro bulk Interval time 2 1 interval time scanrateE_step IR feedback
104. Data reduction ChronoAmperometry ChronoPotentiometry standard mode MixedMode PC Interval time 0 002 average 500 1 1 600 10 1 2 2m 0 5m 1 amp 2 Data reduction average 65535 Deposition time ElectroAnalysis Potent
105. D iviumstat manualicp1 FF LinearSweep Scan Diay 1 ce HTransients HElectro amp nalysis F scan 1 lcycle 1 Impedance scan 2 cycle 2 scan 3 cycle 3 scan 4 eycle 4 Mode Standard Title Mulicycle CP _Levels 2 _ levels Cycles 4 ck Gcessmaae Pon Thresholds I nn Mt 0300 Save dala min 0 200 Interval time 001 s Save dataset Current Hange 1u amp Delele Potentialrange 4V Delete al IPretreatment 0 _ levels AUX gf Potential scan completed Same experiment as above with CyclesSeparate option activated gnd plotted in 3D with cycles index as depth axis 37 5 Transients ChronoPotentiometry Method Value Mode Standard HiSpeed Title I Levels 255 Cycles 0 65535 Cycles seprate On Off Thresholds On Off On Of E max 20V E min 20V
106. HiSpeed 2Hz 50kHz Hispeed standard high stabirity Basic High speed DC Method Method Transients Mixed Mode 1 255 Mode Leveln Stage Properties E applied Stage Properties SweepE On Level Stage Properties Sweepl On Level Stage Properties SweepE E
107. M Cell after measurement E standby Cell after measurement E standby Connect to Cel 2EL C W Dummy 1 1kQ Dummy 2 100kQ Dummy 3 10MQ Dummy 4 1kQ 1F 1006 Current range AutoCR 3 3 4 Current stripping Current stripping Off On
108. On Off 1 max 40A 1 min 40A Vertex 1 10 9226V 1 Vertex 2 10 9226V 2 E step 0 125 1000mV N scans 1 65535 Scanrate 0 00001 lt 1000V s Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 5 1 4294901760s Data Options P 57 AUX
109. 1 4294901760s Data Options P 57 AUX 10 5 ElectroAnalysis Potentiometric Stripping OCP Off On dt d
110. 5 1 4294901760s Data Options 7 P 57 AUX 10 AutoCR Current Range Max Min 49 Impedance Constant E Methodgrid Frequencies Frequency scan Start Frequency scan End Frequencies 1 Frequency each decade Frequench each decade
111. Connect serial number box IviumSoft 1 IviumSoft Eovl C R lovl W 3 Ext 1 13 2 current range AutoCR ON
112. Cycles seprate On Off Interval time 0 00001 2 5s Amplitude 0 05 1000mV AC Frequency 10 2000000Hz Current Range 1pA 10A Potential range 1mV 10V AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Data Options P 57 Data reduction On Off On Off Aerage every 1 65535 AUX 810 AutoCR Current Range Max Min x 41 Transients Elec
113. W Scanrate W2 W W2 E offset W 01V E offset 1V W 0 1V W2 1 0V W W2 E offset Apply wrt OCP Estart wrt OCP On E sart OCP E offset W2 BiStat W2 W2 Result data W 59 S6 lt S 6 Batch 5 4 Method BatchMode Method
114. alldata extended data 7 070P2DRR ME A CV ChronoAmpero metry etc Current units Potential units Time units Impedance 1 Z2 Z phi 28 5 S Methods LinearSweep LSV Standard CurrentAveraging TrueLinear LinScan Galvanostatic CyclicVoltammetry CV Standard CurrentAveraging T
115. Interval time 2m average 500 1 PC interbval time 2m 0 5m ChronoAmperometry ChronoPotentiometry standard mode MixedMode luCtWWriirl File Options Tools Help About Connect lt 1ma Advanced il sigyiewl Direct Melhod Fesuk graph Result data D MyiumstalNmanualNchronoampFlaalle Scale Analysis gt Edit Chrona amp mperometry 2D A Scan Olay ChronoPotentiometry ER Scan 1 RE 1 OOOGGGGGOGGGGGGGO6S Electrodnalysis Amperometric Detection scan 1 chronodr Differential Pulse zm Sauare Wave lt Cor Mode HiSpeed Tile Scan 1 Leve 5 _ levels Interyal time O0001 essesoo Equilibration tme Ds Current Range 1ma Filter automatic 3 EPC Stability automatic 1 Connect to Cel4EL Se Analog inpuls none Delele apply wrt OCP NH Delete al FIR feedback Of F BiStat nf nr Cell after meas 35 NN 5 Transients ChronoAmperometry Method Value Mode Standard
116. 87 10 S 10 IviumStat IviumStat20V CompactStat CompactStatPlus a 30mA i PR USB ImA 250mA 10V 20V 7 5V 20V 1MHz small 300kHz large 1MHz High Speed Standard High stability 1MHz 100kHz 10kHz 1kHz 10Hz 16bit 100000 10g 10V IE 4 096V 20V 0 33mV 0 125mV 0 66mV 0 2 2mV 6 10nA 10A 10 i a 1pA 10pA 100pA 1nA 0 015 0 15fA 1 V s 10000V s 0 033 0 0125 0 2 G 1mV 10V 5 a hm S 5 5 0 003 40nV 0 003 16nV F 10 Hz 2MHz R 0 015mV 1 0V PS 0 03 100 GS A
117. Chan WMF Olay df CTRL Shift ids Scan Chan nlal channel 1 channel 2 channel 3 channel 4 channel 5 channel 5 channel channel 8 Dat
118. Method Direct 3 standard stability lt lt 100u amp fo kHz filter Direct C 10uA Ap oo 1uA DC AC DC AC 1mmnA AC 1nma AC 0 Analog outpu ch1 nnnn V Eh2 nnnn IRcorr IR IR comp Digital output Digout1 HiSens 4 Fs Digital input IRcorr 1 E Rs Cs Current Range
119. Peakfind advanced Clear peaks Impeadance plot selection IPhi Rs Cs Rs Cs ZZ 3 D 3 YY Y Y 3D 3 Ziffreq Z Z Yijfreq Y Y 27 S4 Method Result data Hesult qraph Refresh Export Refresh Show data Export selected dala lt alldala Ref
120. Windows WMF Copy graph Copy TAB CR WORD EXCEL 1 1 Export Result 63 7 Beneral Lowpassfilter Cut off Cut off Apply FBand reject flter 50 Hz Badwdn 056 Hz remaye harmanics Apply _Frequency spectrum 5 Hz Log signal kHz nA 100 6 50 O 0 p 200 400 600 BOO time ms Lndo Accept and close Canc
121. AC CVplots CV252 ET SE CV plots 23 S4 Method 3 Graph options Display X Y 3D parameters 3 Granh Disnlay Options Graph Disnlay Options Result E Volt Current IPBHGHtIOTIS SEDDONS 24 Scan Result graph scan Save data Save dataset Delete Delete all
122. i E ysi Hescal Surface area 10 am2 Leg SE EE Equivalent weight 10 B Corrosion rate analysis Density ip gcm 3 CE EE 01841 01717 rer A B125E6 5 125E 5 6052 7882 0171 E 0317 0 02004 IZ Automatic analysis Slope Analysis 7 Tafel Analysis Model Analysis minimize logarithmic errors Clear results Copy results Exit Log Current T T 0 4 0 3 0 2 0 1 nn Potential Potential range markers Eal Ea2 Ec1 Ec2 035 VIn2e1 MM 0127 0057 Clear Tafel Amalysis Slope Analysis Rp Tafel Analysis Model Analysis 3
123. malk polynomial marked 0 eiponential makedl CCa Fautomatic calculate subtract baseline Cautomatic C3 Bd clearmarkers Calculate baseline undo subtraction Search Peaks Baseline subtract Peak search 3 Fe in KNO3 D 5 4 0 2 In 0 2 Potential V Set markers with Left Mouse button and press subtract baseline when ready Baseline hpe Marked baseline properles polynomial marked order I MT 2 WoWY II UR CY reyerse scan IF aulomalic calculale acl aulomalic 3 ECd clearmakers calculate baseline undo subtacion exponential marked 75 7 lviumSoft level finding Analysis Find Levels 9 LIIS Valuc Unit Search pi plsicao ThreshoH aope 0005 Chro
124. 1 gt 2D 3D 3Di 2 3 ee 5 3 Result 6 2 F 3Di 1 3 iri Zm Cor Zoom Correct L R 2nd Delete Point
125. E start 10 9226V Frequencies AC P 50 Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A DualCR On Off 2 On Off AutoCR Max Min SwitchFreq Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 1 4294901760s 5 Data Options P 57 AUX S10 AutoCR Current Range
126. S 5 Method S 9Method F1 22 S4 Method 2 Resul tgraph 1 Result data DPV ps sensor a RS 1 2 Ain 8 SS 94 32 i 4 es otentia v HH Pretreatment
127. 00000s On completion On Off On Modules 58 S6 BiStat BiStat P 11 12 Method LSV Standard CurrentAveraging TrueLinear CV Standard CurrentAveraging TrueLinear Transients ChronoAmperometory ElectroAnlysis Amperometric Detection Method Advancemode Method BiStat On BiStat BiStat Mode Mode Standard Scanning Standard 3 R W E offset Apply wrt OCP Estart wrt OCP On E offset Scanning Scanning Method LSV CV
128. 2 23 23 24 25 26 28 29 30 30 30 30 31 32 33 33 CyclicVoltammetry Galvanosstatic 33 ChclicVoltammetry CV Method 34 Transients Amperometory 35 Transients Amperometory Method 36 Transients ChronoPotentiometry 37 Transients ChronoPotentiometry Metyod 38 Transients MixedMode 39 Transients MixedMode Method 41 Transients ElectroChemicalNoise 42 Transients ElectroChemicalNoise Method 42 ElectroAnalysis Amperometric Detection 43 ElectroAnalysis Amperometric Detection 43 ElectroAnalysis Differential Pulse 44 ElectroAnalysis Differential Pulse 44 ElectroAnalysis Square Wave 45 ElectroAnalysis Square Wave 45 ElectroAnalysis AC Voltammetry 46 ElectroAnalysis AC Voltammetry 46 ElectroAnalysis Potentiometric Stripping 47 ElectroAnalysis Potentiometric Stripping 47 ElectroAnalysis AC Detection 48 ElectroAnalysis AC Detection 48 ElectroAnalysis Normal Pulse Voltammetry 49 ElectroAnalysis Normal Pulse Voltammetry 49 Impedance Constant E 50 Impedance Constant 52 Impedance Constant I 53 Impedance Constant I 53 Impedance PotentialScan 54 Impedance PotentialScan 55 Impedance CurrentScan 56 Impedance CurrentScan 56 DataOption
129. 3 Dummy4 Analog inputs Apply wrt OCP On Off Method OCP Monitor Time 1 2147483647s OCP Monitor interval 1 600s OCP Estart wrt OCP On Off OCP Vtx End wrt OCP On Off OCP Record real E On Off IR feedback On Off On Off Compensation 0 0001 400000000Q IR BiStat On Off On Off E offset 2 5V W2 Current Range 1pA 10mA W2 CR max 1pA 10mA Auto CR min 1pA 10mA Auto Mode Standart Scanning Automatic save On Off On Off Filename Save every 1 10
130. 4 E end E step E start 1 7SQRWV frequency ElectroAnalysis Square Wave Method Value Mode Standard Hispeed Title E start 10 9226V E end 10 9226V Pulse amplitude 1 100mV SQRWV frequency 2 50kHz E step 0 125 1000mV Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A Cell after meas On Off On Off E standby 10 9226V Pretreatment Leve 1 5 5 1 4294901760s Data Options P 57 AUX
131. 73E 01 3 2237259E 01 Clear al peaks Femovepeaknr Automatic peakfind exarmple with whole peak and Tst derivative selected Automatic peak find Oonstruct from whole peak front flank rear flank whole peak front flank rear flank Whole peak Front peak Cyclic Voltammetry Find Method 1st derivative 2nd derivative 1 st derivative 2nd derivat
132. E ElectroAnalysis Potentiometric Stripping Method Value Title E start 10 9226V 1 Deposition time 1 65535s 1 Current Stripping On Off 2 On Off Stripping currert 1nA 10A 2 Current Range 1pA 10A Pretreatment Leve 1 5 5 1 4294901760s AUX 10 47 NN 5 ElectroAnalysis AC Detection AC Voltammetry DC Rs Cs Rs Cs
133. Tools Help abouk mn Diect Mehod ID WyiumstamanuaNTEST1 LinearSweep Standard Current amp veraging TrueLinear Cyclicvoltammetry Standard Mode Standard DNS CE SS E start oo000 V Eend 10000 E step 5 my Scanrate D005 Vs Current Hanae AutoCR Cell after meas Pretreatment _ levels AUX a a Hesul graph Result data seae R Et mn TEST 2 A T T nn 04 T 05 Potential Scanlalal no labels scan 1 Save dala Save dataset Delete Delete all Data appear 201 pnts Start abort lscan completed 15 2 Test3 BiStat TEST3 imf File Load method Start
134. a appear Copy Data appearance show all hide all 25 S4 Method Data appearance Data appearance 5 msgbn Lines none filed circle circle filed square Symbols square filed triangle triangle filed diamond diamand indexed cross lnes symbols Result Resul graph Resull data E scan Scale Analysis Edit ELPhi Rs Cs YY Et5 perlpheral port 3 2ml o Ce
135. by 10 9226V Pretreatment Leve 1 5 1 lt 4294901760s 5 Data Options P 57 AUX S10 AutoCR Current Range Max Min 43 NN 5 ElectroAnalysis Differential Pulse DPV 2 1
136. dard interval time 1 4000000000 HiSpeed 8192 Standard 1 65535 HiSpeed 32678 Standard HiSpeed Standard 500 2mSec HiSpeed 100 000 Standard PC HiSpeed PC Standard AC Voltammetry Y N phase sensitive current detection ny RMS 0 AC Voltammetry RMS Phase sensiti
137. e Standard 2m HiSpeed HiSpeed 32 000 I start Ivertex1 Istart Ilvertex1 Ivertex2 srart Ivertex2 I step 1 Lscanrate A sec I scanrate 1 step 33 5 CyclicVoltammetry CV Method Value Mode Standard HiSpeed Title E start 10 9226V DynamicVertexes On Off
138. el and close Edit General 50 60Hz Fourier General Savitzky Golasy Savitzky Golay 5 11 25
139. end Stage Properties Sweepl lend Stage Properties SweepE scanrate Stage Properties SweepIl scanrate Stage Properties Duration Stage Properties Record ac On Method Frequency Amplitude Stage Properties UntilE gt On value Level Level Stage Properties UntilE On value Level Level 85 S9 Method Stage Properties UntilI gt Level Level Stage Properties UntilI lt
140. f Charge On Off Unit text value 76 7 Smoothing none 5 11 25 Savitzky Golay lviumSoftiict Copy results Copy graph MSWORD EXCEL idf 77 8 S8
141. gt Until lt Until dE dt gt OCP Until dE dt lt OCP Until dl dt gt Until dl dt lt Until An1 gt Until An1 lt 7 Until dAn1 dt gt 7 Until dAn1 dt lt 7 Until Ifraction Until Ql gt DC 2ch
142. hod 1 Start close Device Mentenance Reboot Device PC Method 1 Method 2 Start restore instrument 78 8 IviumStat CompactStat
143. iometric Stripping Method E_start Dual CR On SwitchFreq 2 AutoCR Max Min range Dual CR SwichFreq DynamicVertexes On LSV CV DynamicVertexes L max LSV CV DynamicVertexes L min LSV CV E end 82 S9 Method E start
144. ive Linear Sweep Cyclic Voltammetry Height mode proportional absolute 71 7 Minimum height Height mode absolute proportional Width mode propotional absolute Minimum width Width mode sabsolute Proportional Sensitivity Smoothing Search Peaks Baseline subt
145. n 1 1 1 1 1 10logIEn NV 10logIRp ohm ma 1 MO MD a Rndlysis type Noise power spectra FT MEMS FFT MENS MEMS co flicirts 30 Wirccw funclior squzer Berilelt wach Hann Heamming Blackmen Subraci bsseine 1 10log frequency Hz Noise impedance 1 n 10log frequency Hz 67 7 Analysis Equivalent circuit Trium Equiyalent Circuit Eyaluator File Edit Optians Graph Dala RlclwlalLlrlolc da il Rescale Option Data ELPhi Fs Ei 2 gt yl eno 1 Equivalent circuit fitting BU R1 R il Accept Clear 40 o et Model R1 C1 R2 Cpc RIC1R2 Apply Par Fixed Value Emor Unit a 20 2 Parl1 R1 1 028E 01 7 55E 02 hm Ft Droge Parl2 R2 1 138E 03 1 3EE n1 Ohm si iteratians 15 Par3 C1 9 653E 05 2 48E 09 F chisquare 2 3E 01 T T T 1 T 1 2 3 4 Fit range start 0 10log frequency Hz end 0 Simulate Stop Accept Cancel File load fitresult
146. noPotentiometry leve find Ninrrur sepaictior 500 Value rclcrcncc absclute 1Ccryett resuk nn factor 1 000 J tims Dff chargs Dn unt Smocthing 5 ports a 30 237E 02 237E 02 5 Jls _Ceprresi 2 1 1 54E 1 1 54E1 Close Find gt find Search for Threshold slope Minimum separation Value refernce absolute differential absolute time 0 differential Convert result On Off Off On Factor 1 Time On Of
147. ract Peak search FeScale Copy graph Copy peaks Search parameters automatic peakfind AA Fe in KNO3 Construct from front lank Find method 2nd derivative Height mode proportional Minimum height 0 025 Width mode absolute Minimum width 0 025 Sensitivity Smoothing 5 points Manual peak addition Add marked peak mark CV reverse scan HH ai oo 2 Clear markers Potential Peak results 4 4081077E O6 0 220 9 2464822E 08 1 8492964E O5 3 4E42724E 0UE 0 134 7 4435075E 10 1 4887015E 08 Clear al peaks Femove peak 1 auiomaiic peakfind exampie with front flank and 2rnd derivative seigofgg Peaksearch parameters
148. resh Export extended dataset Current units A Cm ma pa Ca time unis Copy all to clipboard Copy selected to clipboard Save all data to disk Ss 7 ms ps Save selected to disk Copy all data clipboard Microsoft Excel Show data selected data
149. rueLinear LinScan Galvanostatic Transients TR ChronoAmperometry 255 ChronoPotentiometry 255 MixedMode ElectrochemicalNoise ElectroAnalysis Amperometric detection Differential Pulse Square Wave Potentiometric Stripping Analysis AC Voltammetry AC AC detection AC Normal Pulse Voltammetry Impedance EIS Controlled E Controlled I PotentialScan
150. trochemical Noise viumStat CompactStat Runtime 500 0 15fA 40nV IviumStat 16nV CompactStat R W S 1 Gnd 2 Time domain Frequency domain Transients Electrochemical Noise Method Value Title Interval time 0 002 2 5s Run time 2 2000000000s Current Range 1pA 10A Potential range 1mV 10V Data Options
151. tt Schottky 1 Cs 2 vs E E start lt E step Scanrate Resuk graph Resukdsa Escan Upase TSelect plottype CGCsvse ZlvsE 7 Z2wvsE 7 Y1vsE 7 Y2vsE CMott Schottky 5539 Hz 3155 Hz 1773 Hz 1000 Hz Select potentials fom foov tooov Select frequencies Select potentials from to 54 Impedance PotentialScan Method 5 Value Title E start 10 9226V E end 10 9226V E step 0 125mV 1000mV Frequencies AC P 50 Current Range 1pA 10A AutoCR On Off On Off Max range 1pA 10A Min range 1pA 10A
152. ve AC Voltammetry Levels 5 IviumSoft Pretreatment Method 84 Pulse amplitude Pulse time Run time Scanrate SQRWV freqguency Stability Stage Stage Levels Stage Properties S9 Method Extra View 1 1000mV 0 1m400m scanrate E_step 2Hz 1kHz

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