On-line Micro reaction sampler
Contents
1. A 3 Ver 1 15 5 uL 5 uL 400 4002. Fig 4 4 Step 5 4 2 Ver 1 15 Fig 4 4 Step 5 34 mm 34 mm 4 3 Ver 1 15 4 2
3. 7 1 Ver 1 15 B 40 S3 20 1 Appendix 1 Ver 1 15
4. 5 uL 1 ug uL 5nL GC Fig 6 1 5 ug 5 uL NaOH 0 01 wt 200C 10 min TD 60 270C GC 60 3 220C 509C min 5 5 min 60C 270C GGC UACW polyethyl
5. 9 1 2 Ver 1 15 2 2 1 EGA PY 3030D PY 2020iD PY 3030S PY 2020iS PY 2020iD PY 2020iS 2 2 2 2 5 mm 25 34 mm 2 3 400C 5 uL GC
6. Fig 4 5 4 3 Fig 4 6 Fig 4 6 4 4 Ver 1 15 4 4 B Fig 4 7 B Fig 4 7 5 uL 5 uL
7. Fig 5 2 A Fig 5 2 5 1 Ver 1 15 5 2 GGC 5 3 GC 400C 5 2 Ver 1 15 6
8. On line 1 2 Fig 1 1 Fig 1 2 MPa Pressure 100 200 300 400 Temperature C Fig 1 1 100 uL 1 1 Ver 1 15 Pressure MPa OO on on Oo 100 200 300 400 Temperature C Fig 1 2 100 uL 5 uL 5 uL 400C
9. GC GC 1 Double Shot 1 Fig 4 8 250C 10 250C 60C 2 Double Shot Fig 4 8 Accessories Setting SS Sampling TD 1st Sampling Ready for desorption
10. 4 8 2 1 Ver 1 15 3 3 1 On line Fig 3 1 _ 1 2 oe 7X 1 30 mm 7Nv 4 Fig 3 1 On line 3 1 Ver 1 15 3 2 On line Fig 3 2
11. J A 4 Ver 1 15 PY1 1050 PY1 7052 UV1 3802 On line 1 CD PDF 1 S4 2 1 PY1 1050 PARTS BOX 3 PY1 5311 O O oO 4 iL OO at o 1 1 I i l I 1 a Ht 3 pt PY ET m EE S4 5 oe am 1 Re order UV1 7701 10 RON 1 i S3 3 Re order PY1 5319 20 I B
12. 1 U Fig 4 1 2 Fig 4 2 Step 1 3 Fig 4 2 Step 2 4 Fig 4 2 Step 3 4 1 Ver 1 15 SteD 2 Step 3 Fig 4 2 Step 1 3 5 Fig 4 3 Step 4 Step 4 Fig 4 3 Step 4 6
13. 7 7 A 2 Ver 1 15
14. Fig 3 2 a Pe LE EO I CE 30 mm Fig 3 2 3 2 Ver 1 15 4 CDROM 4 1
15. Fig 4 11 4 8 Ver 1 15 4 9 On line 6 6 GC Fig 4 12 6 6 gt Nylon 6 6 40 pg TMAH 25wt 10 uL Py 300 C Py GC ITF 320 C 1 hr GC 40 2min 320 C 20 C min He 1 mL min Ultra ALLOY 5 5 95 30 m 0 25 mm 0 25 um He 1 0 mLmin 17100 1 4x107 CHyN NCHs NF 4 6 8 10 12 14 16 18 min Fig 4 12 6 6 GC Ver 1 15 5 5 1 Fig 5 1
16. Start 60C 250C GC GC Double Shot Analysis Fig 4 9 4 Ver 1 15 2 Double Shot 2 Fig 4 10 250C 10 Ready for desorption Star Prepare for pyrolysis step No GC
17. 400 4 5 GC GC 4 6 GC 4 5 Ver 1 15 4 7 Double Shot
18. 60C Star 60C 250C 60C Sampling OFF GC Double Shot Analysis Pyrolyzer Furnace TD Initial Initial Rate Final Final Total 8 min Cmin C min min 1st 60 000 600 250 1000 vo31 2nd 0 0 000 ET PY 40 000 y Interface UpperTemp 300 ec lt Auto Manual Accessories SS Settinds Samplind Sampling Cryo Trap TD 1st TD 2nd RY Fig 4 8 4 6 Ver 1 15 Fig 4 9 60C Sampling TD 1st Sampling Ready for injectton
19. 40 2 Reorder PY1 3321 1 a A 5 Ver 1 15 SR ON EN NR NE CN A 2 RR EN EN ECHOECECCEOO PE A 2 NER CC SARA A NRN A 2 0 RO ESC A 3 N A 5 A 6 OWENG RGY2DN2IN 0 1 1 OnneE O NN 1 1 E ES FPP 3 TFPFHFPFYW FFPRITW FPP FFP 1 1 PRMU0ER006M00R00SeNeHSDSKN SNRMNNB08RENNBG0EWBBhSPDSOR HRPIORBEBEERBSRGRRESOG 2 1 OR 2 1 Neeeeieeegreeteae 2 1 MC 2UUYslE f NEWS EPR POP EPC PT 2 1 22 ON 2 1 9 CU en 3 1 3 SS SN RS ERR 3 1 2 SR 3 2 MRRHR Meheeteeoae 4 1 EN CC EN EE 4 1 SS 4 4 4 0 NO RS NNE 4 4 2 LD SC RRM SE CR NE 4 5 2 co UIG 68RG 3 11 EPCL PO 4 5 A TD OO NNN I 4 5 OE RN i 4 6 500 0 Ii 4 8 EE SS 4 9 Ne PP 5 1 5 Ft NAS NAN 5 1 SS SS RA NM PPPRPnPPFP PP 5 2 5 5 2 1 CZKP PITPFTY FFPr
20. Double Shot Analysis olyzer Furnace TD Initial Initial Rate Final Final Total C min Cmin C min min 250 1000 00 00 1000 2nd 0O 0O 000 wv PY 250 0 00 w Interface UpperTemp 300 ec Auto Manual Fig 4 10 Double Shot 4 8 GC GC GC GC 5uL GC Fig 4 11
21. PPPPFHHHPFPHPHPPPYN FFP HREF FFP PH FFP FE PH 6 1 1 5 S p CO PP O00 77000 7 1 HRP Appendix 1 A 6 Ver 1 15 1 On line 1 1 On line TMAH GC
22. Ver 1 15 On line P N PY1 1050 FRUIITIER LAB WWw frontier lab com 1 On line 2 On line GC GC MS
23. englycol PEG20M 30 m 0 25i d 0 25 um fim 1 mL min 1 100 Fig 6 1 6 1 Ver 1 15 7 On ine GC MS 3 0
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