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17. 2200000 gJdgBul T 0 0U H H Developments and their Applications of Auto Sumitomo Chemical Co Ltd mated Systems for Organic Synthesis Organic Synthesis Research Laboratory Hideho Atukazu lwarA Versatile automated systems for organic synthesis have been developed in order to increase the efficiency of chemical experiments and reduce the amount of the chemists work involved therein The design concepts required for our systems are flexible and integrated independent of the developer s tastes Flexible means the use of commercially available softwares and hardwares Integrated means that 1 synthesis and analysis zones are linked in the system and 2 obtained data should be commonly applied to from laboratory to pilot plant or even commercial production Our two types of automated systems based on the same design concept are explained One is a PC personal computer controlled system with DC distributed control systemi functions which manipulates 50 to 100 inputs and outputs in both analog and digital quantities The software of FIX DMACS M was used for its SCADA supervisory control and data acquisition system Another system is a robotic workstation for optimization of reaction conditions which can perform 16 different reactions simultaneously The range of reaction temperature is from 30 to 160 C Typical reactions executed by our robotic syst
18. i80 0 b brj c c 0 0 U D 19 12481 1880 D nud dtd dU 6320 0 00 210 U L 1 3 4 3 D UU 54 278 1996 2000 630 1 211 1999 soo 0 57 90 805 1999 4 T Sugawara et J Autom Chem 16 33 1994 s00 0 31 1159 19951 0 uuguuHuuauuulllul 4 276 1998 Sugawara and D G Cork Lab Robot Automat 8 195 1996 7 J S Lindsey et all
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20. Orchid Biocomputer Inc 10 ny e mu ue 94 2000 1 LA Laboratory Automation O0 000000000000000 uuuiuiuuliiuluulllilLulllullill GUO Graphic User Interface LLL uuauuluiuulluluuiliuliu5llilLilitLtLlL 0000000000 Ncsulll Lindsey uuaubiuuulluiililiiLlititlLilLlLtLutLl Kramer 1 0 O O Rh ne Poulenc wnygpgpgme gmmmgmauggusau uuuiuliiullli B uuulltiututLitL ii lLl LL Combinatorial Chemistry T 0 OOO HATS High Throughput Screening uuuiuiuulluliiiuliilululululululul EBENE
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22. New J Chem 15 153 1991 8 J S Lindsey L A Corkan D Erb Rev Sci Instrum 59 6 940 1988 9 G W Kramer et al Adv Lab Auto Robot 3 361 1986 10 P Metivier et al Chemmetr Intell Lab Syst 17 137 1992 11 OUUU utitulut ull 10 132828 1200 0 00 1997000 13 H Okamoto K Deuchi Lab Robot Automat 12 2 2000 1400 00 00 JDUDUDDUDUDUUDUDU 28 18 14 1999 15 942 313 1973 160 0 O00000 LU 64 8 817 1995 170 19 321 2000 181 420 1 10 1997 19 H Du S Jindal J S Lindsey Chemmetr Intell Lab Syst 48 235 1999 20 W Ehrfeld Ed Microreaction Technology Springer Berlin 1998 2 1999 Hideho PROFILE ut Atukazu lwarA 2000 1
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25. em range from oximation N t Butoxycarbonylation alkylation and cyanation to Grignard reactions The related topics including the algorithm of reac tion optimization combinatorial chemistry and microreactors are also discussed 1 l U 1 14000 0 0 t lID 200071 93
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