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T64000 User manual October 2009

1. Micro Macro Commutation Microscope Figure 2 4 Macroanalysis System using the back scattering configuration T64000 User Manual 64 HORIBA Scientific Using 764000 with the Back scattering Macroanalysis System 10 07 2009 Premonochromator Entrance Slit Filter holder scattered beam see figure 2 2 page 57 Beam splitter see figure 2 2 page 57 Laser Filter wheel with 6 neutral density filters Laser vertical entrance axis Micro Macro commutation knob e Confocal hole adjustment see figure 2 2 page 57 Mirror sliding rail Focusing lens sliding rail 10 Entrance optics XZ adjustments 11 Mirror 12 Focusing lens adjustment T64000 User Manual 13 Focusing lens adaptor 14 XYZ sample holder adjustment 15 Collecting lens adaptor 16 Collection lens focusing adjustment 17 XvY adjustment 18 Back scattering mirror 19 Back scattering selector with the fine tune knob 20 Transfer optics to entrance slit focusing adjust ment 21 Holder for analyzer half wave or quarter wave plates 22 Access to entrance filters holder 65 10 07 2009 HORIBA Scientific CHAPTER 3 Appendix This chapter lists the Options and Accessories available for T64000 System This list is not ex haustive Please ask us for an accessory you have not found here ji BASICINSTRUMENT Basic T64000 Basic T64000 configuration see descrip
2. 300 or 600 g mm to make a one shot spectrum 1200 g mm which is infrared optimized only for NIR version 2 Select the correct grating setting in the software If you change the grating do not forget to go to the zero order position in the software This will give the correct 4 calibration for the particular grating you will use Set the spectrograph to the desired spectral position Select the size of the confocal hole and the slit aperture Select the acquisition time and the number of accumulations this will improve the signal noise ratio Then you have 2 possibilities The icon SREB is a spectrum adjustment so it can help you to maximize the sig nal the new spectrum refreshes the old one and so on No repeated accumu lations or extended spectral ranges are acquired If you press the icon heey it will make a spectrum accumulation and stop T64000 User Manual 56 10 07 2009 HORIBA Scientific Premonochromator o Micro Macro E C ommuta ti on Microscope Premonochromator Entrance Slit 6 Filter holder scattered beam 7 Beam splitter 8 Laser Filter wheel with 6 neutral density filters A WN Laser vertical entrance axis Using T64000 with the Microanalysis System 5 Figure 2 2 Using Microanalysis System Micro Macro commutation button Confocal hole adju
3. Most high end spectroscopic CCD sen sots ate two dimensional with rows and columns of pixels Sensors used in spec troscopy ate typically between 25 mm and 28 mm long and between 5 mm and 12 5 mm high corresponding closely with the size of the focal planes of mod ern spectrographs The fabrication meth ods employed can be modified to optimize sensitivity in the UV VIS or NIR regions of the spectrum HORIBA Scientific offers a wide variety of sensors providing several alternatives in balancing wavelength response sensi tivity and price There are two main cate gories of CCD sensors Front Illuminated and Back Illuminated Front Illuminated CCDs are designed so that the light 1s incident on the CCD but must pass through the CCDs silicon gate before reaching the optically active sili con Standard front illuminated CCDs FIVS are best used for applications where teduced UV response and high full well potential dynamic range are desirable P type Si Charge Packet photoelectrons Front Illuminated CCD Detailed Description Thermoelectric cooling series Back Illuminated CCD Deep UV response of a front illuminated chip is enhanced by either add ing a lumogen coating to the CCD FIUV or by etching a small opening on the electrodes to allow UV light to pass to the silicon The latter type is known as photoelectrons an Open Electrode OPEN CCD Front illuminated chips are free from etaloning Front
4. on page 66 T64000 User Manual 41 10 07 2009 HORI BA Detailed Description Scientific 1 5 13 Macroanalysis System Destination T64000 System Description This option is used to per form analysis on various samples sizes and structures which cannot be processed by the Microanalysis Sys tem Option There are different options according to your needs Visible version UV Visible version Laser periscope for lifting the beam of a laser installed at the front of the system up to the level of the entrance axis of the Macrochamber Macrochamber attachment with laser shutter interference filter and half wave plate holders To be used at entrance of the Macrochamber when no laser entry is on the system See detailed composition of each option in the Appendix on page 66 Requirements The overall configuration must be known to adapt the devices Figure 1 8 Macrochamber overall view T64000 User Manual 42 10 07 2009 HORIBA Scientific slit sample distance E 8 7 6 From Micro Macro Commutation Box Detailed Description Step by step vertical adjustment of the sample platform Vertical fine tune adjustment of the sample platform Knurled button to remove the platform XY fine tune of the sample plat form Back collecting mirror Platform Optional focusing a
5. 11 Power ON the Computer and the screen 12 Switch the laser source ON please refer to the Manual delivered with the unit 13 Do not forget to wait for temperature stabilization Estimation time for each sub unit is the following 14 PMT Detector Maximum cooling temperature will be reached in several hours To 1 get the best performance in dark noise we recommend to keep the SpectraLink turned on so that the PMT 1s kept powered and to never stop the water circulation in the PMT housing 15 SpectraLink this unit must be powered for at least 30 minutes 16 CCD Detector please refer to the explanations detailed in the related User Manual 17 Laser please refer to the Manual delivered with the unit 18 2 Load the LabSpec software The software has been already installed and setup per formed Please refer to the LabSpec User Manual T64000 User Manual 54 10 07 2009 HORI BA Using T64000 with the Microanalysis System Scientific Push down the Micro Macro selector see Micro Macro Mirror on page 40 and 6 fioure 2 2 Position your sample on the Microscope Stage Refer to the Microscope User Manual Confocal feature The T64000 Microanalysis System includes an integrated confocal microRaman system The confocal microscope is coupled to the Single Triple stages spectrometer On the incoming path the laser beam is reflected towards the microscope by the means of a special filter dielectric edge filter used in injec
6. Appendix Chaptet Many different microscope types are available Visible Standard as shown on the photo Visible open microscope free space below the objectives Visible standard with line scan feature UV Visible UV Visible open version Visible Inverted microscope UV Visible Inverted microscope See detailed composition of each option in the Appendix on page 66 The Micro Macro Triple Single Commutation sub unit is required for the signal which exits the microscope and enters the 164000 third stage see page 39 Video Camera neutral Density Filters are required These filters are located on the Laser Entrance path Microscope operation instructions please refer to the manufacturer manual delivered with each System T64000 User Manual 40 10 07 2009 HORI BA Detailed Description Scientific Exchangeable beam splitter Half wave plate u NUV UVB NIR UVB NUV1 NUV2 Visible NIR1 NIR2 Video camera Analyzers UV Visible NIR Scrambler Coupling Optics Point illumination Line scanning U V coupling White light Illuminator optical fiber with Koehler Micro Macro Commutation option Objectives 10X 50X 100X Options UVB NUV LWD ULWD NIR LWD NIR Interferential filters and A 2 plates XY Stage manual Condense Safety filters wheel and safety shutter with key Figure 1 7 Microscope general presentation see the options in the Appendix
7. HORIBA Scientific 164000 System User Manual Part Number 31 087 146 Explore the future Automotive Test Systems Process amp Environmental Medical Semiconductor Scientific HORIBA 10 07 2009 HORIBA Scientific COPYRIGHT Copyright 2009 HORIBA Jobin Yvon All rights reserved No parts of this publication may be reproduced transmitted transcribed stored in a retrieval system or translated into any language or computer language in any form or by any means electronic mechanical magnetic optical chemical manual or otherwise without prior written permission of HORIBA Jobin Yvon FRANCE NOTICE TO THE USER This manual should not be construed as any representation or warranty with respect to the unit named herein Occasionally changes or variations exist in the unit that are not reflected in the manual Generally should such changes or variations exist and affect the product significantly a release note would accompany the manual In such a case be sure to read the release note before using the product Trademarks LabSpec are registered trademarks of HORIBA Jobin Yvon Windows NT 98 2000 XP VISTA are registered trademarks of Microsoft Corporation All Rights Reserved Printed in France NP T64000 fm 10 07 2009 HORIBA Jobin Yvon S A S 16 18 rue du Canal Headquarters 91165 LONGJUMEAU CEDEX France Tel 33 0 1 64 54 13 00 Fax 33 0 1 69 09 93 19 33 0 1 69 09 90 88 Internet site h
8. TS screen or video camera This VAY ZZ Z77777777777Z7777777777777Z77777Z7 Z4 device allows the user to moni tor the alignment of the sample image on the entrance slit L N 1 SR S EAA i tes 1 Viewer for Visible range sup plied with a viewing screen 2 Viewer for Visible range sup plied with a C mount adapter and density filters attachment ON Camera not included 3 Viewer for UV Visible range down to 240nm supplied with a C mount adapter and density fil ters attachment Camera not included N A B d K y E NI LIIT L 6 ERE SESE 09 0 N C i H CR WE NN NN SN NNN L From the Axial Entrance Slit Color Camera 1280x1024 pixels with cable none 38 10 07 2009 HORIBA Scientific Detailed Description 1 5 9 Micro Macro Single Triple Entrance Commutation Wheel for Visible Range Destination Description Option Additional Requirements T64000 System The Micro Macro Triple Single Commutation Sub unit commutes the analyzed beam to four different paths From the microscope to the double premonochromator entrance From the microscope to the third stage entrance From the macro sample compartment to the double premonochroma tor entrance From the macro sample compartment to the third stage entrance 1 Micro Macro Ttriple Single Commutation wheel 2 For System equipped only with a Visible Microscope for selecting either tri
9. ERU AREE PEE 29 D CO L oes p eee eee eer eres ban IURE SRL gap TESI PIRE IE E 29 IS eee 22242929 sasaxa 2644 aa a ooh aa AeA ea z d Ru R ROROR x Pa S squa a E 32 Overall DIDielsIOHS 2 20 sssi EGRE URGES RE RE a asha sus RE wass dod sua aa 33 Environmental conditions 34 JUD P 34 Cleaning InSIrIUCHOnS suu accu Cera o e e o Ogni EG Sao eee OQ 34 Detailed DeSCEIDUO u s y ss x vos DEN E cate een E PSEDUIPES S P ED RPEEOTLEPEPEIE CLE S 34 Ist Stage Lateral Entrance Slit _ 35 T64000 User Manual 16 10 07 2009 HORIBA Scientific Intermediate Slit Motorization 35 Spectrograph Lateral Entrance Slit 36 Manual Axial Entrance Slit _ 36 2nd Stage Manual Axial exit Slit 0 21 as 37 Double Additive Adaptation 97 Spectrograph Axial BOSE Soo ied a RR AR ote e de git dob si ian a R aqa qaqas dup woods 38 big Arm 38 Micro Macro Single Triple Entrance Commutation Wheel for Visible Range 39 Micro Macro Single Triple Entrance Commutation for UV VIS Range 39 Micro M CPO dili MP 40 Confocal Microanalysis System es 40 Macroanalysis Vee 220 2644 han dagen hed dodo doe does Row RRR doa G9 ae ds 42 Stokes Antistokes accesso
10. Item T MAC LAS ENTRY inch Lambda 2 plate in holder for UVB range 250 nm to be used on laser beam at T LAMBDA 2 UVB entrance of system equipped with a microscope or with a macro laser entry attachment Item T MAC LAS ENTRY 2 inch Lambda 2 plate in holder for NU V range 325 nm to be used on beam at entrance T LAMBDA 2 NUV1 of system equipped with a microscope or with a macro laser entry attachment Item T T LAMBDA 2 HOLD MAC LAS ENTRY 2 inch Lambda 2 plate in holder for NUV range 350 nm to be used on beam at entrance T LAMBDA 2 NUV2 of system equipped with a microscope or with a macro laser entry attachment Item T MAC LAS ENTRY 5 inch Lambda 2 plate in holder for Visible range 400 700 nm to be used on laser beam T LAMBDA 2 VIS at entrance of system equipped with a microscope or with a macro laser entry attachment Item T MAC LAS ENTRY 5 inch Lambda 2 plate in holder for NIR1 range 750 800 nm to be used on laser beam T LAMBDA 2 NIR1_ at entrance of system equipped with a microscope or with a macro laser entry attachment Item T MAC LAS ENTRY 5 inch Lambda 2 plate in holder for NIR2 range 800 900 nm to be used on laser beam T LAMBDA 2 NIR2 at entrance of system equipped with a microscope or with a macro laser entry attachment Item T MAC LAS ENTRY W asss 2 3 2 2 Manual Macro Micro Mirror Manual macro micro entry swing away mirror Required on the laser incidence beam for T MACMIC MIR commuting
11. Micro Macro Mirror on page 40 and 6 figure 2 2 Open the Macro sample compartment 3 Place a sample on the sample holder 14 located in the macro sample compartment 4 Displace the mirror 11 along the sliding rail by slightly unscrewing the knurled knob below the mirror holder 5 Install the Back Scattering mirror by sliding the 19 knob This will perform a rough adjustment by steps Fine tune the position using the rotative part of the 19 knob 3 and the a and b screws located on the mirror holder see figure 2 4 page 64 6 Turn the XYZ adjustment screws as to perform a Raman type light emission through the collimator lens at the output of the macro sample compartment The following devices can be fine tuned Mirror orientation 11 XYZ sample holder adjustment 14 collecting image focusing 16 or change the exit focusing adapter 15 option T64000 entrance slit focusing with the transfer optics 20 NOTE These adjustments would be easier using the Macro Camera Viewer or and the entrance slit Viewer Screen or Camera T64000 User Manual 62 10 07 2009 HORI BA Using 764000 with the Back scattering Macroanalysis System Scientific 7 Place an entrance filter for example an interferential laser filter in the filter holder 22 located on the T64000 front panel below the Micro Macro Communication box useful to eliminate the plasma lines of the laser 8 Insert the exit filters for example ana
12. Order Date june 2004 This Instrument comply with 21 CFR 1040 10 T64000 User Manual 15 10 07 2009 HORIBA Scientific General safety Instructions a s 5 DUNNING PETENTE OEE EEPE EENET EEE EE E E E NEEE E E E 5 P TTT 5 Inended Readers 2 usus ds 99 3583 83 93 928 3780 9 25456584 G0 9 9 3 9 2 8 103 4 a sassa oba GEET ETIT L bc bu RER eb a a PPS Fd A PH es dun AM n 9 6 Laser dH Safely vee wa wa w w washa Qs w eee wapus w w A w h e wapu E k aska SE SEES 6 User visual indicators 9 Laser Safety Key and filters _ 9 LSO df pl suce I L TRR moss aysayan ss RE S ll Lanes 1OCOU PLEBE 14 CHAPTER 1 TOOT SWINE sant Tipp l ERT EE TER E 18 KAROH T T 624 roren EENE EEE EEE EE ES 18 IIE E E E TEA on 18 InstalldtlOH 2923290729909 527 Pes PEETA TEUER E dh EE uapa Ee d adii ds 19 Software Installation 4 ae NR a cro Ro rent Mad a ewe Aw ewe boo odes eae 19 Oprane R 422 d ERR a ORA RU d EE RVR Rx Eit qot doc np d dox de d 19 Composition ofthe equipment es 19 Sal l ES si S a APIs Arr d ird 19 lagu c rreeem 21 Monochromator Spectrograph n 26 SD II Ei E TE as paqupa a S on ene 27 PNGCrCONNCCHON aco ia 5 992 239 0999 2719 4 915 9 9 9 36 ENEE ERAEN R E dL V Ud 27 PPCCHICAUONS serron H E RR GRE EEEN EELE RENEE REENEN CENA
13. This label will also be placed near to the identification label see Figure 1 3 Labels lateral view page 15 DANGER AVOID EXPOSURE OF THE LASER BEAM TO THE EYES Figure 1 1 Safety label 1 Label 2 DANGER DURING OPERATION THE LASER BEAM IS EMIT TED IN THE T64000 SYSTEM Figure 1 2 Safety label 2 Label 3 A laset beam is emitted through that aperture DANGER AVOID EXPOSURE TO THE BEAM Figure 1 3 Safety label 3 T64000 User Manual 11 10 07 2009 HORIBA Scientific Label 4 The T64000 System has panels which is fixed in place and secured by screws These panels must not be opened or removed Doing so may pose a risk to accidental exposure to the laser beam s and will invalidate any warranty DANGER the laser product class may increase if covers or casings are removed Dangerous visible and or invisible laser beams may become accessible and pose a possible risk to exposure Figure 1 4 Safety label 4 Label 5 DANGER Microscope objectives are designed to be removed ot switched over during normal opera tion and are not protected by any safety interlocks SWITCH off the laser before changing or replacing microscope objectives Figure 1 5 Safety label 5 NOTICE if one or several objectives are not mounted on the microscope turret the empty positions must be blocked with a suitable cap Replacement or additional cap can be purchased from HORIBA Jobin Yvon if requir
14. 100 mm back scattering mirror does not include back collecting mirrors and liquid cell with holder T MACRO Laser periscope for lifting the beam of a laser installed at the front of the system up to the PERISCOPE level of the entrance axis of the macrochamber Macrochamber attachment with laser shutter interference filter and half wave plate T MACRO ENTRY holders To be used at entrance of the macrochamber when no laser entry T LAS ENTRY is on the system T FOC LENS 200 Macrochamber glass focusing optics F 200 mm Macrochamber glass collection optics F 160 mm Macrochamber liquid cell holder liquid cell not included Macrochamber spinning cell for powers and liquids T64000 User Manual 7 e 10 07 2009 HORIBA Scientific T LIQUID CELL Macrochamber liquid cell 0 3 cc MEN 2 3 3 Electronics extensions T COM CARD Commutation card with cables Monochannel detection card and necessary cables including a high voltage power supply x 234 Monochannel detection system parts T ASGA PMT AsGa photocathode PMT noise below 10 cps PN 43 921 349 T PMT HOUSING PMT cooled housing NENNEN 2 3 5 Computerization of system T PRINTER Color printer with cable NENNEN 2 3 6 Multichannel CCD detectors MPP MultiPin Phase air cooled open electrode 1024x256 pixels CCD Working from 200 up to 1050 nm with a quantum efficiency gt 30 between 500 nm and 800 nm Pixel size 26 x 26 um Chip size 26 6 x 6 7 mm Typical read
15. Illuminated CCD effects due to their thickened substrate 45 10 07 2009 HORIBA Scientific Option Additional Requirements Installation T64000 User Manual Detailed Description Back Illuminated CCDs are physically thinned so that the capture zone is closer to the surface which improves the UV quantum efficiency Opti mized antireflection coatings also help in improving the photo conver sion and therefore the quantum efficiency of the sensor Choose BIVS for Visible optimized CCDs For Visible to NIR measurements 600 nm to 1000 nm Back Illumi nated Deep Depletion BIDD CCDs have been created to increase NIR tesponse over standard Back Illuminated CCDs and to reduce etaloning effects Each chip type has its own quantum efficiency and noise characteristics The graph shows the typical QE curves for each type of CCD chip When selecting a CCD remember that the signal to noise ratio increases as a square root of the increase in the quantum efficiency For example select ing a CCD with 4 times the QE will increase the signal to noise by a fac tor of 2 Sensor selection should be based upon image size on the entrance slit of the spectrograph whether the sensor is responsive in the spectral region of study and if it is sensitive enough to distinguish the signal from the accumulated noise within any temporal constraints of the measurement Quantum efficiency becomes an issue only when the light level appro
16. Macro Commutation Using 764000 with the Macroanalysis System 2D CD 19 18 7 t9 05 14 LL M crochambetr Figure 2 3 Using Macroanalysis System 12 Focusing lens adjustment 13 Focusing lens adaptor 14 XYZ sample holder adjustment 15 Collecting lens adaptor 16 Collection lens focusing adjustment 17 XY adjustment 18 Back scattering mirror 19 Back scatteting selector with the fine tune knob 20 Transfer optics to entrance slit focusing adjust ment 21 Holder for analyzer half wave or quarter wave plates 22 Access to entrance filters holder 61 10 07 2009 HORI BA Using 764000 with the Back scattering Macroanalysis System Scientific 2 4 Using T64000 with the Back scattering Macroanalysis System 2 4 1 Preliminary The T64000 System has been installed and implemented by HORIBA Jobin Yvon or an authorized representative Check to ensure that the T64000 Unit and its sub assemblies are correctly connected to the power water laser PMT Housing and nitrogen multichannel CCD detector The use of specific accessories are detailed in the Description section 2 4 2 Procedure 1 Please follow the powered ON procedure described in the step 1 page 58 2 Load the LabSpec software The software has been already installed and setup per formed Please refer to the LabSpec User Manual 1 Pull down the Micro Macro selector see
17. P T AUTOFOC VIS M T AUTOFOC UV P T AUTOFOC UV M T PIEZOZ100 T PIEZOZ350 T ZMOT T ZMOT ELEC T64000 User Manual XY motorised stage X 75 mm Y 50 mm for BX41 and BXFM microscopes step size 0 1 um Including positioning joystick controller computer interface card drive electronics and software Allows automated positioning of samples and acquisition of Raman maps Visible autofocus device 400 nm 800 nm to be used with a Piezo stage Including the necessary opto mechanical attachment and detection system for controlling the focus at the surface of the sample with accuracy and speed Ideal for automated mapping analysis of rough samples Requires one of the piezo stages described hereafter Visible autofocus device 400 nm 800 nm to be used with a motorized Z stage Including the necessary opto mechanical attachment and detection system for controlling the focus at the surface of the sample with accuracy and speed Ideal for automated mapping analysis of rough samples Only required when no autofocus for a piezo stage 1s included Requires a motorized Z stage UV autofocus device 330 nm 360 nm to be used with a Piezo stage Including the necessary opto mechanical attachment and detection system for controlling the focus at the surface of the sample with accuracy and high speed Ideal for automated mapping analysis of rough samples Requires one of the piezo stages described hereafter UV autofocus device 330
18. holder Dielectric Edge filter XXX wavelength in nm Set of wavelengths 229 nm 244 nm T EDG FILTI XXX 557 nm 266 nm Dielectric Edge filter XXX wavelength in nm Set of wavelengths 325 nm 355 nm T EDG FILT2 XXX 564 nm 442 nm 457 nm 473 nm 568 nm Dielectric Edge filter XXX wavelength in nm Set of wavelengths 488 nm 514 nm T EDG FILTS XXX 532 nm 632 nm 752 nm 785 nm 830 nm Super Notch filter for XXX wavelength in nm Set of wavelengths 473 nm 568 nm T SHN FILT1 XXX 755 nm 830 nm 860 nm 1064 nm Super Notch filter for XXX wavelength in nm Set of wavelengths 442 nm 633 nm T SHN FILT2 XXX 647 nm 785 nm Super Notch filter for XXX wavelength in nm Set of wavelengths 457 nm 488 nm T SHN FILT3 XXX 514 nm 532 nm Fiber adaptor on the single monochromator option mirror attachment With SMA T SMA ADAPT connector Allows to focus on the axial entrance slit of spectrograph stage with a 4X SINGLE magnification optics T SINGLE VIS Fiber adaptor on the single monochromator option mirror attachment With FC connector T FIB ADAPT Allows to focus on the axial entrance slit of spectrograph stage with a 4X magnification SINGLE optics DENN 2 3 2 5 Confocal microanalysis attachments and accessories options 2 3 2 5 1 Confocal microanalysis attachments T64000 User Manual 70 10 07 2009 HORIBA Scientific Visible confocal microanalysis attachment for punctual analysis delivered
19. m 20 50000 0 597 149 33 0 199 4978 3333333 0 559 62 06 0 186 20 69 400 0 508 31 74 0 169 10 58 EUM EAM w T64000 User Manual 31 10 07 2009 H O Ri BA Specifications Scientific 3600 gr mm grating Spectrograph stage Triple Additive dispersion dispersion 50000 0 372 93 09 2295328 0 318 35 36 25000 0 239 14 91 Fast Comparison table Snr eene ore T at800nm at300nm at500nm at800nm 5 0 78 2 1 70 189 1 1 69 67 6 1 67 26 1 om eoj one DETI 1 4 2 Electrical e The SpectraLink is connected to the main by a removable cord e Consult the laser source user manual for special electrical safety requirement e A full electrical specification of the SpectraLink is detailed in the table below saon r OOOO r o o Safety Class a Pain krer Mains supply 115 230 VAC The fuse must be selected following the line voltage Voltage variation 10 Phase Single Frequency 50 60 Hz Frequency variation 2 Nominal system power 250 VA mEEEM consumption T64000 User Manual 32 10 07 2009 H O RI BA Specifications Scientific KIS ras 115 Volts T 2 5 A 250V 230 Volts T1 A 250V T64000 is a class 1 instrument and must be connected to the ground Refer to local regulations Grounding For safe servicing of the instrument always remove the main cord before opening the rack 1 4 5 Overall Dimensions 1091 mm Ga Ra ART RET TR ay a ea c
20. nm NA Numerical Aperture WD Working Distance LWD Long Working Distance ULWD Ultra Long Working Distance T64000 User Manual 7 e 10 07 2009 HORIBA Scientific 60X objective 350 950 nm NA 0 90 WD 0 2 mm OBJ60XNUVFL OBJ5XVIS 5X visible objective NA 0 10 WD 19 6 mm OBJIOXVIS OBJ50XVIS 0BJ100XVIS OBJ50XLWDVIS OBJ50XULWDVIS OBJ100XLWDVIS OBJ10XNIR OBJSOXNIR OBJ100XNIR OBJ50XLWLNIR Visible macro lens of 40 mm focal length on an horizontal exit equipped with a 10mm x 10mm cell holder for Visible range provided with a spherical back mirror to get a multipass effect The signal intensity can be increased by more than a factor 3 with clear liquids MACROICH VIS UV macro lens of 40 mm focal length on an horizontal exit equipped with a 10mm x MACRO CH UV 10mm cell holder for UV range provided with a spherical back mirror to get a multipass effect The signal intensity can be increased by more than a factor 3 with clear liquids 2 3 2 5 4 Microscope Raman polarisation components T LAMBDA 2 MICRO UVB T LAMBDA 2 MICRO NUV T LAMBDA 2 MICRO VIS T LAMBDA 2 MICRO NIR1 T LAMBDA 2 MICRO NIR2 T LAMBDAAM MICRO UVB T LAMBDA 4 MICRO NUV T LAMBDA 4 MICRO VIS T LAMBDA 4 MICRO NIR1 T LAMBDAAM MICRO NIR2 T64000 User Manual 7A 10 07 2009 HORIBA Scientific TseRmeRo Pang s a SaOsoIyvtT a Onur cs a s ns9s Ua a saa nh S E inn O XY75x50 T AUTOFOC VIS
21. of controls or adjustments or performance of procedures other than those specified within this manual may result in hazardous radiation exposure Caution The laser exit is through the microscope objective Before the System use check that all objectives ot caps ate mounted on the microscope as shown below Example two objectives are mounted on a 5 location turret White light shutter switch Three caps are mounted in 908 the unused objectives on the microscope turret These block the laser from exiting from these positions Mounted objectives T64000 User Manual 10 07 2009 HORIBA Scientific S7 User visual indicators The laser can only be switched ON with the key switch located on the laser source When the key is turned on an indicator shows that the laser source is ON The key prevents inadvertent or unauthorised starting of the laser S8 Laser Safety Key and filters Laser Safety Key Laser Safety key main function is to cut off the laser incidence beam A laser shutter with filters have been mounted on the laser path just before the Micro Macro commutation The Safety Laser key cuts the laser beam when the key is turned to ON This pre vents inadvertent or unauthorized activation of the laser As further precaution the key cannot be removed in OFF position Remove the control key when the laser or System is not in use This key belongs to the laboratory responsible or to the authorized
22. source to the T64000 must be secured by the user with an adequate housing when installing the laser source Additional safety labels must be stick on the exposed parts The various parts of the T64000 giving access to the laser beam have been secured by the means of enclosures and tubes from the laser source input to the microscope These tubes are firmly tightened and prevent any exposure from the operator to any laser radiation To use the Instrument it is necessary to access to the laser beam particularly for the microscope and the macro sample compartment to place and adjust the position of the sample into the beam Some parts of the laser path between microscope or macro sample output to mono chromator input are not housed light diffused by the sample See Figure 1 1 Laser path and label upper view page 14 T64000 User Manual 7 10 07 2009 HORIBA Scientific The following precautions must be observed Refer to your laser source manual for specific safety requirements In case of modification of the laser source the T64000 labelling may be adapted to conform the laser source class Personnel must never look directly into the laser beam and should wear protective eye wear at all times if protective covers are removed while the laser is switched on All personnel in the vicinity of the laser should also be ordered to wear protective eyewear if protective covers are removed while the laser is
23. switched on Only qualified and trained personnel should be permitted to operate the laset Precautions must be taken to ensure that there are no reflecting objects in the path of the laser beam e g gold ring on the finger Warning signs indicating the area in which the laser is enclosed should be clearly dis played Local and national regulations governing the safe use of lasers should be adhered to at all times Ensure that the laser is properly ventilated using a suitable exhaust Do not connect the exhaust to breathing air systems i e air conditioning or ventilation systems Viewing laser beam with certain optical instruments eye loupes magnifiers binoculars or telescopes within a distance of 100 mm may pose an eye hazard and must therefore be avoided The extracting fan located at the rear of the laser must not be blocked at any time The laser warning labels affixed to the system according to the safety regulations see warning chapter must not be removed The laser can only be switched on with the key switch This prevents inadvertent or unau thorised starting of the laser It cannot be operated with the key in the OFF position and the key cannot be removed in ON position If mishandling of the instrument or of the safety devices results nevertheless in direct eye exposure to the laser beam the exposed operator should consult a doctor or a competent eye testing institution Caution Use
24. up by HORIBA Jobin Yvon or an approved representative the user should follow certain rules and recommendations listed below 2 1 1 Safety Read carefully the Safety instructions described in the chapter General safety Instructions on page 5 2 1 2 Hardware Foresights The CCD detectors must not be continuously exposed to bright light especially in the ultra violet wavelengths This exposure will increase dark current This damage can occur inde pendent of power applied to the device The camera head is supplied with a protection cover Most of the electronic components utilized in the detector system are highly electrostatic sensitive Full ESD ElectroStatic Discharge handling procedures of the components of the system are essential Failure to comply will damage the system Improper use or grounding of the T64000 System could damage the system and or present the user with a potentially lethal hazard Do not connect or disconnect the cables while the System is on The resulting power surges may damage the Units Reliability Electronic and electric circuits are subject to the following constraints whenever the unit is turned on or off abrief transient period subjecting certain components to a severe operating mode a slow transient period several hours during which the electric and electronic circuits will progressively reach a stable operating mode from both electronic and thermal viewpoints T6400
25. user manual contains important information on how to operate the T64000 System correctly safely and most efficiently Observing these instructions will enable safe operation of the equip ment and will help to avoid accidental damage to reduce repair costs and to increase the instru ment lifetime and reliability HORIBA Jobin Yvon equipment is perfectly safe as long as it has been properly installed and is operated according to the instructions which are given in this instruction manual The installation of the equipment is to be strictly carried out by properly trained personnel who are designated by HORIBA Jobin Yvon and should not be attempted by the end user This manual must always be available whenever operating the equipment Any person working with the T64000 system whether it is an engineer or an operator must be aware of the statements enclosed within this document and apply its contents Tasks requiring familiarity with the manual include routine operation including setting up sample loading and instrument troubleshooting A WARNING Never make any modifications additions or conversions to the equip ment especially those which might affect safety without the supplier approval This also applies to the installation and adjustment of safety devices and accessories T64000 User Manual 5 10 07 2009 HORIBA Scientific In the event of safety relevant modifications or changes in the behavior of the T64000 during operat
26. 0 User Manual 51 10 07 2009 H O RI BA Preparation Scientific It is thus strongly advised to leave the unit turned on with the exception of the light source the computer and monitor unit Reproducibility Extreme temperature variations within a short period of time can influence measure ment results For example measurement reproducibility will be optimal if a temperature regulation of 1 C is observed Powered on the system The first time the T64000 System is connected to a power supply or after a long shutdown period the need for an electronic and thermal stabilization period should be taken into account in order to obtain good results For example the following minimum periods should be taken into account Mechanical and optical part of the T64000 unit approximately 24 hours in a climate controlled regulated environment SpectraLink approximately 30 min 2 1 5 Use The T64000 System unit may be used after it has been installed by HORIBA Jobin Yvon ot an authorized tepresentative Only general guidelines for use will be given since every element or sample analysis proce dure has its own specific characteristics related to the nature of the element or sample T64000 User Manual 52 10 07 2009 HORI BA Using 164000 with the Microanalysis System Scientific 2 2 Using T64000 with the Microanalysis System 2 2 1 Preliminary The T64000 System has been installed and implemented by HORIBA Jo
27. 2 3 2 5 6 Microscope Off Axis Option 10 07 2009 HORIBA Scientific Off axis Laser illumination system Laser is directed onto the sample from the T64000 coupling optics and not through the microscope objective allowing a higher rejection of the reflected laser beam on sample Angle is adjustable between approximately 90 and 65 Signal collection via a microscope objective 50XULWD and excitation via a lens of 15 8mm focal length 2 3 2 6 Macro sample attachment Will not require the laser entry attachment item T LAS ENTR Y and the macro micro entry swing away mirror item T MACMIC when there is no microscope The entry of T OFF AXIS ILLUM the laser will then be directed at level of the chamber axis and will only require the shutter and filter attachment item T MACRO ENTRY Visible macro sample chamber Permits to excite the sample under variable angle from 90 to back scattering XYZ sample holder solid sample plattform T MACRO VIS analyser and half wave plate on collecting beam glass collection optics F 80 mm and glass focusing optics F 100 mm back scattering mirror does not include back collecting mirrors and Liquid cell with holder UV Visible macro sample chamber Permits to excite the sample under variable angle from 90 to back scattering XYZ sample holder solid sample plattform T MACRO UV analyser and half wave plate on collecting beam Silica collection optics F 80 mm and silica focusing optics F
28. 57uW P5314uW P gt 7 8uW P gt 78 5uW P gt 785uW P gt 7 8mW 30s exposure 302 5 to 315 P gt 0 8 uW P gt 1 6 uW P gt 3 3 uW P gt 8 3 uW P gt 83 uW P gt 830 u W P gt 8 3 mW 30s exposure 315 to 400 P gt 78 5 uW P gt 157u Ww P gt 314u W P gt 785 uW P gt 7 85 mW P gt 78 5 mW P gt 785 mW 400 to 700 P gt 385 u W P gt 770u W P gt 1 5mW P gt 3 8 mW P gt 38 4 mW P gt 384 mW P gt 3 8 W RG mone G GRN masama posom any 700 to 1100 i i i 700nm 3W 700nm 30 P gt 2 98mw 6m W 12mW 30mW 300mW 1100nm W 1100nm 1100nm 1100nm 1100nm 1100nm 1100nm Chart 1 0 Glass wearing recommendations as function of waveleneths ranges This chart shows the necessity to wear the security glass in particular when UV laser is used T64000 User Manual 10 10 07 2009 HORIBA Scientific S9 List of safety labels The following safety labels are affixed to the system and or to the optional parts according to the different options installed Not all the labels will be present where a class 1 safety enclosure has been included Labels 1 to 5 indicate a hazardous situation where there is a risk of serious injury due to possible laser radiation Label 1 The T64000 System operates with laser source s emitting visible and or invisible continuous laser radiation typically below 500 mW The class of the laser product is 3B or 4 The laser class depends on the end user laser source and must be placed on the laser source
29. CCD ELECTRONIC UNIT In such case it would be necessary to empty the Dewar vessel before restart ing the electronic unit If the CCD camera is a UV coated version never expose the CCD window to the sun or to fluorescent light source Power ON the PMT Detector if applicable 10 Power ON the SpectraLink 11 Power ON the Computer and the screen 12 Switch the laser source ON please refer to the Manual delivered with the unit T64000 User Manual 58 10 07 2009 HORI BA Using T64000 with the Macroanalysis System Scientific 13 Do not forget to wait for temperature stabilization Estimation time for each sub unit is the following PMT Detector Maximum cooling temperature will be reached in several hours To get the best performance in dark noise we recommend to keep the SpectraLink turned on so that the PMT is kept powered and to never stop the water circulation in the PMT housing SpectraLink this unit must be powered for at least 30 minutes CCD Detector please refer to the explanations detailed in the related User Manual Laser please refer to the Manual delivered with the unit 2 Load the LabSpec software The software has been already installed and setup per formed Please refer to the LabSpec User Manual 1 Pull down the Micro Macro selector see Micro Macro Mirror on page 40 and 6 figure 2 2 Open the Macro sample compartment 3 Place a sample on the sample holder 14
30. CIT OR IMPLIED WARRANTY IT SHALL HAVE NO LIABILITY FOR INJURY TO THIRD PARTIES DIRECT OR INDIRECT COMMER CIAL OR FINANCIAL INJURY CONSEQUENTIAL DAMAGES OR FOR ANY OTHER REASON Obligations The products are for professional application and the Seller s acceptance of an order is with the understanding that only qualified individuals trained and familiar with users procedures will han dle them If Buyer fails to observe this obligation Buyer agrees to hold the Seller harmless from any liability resulting from the operation of the products T64000 User Manual 4 10 07 2009 HORIBA Scientific General safety Instructions S1 Summary This User Manual contains the facilities design and equipment installation requirements for the T64000 System S2 Purpose The purpose of the document is to enable the facilities manager at the customer site and HOR IBA Jobin Yvon representatives and service engineers to prepare for the installation of the T64000 System and to determine the necessary requirements for the environment in which the T64000 System is to be installed It also provides a guidelines and directions for the correct use and operation of the T64000 system S3 Intended Readers This document is intended for customers HORIBA Jobin Yvon representatives sales and service engineets S4 General instructions A WARNING The T64000 System must not be operated without prior reading of this docu ment The
31. ORIBA Scientific jdo2uo SOTAOSSIIIV 000F9 L I WL UOI EZIIO O N WIS d JONI uoI eINWWOD EN sondo HIS 9jyeipeuJeju 99UEJU WWG d udeJ60Jj2eds WIS SAPPY uu 4 uonezuojoy HIS L d JOIN UOIEINWWOD ZIN Ayosse00e juno N 9Anppv ils ejeipeuueju uu 0G c UZ epis yoeg HIS eAQgppy WLW or Cd HIS eoueque IEIXY WW c 4 WS g0UeJJUF uo Jennus G99 Pleo 1dSN sDutjeJc abels Anoenqns ejqnoq I DuneJo Jejeuogoedg oun BuijeJc UM Jennus 030 Gb Uu q29 uonejdepy jee A99 uonejdepy 70 31 6uisnoH LWd v0L 31 Nr d yiduiy wuosip ZOE Wd uoneydepy E9JeA G99 eqn J I d nuuol oud JoJ uonejnuJuJo LIN epis yy4fiy IIS ocuenu3 epis wwz 14 JOJN OODIA JO U99J9G do5Ssu d uonejnuuo GN yis 9uenu3 Joy uolje nuuuu0O VN uuc G4 10 99 9q q29 WIS UX wwe p4 WIS x43 WW 94 JOJJIN UOHEYAWWOYD IX3 9N 600C L0 0T 25 T64000 User Manual 10 07 2009 H O RI BA Description Scientific 1 2 1 Monochromator Spectrograph Subtractive configuration double stage monochromator includes the f
32. V to the NIR The actual instrument may differ slightly in appearance from images and illustrations shown in this manual depending upon which options are included within your chosen system If you have any questions regarding the installation or the maintenance of your instrument please contact one of out tepresentatives HORIBA Jobin Yvon SAS Molecular amp Microanalysis Division 231 rue de Lille 59650 Villeneuve d Ascq France raman horiba com Tel 33 0 3 20 59 18 00 Fax 33 0 3 20 59 18 08 ot visit our website www horiba com to find the local HORIBA Jobin Yvon office nearest to you T64000 User Manual 3 10 07 2009 HORIBA Scientific Warranty HORIBA Jobin Yvon warranties each instrument for two years from the date on which the equip ment leaves the plant The warranty is limited to repair of operating or manufacturing defects which come to light in that period It shall apply in said period only if the equipment has been used properly It will determine inter alia in event of faulty maintenance or use or of repairs by the Buyer or a third party The Seller s warranty does not cover consumable parts such as filaments zeolite joints electron multipliers electronic components membranes diaphragms crucibles glass etc In the case of components covered by the manufacturer s warranty such as computers the Seller shall cooperate with the Buyer in enforcement of the manufacturer s warranty but the Sell
33. aches the lowest limits of detectability see Appendix on page 66 or CCD HORIBA catalogue see Appendix on page 66 or CCD HORIBA catalogue none Please refer to the CCD User Manual delivered with the CCD Detector 46 10 07 2009 HORIBA Scientific Detailed Description 1 5 17 Monochannel Detection System The system described below is the regular Photon Counting Detection System Many other different configurations are available according to the applications Destination Description Option Additional Requirements T64000 System A Photon Counting Detection System in the visible range usually incor porates the following devices AsGa photocathode photomultiplier in a LCT50 housing The housing includes a Peltier effect cooling device Discriminator amplifier with cable PMT housing adaptor axial exit slit only none none DM302 preamplifier discriminator device PCNO01 photons counting and High Voltage card figure below shows the electronic devices CCD Shutter is required on each entrance slit T SHUTTER PCNO1 photons counting and High Voltage Card High voltage output connector DM302 Preamplifier Discriminator Device T64000 User Manual 47 10 07 2009 HORI BA Detailed Description Scientific 1 5 17 1 Detailed Description General The detection occurs as follows a group of lenses focuses the light beam from the exit slit on the photosensitive elem
34. and namely the optical drawer and spectrograph Before cleaning the SpectraLink Unit switch OFF the unit and remove the mains A cable Never clean the inside of the SpectraLink Unit 1 5 Detailed Description The Description chapter has explained the elements or sub units of the T64000 Basic Con figuration Numerous options and accessories can be added to enlarge the use or improve automation This chapter will list and describe each of the most important options accesso T64000 User Manual 34 10 07 2009 HORI BA Detailed Description Scientific ries The detailed and non exhausted list has been added and the end of this manual in the Appendix section 1 5 1 1 Stage Lateral Entrance Slit 1 Variable height H 0 1 2 5 15 mm Destination T64000 Double Stage Monochromator Description Used in System which required two selectable entrances 0 2mm width and 0 1 2 5 15mm height limiter Option 1 SMA connector fiber adapter 2 FC fiber adapter Additional This option is delivered with a motor i i Variable width ized commutation mirror ariable wi Requirements Commutation card T COM Q 1 5 2 Intermediate Slit Motorization width height Destination T64000 Double Stage Monochromator Description Computerizes the 0 50mm slit width with manual 0 15 height Option 1 Stokes Anti Stokes accessory Additional none Requirements delivered with MDR motor driver card and cable T64000 User M
35. anual 35 10 07 2009 HORIBA Scientific 1 5 3 Spectrograph Lateral Entrance Slit Destination Description Option Additional Requirements T64000 Spectrograph lateral entrance slit intermediate slit between the double monochromator and the spectrograph Computerizes the 0 25 mm slit width with manual 0 15mm height lateral entrance slit of the spectrograph inter mediate slit between the Double Mono chromator and the Spectrograph none delivered with MDR motor driver card and cable none 1 5 4 Manual Axial Entrance Slit Destination Description Option Additional Requirements T64000 User Manual T64000 Spectrograph Used in System configuration which requires a selectable third stage entrance 0 2mm slit width and 0 1 2 5 15mm height limiter nonc This option is delivered with a motor ized commutation mirror Commutation card I COM Detailed Description height width Variable height H 0 1 2 5 15 mm Variable width e 36 10 07 2009 HORI BA Detailed Description Scientific 1 5 5 2 d Stage Manual Axial exit Slit free E 0 1 2 5 15 mm Destination 164000 Double Stage Monochromator Description Used in System requiring a second stage axial exit 0 2mm slit width with 0 1 2 5 15mm height limiter Option none Additional This option is delivered with a motor ized commutation mirror Variable width Requirements Commuta
36. aph mirror design A visible half wave plate and analyser on Raman beam A filter wheel with 6 neutral density filters 0 3 0 6 1 2 3 and 4 Adaptation of an inverted IX71 inverted microscope replacing the standard BX41 model on the spectrometer The microscope is hardly coupled to the spectrograph on the same work bench for maximum mechanical stability and ease of use The standard version includes white light illumination by reflection and transmission a binocular one condenser IX2 LWUCD 0 55 WD 27 mm one colour video camera on top of the binocular two objectives UPFL 20X 0 50 and UPFL 40X 0 75 corrected for viewing through a slide All standard options of IX71 including a large range of objectives are available on request Adaptation of an inverted IX71 inverted microscope replacing the standard BX41 model on the spectrometer The microscope is hardly coupled to the spectrograph on the same work bench for maximum mechanical stability and ease of use The standard version includes white light illumination by reflection and transmission a binocular one condenser IX2 LWUCD 0 55 WD 27 mm one colour video camera on top of the binocular two objectives UPFL 20X 0 50 and UPFL 40X 0 75 corrected for viewing through a slide All standard options of IX71 including a large range of objectives are available on request 232RPMimwewaumeds 2 3 2 5 3 Objectives Visible 400 800 nm NUV 325 500 nm UVB 240 360 nm NIR gt 800
37. bin Yvon or an authorized representative Check to ensure that the T64000 Unit and its sub assemblies are correctly connected to the power water laser PMT Housing and nitrogen multichannel CCD detector The use of specific accessories are detailed in the Description section 2 2 2 Procedure If the 164000 System is not powered ON follow the following procedure 1 2 3 Open the water circulation for PMT Detector housing and laser if necessary Open the Nitrogen circulation if needed If the System is equipped with the optional CCD Camera the following steps must be ensued 4 Turn the power to ON on the CCD electronic unit 5 Fill up the CCD Dewar vessel with the Nitrogen 9 Wait for the decreasing of the CCD head temperature up to 140 K or 133 C This temperature can be controlled using the Software see Software User Manual This step should take up to 2 hours Refer to the CCD User Manual to know how long the CCD temperature will be kept NEVER CUT OFF THE POWER SUPPLY OF THE CCD ELECTRONIC UNIT In such case it would be necessary to empty the Dewar vessel before restart ing the electronic unit If the CCD camera is a UV coated version never expose the CCD window to the sun or to fluorescent light source Power ON the PMT Detector if applicable 10 Power ON the SpectraLink T64000 User Manual 53 10 07 2009 HORI BA Using T64000 with the Microanalysis System Scientific
38. cc EA Naeem HR KE EE aT REE rh aat GET TETE Rr Kr 5 SR i Laser Entrance BO mm era Mie ethane 500 mm 3 leveling feet D KT ExtSit H Entrance Slit 40 70 mm ime Standard 55 mm Weight 162 ke WEIGHT PRECAUTION T64000 Unit weights 162 kg According to the mover staff test the weight of the load to ensure it can be lifted securely if not make adjust ments grip the load securely protect hands against pinch points T64000 User Manual 33 10 07 2009 HORI BA Detailed Description Scientific 1 4 4 Environmental conditions Environmental n M Conditions Remarks conditions Indoor use LI MENS es in a 1 C range regulation 1s required Uptoe80 6 to 8096 No Nocondensaion AW 5 as a The room in which the instrument is installed must be properly ventilated 1 4 5 Storage If this unit has to be stored before it is installed it must be kept in a store room where the storage conditions are listed in the following table t5 10 140C Up to 80 RH Packing Must stay closed during storage to prevent Special packing requirements moisture and dust entering the unit 1 4 6 Cleaning Instructions The outside part of the unit should be cleaned once a year to mainly get rid of dust Use a lint free cloth with 90 alcohol Do not use any other chemical products No cleaning should be undertaken inside the optical parts of the instrument
39. ctors and sampling optics enabling operation from the UV to the NIR Specifications Focal length 640 mm single stage 3x 640 mm triple additive Low frequency lt 100 cm single stage typically 2 5 cm t double filter stage Stray light rejection 10 14 at 20 cm 1 514 nm laser Step size 0 00066 nm with 1800 gr mm gratings Reproducibility better than 1 pixel Gratings 100 to 3600 gr mm covering UV NIR Tables of dispersions 300 gr mm grating Wavelength Spectrograph stage Triple Additive dispersion dispersion m mama Se m cR of we sw sas 18 0 eN ow wmur o3 free 0 Am T64000 User Manual 29 10 07 2009 H O RI BA Specifications Scientific 600 gr mm grating Wavelength Spectrograph stage Triple Additive dispersion dispersion m an a RRR m mmm w ws 39 900 gr mm grating Spectrograph stage Triple Additive Wavelength dispersion dispersion cm mm 1200 gr mm grating Wavelength Spectrograph stage Triple Additive dispersion dispersion T64000 User Manual 30 10 07 2009 H O Ri BA Specifications Scientific 1200 gr mm grating 1800 gr mm grating Wavelength Spectrograph stage Triple Additive dispersion dispersion a ee a m wom om 3 m m wn s ws m EE LG DEL MN ERE GM 2400 gr mm grating Wavelength Spectrograph stage Triple Additive dispersion dispersion mm em mm cm mm nmmm a
40. daptor Optical focusing input device Fine tune adjustment of the in put device 10 Input mirror Oo ONAN Ul Right View Step by step vertical adjustment of the sample platform Vertical fine tune adjustment of the sample platform Knurled button to remove the platform XY fine tune of the sample plat form Back collecting mirror Platform Exit focusing adaptor Filters holder Back scattering mirror 10 Three directional sample orien tation platform Top View T64000 User Manual 43 10 07 2009 HORI BA Detailed Description Scientific 1 5 14 Stokes Antistokes accessory Destination T64000 Description The stokes and Antistokes simultaneous measurements can be performed with the T64000 Instrument using a dedicated accessory This accessory replaces the standard height limiter on the intermediate slit by a special height limiter 2 3 and 4mm with a central mask to eliminate the excita tion beam Option none Additional none Requirements none 1 5 15 Two Grating Turret Motorization Destination T64000 Spectrograph Description With this option the grating change will be controlled by the Software Option None Additional None Requirements Commutation card I COM T64000 User Manual 44 10 07 2009 HORIBA Scientific 1 5 16 CCD Detector Destination Description Surface electrodes Ni Insulating layer N type Si T64000 User Manual T64000 axial exit slit third Stage
41. different software and hardware the T64000 System has an integrated software and hardware package which combines all functions in a simplified easy to use fashion The package contains a large number of security and validity tests which are only possible with the complete integration of all functions Con ceived initially for the demanding performance of Raman spectroscopy the T64000 is also su perbly adapted to most other spectroscopic techniques As the software allows the T64000 System to be used in wavelength and wavenumber units other spectroscopic techniques such as fluorescence luminescence and absorption transmission can also be easily performed on both macro and micro samples The ability to use the T64000 as a single or triple with subtractive or additive premonochromator stages spectrometer with either standard scanning or multichannel acquisition of data permits the user to optimize the spectrometer to the spectral and sampling requirements This flexibility is achieved without having to disturb the sample under investigation and is completely automated For industrial research or analytical laboratories the T64000 System is the safest easiest to oper ate and most flexible spectro analytical system available 1 1 System Installation 1 1 1 Packaging The T64000 System is delivered in packaging designed for protection during shipment However if the packaging is damaged or it appears after unpacking that the instrument has d
42. dispersive Raman spectrometer systems for over four decades We have been at the forefront of Raman spectroscopy since its infancy introducing ground break ing innovations such as the first Raman microscope and the world s first commercial remote Ra man sampling probe HORIBA Jobin Yvon Raman Division today comprises of the combined expertise of the HORI BA Jobin Yvon Dilor and SPEX companies and is proud of having more than 3000 Raman sys tems installed worldwide Well equipped applications Labs and technical support enable HORIBA Jobin Yvon to provide services right through from the earliest proof of principle investigations With a broad range of technologies available HORIBA Jobin Yvon can uniquely provide solutions in analytical research and industrial measurements Following the established high performance Raman systems of the Jobin Yvon Dilor and SPEX brands the new T64000 series II triple spectrometer system is a versatile high performance re search grade system Three stage monochromator with optics aperture and coupling optimized for perfor mance and stability Multiple motorized switching mirrors for ease of operation Multiple entrance and exit ports Directly coupled microscope options and Macrochamber if required rigidly coupled to the spectrometer Alarge choice of options and components to enable full customizing of the system e g gratings detectors and sampling optics enabling operation from the U
43. ed Label 6 CAUTION Indicates a situation where equipment could be damaged or there is a risk of minor injury Symbol depends on particular situation see the additional Microscope manual Label 7 This symbol located on a device indicates that the device can be moved and could caution should be taken to avoid a potential injury gt Location on the motorized XY Stage Never put your fingers on the XY Stage during the moving sequence T64000 User Manual 12 10 07 2009 HORIBA Scientific Label 8 Identifies any terminal which is intended for connection to an external conductor for protection from electric shock in case of a fault or the ter minal of a protective earth ground electrode Located on the Spectra Link Label 9 Recycling This symbol located ON A DEVICE shows that this DEVICE HAS BEEN PLANNED FOR ECOLOGICAL DESTRUCTION AT ITS END OF LIFE Ee T64000 User Manual 13 10 07 2009 HORIBA Scientific S10 Labels location Access to the filters C Area without housing Laser path Raman beam path Removable panels l Laser source entrance I Aperture labels Figure 1 1 Laser path and label upper view T64000 User Manual 10 07 2009 HORIBA Scientific Figure 1 2 Labels Removable panels front view and or E Figure 1 3 Labels lateral view Model T 64000 Identification EEE Villeneuve sere nu mb er SIN
44. efects fill out the necessary forms with the shipper the guarantee is limited to 3 days It is recommended that the original packaging materials be saved for possible storage or transport of the instrument Should it be necessary to send the instrument back to the fac tory contact Jobin Yvon or your local representative for prior approval Pack the instrument in its original packaging if undamaged Otherwise contact your local representative for new T64000 User Manual 18 10 07 2009 HORI BA System Installation Scientific packaging material Once the return slip has been recetved send the instrument to the address that has been specified by your local representative 1 1 2 Installation The T64000 System must be installed and started by HORIBA Scientific or an approved representative 1 1 3 Software Installation The Software has to be installed and started up by HORIBA Jobin Yvon or an approved representative Therefore the installation procedure is detailed in the Software User Manual 1 1 4 Operating Defects If an operating defect exists even after carefully reading this manual contact HORIBA Scientific or your local representative for prior return approval If the instrument is returned to the factory the fault should be explained as clearly as possible 1 1 5 Composition of the equipment The T64000 System is composed of the following Basic System Optional Sub units e Accessories 1 1 6 Requir
45. ements See the requirements list delivered with the quotation Figure below shows a sample installation for the T 64000 System T64000 User Manual 19 10 07 2009 HORI BA System Installation Scientific MO OQWOAO O C O N TA nar S O 1 T64000 unit 2 Water supply Monochannel Multichannel Detectors Laser Source 3 Nitrogen supply specific experiments 4 Water outlet 5 Line power distribution box ground cable 6 SpectraLink controller 7 Computer and monitor Window air conditioner 9 Storage for software accessories 1 1 6 1 Water Supply The water supply is necessary for cooling the PMT e Water inlet outlet flow 0 6 1 min about 10 gal hour Water temperature Best result will be reached at 10 C A water supply is also necessary for the Laser Source refer to the manufacturer user manual T64000 User Manual 20 10 07 2009 H O RI BA Description Scientific 1 2 1 1 6 2 Liquid Nitrogen LN5 Supply The Liquid Nitrogen is required for a CCD Detector which includes a Dewar recipient mounted on the CCD chip The Liquid Nitrogen is filled inside the Dewar and thus the CCD detector can be cooled up to 196 C 320 F 1 1 6 3 Nitrogen N Supply The nitrogen supply is required for specific experiments The nitrogen flow must be very low regulated by a control with gauge The average flow rate must be approximately 0 5 1 min The nitrogen supply can al
46. ent of the photomultiplier A discrimination amplifier amplifies the signal from the photomultiplier The assembly is powered by a separate power supply The Monochannel detector is housed in a parallelepiped metal box equipped with the fol lowing accesses A coaxial connector marked anode A coaxial connector marked cathode A power supply connector for Peltier effect cooling system nlet Outlet water circulation used for the Peltier effect cooling system The Monochannel Detection Unit will be mechanically and optically adapted using a LCT50 Housing adapter see figure 1 9 and figure 1 10 Figure 1 9 LCT50 Optical Adaptation performance 50 C cooling below cooling liquid at 15 C regulation 0 1 C for 5 C change in liquid temperature at 20 C cool down time 120 minutes window material double walled pyrex quartz optional supply 220 V 50 60 Hz 150 W 110 V 60 Hz optional connectors signal BNC TNC optional HV MHV SHV optional connecting cables 1 5m weight housing 5 5 kg power supply 5 9 kg Figure 1 9 LCT50 Optical Adaptation T64000 User Manual 48 10 07 2009 HORI BA Detailed Description Scientific 130 179 housing 210 280 e e Tar ses Cadar wee LCT50 Control Unit S power supply Figure 1 10 LCT50 dimensions Photomultiplier Tube Principle A photomultiplier tube is an electronic tube using photoemission effect to co
47. er assumes no obligation for such components The warranty is limited to replacement of parts found by the Seller to be defective To be able to claim the benefit of said warranty the Buyer will have to advise the Seller by return receipted reg istered mail within 28 days of discovery of the defects which come to light The contractual war ranty is limited at the Seller s option to reconditioning or replacement of parts found by it to be defective expenses of dismantling reinstallation and technicians travel excepted All warranty work shall be done by the Seller or a contractor of its choosing according to its instructions All shutdown related expenses shall in any event be incumbent on the Buyer The warranty does not cover the following Any malfunction attributable to improper operation Any malfunction attributable to repair or modification by any party not authorized by HORIBA Jobin Yvon Any malfunction attributable to the use in an improper environment Any malfunction attributable to violation of the instructions in this manual Any malfunction attributable to operations in the manner not specified in this manual Any malfunction attributable to natural disasters or accidents or mishaps not involving HORIBA Jobin Yvon Any deterioration in appearance attributable to corrosion rust and so on Consumables and replacement of consumables Products of other companies THE SELLER MAKES NO OTHER TA
48. er delivered with 2 Motor Driver MDR boards for controlling the scanning of the 2 monochromatotrs 1 computer interface card LabSpec Software LabSpec Software developed for Windows supplied with two computer package dongles permitting multichannel and monochannel detection data acquisition Raman mapping and a wide range of data treatment and storage options This software also includes macro pro gramming capabilities T64000 User Manual 22 di 4 JOLUUC Indino LUSISAS Buiss Soiud DOC PUD OUO sOuues P ZUOJOW IONUDOIN UOIIO S D ZIIO O AJ 99UDJJU3 DJOJD T IDIXV S 2 oODIS ZAX pezuoIo N IonubJ a DIOUUDD SOWD e8doosoloi d uo suondo 000F9 L I I QLL 74 I uodo uoupcunOiuo2 SAPPY JOQUUDUD OPON uoojdopy Pa oouoosolon J s p N OD lt 10409400 l Ruah N ES UOI O S D ZIIO O AJ x 1019849 Jeun O TAGS do IX3 IDixV dol BullD1O ulW ba SeluiiODdO 3 JOJDUJOJUOOUO A ejdur ejanoq eiBurs 600C L0 0T 23 T64000 User Manual Description weiselg I6e9DdO 000rF91 C T AQEL dg u S LL 3 EG er lt lt O LE TEC W Scientific HORIBA 600C L0 0T 24 T64000 User Manual Description H
49. ion stop the equipment and namely the laser source immediately and report the malfunc tioning to HORIBA Jobin Yvon or your authorized local representatives S5 Warnings Performance of any procedures not specified by the manufacturer may result a hazard ous radiation exposure This includes removal of covers with laser power ON There is no user maintenance or service internal to the system with power ON When covers or enclosures are removed for any reason extreme care must be taken to prevent the beam being viewed directly by external optics or mirror There are no user maintenance parts for the T64000 System The System including peripherals must never be opened with the exception of parts mentioned in this man ual Maintenance must only be performed by a designated members of HORIBA Jobin Yvon Service Team or by authorized local representatives S6 Laser Radiation Safety The T64000 is class 3b or 4 and depends on the laser source s class the customer is going to use with It is important that the user understands which version of the system he will be operating and familiarizes himself with the appropriate safety precautions The maximum acceptable laser parameters for a laser included in the T64000 are Beam diameter 5 mm Wavelengths range 200 1100nm Beam divergence 1 mrad Maximum laser power acceptable 10W visible range for class 2 400mW UV range for class 3R 2 2W near IR for class1 These value
50. it of the second stage Includes a 0 2 mm slit with a height limiter and T EX SLIT S2 a motorized commutation mirror Requires the Commutation card item T COM N I e laz R wi 67 10 07 2009 HORIBA Scientific 2 2 Spectrograph stage options 2 2 1 Additional gratings delivered prealigned in cassettes 300 gr mm ruled grating XX X blaze wavelength in nm 500 600 or 1000 T RG300 XXX SP T RG600 XXX SP 600 gr mm ruled grating XX X blaze wavelength in nm 300 400 500 630 750 or 1000 600 gr mm blazed aberration corrected holographic grating XX X correction wavelength T BHG600 500 SP 600 gr mm blazed holographic grating at 500 nm T ACHG900 750 SP 900 gr mm blazed aberration corrected holographic grating at 750 nm 1200 gr mm blazed aberration corrected holographic grating XX X blaze wavelength in T BHG1200 XXX SP un 330 500 630 750 or 900 T HG1800 SP T BHG1800 XXX SP 1800 gr mm blazed holographic grating XX X blaze wavelength in nm 250 400 500 1800 gr mm standard holographic grating 450 850 nm T BHG2400 XXX SP 2400 gr mm blazed holographic grating XX X blaze wavelength in nm 250 330 or 400 T HG3600 SP 3600 gr mm holographic grating 200 450 nm 2 2 2 Lateral entrance slit 0 25 mm Motorization of the width of the slit including stepping motor adaptation supplied with T INT SLIT S283 MDR motor driver board and cable 2 2 3 Manual a
51. laser from Macrochamber to microscope when the system is equipped with both attachments BEEN 2 3 2 3 Manual Macro Micro Single Triple Commutations Manual Macro Micro Single Triple commutation wheel for visible range Required when T COM VIS WHEEL using both visible macrochamber and visible microscope Manual commutation device to be used when the system is equipped with only a visible T COM MICRO microscope for selecting either triple or single configuration Manual commutation device to be used when the system is equipped with only a T COM MACRO macrochamber for selecting either triple or single configuration T64000 User Manual 69 10 07 2009 HORIBA Scientific MEN 2 3 2 4 Single monochromator options Single monochromator option for visible range Permits to enter directly the 3rd stage Requires an axial entrance slit item T ENT SLIT S3 on the spectrograph stage and either a commutation wheel item T COM VIS WHEEL or a micro or macro commutation device T COM MICRO or T COM MACRO Single monochromator option for UV Visible range Permits to enter directly the 3rd T SINGLE UV stage Requires an axial entrance slit item T ENT SLIT S3 on the spectrograph stage single monochromator option for Visible NIR range up to 1500 nm Permits to enter T SINGLE NIR directly the 3rd stage Requires an axial entrance slit item T ENT SLIT S3 on the spectrograph stage T RF TILTER Rayleigh rejection filter tilting
52. located in the macro sample compartment 4 Turn the XYZ adjustment screws as to perform a Raman type light emission through the collimator lens at the output of the macro sample compartment The following devices can be fine tuned Mirror orientation 11 Entrance beam focusing 12 or change the entrance focusing adapter 13 option XYZ sample holder adjustment 14 collecting image focusing 16 or change the exit focusing adapter 15 option T64000 entrance slit focusing with the transfer optics 20 NOTE These adjustments would be easier using the Macro Camera Viewer or and the entrance slit Viewer Screen or Camera 5 Place an entrance filter for example an interferential laser filter in the filter holder 22 located on the T64000 front panel below the Micro Macro Communication box useful to eliminate the plasma lines of the laser 6 Insert the exit filters for example analyzer polarizing half wave quarter wave plate 21 7 If the T64000 System is equipped with a Viewer sub unit optional the settings can be fine tuned the Viewer is located on the premonochromator entrance T64000 User Manual 50 10 07 2009 HORI BA Using T64000 with the Macroanalysis System Scientific From the LabSpec software follow the standard acquisition procedure described below see the LabSpec User Manual for detailed explanation 1 Select the appropriate 3rd stage grating 1800 g mm for a high resol
53. ly adjustable confocal pinhole from several microns to 1 2 mm to define with accuracy the size of the analysed volume Achromatic coupling optics to focus the Raman beam on the entrance slit of the spectrograph mirror design A visible half wave plate and analyser on Raman beam A filter wheel with 6 neutral density filters 0 3 0 6 1 2 3 and 4 T64000 User Manual T2 10 07 2009 HORIBA Scientific T UV VIS OPEN MICRO T ADAPT MICRO INV VIS T ADAPT MICRO INV UV Open UV Visible confocal microanalysis attachment for punctual analysis Delivered with Laser entry attachment including laser shutter and interference filter and half wave plate holders An XY manual mechanical stage A Koehler illumination for reflected white light over wide field An internal illumination for transmitted white light supplied with an Abbe condenser A revolver equipped with 3 plan achromatic objectives 10X visible NA 0 25 WD 10 6 mm 50X visible NA 0 75 WD 0 37 mm 100X visible NA 0 9 WD 0 21 mm White light illumination by transmission through Abbe condenser A high definition 785x480 pixels USB colour camera for simultaneously visualising the sample under white light illumination and the laser spot A continuously manually adjustable confocal pinhole from several microns to 1 2 mm to define with accuracy the size of the analysed volume Achromatic coupling optics to focus the Raman beam on the entrance slit of the spectrogr
54. lyzer polarizing half wave quarter wave plate 21 9 If the T64000 System is equipped with a Viewer sub unit optional the settings can be fine tuned the Viewer is located on the premonochromator entrance From the LabSpec software follow the standard acquisition procedure described below see the LabSpec User Manual for detailed explanation Select the appropriate gm stage grating 1800 g mm for a high resolution 300 or 600 g mm to make a one shot spectrum 1200 g mm which is infrared optimized only for NIR version 2 Select the correct grating setting in the software If you change the grating do not forget to go to the zero order position in the software This will give the correct 4 calibration for the particular grating you will use Set the spectrograph to the desired spectral position 4 Select the slit aperture Select the acquisition time and the number of accumulations this will improve the signal noise ratio Then you have 2 possibilities The icon SREB is a spectrum adjustment so it can help you to maximize the sig nal the new spectrum refreshes the old one and so on No repeated accumu lations or extended spectral ranges are acquired If you press the icon K 1t will make a spectrum accumulation and stop T64000 User Manual 63 10 07 2009 HORI BA Using 764000 with the Back scattering Macroanalysis System Scientific 20 Qo CD DS C t6 15 Premonochromator
55. m 100X visible NA 0 9 WD 0 21 mm White light illumination by transmission through Abbe condenser A high definition 1280x1024 pixels USB colour camera for simultaneously visualising the sample under white light illumination and the laser spot A continuously manually adjustable confocal pinhole from several microns to 1 2 mm to define with accuracy the size of the analysed volume Coupling optics to focus the Raman beam on the entrance slit of the spectrograph lens system A visible half wave plate and analyser on Raman beam A filter wheel with 6 neutral density filters 0 3 0 6 1 2 3 and 4 UV Visible confocal microanalysis attachment for punctual analysis Delivered with Laser entry attachment including laser shutter and interference filter and half Laser entry attachment including laser shutter and interference filter and half wave plate holders An XY manual mechanical stage A Koehler illumination for reflected white light over wide field An internal illumination for transmitted white light supplied with an Abbe condenser A revolver equipped with 3 plan achromatic objectives 10X visible NA 0 25 WD 10 6 mm 90X visible NA 0 75 WD 0 37 mm T UV VIS MICRO 100X visible NA 0 9 WD 0 21 mm White light illumination by transmission through Abbe condenser A high definition 1280x1024 pixels USB colour camera for simultaneously visualising the sample under white light illumination and the laser spot A continuously manual
56. ngs XX X blaze wavelength in nm 330 500 630 T BHG1200 XXX DS 756 or 900 T HG1800 DS 1800 gr mm standard holographic gratings 450 850 nm T BHG1800 XXX DS 1800 gr mm blazed holographic gratings XXX blaze wavelength in nm 250 400 500 T ACHG600 XXX DS T BHG2400 XXX DS 2400 gr mm blazed holographic gratings XX X blaze wavelength in nm 250 330 or 400 T HG3600 DS 3600 gr mm standard holographic gratings 200 450 nm 2 1 4 Double Additive configuration adaptation Includes 2 manual intermediate slits 0 10 mm and motorized commutation mirrors Requires the Commutation card item T COM T ADD ADAPT Requires the Double Additive mount for using the instrument in the triple additive dispersion configuration item T ADDMOUNT 2 1 5 Viewers Permit to check the image of the entrance slit to maximize the alignment of sample T SCR VIEW Viewer for Visible range supplied with a viewing screen Viewer for Visible range supplied with a C mount adapted to most color or black and T VIDEO VIS VIEW White video cameras Supplied with density filters attachment camera not included Viewer for UV Visible range down to 240 nm supplied with a C mount adapted to most color or black and white video cameras Supplied with density filters attachment camera not included USB CAMERA Color camera 1280x1024 pixels with cable 2 1 6 Manual axial exit slit of the second stage T VIDEO UV VIEW Manual axial exit sl
57. nm 360 nm to be used with a motorized Z stage Including the necessary opto mechanical attachment and detection system for controlling the focus at the surface of the sample with accuracy and high speed Ideal for automated mapping analysis of rough samples Only required when no autofocus for a piezo stage is included Requires a motorized Z stage Piezo Z stage Maximum Z displacement 80 um 40um including a servo control loop for maximizing precision of positioning The minimum step size and precision 1s 0 1 micron The unit is screwed on the microscope objective revolver and is compatible with all the objectives Requires an IEEE card Piezo Z stage Maximum Z displacement 300 um 150um including a servo control loop for maximizing precision of positioning The minimum step size and precision is 0 1 micron The unit is screwed on the microscope objective revolver and is compatible with all the objectives Requires an IEEE card Micrometric motorised Z stage the maximum distance of movement depends on the objective working distance The minimum step size is 0 5 micron The movement is controlled by software or by joystick Requires a motorized XY stage Micrometric motorised Z stage the maximum distance of movement depends on the objective working distance The minimum step size is 0 5 micron The movement is controlled by software or by joystick To be ordered when no XY motorized stage is included in the configuration BEEN
58. nvert an inci dent radiation ultraviolet to infrared into an electrical signal which is amplified to a usable level by means secondary electron emission See figure 1 11 CATHODE ANODE J 8 D9 D10 D11 LIGHT I l BEAM ee n N LAM t I _ vn WF K ae tj sess E GROUND Figure 1 11 Photomultiplier Tube principle Amplification T64000 User Manual 49 10 07 2009 HORI BA Detailed Description Scientific The current provided by the photomultiplier 15 very small and therefore must be amplified The amplifier is located in the photomultiplier in order to avoid connection losses It pro vides the following functions 100X amplification of the signal from the photomultiplier This function is performed by a discriminator amplifier Power supply access The power supply pack is housed in a metal parallelepiped box The front panel includes the following components ON OFF switch e 10A fuse e Peltier power supply failed LED indicator Cooling system specifications Cooling temperature depending on room temperature 35 C nominal Maximum room temperature 52 C Maximum water temperature 24 C Minimum water flow 0 5 1 mn T64000 User Manual 50 10 07 2009 HORIBA Scientific CHAPTER 2 Getting Started 2 1 Preparation After the T64000 System has been installed and started
59. ollowing components see figure 1 4 One manual axial entrance slit 0 2 mm with height limiter No 1 figure 1 4 One manual intermediate slit 0 50 mm with height limiter No 4 figure 1 4 Two fixed mirrors on each side of the intermediate slit No 3 and 5 figure 1 4 One fixed mirror in front of the exit slit No 7 figure 1 4 One set of aberration corrected holographic gratings 1800 gr mm 76 x 76 mm No 2 and 6 figure 1 4 Third stage in spectrograph configuration includes the following components see Figure 1 One manual intermediate slit 0 25 mm with height limiter No 8 figure 1 4 One fixed mirror ensuing the intermediate slit No 9 figure 1 4 One aberration corrected holographic grating 1800 gr mm 76 x 76 mm No 10 figure 1 4 One top exit for the Multichannel Detector CCD Charge Coupled Device LN2 cooled Linear InGaAs detector etc Figure 1 4 Basic configuration Optical Diagram T64000 User Manual 26 10 07 2009 H ORI BA Interconnection Scientific 1 2 2 SpectraLink The new SpectraLink includes the cards which controls the motorized hardware of the instrument Without option it includes 2 Motor drivers to control the scanning of the dou ble monochromator and the scanning of the spectrograph It also includes of course the interface board for PC communication On its basic state it already includes all of the con nectors rear panel for future options or accessories Additi
60. onal cards are plugged on the front panel Figure 1 5 SpectraLink Rear Panel 1 3 Interconnection The T64000 System is a Raman diffusion spectrometry system A wide variety of options are available to allow users to perform analysis in minimal time thanks to the modular options and the specific Software developed by HORIBA Scientific Jobin Yvon technology The figure 1 6 shows the T64000 Interconnection T64000 User Manual 27 10 07 2009 HORIBA Scientific PC Unit SCSI Port Laser Shutter Mains Supply T64000 User Manual Interconnection Front Panel T64000 rear panel Eo Ee e o 5V 12V d T10A 250V T1A 250V 5V T1A 250V T1A 250V T2A 250V A3 Slit 2 3 Slit 1 2 A1 2 100 240V 2 FUSES T2A 250V 250 VA Figure 1 6 T64000 System Interconnection 28 10 07 2009 H O Ri BA Specifications Scientific 1 4 Specifications 1 4 1 Optical Features Three stage monochromator with optics aperture and coupling optimized for perfor mance and stability Multiple motorized switching mirrors for ease of operation Multiple entrance and exit ports Directly coupled microscope options and Macrochamber if required rigidly coupled to the spectrometer e A large choice of options and components to enable full customizing of the system e g gratings dete
61. out noise 4 amp pixel Dark noise lt 0 002 e pixel sec at 70 C MPP air cooled UV Visible Back Illuminated 2048x512 pixels CCD Working from 220 T TE BIUV up to 700 nm with a quantum efficiency gt 40 between 220 and 400 nm and gt 60 2048x512 above Pixel size 13 5 x 13 5 um Chip size 27 65 x 6 91 mm Typical read out noise 3 pixel Dark noise lt 0 002 e pixel sec at 70 C MPP LN cooled open electrode 1024x256 pixels CCD Working from 200 nm to 1050 nm with a quantum efficiency gt 40 between 200 nm and 900 nm Pixel size 26 x 26 um Chip size 26 6 x 6 7 mm Typical read out noise 4 amp pixel Typical dark noise 0 5 e pixel hr at 133 C Including a 3L LN Dewar for 72hr autonomy MPP LN cooled Back Illuminated Deep Depleted 1024x256 pixels CCD Working from 300 nm to 1050 nm with a quantum efficiency of 90 at 800nm and gt 60 between 500 nm and 900 nm Pixel size 26 x 26 um Chip size 26 6 x 6 7 mm Typical read out noise T TE 0E 1024x256 T LN OE 1024x256 T LN BIDD 1024x256 4 e pixel Typical dark noise 2 pixel hr at 133 C Including a 3L LN Dewar for 72hr autonomy MPP LN cooled Back Illuminated 1024x256 pixels CCD Working from 200 nm to 700 T LN BIUV nm with a quantum efficiency gt 50 between 250 nm and 700 nm Pixel size 26 x 26 um 1024x256 Chip size 26 6 x 6 7 mm Typical read out noise 5 pixel Typical dark noise 0 3 amp pixel hr at 133 C Including a 3L LN Dewa
62. person using the 164000 it is strictly personal Remove the control key when the laser or System is not in use Manual command of density filters wheel Laser Safety key L VN I NEM n dS R pus Ep et ieee L Ea k R ae BE D i dr TEES A MIR T64000 User Manual 9 10 07 2009 HORIBA Scientific Safety shutter ON In this position the T64000 is unusable a shutter keeps the beam from going into the microscope and the macro chamber Safety shutter OFF In this position microscope and macro chamber are usable In this posi tion all personnel in the vicinity of the laser should also be ordered to wear protective eyewear according to the laser wavelengths and power see charts 1 0 below Density filters wheel This density filters wheel has 2 functions Security recommendations for personal protection aset beam attenuation for sample protection Security recommendations The following charts provide security recommendations for the user it shows the power threshold of the laser beam above which it is necessary to wear security glasses These thresholds correspond to the EMP allowed maximum exposure relative to the 60825 EN safety standards they have been calculated according to the density filters Laser source max power Threshold for glass wearing Wavelengths Without any DO 0 3 DO 0 6 DO 1 DO 2 DO 3 Range nm DO 200 to302 5 IfP gt 0 78uW P gt 1
63. ple single configuration 3 For System equipped only with a Visible Macrochamber for selecting either triple single configuration nonc For Visible range only Required when using Visible Macrochamber and or Visible Microscope 1 5 10 Micro Macro Single Triple Entrance Commutation for UV VIS Range Destination Description Option Additional Requirements T64000 User Manual Located on the Double Monochromator Entrance The Raman beam exiting from the Microscope or the Macrochamber must be redirected to the Double Monochro mator Entrance Slit or the Entrance Slit Spectrograph A Collimation mirror is used to focalize the beam 1 Micro only to Single Triple for Visible EEX range 2 Macro only to Single Triple for Visible range none see above 39 10 07 2009 HORIBA Detailed Description Scientific 1 5 11 Micro Macro Mirror Focalization Confocal Lens UV Vis adjustment Destination T64000 with Microscope and Macrochamber Description Swing away mirror which commutes the laser beam to Microscope or Macro chamber Option none Additional none Requirements Microscope and Macro chamber Micro Macro commutation Push Micro Pull Macro 1 5 12 Confocal Microanalysis System Destination Description Option Additional T64000 System This System added to the Basic T64000 allows to use micro samples for Raman analysis Due to numerous accessories they are listed in the
64. r for 72hr autonomy MPP LN cooled Back Illuminated 2048x512 pixels CCD Working from 200 nm to 700 T LN BIUV nm with a quantum efficiency gt 50 between 250 nm and 700 nm Pixel size 13 5 um 2048x512 Chip size 27 65 x 6 91 mm Typical read out noise 3 amp pixel Typical dark noise 0 3 pixel hr at 133 C Including a 31 LN Dewar for 72hr autonomy LN cooled Linear InGaAs array detector of 512 pixels Working from 800 nm to 1550 nm with a quantum efficiency of 80 between 1000 nm and 1500 nm Pixel size 50 um x T LN IGA512x1 50 500 um Array length 25 60 mm Read out noise 900 1000 amp pixel High Sensitive Mode HiS or 9000 10000 rms High Dynamic Range Mode HiD Fixed pattern noise lt 1 5 k sec at 133 C Including a 3L LN Dewar for 72hr autonomy T64000 User Manual 77 10 07 2009 HORIBA Scientific CCD shutter mounted on axial entrance slit supplied with electronics 23880142 and T SHUTTER cable 41195032 T ADDSHUTTER Additional CCD shutter required on every other entrance slit T64000 User Manual 78 10 07 2009 HORIBA Scientific Index CHAPTER 4 Numerics Ist Stage Lateral Entrance Slit 35 2nd Stage Manual Axial exit Slit 37 A Accessories table 25 Accessories and options list 66 Appendix 66 Axial Entrance Slit 36 Axial Exit 38 Axial exit Slit 37 B Back Illuminated CCD 46 Back scattering Macroanalysis System using 62 C caps for micro
65. ral entrance slit Includes a 0 2 mm slit with a height limiter and a motorized T LAT ENT SLIT S1 commutation mirror Requires the Commutation card item T COM Fiber adaptor to be mounted on any T64000 entrance slit With SMA connector Allows to T SMA SLIT ADAPT focus on a slit equipped or not with a CCD shutter with a 4X magnification visible optics Fiber adaptor to be mounted on any T64000 entrance slit With FC adaptor Allows to focus on a slit equipped or not with a CCD shutter with a 4X magnification visible optics 2 1 2 Intermediate slit 0 50 mm Motorization of the width of the slit including stepping motor adaptation supplied with T INT SLIT S152 MDR motor driver board and cable Stokes Anti Stokes accessory Replaces height limiter with central masks 1 2 and 4mm wide for blocking the laser beam in the center of the range collected on the multichannel T FC SLIT ADAPT T SAS detector 2 1 3 Sets of 2 gratings delivered prealigned in cassettes T RG300 XXX DS 300 gr mm ruled gratings XXX blaze wavelength in nm 500 600 or 1000 600 gr mm ruled gratings XXX blaze wavelength in nm 300 400 500 630 750 or 600 gr mm blazed aberration corrected holographic gratings XX X correction wavelength in nm 500 750 T BHG600 500 DS 600 gr mm blazed holographic gratings at 500 nm T ACHG900 750 DS 900 gr mm blazed aberration corrected holographic gratings at 750 nm 1200 gr mm blazed holographic grati
66. ry 44 Two Grating Turret Motorization 44 COD Der 22 canes bag ee ande motibus aetna daneehesee gaan 45 Monochannel Detection System 47 CHAPTER 2 GALU MONEO ausa deed WARS EREE EERO ES JI Prepara onara arra y ee ee oes ease 51 DI d 51 Hardware Foresights 51 WSC 2 eee ee Oe ee ee ee s ee eee ee ee ee ee eee eee ZY 52 Using T64000 with the Microanalysis System 53 J iii ti nex eee EEATSERE AENAVEMA NEMESIS SERT MEM ANA qES S M 53 lnc M M 53 Using T64000 with the Macroanalysis System 58 Pil oko oo ons HR ee ee ea ETT PPP 58 POCO 92 2 5 444s ea ees ae Oe es eee OES ee E 58 Using T64000 with the Back scattering Macroanalysis System 62 EE RR TT TT TETTE 62 EE S SS E E Ass 62 CHAPTER 3 ES qecsukbun eAREESSSSAAEROES S RITSSS REPOS 66 CHAPTER 4 LD rcr 79 T64000 User Manual 17 10 07 2009 HORIBA Scientific CHAPTER 1 164000 System The T64000 System Series II is a new generation fully computerized triple spectrograph scan ning spectrometer system Unlike the current generation of Raman spectrograph in which spec trometer control and data acquisition are independent functions requiring
67. s 19 Operating temperature 34 Optical Diagram 26 Optical Diagram table 24 Optical specifications 29 Options and Accessories 66 Overall Dimensions 33 D Packaging 18 PCN01 photons counting card 47 Photomultiplier Tube Principle 49 Photon 47 Photon Counting Detection System 47 R Reliability 51 Reproducibility 52 Requirements 19 S safety 5 safety labels 11 safety requirements 8 Safety shutter 10 shutter safety 10 Software Installation 19 Specifications 29 SpectraLink 22 27 Spectrograph 26 Spectrograph Axial Exit 38 Stokes Antistokes accessory 44 Storage 34 Subtractive configuration 26 System Installation 18 System use 52 T temperature stability 52 temperature variation 52 Two Grating Turret Motorization 44 V Viewers 38 W Warranty 4 Water Supply 20 Weight 33 T64000 User Manual 80
68. s correspond to the LEA values for each range of wavelengths when safety position red button is com muted Duting installation of T64000 System be careful that the laser source installation com plies with all the legal safety requirements during operation maintenance and service Laser sources used with the T64000 constitutes a hazard to personnel during periods of operating and servicing Lasers ate high intensity light sources producing visible or invisible light at specific wavelengths This concentrated energy in a narrow laser beam may cause damage to biological tissues especially to eyes To use lasers safety it is important to understand that laser s required final product safety classification is determined by essentially three elements the laser s power wavelength and housing Class 3B laser system Laser beams and reflected beams could be dangerous Diffused reflected beams in most cases do not present any problem Class 4 laser system Laser beam represents an acute hazard to the skin and eyes from direct and scattered radiation Fire hazard must be considered T64000 User Manual 6 10 07 2009 HORIBA Scientific The T64000 System itself does not included the laser sources On request the laser sources can be ordered but are not integrated inside the T64000 System The end user must comply the legal and safety requirements during the installation and the use of the lasers The beam path from the laser
69. scope 8 CCD Detector 45 CCD sensors 45 Cleaning Instructions 34 Commutation Wheel for Visible Range 39 Composition 19 Confocal feature 55 Confocal Microanalysis System 40 Confocal principle 55 Contents 16 D Density filters wheel 10 Description 21 Description detailed 34 Detailed Description 34 Dimensions 33 DM302 preamplifier discriminator device 47 Double Additive Adaptation 37 E Electrical specifications 32 EMP 10 Entrance Commutation for UV VIS Range 39 Entrance Slit 35 Environmental conditions 34 F filters wheel 10 G Getting Started 51 Glass wearing 10 Grounding 33 H Hardware Foresights 51 High Voltage Card 47 I Indicators 9 Installation 19 Interconnection 27 Intermediate Slit Motorization 35 K Key laser safety 9 L labels safety 11 Labels location 14 LabSpec Software 22 Laser path 14 Laser Radiation Safety 6 Laser Safety Key 9 Laser source max power 10 Lateral Entrance Slit 36 LCT50 47 LCT50 dimensions 49 LCT50 housing adapter 48 LCT50 Optical Adaptation 48 T64000 User Manual 79 10 07 2009 HORIBA Scientific M Macroanalysis System 42 Macroanalysis System using 58 Macrochamber 42 Micro Macro Mirror 40 Micro Macro Single Triple 39 Microanalysis System Using 53 Microscope general presentation 41 microscope safety 8 Mirror 40 Monochannel Detection System 47 Monochromator 26 N Nitrogen supply 21 O Operating Defect
70. so be required for Laser source Protection of the windows from the dust Experiments Air free samples CIC 1 1 6 4 Liquid Nitrogen LN5 Supply The Liquid Nitrogen is required for a CCD Detector which includes a Dewar recipient mounted on the CCD chip The Liquid Nitrogen is filled inside the Dewar and thus the CCD detector can be cooled up to 196 C 320 F Description The table T64000 Options Concept on page 23 shows the options and accessories for the System All the options are organized around a Basic configuration which includes the following sub units Entrance double stage monochromator in a subtractive mount including 1 manual axial entrance slit 0 2 mm with a height limiter 1 manual intermediate slit 0 50 mm with a height limiter e 2 fixed mirrors on each side of the intermediate slit 1 fixed mirror in front of the exit slit lateral entrance slit of spectrograph stage 1 horizontal shaft with 2 gratings cassette holders e 1 set of aberration corrected holographic gratings 76 x 76 mm 1800 gr mm Spectrograph stage including 1 manual lateral entrance slit 0 25 mm with a height limiter 1 horizontal shaft with a grating cassette holder T64000 User Manual 21 10 07 2009 H O RI BA Description Scientific 1 aberration corrected holographic grating 76 x 76 mm 1800 gr mm in a cassette 1 top exit for a multichannel detector New SpectraLink Controll
71. stment Lens focusing adjustment of the scattered beam to the confocal hole This is required when several laser wavelengths are used axial chromatism aberration compensation T64000 User Manual 57 10 07 2009 HORI BA Using T64000 with the Macroanalysis System Scientific 2 3 Using T64000 with the Macroanalysis System 2 3 1 Preliminary The T64000 System has been installed and implemented by HORIBA Jobin Yvon or an authorized representative Check to ensure that the T64000 Unit and its sub assemblies are correctly connected to the power water laser PMT Housing and nitrogen multichannel CCD detector The use of specific accessories are detailed in the Description section 2 3 2 Procedure If the 164000 System is not powered ON follow the following procedure 1 2 3 Open the water circulation for PMT Detector housing and laser if necessary Open the Nitrogen circulation if needed If the System is equipped with the optional CCD Camera the following steps must be ensued 4 Turn the power to ON on the CCD electronic unit 5 Fill up the CCD Dewar vessel with the Nitrogen 6 Wait for the decreasing of the CCD head temperature up to 140 K or 133 C This 9 temperature can be controlled using the Software see Software User Manual This step should take up to 2 hours Refer to the CCD User Manual to know how long the CCD temperature will be kept NEVER CUT OFF THE POWER SUPPLY OF THE
72. the instrument T BENCH 1LAS Equipped with one fixed mirror for reflecting laser beam at 90 10 07 2009 HORIBA Scientific Bench at back of T64000 holding coupling optics for making lasers enter the instrument T BENCH 2LAS Equipped with one fixed and one swing away mirrors Bench at back of T64000 holding coupling optics for making lasers enter the instrument Equipped with one fixed and one swing away mirrors together with a laser filtering column T BENCHIFILT 2LAS Laser entry attachment including laser shutter interference filter and half wave plate holders Necessary for a configuration with only a macrochamber when lasers are installed at the back of the spectrometer Not required when the system is delivered with a microscope as it is included in this attachment T MACRO LAS ENTRY Holder for 2 inch bandpass filter to be used on laser beam at entrance of system T BPF HOLD equipped with a microscope or with a macro laser entry attachment Item T MAC LAS ENTRY Bandpass filter for eliminating the plasma lines of the laser XX X 488 514 532 633 BPF1 XXX 661 785 and 830 nm Delivered mounted in T BPF HOLD Bandpass filter for eliminating the plasma lines of the laser XX X 325 355 364 442 BPF2 XXX 457 568 647 and 1064 nm Delivered mounted in T BPF HOLD Holder for 2 inch half wave plate to be used on laser beam at entrance of system equipped with a microscope or with a macro laser entry attachment
73. tion below x see description below BASIC CONFIGURATION INCLUDING Entrance double stage monochromator in a subtractive mount including manual axial entrance slit 0 2 mm with a height limiter manual intermediate slit 0 50 mm with a height limiter 2 fixed mirrors on each side of the intermediate slit 1 fixed mirror in front of the exit slit lateral entrance slit of spectrograph stage horizontal shaft with 2 gratings cassette holders 1 set of aberration corrected holographic gratings 76 x 76 mm 1800 gr mm Spectrograph stage including manual lateral entrance slit 0 25 mm with a height limiter 1 horizontal shaft with a grating cassette holder l aberration corrected holographic grating 76 x 76 mm 1800 gr mm in a cassette 1 top exit for a multichannel detector T 64000 New Spectra Link Controller delivered with 2 Motor Driver MDR boards for controlling the scanning of the 2 monochromators Refer to 2 3 3 for electronics extensions computer interface card LABSPEC Software LabSpec Software developed for Windows supplied with two computer package dongles permitting multichannel and monochannel detection data acquisition Raman mapping and a wide range of data treatment and storage options This software also includes macro programming capabilities OPTIONS 2 1 Entrance Double stage options s 2 1 1 Manuallateral entrance slit T64000 User Manual 66 10 07 2009 HORIBA Scientific Manual late
74. tion card I COM 15 Variable height B 0 5 2 5 15 mm 0 5 E O 1 5 6 Double Additive Adaptation Destination T64000 Double Stage Monochromator Description Used in System configuration which gt requires a double additive stage optical configuration Option none Additional none Requirements Commutation card item T COM Double Additive mount accessory pni Q T64000 User Manual 37 10 07 2009 HORIBA Scientific 1 5 7 Spectroeraph Axial Exit Destination Description Option Additional Requirements 1 5 8 Viewers Destination Description Option Additional Requirements T64000 User Manual Detailed Description S Variable height H 0 1 25 15 mm T64000 third Stage Used in System configuration which requires selectable third stage exits 1 0 2mmi slit width with height limiter 2 Axial Multichannel Port This option is delivered with a motor ized commutation mirror Variable width Commutation card T COM Recommended adaptation ref1 with feet for reinforcing the stability of any D HJY LN2 CCD mounted on axial exit III III Recommended adaptation ref2 with feet for reinforcing the stability of any HJY LN2 CCD mounted on axial exit when a fiber adapter is mounted on axial entrance slit of the Spectro graph Stage lt 1 UU gt T64000 double monochromator Camera or Viewing screen Swing away periscope with
75. tion rejection mode On the return path to the spectrograph the Raman back scattered light is fully transmit ted through the filter towards the confocal slit hole adjusted by a rotative button 7 located on the Micro Macro Commutation Box If several laser wavelengths are used a focalization adjustment chromatic aberration compensation can be made with the but ton 8 The Single Triple spectrometer disperses the multichromatic Raman signal onto the detector PMT CCD Once the confocal slit hole is set the analysis point can be focused on a specific Z axis value The figure 2 1 shows how a confocal pinhole determines the optical slice thickness of a sample Thus if the sample is located on a motorized XY stage it becomes easy to make an analysis surface inside a sample using the mapping feature Using a Z motorized Sample Stage this measure can be completely automated A 3 D Raman image can be then obtained scattered Light Confocal Pinhole Figure 2 1 Confocal principle Objective m Y P3 AVY 4 Thickness of le Sample 7 optical slices A E Stage positioning T64000 User Manual 55 10 07 2009 HORI BA Using T64000 with the Microanalysis System Scientific From the LabSpec software follow the standard acquisition procedure described below see the LabSpec User Manual for detailed explanation 1 Select the appropriate 3rd stage grating 1800 g mm for a high resolution
76. ttp www horiba com HORIBA Jobin Yvon S A S 231 rue de Lille Molecular amp Microanalysis Division 59650 Villeneuve d Ascq France Tel 33 0 3 20 59 18 00 Fax 33 0 3 20 59 18 08 Email raman horiba com HORIBA Jobin Yvon Inc 3880 Park Avenue EDISON New Jersey 08820 USA Tel 1 732 494 86 60 Fax 1 732 549 51 25 HORIBA Jobin Yvon GmbH Neuhofstr 9 64625 Bensheim Tel 49 0 6251 8475 0 Fax 49 0 6251 8475 20 Email info sci3 de horiba com Hauptstr 1 82008 Unterhaching Tel 49 0 89 462317 0 Fax 49 0 89 462317 99 HORIBA Jobin Yvon Ltd 2 Dalston Gardens STANMORE Middlesex HA 7 1 BQ Great Britain Tel 44 20 8204 8142 Fax 44 20 8204 6142 HORIBA Jobin Yvon Srl Via Cesare Pavese 35 AB 20090 OPERA Milano Italy Tel 39 2 57 60 30 50 Fax 39 2 57 60 08 76 HORIBA Jobin Yvon S A S China Room 1801 Capital Tower No 6 Jia Jianguomenwai Avenue Chaoyang District Beijing 100022 P R China Tel 86 0 10 8567 9966 Fax 86 0 10 8567 9066 HORIBA Jobin Yvon Japan Higashi kanka Daiji Building 1 7 8 Higashi kanka chiyoda ku TOKYO 101 0031 Japan Tel 81 0 3 3861 8231 HORIBA Jobin Yvon Korea 5 Yangjae Dong SEOCHO GU SEOUL 137 150 Korea Tel 82 0 2 753 7911 T64000 User Manual 2 10 07 2009 HORIBA Scientific Thank you for choosing HORIBA Scientific HORIBA Scientific is the world leader in Raman spectroscopy designing and manufacturing state of the art
77. ution 300 or 600 g mm to make a one shot spectrum 1200 g mm which is infrared optimized only for NIR version 2 Select the correct grating setting in the software If you change the grating do not forget to go to the zero order position in the software This will give the correct 4 calibration for the particular grating you will use Set the spectrograph to the desired spectral position Select the slit aperture Select the acquisition time and the number of accumulations this will improve the signal noise ratio Then you have 2 possibilities The icon SREB is a spectrum adjustment so it can help you to maximize the sig nal the new spectrum refreshes the old one and so on No repeated accumu lations or extended spectral ranges are acquired If you press the icon it will make a spectrum accumulation and stop you p D D T64000 User Manual 60 10 07 2009 HORIBA Scientific Premonochromator Box ke Premonochromator Entrance Slit p Filter holder scattered beam see figure 2 2 page 57 Beam splitter see figure 2 2 page 57 Laser Filter wheel with 6 neutral density filters Laser vertical entrance axis Micro Macro commutation knob Confocal hole adjustment see figure 2 2 page 57 Mirror sliding rail 00 10 Un amp UU Focusing lens sliding rail 10 Entrance optics XZ adjustments 11 Mirror T64000 User Manual Micro
78. volver equipped with 3 plan achromatic objectives 10X visible NA 0 25 WD 10 6 mm 50X visible NA 0 75 WD 0 37 mm 100X visible NA 0 9 WD 0 21 mm White light illumination by transmission through Abbe condenser A high definition 1280x1024 pixels USB colour camera for simultaneously visualising the sample under white light illumination and the laser spot A continuously manually adjustable confocal pinhole from several microns to 1 2 mm to define with accuracy the size of the analysed volume Coupling optics to focus the Raman beam on the entrance slit of the spectrograph lens system A visible half wave plate and analyser on Raman beam A filter wheel with 6 neutral density filters 0 3 0 6 1 2 3 and 4 71 10 07 2009 HORIBA Scientific Visible confocal microanalysis attachment for punctual and line scanning analysis Delivered with Laser entry attachment including laser shutter and interference filter and half wave plate holders Confocal Line scanning attachment including 2 scanners vibrating for illuminating a line on sample and imaging it on the entrance slit of the spectrometer An XY manual mechanical stage A Koehler illumination for reflected white light over wide field An internal illumination for transmitted white light supplied with an Abbe condenser A revolver equipped with 3 plan achromatic objectives T LINE SCAN 10X visible NA 0 25 WD 10 6 mm MICRO 50X visible NA 0 75 WD 0 37 m
79. with T VIS MICRO Laser entry attachment including laser shutter and interference filter and half wave plate holders An XY manual mechanical stage A Koehler illumination for reflected white light over wide field An internal illumination for transmitted white light supplied with an Abbe condenser A revolver equipped with 3 plan achromatic objectives 10X visible NA 0 25 WD 10 6 mm 50X visible NA 0 75 WD 0 37 mm 100X visible NA 0 9 WD 0 21 mm White light illumination by transmission through Abbe condenser A high definition 1280x1024 pixels USB colour camera for simultaneously visualising the sample under white light illumination and the laser spot A continuously manually adjustable confocal pinhole from several microns to 1 2 mm to define with accuracy the size of the analysed volume Coupling optics to focus the Raman beam on the entrance slit of the spectrograph lens system A visible half wave plate and analyser on Raman beam A filter wheel with 6 neutral density filters 0 3 0 6 1 2 3 and 4 Open Visible confocal microanalysis attachment for punctual analysis delivered without any bottom frame for offering a totally free space below the objectives Delivered with T VIS OPEN MICRO T64000 User Manual Laser entry attachment including laser shutter and interference filter and half wave plate holders An XY manual mechanical stage A Koehler illumination for reflected white light over wide field A re
80. xial entrance slit Manual axial entrance slit Includes a 0 2 mm slit with a height limiter and a motorized commutation mirror Requires the Commutation card item T COM 2 2 4 Motorized 2 gratings turret Motorized 2 gratings turret Includes the motor adaptation Requires the Commutation card item T COM 2 2 5 Axial exit Manual axial exit slit Includes a 0 2 mm slit with a height limiter and a motorized commutation mirror Requires the Commutation card item T COM T ENT SLIT S3 T TUR T EX SLIT S3 Axial Multichannel Port Includes the multichannel detector port and a motorized T MULTEPORT commutation mirror Requires the Commutation card item T COM Also see next 2 lines Adaptation with feet for reinforcing the stability of any HJY LN2 CCD mounted on axial T ADAPT1 LN CCD Adaptation with feet for reinforcing the stability of any HJY LN2 CCD mounted on axial T ADAPT2 LN CCD exit when a fibre adaptor 19 mounted on axial entrance slit of spectrograph stage 2 3 Accessories for the system Special silvered coating on all reflective optics of the system for improving its throughput T SILVCOAT in the visible NIR range Only for working above 380 nm 2 3 1 Additive mount accessory T ADD MOUNT Additive mount accessory Requires the adaptation T ADD ADAPT BEEN 2 3 2 Sampling attachments BEEN 2 3 2 1 Laser entry items Bench at back of T64000 holding coupling optics for making lasers enter

T64000 User manual October 2009

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