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FPP 5G & FPP 5Gs User manual

1. Displays Meaning of different menus Field values Diagnostics menu Going from left to right and from top to bottom gt For upper part of display see Table 10 zam pe 22 1 108 310 A D DDE C Unit enables to start cooling unit diagnostic Cool enables entering a percentage of cooling Coolin gang D A Heat 0 o N N Heat enables entering a percentage of heating 3 men Heat ee Diagnostics menu Display 1 Next display For upper part of display see Table 10 Pressure 1 mmH20 A D F97 200 1600 Pump O mmH20 DA 0 oe mmH20 200 mmH20 OFF OFF OFF Diag vacuum setting e 16 Kal mbar EE M N DA Airsy Diagnostics menu Display 2 Pump manual pump start ON OFF Suct SV open shut suction solenoid valve ON OFF AirSV open shut leak solenoid valve ON OFF Diag 200 mmH20 Pump ON gt Suct SV ON OFF Diag 1600 mmH20 Pump ON gt Suct SV ON or OFF set before pump start gt AirSV OFF gt AirSV ON Next display Optical detector Upper opt det Lower opt det Emitter number of points emitted F 0 pts no light emitted Receiver Opts Receiver Opts a as 4095 pts maximum light emitted Emitters pts Emitteri Pts Receiver number of points received Emit WEE Opts no light received Diagnostics menu Display 3 4095 pts maximum light received Auto automatic control of emitter to obtain a 0 gt 4095 pts given no of points on the receiver 2
2. If there are several fruitless communications the host computer may decide to abort transmission by sending an EOT 04H character ANALYZER HOST COMPUTER Successfull transmissions ENQ 1 result message XXXXX gt ACK lt ENQ Next result YYYYY gt ACK lt ENQ No more result ACK gt ANALYZER HOST COMPUTER Result sent faulty reception ENQ 1 result message XXXXX gt not properly received AG NAK __ ENQ Same message XXXXXX gt not properly received AG NAK __ ENQ Same message XXXXXX gt not properly received Host ends the communication e EOT Abort DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix B 89 DL FPP 5G amp FPP 5Gs 5 Transmitted data Example 1 R ISL 3419 E8 N 05 1 99 0 15 0 32 0 9999 9 9999 9 9999 9 1 69 1 C LG 99 99 9 999 9 0 9 999 9 28 04 1999 4 12 29 46 1 T1 CFPP C 0 0 0 10 5 25 0 70 0 60 60 1 13 1 T2 1 CFPP p 0 5C OJEC 1 T2 1 3 45 0 0 0 0 0 0 57 1 T2 2 4 33 5 20 0 1 1 0 89 1 T2 3 4 50 5 35 0 1 1 0 8F 1 T2 4 4 66 5 70 0 1 1 0 96 1 T2 5 13 25 0 0 0 0 0 0 6A 1 T2 6 1 0 0 0 0 0 0 0 41 1 T3 1 CFPP 0 2B 1 T3 1 2 200 00 0 9C The data which can be transmitted are divided in 5 groups pe pe Results See messages R below AS To be transmitted a result must be validated manual validation must be per
3. None ARTS CTS Xon Xoff ENQ ACK Flow control Type Comments Transmitted messages are sent without any way to stop them from the host computer However a special parameter Time between two messages in the ISL analyzers allows to define a pause between to successive message from 0 0 s to 10 0 s by step of 0 1 s Note This time is applied between 2 entire messages not between RTS CTS Hardware Existing signals defined in the RS232 interface standard are used to control the transmission Connect the host computer serial RTS signal to the analyzer CTS signal When the input buffer of the host computer is full the RTS signal changes its state Seeing its CTS signal changing the analyzer stops transmission until CTS changes again Note This hardware handshake is controlled by the communication hardware devices and can stop restart transmission between any characters Xon I Xoff Software This well known handshake is qualified as software protocol because it Xon 11H is controlled by the host computer reception software to control Xoff 13H the data flow If the software needs time to process the last incoming message it can send the Xoff character to the analyzer which immediately stops the transmission until it receives from the host computer the Xon character ENQ ACK Software This is a full protocol It allows flow control and data Developed acknowledgment by ISL this The transmission is fully controll
4. 70 0 60 60 1 13 T message Field name Format Number of Field value Example characters Analyzer no from 00 to 99 2 1 Message type string 2 T1 test program T1 Program name string 12 CFPP C Temperature unit 00 or 01 2 0 C 0 1 F Test type 00 at 01 2 O CFPP 0 1 Simul Checking test 00 or 01 2 0 no test 0 1 test Start temperature 99 at 999 3 10 Tmp start at cloud 00 at 999 3 5 Alarm temperature 999 9 at 9999 9 6 25 0 Stop temperature 99 9 at 9999 9 6 70 0 Max up time 000 at 999 3 In seconds 60 Min down time 000 at 999 3 In seconds 60 Display print end type 00 at 01 2 0 no display 1 display 1 Checksum 2 Sum of all the characters 13 5 5 Cooling profile message Appendix B 92 1 T2 1 3 45 0 0 0 0 0 0 57 1 T2 2 4 33 5 20 0 1 1 0 89 1 T2 3 4 50 5 35 0 1 1 0 8F 1 T2 4 4 66 5 70 0 1 1 0 96 1 T2 5 13 25 0 0 0 0 0 0 6A 1 T2 6 1 0 0 0 0 0 0 0 41 T message Field name Heading 1 message Analyzer no Message type Cooling profile no Cooling profile name Temperature unit Checksum Cooling profile stages 1 message per stage Analyzer no Message type Stage no Stage type Setting Limit Test type Test frequency Checksum Format Number of Field value characters 00 to 99 2 string 2 T2 Cooling profile 01 to 05 2 string 12 00 to 01 2 0 C 1 F 2 Sum of all the characters 00 to 99 2 string 2 T2 Cooling profile 00 to 20 2 0
5. The analyser screen will display the type of transfer PC Start the transfer to the PC as explained in the Read me file section 9 9 4 2 page 2 74 eEnter the number of the serial communications COM port used 1 or 2 Downloading analyzer program code and software texts eKey in the data file name ISLFPP Vxx xx version of software code and validate with ENTER Key in the name and the extension of the file Downloading internal parameters eEnter the required file name and then validate with ENTER Key in the name and the extension of the file For downloading internal parameters to a PC use a new file name for each download for example use the date as a name IPDDMMYY NVM A display on the PC informs the operator of the type of operation running Analyzer A display on the analyzer informs the operator of the type of operation running End of transfer If the transfer was OK The analyzer is automatically reinitialized 9 9 4 4 Transfer fails or screen not lit If the transfer fails the analyzer will automatically detect a download request Also on powering up if the analyzer screen does not light up the analyzer will similarly detect a download request ePower down the PC and the analyzer ePower up the PC and the analyzer eRun the downloading program as explained above in 9 9 4 3 page 2 74 If downloading is necessary the analyzer will detect this automatically When the analyzer is waiting fo
6. a Results printing with Printer setup Program printing of program used for the test Yes No Results printing with Suctions printing of data associated with YES YES suctions Yes No C Program TT Setup menu display 2 Next display Printer Select selection of a printer compatible 40 or 80 columns Printer setup with the analyzer using ESC P or PCL 3 language 40 col 18 91 2 Red code code for printing in red See printer doc Degree code ASCII code designating See printer doc O Baltes Me code MICE degree code see printer doc Setup menu display 2 Line feeds number of line feeds after printing Oto 5 or form feed Ege Configuration of a 40 column CITIZEN printer 40 18 91 2 Configuration of an 80 column EPSON printer 80 248 2 For the exact configuration however reference must be made to the manual supplied by the printer manufacturer Table 1 Print Setup menu display FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 5 Choosing a program and display for these parameters the Program FPP 5G S N 212 FPP 5G S N 212 FPP 5G ae ae 212 Software V 2 4 2 4 0 ISL 1999 Software V 2 4 2 4 ISL 1999 Software V 2 see 2 4 ISL 1999 ser Start J PISJE al mane Program Service Quality al AN Program No 1 Name CFPP C Unit C 5 Program No 1 Program No 1 at or Cloud CFPP 10 C 5 C CFPP C C ER id L First tes
7. 1 Automatic result validation NO Rate 9600 Databits 8 Stopbits 1 Party NO End of transmission character 0 Flow control NO Time between two messages if no flow control used 0 1 s PClinksetup ID ISLFPP5Gs Online YES Address 22 Date time setup Date MM DD YYYY Time 24 hours Laboratory setup Laboratory name Laboratory Manager name Title Alams setup Buzzer ON Modulation 30 Prom ON Ram ON Safe mem ON Keyboard ON Screen ON Battery ON AD Cnv ON Upper OD ON Lower OD ON A light ON t1 1500 5s 2 2000 Vacuum ON t 20 t 20 10s Cooling ON Heating ON Sample T ON t 100 C t 55 C 30s Jacket T ON t 112 C t 55 C 10s Refrig T ON t 120 C t 55 C 30s PrepaJaq OFF RunRefus OFF ChkTest ON Pipette ON ChkProbe ON Cu Temp ON Cu Stoke ON Cu board ON End Cfpp ON End1Aspi ON EndStopT ON EndRehea ON EndClean ON End Dry ON TmpReach ON TmpPrepa ON Regulation parameters Kp1 25 0 Ki1 0 40 Kd1 225 0 Km 10 0 Kp2 6 0 Ki2 0 10 Kd2 0 0 Kef1 0 Kef2 30 Optical detection parameters ThresholdL 150 EdgeL 350 ThresholdH 4095 EdgeH 300 ISL 400 DFFF 1 FFFF 24 A9F4 2 4 41DD 1 4 06 16 2003 10 DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix A 83 FPP 5G amp FPP 5Gs Cooling unit parameters SIN M100B3 372 11 04 2002 Runs 125 12 06 2002 704 43 152 05 6 51 13 37 12 50 1 16 0 00 0 00 0 00 11 04 2002 12 241 100 17 1min24 230 O 2min17 231 9 2min48 234 17 3min18 233 34 4min29 237 51 5min55 239 468
8. CALIBRATION OF VACUUM CIRCUIT THE VACUUM CALIB MENU 7 5 JACKET TEMPERATURE CHECKING PROCEDURE DOCV211A001 D FPP 5G amp 5Gs User Manual 1 23 1 25 1 25 1 26 1 26 1 28 1 29 1 30 1 31 1 33 2 35 2 37 2 37 2 39 2 41 2 42 2 42 2 43 2 43 2 43 2 44 2 45 2 48 2 50 2 52 2 52 2 54 2 57 2 58 2 58 2 60 2 61 2 62 Page 9 aa 8 ALARM TREATMENT 8 1 TYPES OF ALARM 8 2 DISPLAYING ALARMS STOPPING THE BUZZER 8 3 ALARM PROCESSING 8 4 ALARMS HISTORICAL 9 CONFIGURATION THE SETUP MENU 9 1 POWER ON PARAMETERS THE PWR ON MENU 9 2 CONFIGURING RESULTS DISPLAY THE DISPLAY MENU 9 3 CONFIGURING ALARMS THE ALARM MENU 9 4 FAULTS AND INDICATIONS 9 5 PERSONALIZATION AND ACCESS AUTHORIZATION TO LEVEL 1 THE LABO MENU 9 6 PRINTER CONFIGURATION THE PRINTER MENU 9 7 FPP SG S lt gt PC COMMUNICATION THE PC LINK AND RS232 MENUS 9 8 DATE TIME SETTING THE CLOCK MENU 9 9 THE SERVICE MENU 10 ACCESS LEVELS AND PASSWORD THE ACCESS MENU 11 CLEANING PROGRAMS THE CLEAN MENU APPENDIX A EXAMPLES OF PRINTOUT TYPES 1 40 COLUMN RESULT PRINTOUT 2 80 COLUMN RESULT PRINTOUT 3 80 COLUMN INTERNAL PARAMETER PRINTOUT 4 80 COLUMN CALIBRATION TICKET PRINTOUT 5 80 COLUMN MEASUREMENT PRINTOUT 6 80 COLUMN TEST PRINTOUT APPENDIX B RS232 LINK FEATURES ON FPP 5G S 1 INTERFACE FEATURES 2 OUTLET CONNECTOR BROACHING 3 COMMUNICATION PROTOCOLS 4 ENQ ACK PROTOCOL DETAI
9. DL FPP 5G amp FPP 5Gs 4 Unpacking and installation 4 1 Care in unpacking After unpacking check the device and its accessories as well as any possible damage sustained in transit which must immediately brought to the attention of the carrier so that a statement of damage can be made The various parts of the FPP 5G s are carefully checked and tested before shipping Nevertheless it is worth checking that the equipment received corresponds to the packing list enclosed On taking delivery of the FPP 5G s unpack all these parts Put the analyzer on a work bench near electrical sockets and connections to cold sources Allow enough space for access to the rear connectors 4 2 Installing the FPP 5Gs unlocking the shock absorber The FPP 5Gs cooling compressor is mounted on a shock absorber that must be locked during transportation The shock absorber is locked by bolts that screw in underneath the unit To ensure that the bolts are removed after transportation the unit will not sit flat on its base until they are removed When unwrapping the unit 1 Remove the shock absorber locking bolts from undemeath the unit 2 Screw them into the special storage panel at the back of the unit as shown below Shock absorber locking bolt Special storage panel for shock absorber locking bolts Figure 1 Locking unlocking the shock absorber 4 3 Connections 4 3 1 Connecting to the electric power supply After unpacking the FPP 5G the diff
10. ST ETES EMI CAES Cleaning No 1 gt Name lt Name gt Unit mmH20 SEK Details Cleaning No 1 lt lt Name gt mmH20 r name Unit Cleaning No 1 lt Name gt Solvent1 Cleaning No 1 lt Name gt Solvent1 Cleaning No 1 lt Name gt Solvent1 KF KI 3s 5s 1s lt Message gt 150mmH20 Message D G a Depressure F gt Ete kl Cleaning No 1 lt Name gt Solvent2 Cleaning No 1 lt Name gt Solvent2 Cleaning No 1 lt Name gt Solvent2 KI KI 3s 5s 1s lt Message gt 150mmH20 re Message g a a D Es Etag Diagram 2 The Clean menu As indicated previously the FPP 5G has two cleaning programs The choice of cleaning program depends on the needs of the user A change of program can for example occur when there is a change in the nature of the sample When the Clean menu is activated the display below allows a choice of cleaning program Cleaning No 1 Name lt Name gt Unit mmH20 CS a NTS Figure 48 Clean menu Display 1 DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 77 FPP 5G amp FPP 5Gs The following displays are set out in the table below Displays Meaning of different menus Field values menu Clean Going from left to right and from top to bottom Cleaning program No1 Cleaning No 1 Permanent field Name program name String mmH20 Name mmH2O Unit vacuum
11. SaJNSBaU 49421 uonesqijeD Bunuud A end Buguud juawuoliAua jsaj Bunuud sjjnsay EU O vz p 2 aaeMayos DS ddd 0 813 0 y2eg 22141195 SS9990 Z 1897 Asojes0ge7 SS 9 J8187 Aejdsip sjiejap jjnsay UOISSIWSUBJ S INSAY uonsajas syjnsay Bunuud synsey HEIA GENE SUu99319S NUSUI UIEN 666T ISI OPZ N S O vz v 7 A ueMI4OS Aejdsip Seinseoul JUSLINJ Aqua weu JOJEI2dQ uonsejes we1Boid Aqua asnjesaduiay jujod pnopg Gj 4equinu ajdwes Aqua qj ajdueg uonesedasd jayoer Bunes 1521 TET ENES DS ddd FPP 5G amp 5Gs User Manual DOCV211A001 D Appendix C 98 Appendix D Manual Mode Page intentionally blank Appendix D 100 FPP 5G amp 5Gs User Manual DOCV211A001 D Manual Mode The manual mode consists in use only the temperature regulation function of the FPP 5G s jacket to perform manual tests of cooling behavior for example to measure the pour point of a petroleum product a manual CPP kit to install on the FPP exists These tests are carried out via the Jacket Preparation menu screen 1 of the FPP Run Start menu PF sr ww isl france com pe Tel 33 2 31 26 43 00 Welcome 14790 VERSON Fax 33 2 31 26 62 93 FRANCE screen Francais Main menu screens FPP 5G s S N 212 FPP 5G s S N 212 FPP 5G s S N 212 Software V 2 4 2 4 C ISL 1999 k gt software v 2 4 2 4 C
12. This menu also contents software downloading commands and file loading command as well as a function to delete Ram memory content Activating the Service menu gives access to two displays Displays Meaning of different menus Field values menu Service Going from left to right and from top to bottom AccCode access code to level 2 32768 gt FPP 5G S N 212 maintenance 32767 Regul regulation parameters entry Calib entry of setting values for vacuum pump sample temperature probe and jacket D ATE Regul temperature probe Service menu Display 1 ISL UDS software downloading commands and command for data transfer to PC Service setup Next display Detect entry of optical detection parameters FPP 5G S N 212 Result memory reset saved memory results Service setup deletion Result memory reset Service menu Display 2 Table25 Service menu displays Page 2 72 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 9 9 1 Entering regulation parameters the Regul menu The regulation parameters can be entered directly on to the following display Refer to the list of parameters supplied with the device FPP 5G S N 212 Regulation parameters mor ee Kos mim 5 FPP 5G Regulation parameters Soe oe ares Figure 43 Regul menu display 9 9 2 Entering calibration values the Calib menu If data are lost the calibration values can be entered direc
13. Vacuum profile No 1 Name CFPP Type CFPP Segment 1 Constant at 200mmH20 Vacuum profile FPP 5G amp 5Gs User Manual DOCV211A001 D Examples of printout types 3 80 column internal parameter printout 07 10 2003 09 50 ISL FPP5Gs Software V2 4 24 SIN 241 ALAN ID ISL FPP 5Gs Intemal parameters Sample Temp measurement calibration Next calibration date 04 17 2004 Calibration frequency 365 days Start test refusal NO 50 C 58 F 80 310 ohms A D 88DF5D 50 C 122 F 119 400 ohms A D CBA045 Sample probe corr table 100 C 0 0 90 C 0 0 80 C 0 0 70 C 0 0 60 C 0 0 50 C 0 0 40 C 0 0 30 C 0 0 20 C 0 0 10 C 0 0 0 C 0 0 10 C 0 0 20 C 0 0 30 C 0 0 40 C 0 0 50 C 0 0 60 C 0 0 70 C 0 0 80 C 0 0 90 C 0 0 Jacket Temp measurement calibration Set point 10 00 C correction 0 81 C Set point 34 00 C correction 0 16 C Vacuum measurement calibration at OmmH20O correction FFF854 Vacuum measurement calibration at 200 mmH20 AD 7B922 D A 1AC Vacuum measurement calibration at 160 0 mbar A D 3F0902 D A BD3 Power on parameters Access level 0 Auto edition 2 Program 1 CFPP C Cleaning 1 HEPTANE Time display format 99 seconds Printer setup Automatic results printing YES Results printing with Program YES Aspirations YES Printer 80 columns Degree 91 Feed 2 lines RS232 setup Transmitted data with the result Conditions of run NO Program NO Online NO AnalyzerID
14. secs Limits Threshold ve 120 C to 55 C Threshold ve 120 C to 55 C Time 0 120s Defaults Threshold ve 100 C Threshold ve 55 C Time 30s Alarm is stopped each time a test is run Checking is continuous Stops a test currently Fault condition if jacket temperature is outside limits after recognition time running Two thresholds programmable in C Lower threshold ve and upper threshold ve recognition time secs Limits Threshold ve 120 C to 55 C Threshold ve 120 C to 55 C Time 0 120s Defaults Threshold ve 100 C Threshold ve 55 C Time 30s Alarm is stopped each time a test is run Checking is continuous Does not stop a test Fault condition if jacket temperature is outside limits after recognition time currently running Two thresholds programmable in C Lower threshold ve and upper threshold ve recognition time secs Limits Threshold ve 120 C to 55 C Threshold ve 120 C to 55 C Time 0 120s Defaults Threshold ve 120 C Threshold ve 55 C Time 30s Indicated only during automatic preparation at end of test During operator preparation this alarm is not indicated but simple screen messages appear Possible type of problem no jacket level off programmed in the cold profile Indicated only during testing by PC During testing by PC this alarm is not displayed but simple screen messages appear
15. 1 3 page 21 Press the ALARM STOP key to display the alarm message and acknowledge it or not The red LED stays on for as long as the failure persists even if the alarm has been acknowledged The failure alarms and the corresponding message are shown in the section 9 4 2 page 2 67 The limits of certain of these failure alarms can be set refer to the section 9 3 Configuring alarms the Alarm menu page 2 66 8 1 2 Warning alarms The waming alarms wam the operator of an expected event End of test with CFPP for example They are accompanied as for them by a discontinuous audio alarm the signal modulation width is adjustable refer to the section 9 3 Configuring alarms the Alarm menu page 2 66 The red LED on the ALARM STOP key lights up on the keypad It goes off when the alarm is acknowledged The waming alarms and the corresponding message are shown in the section 9 4 3 page 2 69 8 2 Displaying alarms stopping the buzzer When an alarm is triggered press the ALARM STOP key to display the cause The following screen is displayed No alarm to signal Figure 40 Alarms displaying screen The alarms screen display contains the following menus and buttons Exit to go back to the previous screen without acquitting the alarm Acquit to acquit the alarm and to go back to the previous screen Press the Acquit key to stop the buzzer and return to the previous screen Note that the red LED on the ALARM STOP key s
16. 212 FPP 5G S N 212 FPP 5G S N 212 Software V 2 4 2 4 ISL 1999 lt gt Software v 2 4 2 4 O ISL 1999 lt gt Software v 2 4 2 4 C ISL 1999 FPP RUN Start Display Kal Print Program service EA Printing Printing gt KP Diagram 4 The Print menu The FPP 5G s can print out the following information the results the calibration ticket or the parameters of a given program To be able to do this make sure that the device is linked up to a printer compatible with analyzer using the PCL 3 or the ESC P language and configured on line The printer is connected to the analyzer rear panel see Figure 2 page 17 To initiate printing activate the main level Print menu this display will appear Printing Mp Results BRun env Quality Stop Figure 26 Print menu Display 1 The first screen of the Print has the following menus e The Results menu to print out results e The Run env menu to print out a test or cleaning program e The Quality menu to print out the calibration ticket e The Stop button to stop printing in progress The second display of the menu Print menu appears thus Printing Figure 27 Print menu Display 2 Display 2 has the following menus e The Service menu for printing out among other things the values of measurements in progress sample temperature jacket temperature and cryostat e The Check menu to check the printer link e The Setup menu to set
17. 25 0 c 34 0 C Prepar re Cancel Jacket setpoint DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix C 97 y g Anue uueje asojaq auily Aqua aun uopong Anua aust ajp Aus jane ainssaidag Aqua saquinu s jp Bujueaj Anue eBesseu uoneuuojup uon29jes yun Ajue eueu wesBoid Bujues a uonoees weiBoid Bujueajg hart Ion C 2 Act dnjes peojdn peojumop wesBoid asemyos Aiowayy AUS senjen 10 28 ep je ndo AUS senjen uonesqujeo Anua suajyowesed uonenb y Aqua poo ssaoze Z janaT Jsn pe eu ajeq dmes 8rsu Yul 24 dnjes un ZEZ SY dnjas 191ulid Aud poo SSa292e jana7 uonez1WojsnJ dnes sunejy uonezyensi dnjas suajawesed dnyejs Bunuud 18491 uoneiqyeg uonesqyes WINNJEA uoneiqijeo aqoud jay er uoneiqijeo eqoid ajdwes aus ajqe UON 281102 aqoid ajdwes 666T ISI UIZ N S vz 7 z auemayos 10 39 p jeondo samo Jaddn sanjeaos2a 9 duind jonuos syed 1 z jeuy uen Bunuud Aejdsip sainseay uone ep uonsejes SJajaWEJEd eyoid wnnaen uonejap uonosajas ssajouresed ajyosd Buyjoo5 Anua suajowesed say Anue eimeiedue pue Sa Anue einjesodue 159 15114 uon ajas d 1591 uonaejes yun Anua eueu SWEIBOId dnjas uonoejes WEIBOIq WeJbodd 666T ISI UZV N S uoneinByuos 19JULId 1597 Juud ssajawesed ui onejnBa
18. 4 351 145 20C 4 4 524 133 30C 4 4 652 128 40C 4 4 82 129 50C 5 4 955 134 60C 5 4 1132 137 70C 5 5 1322 150 80C 6 5 1523 201 90C 6 5 1722 159 100C 6 5 1924 202 110C 7 6 Suctions 2142 248 120C 7 6 2414 232 130C 7 6 2701 247 140C 8 6 3010 309 150C 8 8 3338 328 160C 9 9 3726 348 17 0C 10 14 4149 423 18 0 C 12 16 4651 502 19 0 C 15 31 5313 622 200 C 23 17 5744 431 210C 33 10 1h00 46 302 220 C 60 Program No 1 Name CFPP C One test for checking YES First test at 5 C or Cloud 5 C Alarm at 55 0 C Stop at 51 0 C Maximum up time 60 s Program Allowed down time 10 s Display Print Detection YES Anomalies Up Time 20 Down Time 20 Cooling No 1 Name CFPP for Omin No test 2 Jacket level at 34 0 C until sample lt 20 0 C test every 1 0 C 3 Jacket level at 51 0 C until sample lt 35 0 C Cooling profiles test every 1 0 C 4 Jacket level at 67 0 C until sample lt 70 0 C test every 1 0 C 5 Final heating jackettemp 25 0 No test 6 End of profile Vacuum profile No 1 Name CFPP Type CFPP 1 Constant at 200mmH20 Vacuum profile DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix A 81 FPP 5G amp FPP 5Gs 2 80column result printout 07 10 2003 09 50 ISL FPP5Gs Software V 24 24 SIN 241 ALAN ID ISL FPP 5Gs Sample ID 2003 No Cloud 5 0 C Program 1 CFPP C Operator Result CFPP 22 0 C at filling up during the step 3
19. 7min40 239 87 10min18 239 11 04 2002 100 17 1min24 230 O 2min17 231 9 2min48 234 17 3min18 233 34 4min29 237 51 5min55 239 68 7min40 239 87 10min18 239 4 80 column calibration ticket printout 07 10 2003 09 50 ISL FPP5Gs Software V 2 4 2 4 SIN 241 ALAN ID ISL FPP 5Gs Calibration ticket Sample Temp measurement calibration Operator MD Calibration reference SV0513 Calibration performed 04 17 2003 Next calibration 04 17 2004 50 C 58 F 80 310 ohms A D 88DF5D 50 C 122 F 119 400 ohms A D CBA045 Sample probe corr table Jacket Temp measurement calibration Operator SM Calibration reference 7171 Set point 10 00 C correction 0 81 C Set point 34 00 C correction 0 16 C Vacuum measurement calibration at OmmH2O correction FFF854 Vacuum measurement calibration at 200 mmH20 AD 7B922 D A 1AC Operator MD Calibration reference V21001 Vacuum measurement calibration at 160 0 mbar A D 3F0902 D A BD3 Operator Calibration reference Laboratory name Laboratory Manager name Title Comments Date Signature 5 80 column measurement printout 07 10 2003 09 50 ISL FPP5Gs Software V 2 4 2 4 S N 241 ALAN ID ISL FPP 5Gs Measures Sample temperature 24 7 C R 109 620hms A D BAEC Jacket temperature 25 0 C R 110 130hms A D BBF4 Cooling 0 0 0 Flags 00000011 Heating 0 0 5 Pump OmmH2OD A 0 Pressure OmmH2OAD 0 Aspi SV OFF Air SV OFF Upper OD Em Opts Rec 5pts Lower OD Em Opts Rec
20. Allows problems to be indicated to PC Possible type of problem Alarms present which prevent test being run Alarm is stopped each time a test is run FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs Verification test fails Suction occurs at the beginning of a test if the program contains a request Alarm condition gt test for verification stopped result not Fault condition if there is a blockage gt Test stopped result not saved saved Alarm is stopped each time a test is run Badly positioned At the beginning of a test if the upper or lower optical detectors give alarm pipette condition gt no pipette Check position of Check made during test Does not stop a test sample probe Fault condition if sample temperature does not vary when difference currently running between sample and jacket temperatures is great Fault condition if difference between sample and jacket temperatures gt 5 C and sample temperature variation lt 0 4 C Cooling unit Tum off the analyzer temperature safety Clean the ventilation filters Tum on the analyzer If the problem continues contact ISL customer service Cooling unit stroke Contact ISL customer service safety Cooling unit board link Tum off the analyzer Tum on the analyzer If the problem continues contact ISL customer service Table 19 List of alarms and the corresponding messages 9 4 3 Indications Indications are made by the red LED and an intermitt
21. Date 04 02 2003 Time 23 46 Time Durat Temp Up Down TempH TimeH 0 00 4 4 36 C 19 206 206 10 C 4 4 18 C 16 351 145 20C 4 4 04C 16 524 133 30C 4 4 08 C 16 652 128 40 C 4 4 19C 14 821 129 50C 5 4 29 C 15 955 134 460 5 4 41 C 15 1132 137 70C 5 5 53 14 1322 150 80 C 6 5 6 1C 16 1523 201 90C 6 5 69 C 16 1722 159 10 0 C 6 5 75 C 17 Suctions 1924 202 11 0C 7 6 80 C 18 2142 218 120 C 7 6 9 1C 17 2414 232 130 C 7 6 99 C 19 2701 247 140 C 8 6 106 C 19 3010 309 150 C 8 8 1150C 21 3338 328 16 0C 9 9 125 C 23 3726 348 170 C 10 14 133 C 28 4149 423 180 C 12 16 142C 31 4651 502 19 0 C 15 31 155 C 51 5313 622 200 C 23 17 159 C 44 5744 431 210 C 33 10 155 C 49 1h00 46 302 220 C 60 218 C 6 Program No 1 Name CFPP C Type of analysis CFPP One test for checking YES Program First test at 5 C or Cloud 5 C Alam at 55 0 C Stop at 51 0 C og Maximun up time 60 s Allowed down time 10 s Display Print Detection YES Anomalies Up Time 0 Down Time 0 Cooling profile No 1 Name CFPP Step 1 Sample preheating at 45 0 C for 0 min No test 2 Jacket level at 34 0 C until sample lt 20 0 C test every 1 0 C Cooling profiles Appendix A 82 3 Jacket level at 51 0 C until sample lt 35 0 C test every 1 0 C 4 Jacket level at 67 0 C until sample lt 70 0 C test every 1 0 C 5 Final heating jacket temperature 25 0 No test 6 End of profile
22. FPP 5G 5Gs 9 4 Faults and indications 9 4 1 Programming Alarm Buzzer active No OFF gt The buzzer is globally inhibited Buzzer active Yes ON The buzzer will be active or inhibited depending on the configuration of each active alarm or signal Buzzer OFF does not affect the alarm or the red LED but only the buzzer Buzzer modulation may be programmed for the signals from 0 buzzer off to 100 continuous buzz 9 4 2 Faults Faults are indicated by the red LED and a permanent buzz Releasing stops the buzzer the LED remains lit as long as the fault is present Faults Tests and complementary information Effects Memory code fault Calculation and checksum comparison check made on powering up Inhibits testing If this failure is reported switch the analyzer off then on again If the failure persists contact the ISL Customer Service Data memory fault Write then read checks made on powering up Inhibits testing If this failure is reported switch the analyzer off then on again If the failure persists contact the ISL Customer Service Saved memory fault The battery for backing up the non volatile back up memory NVRAM has Machine blocked a service life of 7 to 8 years This alarm may therefore be due to a faulty because loading of battery intemal parameters The content of the saved RAM memory where the Analyzer parameters are requested stored is checked by the microprocessor If there is an error the Analyzer g
23. Field values Going from left to right and from top to bottom Analyzer PC ID identifying name of the analyzer on the ALAN network Link on line state of link between FPP5G and Yes No the PC Analyrer netw address FPP 5G s address on network 1931 Next display Interface status possible errors code linked to the FPP5G PC interface Interface initialization initialization of FPP5GPC interface Page 2 71 amp DL FPP 5G amp FPP 5Gs 9 8 Date Time setting the Clock menu The date and time are set by means of Clock menu It is possible to change the date format according to the country in which the FPP 5Gis is being used When the Clock menu is activated the following display appears Displays Meaning of different menus Field values Clock menu Going from left to right and from top to bottom Date format JJ MM AA Adjust Date Time MM JJ AA AA MM JJ AA JJ MM JJ MM AAAA 01 01 1999 JJ MM AAAMA MM JJ AAAA 3 Date rede Clock menu Display 1 AAAA JJ MM Date date in the format selected Next display Time format 12 24 h Adjust Date Time Hours time in the format selected 24 hours 15 45 Time format f Hours Clock menu Display 2 Table 24 Clock menu displays 9 9 The Service menu The Service menu is mainly dedicated to maintenance It contains menus with which regulation parameters can be entered and setting values and optical instrument detection parameters modified
24. Opts 07 10 2003 09 51 ISL FPP5Gs Software V 2 4 2 4 S N 241 ALAN ID ISL FPP 5Gs 6 80 column test printout Printer checking amp ABCDEFGHIJKLMNOPQRSTUVWXYZ4 abcdefghijkimopqrstuvwxyz aeee Appendix A 84 FPP 5G amp 5Gs User Manual DOCV211A001 D Appendix B RS232 link features on FPP 5G s Page intentionally blank Appendix B 86 FPP 5G amp 5Gs User Manual DOCV211A001 D RS232 link features on FPP 5G s In this document analyzer is used for the ISL FPP 5G s while host computer designates the computer to which the ISL FPP 5G s is connected 1 Interface features EIA RS 232C serial link Rate 300 to 19200 bps Data bits 7 8 Stop bits 1 2 Parity none odd even Switchable on line offline state Pre defined message transmission available for test Possibility to define an identifier number for the analyzer Possibility to activate result auto validation Automatic detection of the RS232 interface cable adapter 2 OUTLET CONNECTOR BROACHING The RS 232C connector of the adapter is a 9 pin connector The pin configuration is as shown below SIGNAL 2e _ GND UTG a w EIA RS 232C interface Line status in standby 12 V MARK Input signals used CTS RTS DOCV211A001 D FPP 5G amp 5Gs User Manual TxD RxD CTS Appendix B 87 DL FPP 5G amp FPP 5Gs 3 Communication protocols Flow control Protocol can be
25. Temperature unit 00 to 01 2 0 C 0 1 F Cloud point 999 9 to 9999 9 6 15 0 Results 999 9 to 9999 9 6 32 0 Reserve 9999 9 6 9999 9 Reserve 9999 9 6 9999 9 Reserve 9999 9 6 9999 9 Type of test end 00 to 05 2 0 stopped by the operator 1 plugging at filling up 12 plugging at flow back in Simul 3 plugging at flow back in CFPP 1 4 stop temperature reached 5 end of cooling profile Calibration to be done string 1 OK lt gt to be done Checksum 2 Sum of all the characters 69 5 3 Context message The context of the run is sent in one single message C Example 1 C LG 99 99 9 999 9 0 9 999 9 28 04 1999 4 12 29 46 C message Field name Format Number of Field value Example characters Analyzer no de 00 a 99 2 1 Message type string 2 C context C Operator name string 12 LG Reserve 99 2 99 Reserve 99 2 99 Reserve 9 1 9 Reserve 999 9 5 999 9 Pressure unit from 00 to 02 2 0 mmH20 0 11 mbar 2 Kpa Reserve 9 1 9 Reserve 999 9 5 999 9 Date string 10 28 04 1999 Date format from 00 to 07 2 0 JJ MM AA 4 1 MM JJ AA 2 AA MM JJ 3 AA JJ MM 4 JJ MM AAAA 5 MM JJ AAAA 6 AAAA MM JJ 7 AAAA JJ MM Hour string 6 12 29 Checksum 2 Sum of all the characters 46 DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix B 91 FPP 5G amp FPP 5Gs 5 4 Program message The program information is sent in one single message T4 Example 1 T1 CFPP C 0 0 0 10 5 25 0
26. also possible to print the test and cleaning program parameters contained in the memory Activating the Run env menu calls up the display below allowing a choice between test programs and cleaning programs Run environment printing AB Program _Cleaning _ Figure 29 Run env menu display Print menu Pressing one or other of the buttons gives access to a display that makes it possible to select the program to be printed out Page 2 42 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 4 3 Printing out the calibration ticket The calibration ticket can also be printed out provided it is in access level 1 see Appendix A section Appendix A 4 80 column calibration ticket printout page Appendix A 84 Simply activate the Quality menu and from there call up the following display Quality printing Ca 10 ration Internal Param Ticket 40 80 HH 80 col Figure 30 Quality menu display Print menu The Internal param button gives a choice between e Taking into account the printer configuration 40 80 button e Always printing out in 80 columns 80 col button whatever the printer configuration 4 4 Printing out measurements in progress Print out of Measures can be activated via the measures display screen or by using the Measures button in the following display Service Printing Figure 31 Service Printing The contents of the Regul menu are accessible only with level 2 acce
27. bottom Frequency frequency of calibration 0 gt 365 days 0 days indicates that there is no check for the passing of the calibration date Yes No Test refusal initiation of test denied when date set for calibration passed Next display Operator name of calibration operator String Calib Reference calibration reference String Next display Cancel cancel calibration Retum to display 1 of Samp T Calib menu Continue once calibration has been initiated it is no longer possible to cancel it The keys on the front panel are disabled Next display Position the simulator knob at 50 C 58 F Resistor value enter if necessary the resistance value Ohm Next display When the display becomes almost stable with the first thre characters of the A D conversion stable validate withOK Page 2 59 FPP 5G amp FPP 5Gs 7 3 Calibration of jacket temperature measurement the Jack T Calib menu Page 2 60 Jacket temperature measurement calibration should preferably be carried out after calibration of the sample probe see preceding paragraph Calibration of the jacket temperature measurement can be carried out in one of two ways 1 Automatically by means of the sample probe 2 Manually by means of a calibrated thermometer The FPP 5G s calculates the difference between the temperature indicated by the sample probe and the jacket temperature If this is too big it will consider that the calibration is b
28. continuance of operation Next display Set point selection of the two calibration points Waiting waiting time for cooling of jacket Jacket jacket temperature Sample sample temperature Cancel ending of calibration procedure the only way of stopping the operation Next display Jacket jacket temperature Sample sample temperature Waiting waiting time for stabilization of sample temperature During this time the operator can enter the reference value reference field If the sample probe is used the FPP 5G s will automatically take the value of the sample temperature shown on the screen Cancel stopping of calibration Reference sample temperature read on the thermometer or measured by the probe At the end of the operation the FPP 5G s reheats the jacket to 25 C so as to allow emptying Jack T Calib menu Display 5 Table14 Jack T Calib menu displays FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 7 4 Calibration of vacuum circuit the Vacuum Calib menu Vacuum pump calibration can be carried out at two vacuum levels 200 mmH2Oand 1600 mmH20 For this calibration a manometer able to measure 250 mmH20 for the first level and 2000mmH20 for the second is needed Note Only the vacuum level of the pump can be calibrated The air flow rate in the pump is S enslaved according to the vacuum The vacuum profile is managed by the system Procedure Displ
29. displayed Acknowledge it by pressing the ACQUIT key e To reach the following step press the STEP key of the Next setpoint menu The setpoint temperature of the next step is displayed it is not possible to make scrolling the different steps As above if the setpoint displayed do not meet the requirement of the test enter the jacket temperature desired by pressing the VALUE key of the Next setpoint menu e Press the APPLY key to lower the jacket temperature up to the following step and continue the test The new temperature setpoint appears in the Jacket setup field Proceed in this way until the test is completed If for any reason the manual test of pour point must be stopped simply press on the SToP TEST button on the front panel of the device The control software will ask for confirmation of the command refer to the User Manual Then activate the PREVIOUS LEVEL button the arrow on the left bottom The effect of both these actions is to re establish display 1 of the FPP Run Start menu DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix D 103 DL FPP 5G amp FPP 5Gs Index Appendix D 104 FPP 5G amp 5Gs User Manual DOCV211A001 D Page intentionally blank DOCV211A001 D FPP 5G amp 5Gs User Manual Page index 105 Vacuum pump 2 53 2 55 A Cooling bath 19 Coolingrate 2 49 Fe es 272 Cooling stage 2 48 Adjust EN Correction table Ti Sample probe 2 58 ime Date 272 ALAN 18 1 25 2 39 2 70 2 75 E Network 270 Ala
30. measurement unit Kpa 3 Name Bo unit be Clean menu Display 1 Next display Cleaning program No1 Cleaning No 1 same Solvent1 Solvent 1 or cleaning solvent Message entry of informative message for String operator lt Message gt Message Clean menu Display 2 Next display Cycles number number of suctions 1350 Cleaning No 1 lt Name gt Solvent1 Depressure level of vacuum necessary for 100 220 suction of solvent mmH20 5 150mmH20 cycles number Clean menu Display 3 Next display Idle Time idle time between suctions 1 gt 999s Cleaning No 1 lt Name gt Solventi Suction Time duration of suction 1 gt 9995 Time before alarm time at end of cycle before 1 gt 999s 3s 55 ls triggering of alarm to indicate to operator need to before alarm Clean menu Display 4 Next display Similarly with second solvent Table 27 Clean menu display Page 2 78 FPP 5G amp 5Gs User Manual DOCV211A001 D Appendix A Examples of printout types Page intentionally blank Appendix A 80 FPP 5G amp 5Gs User Manual DOCV211A001 D Examples of printout types 1 40 column result printout 07 10 2003 09 49 ISL FPP 5Gs Software V 2 4 2 4 S N 241 ALAN ID ISL FPP 5Gs Sample ID 2003 No Cloud 5 0 C Program 1 CFPP C Operator Result CFPP 22 0 C at filling up during the step 3 Date 04 02 2003 Time 23 46 Anomaly detected at 20 0 C Anomaly detected at 21 0 C 0 00C 4 4 206 206 10C 4
31. menu DOCV211A001 D FPP 5G amp 5Gs User Manual Page 1 31 FPP 5G amp FPP 5Gs Page 1 32 Display 2 of the Start now menu has the following components e Sample temp Temperature of the sample This field is refreshed in real time e Time t0 gt t Cumulative time from the 1 suction e Durat t 1 lt gt t Time interval between two suctions e Up s Duration of the rise by suction of the sample in the pipette e Down s Duration of the descent of the sample in the testing tube e Temp H C Maximum temperature attained by a sample in a test e tH s Time needed to attain temperature Temp H from the beginning of the current suction e Test Number of the suction displayed over the total number of suctions In testing it is always the last suction that is displayed e at__ C Temperature of the sample at the moment of suction e Next Temperature at which the next suction will be carried out Sample temp 17 5 C Time Durat Up Down Temp H t H tO gt t t l lt gt t Cs 5 C Cs 40 41 3 46 41 9 15 7 80 LY Test 28 28 at 17 C Next 18 C Figure 18 Example of test The FPP 5G s will carry out in accordance with the standard a suction at each lowering of the temperature by 1 C If the cloud point temperature is known the FPP 5G will undertake the first test at this temperature plus 5 C If not the first suction will be performed when the sample temperature reaches 1
32. of different menus Going from left to right and from top to bottom Samp sample temperature C resistance of sample probe Q Jack jacket temperature C resistance of jacket probe Q AD analog digital conversion Cooling unit Effective number of applied points Information given back by the cooling compressor command board DO reserved for ISL use D1 reserved for ISL use D2 reserved for ISL use D3 ventilation 1 ON 0 OFF D4 temperature alarm D5 optical stroke D6 maximum current D7 optical stroke fault Request in percentage sent to the cooling compressor control board Heat Effective number of applied points Information given back by the cooling compressor command board Request in percentage sent to the cooling compressor control board Print printing of three displays Next display Pressure measured depression value AD analog digital conversion Pump vacuum value imposed on pump D A digital analog conversion Print printing of three displays Next display Upper optical detector Receiver number of points received Emitter number of points emitted Lower optical detector Receiver number of points received Emitter number of points emitted Page 2 54 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs The Diagnostics menu can be accessed with the level 2 access authorization maintenance
33. other language than French and English have no contractual value and have been performed under responsibility of the local distributor In any case the reference of the present literature will be the French and or English release provided under ISL copyright Page 4 FPP 5G amp 5Gs User Manual DOCV211A001 D vd tas C U STO M E R Reserved for public relations department N ons REPORT DIENC PURPOSE wish to Report an error Submit a suggestion a comment Get more information In the area of Hardware Software Manual ANALYZER ENVIRONMENT please be complete e HARDWARE Type Of analyzer oo eee eeseestesneeeeeneestenees Serial N oes eecssseceesesseseeseeceeseseeeeeeseeeeeseees Options Parallel printer Graphic printer Plotter RS232C interface Current loop interface OMME ES E e SOFTWARE Vors eee terre ATTACHED SHEETS Listing Diskette Drawing Text Other PROBLEM DESCRIPTION COMMENTS SUBMITTED BY Name Company Address Phone Fax Date Send this report to your local Sales office orto Groupe ISL Service Clients BP 70285 14653 CARPIQUET CEDEX FRANCE Tel 33 2 31 26 43 00 Monday through Friday from 9 00 a m to 5 00 p m French Time Fax 33 2 31 26 62 93 Web http Awww isl france com DOCV211A001 D
34. soon as you have selected the language if it has not been locked in the power on parameters This measure has been taken to accelerate access to test related menus e Activate the Jacket Prepar menu of the FPP Run Start menu display 1 The following screen appears Status idle mode Jacket setup 34 0 c Tmp 25 0 C 34 0 C Next setpoint step Value App ly J Figure 49 Jacket Prepar menu display The control program searches in the cooling profile of the program previously selected for the jacket setpoint temperature of the first step It is displayed on the screen in the field located above the Next sefpoint menu gt If the setpoint displayed meets the requirement of the test press the APPLY key gt If the setpoint displayed do not meet the requirement of the test enter the jacket temperature desired press the VALUE key of the Next setpoint menu and enter the desired temperature value of the first step using the NUMERIC KEYPAD Validate with the ENTER key then press the APPLY key The jacket temperature setpoint is then displayed in the Jacket setup field and the actual jacket temperature appears in the Tmp field see Figure 49 above When the jacket temperature has reached the first step temperature programmed the warning alarm is triggered alarm used in the preparation of a standard CFPP test e Press the ALARM STOP key the alarms displaying screen appears and the message Jacket ready is
35. temperature measurement must be calibrated using the following procedure Procedure Remove the DIN plug fom the probe Insert into the free probe socket the probe simulator socket See spare parts list Activate the Samp T Calib menu Follow the indications on the displays set out below RWON gt FPP 5G amp 5Gs User Manual DOCV211A001 D DOCV211A001 D Displays Samp T Calib menu Sample temp measurement calibration Performed 01 01 1999 Next 01 01 2000 365 days NO EE Se Samp T Calib menu Display 1 Sample temp measurement calibration lt Name gt lt Ref gt EMOT GUM N Samp T Calib menu Display 2 Sample temp measurement calibration CAUTION be sure the Pt100 simulator is connected then press continue Samp T Calib menu Display 3 Sample temp measurement calibration Position simulator on 50 C 58 F 80 310 Q Resistor value Samp T Calib menu Display 4 Sample temp measurement calibration Samp 50 0 C 80 310 0 A D 88D9 Press OK when the reading is stable Ok Samp T Calib menu Display 5 Proceed similarly with the simulator knob set on 50 C 122 F At the end of operation display1 of the Quality is displayed Table13 Samp T Calib menu displays FPP 5G amp 5Gs User Manual Advanced use of the FPP 5G 5Gs Meaning of different menus Field values Going from left to right and from top to
36. to check the condition of the filter Choking of the filter by paraffin crystals or other impurities may cause erroneous results 1 Disassemble the filtration assembly completely see Figure 9 page 1 27 2 Clean the filtration assembly the pipette and the testing tube with a solvent appropriate to the nature of the sample tested Dry the different parts carefully Check the condition of the filter Reassemble the assembly see Figure 9 page 1 27 he measuring assembly is now ready for use again S JORD If the metallic filter remains clogged after this treatment it is advisable to change it 2 7 2 Automatic cleaning To initiate an automatic cleaning program follow the procedure below Procedure 1 Fill two containers of a base wide enough so that they are not unbalanced by the measurement assembly about 400 ml similar to those constituting the measuring assembly receptacle with two different solvents one for washing and the other for rinsing in accordance with the products tested and the degree of cleanliness desired FE It is assumed that the operator has taken all the precautions associated with the use of solvents 2 Remove the temperature probe from the stopper and put it in the probe port in the upper part of the device See Figure 3 on page 18 3 Unclip the testing tube which is to be cleaned separately 4 Activate the FPP Run Display menu then the Cleaning menu to call up the dis
37. 0 C If the filter is not choked when the sample has reached a temperature of 20 C the temperature of the jacket being 34 0 5 C the FPP 5G s will automatically lower the Jacket temperature to 51 1 C second step If there is still no choking when the temperature has reached 51 C third step the FPP 5G s control software stops the test in accordance with the standard E These parameters are those of the standard CFPP test ref NF EN 116 However they may be modified on condition that the necessary access authorizations have been given The personalization of the parameters and the display and printing out of results will be dealt with in the second part of this manual FPP 5G amp 5Gs User Manual DOCV211A001 D Use of the FPP 5G s with pre installed programs 2 7 Cleaning the equipment At the end of each test the measuring assembly must be cleaned This can be done manually or automatically In fact the FPP 5G has two automatic cleaning programs The programs are accessible from the Cleaning menu ID Jacket Preparation we 260 C Jack 25 6 C 05 1999 14 12 Figure 19 Display 1 of the FPP Run Display menu FE The Cleaning menu is not accessible during testing 2 7 1 Cleaning by hand Manual cleaning is recommended by the standard see Standard NF EN 116 and consists of complete disassembly and cleaning of the filtration assembly A Procedure Before each test it is necessary
38. 0 to 13 2 999 9 to 9999 9 6 characters 999 9 to 9999 9 6 characters 00 to 02 2 O pas de test I 1 test C 2 test min 99 9 to 999 9 5 2 Sum of all the characters FPP 5G amp 5Gs User Manual The cooling profiles are sent in several messages T2 Each message corresponds to one step Example 1 T2 1 CFPP p 0 5C OJEC Example 1 T2 1 CFPP p 0 5C 0 EC 1 T2 1 2 3 4 5 6 3 4 4 4 13 1 45 0 33 5 50 5 66 5 250 00 0 0 20 0 35 0 70 0 00 00 0 1 1 1 0 0 00 10 1 0 10 00 00 57 89 8F 96 GCA 41 DOCV211A001 D RS232 link features on FPP 5G s 5 6 Vacuum profile message The vacuum profiles are sent in several messages T3 Each message corresponds to one step Example 1 T3 1 CFPP 0 2B 1 T3 1 2 200 00 0 9C T message Field name Format Number of Field value Example characters Heading 1 message Analyzer no 00 to 99 2 1 Message type string 2 T3 vacuum profile T3 Vacuum profile no 01 02 2 1 Vacuum profile name string 12 CFPP Pressure unit 00 02 2 0 mmH20 1 1 mbar 0 2 Kpa Check sum 2 Sum of all the characters 2B Segments 1 message per segment Analyzer no 00 to 99 2 1 Message types string 2 T3 Vacuum profile T3 For the attention of 01 to 06 2 1 Segment no Segment type 00 to 03 2 0 nd 2 41 end 2 constant 3 dynamic Pressure setting 999 99 to 9999 99 7 200 00 Limits 000 a 999 3 0 Check sum 2 Sum of all the characters 9C 5 7 RS 232C link check messa
39. 000 pts max emission Emit manual entry of number of points to be emitted 0 gt 4095 pts Table11 Diagnostics menu displays Activating the C Unit menu first screen of the Diagnostic menu gives the possibility of running the diagnostic procedure for a built in cooling compressor Ee Before running diagnostics remove pipette tube and basket and place the cover on the jacket The diagnostic procedures may run for up to 80 minutes Diagnostics has three phases 1 Initialization heating to 40 C and regulation for 3 min 2 Cooling cooling to 110 C During this phase the values of temperatures to be noted are taken time required to fall to each notable temperature and effective number of points at this same temperature 3 Reheating retum to ambient temperature The Print button allows a print out to be made of the cooling compressor parameters plus the values noted during phase two see above which can if necessary be sent to ISL s Customer Service for the compressor s condition to be checked The following table explains the cooling unit diagnostic procedure to follow DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 55 A FPP 5G amp FPP 5Gs Page 2 56 Displays C Unit menu Cooling unit diagnostic Remove pipette tube and basket Place cover on jacket then press start 100 Duration 80 min max D Cool C Unit menu Display 1 Cooling unit diagnostic Samp 39 9 C Time
40. 1 NO ESS FA MS Kal bits gt RS 232 menu Display 4 RS232 Link setup NO 0 0s Time between Kad two messages RS 232 menu Display 5 Table 22 RS 232 menu displays 9 7 2 Setting up the PC link PC Link menu Data transmitted with result Conditions of run context of test e g operator Yes No name pressure unit Program test program carried out Yes No Next display Analyz ID identifying name of analyzer Automatic validation automatic transmission of results at the end of the test Yes No EOT caract end of transmission character ASCII code String Next display Rate rate of transfer in bauds 9600 bds Data bit data bits 718 Stop bits stop bits 1 2 Parity parity No odd Even Next display i No Flow control flow control IRTS CTS Xon Xoff ENQ ACK Time between two messages when there is 0 10s no transfer protocol With the PC Link menu the identification parameters of the analyzer FPP 5G s in the ALAN network can be displayed and fixed When the PC Link menu is activated the following displays appear Displays PC Link menu PC Link setup Analyzer PC ID lt PC ID NO 0 Analyser netw I address gt PC Link menu Display 1 PC Link setup Interface status 10 0 Correct _ interface initialisation PC Link menu Display 2 Table23 PC Link menu displays DOCV211A001 D FPP 5G amp 5Gs User Manual Meaning of different menus
41. 1min02s Cooling unit 80 Heat 36 00001001 10 0 14 1 lt Current step gt C Unit menu Display 2 Cooling unit diagnostic Samp 25 0 C Time 15min 32s Cooling unit 80 Heat 36 00001001 10 0 14 1 Diagnostic completed C Unit menu Display 3 Table12 C Unit menu displays FPP 5G amp 5Gs User Manual Meaning of different menus Going from left to right and from top to bottom Cool button for entering percentage cooling required 100 by default Start menu for running the diagnostic procedure Print printing cooling compressor parameters stored during the last diagnostic Next display Samp sampling temperature Time elapsed time Three minute countdown during the initialization phase then diagnostic phase countdown Cooling unit Effective number of applied points Information given back by the compressor control board D7 to DO see Table 10 Request in percentage sent to the compressor control board Heat Effective number of applied points Information given back by the compressor control board Request in percentage sent to the compressor control board Stop stop the diagnostic procedure and retum to the first display of the C Unit menu lt Current step gt one of the three following steps Initialization Cooling Reheating Next display Upper part similar to previous display Print cooling compressor parameters Exit back to first displays of t
42. 3 SE EN analys Temperature Program No 1 Kt 1 CFPP 1 CFPP Cooling Profile Vacuum Profile Program No 1 3 Display Print Anomalies Yes 0 0 nd of tes Up time fi Do Detection Delta Program No 1 70 0 C 51 0 C 60s 10s M Al lowed Home Diagram 5 The Program menu Atest program is made up of the following elements e Test parameters e A cooling profile e Avacuum profile The FPP 5G s has 5 factory pre installed programs viz e CFPP C standard CFPP test Temperature measurement unit C e Simul C filterability test with constant cooling rate of jacket Temperature measurement unit C e CFPP F CFPP test Temperature measurement unit F e Simul F filterability test with constant cooling rate of jacket Temperature measurement unit F e CFPP C memory area with priority use for downloading programs from a PC DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 45 amp DL FPP 5G amp FPP 5Gs The FPP 5G s also has 5 cooling profiles and 2 vacuum profiles Program Cooling profile Vacuum profile 1 CFPP C 1 CFPP C 1 CFPP 2 Simul C 2 Simul C 2 Simul 3 CFPP F 3 CFPP F 1 CFPP 4 Simul F 4 Simul F 2 Simul 5 CFPP C 5 CFPP C 1 CFPP Table 2 Summary table of programs and profiles The Table 2 page 2 46 summarizes all the programs and profiles contained in t
43. FPP 5G amp 5Gs User Manual Page 5 Page intentionally blank Page 6 FPP 5G amp 5Gs User Manual DOCV211A001 D DOCV211A001 D Caution This ISL analyzer has been carefully designed manufactured and inspected for quality It has been equipped with a number of safety features However the use of this analyzer may involve the handling of solvents chemicals and other potentially dangerous flammable toxic etc materials Please exercise caution when handling these materials while operating the analyzer Please eread the manual ewear proper protective clothing eperform all suggested service procedures euse care to prevent accidents The manufacturer accepts no responsibility for any damage or liability arising from the use of analyzers Use of Non ISL Products and Accessories Defects or damage that result from the use of Non ISL branded or certified Products Accessories Software or other peripheral equipment are excluded from warranty FPP 5G amp 5Gs User Manual Page 7 Page intentionally blank Page 8 FPP 5G amp 5Gs User Manual DOCV211A001 D Contents GENERAL 1 INTRODUCTION 1 1 ISL COMPANY PROFILE 1 2 TYPOGRAPHICAL CONVENTIONS 1 3 ABOUT THIS MANUAL 2 TYPE OF ANALYZER 3 CAREIN USE 3 1 MEANING OF SYMBOLS 3 2 CARE IN THE USE OF TESTING AND CLEANING EQUIPMENT 3 3 PRECAUTIONS TO TAKE WHEN USING BUILT IN COOLING ANALYZERS 4 UNPACKING AND INSTALLATION 4 1 CARE IN UNPACKING 4 2 IN
44. Finally a Vacuum source equipped with an electronic Vacuum regulator eRefer to the text of standard NF EN 116 for further details See on Part 2 section 7 Adjustment and calibration the Quality menu on page 2 57 for the temperature probe calibration procedure LU DOCV211A001 D FPP 5G amp 5Gs User Manual Page 19 LA DL FPP 5G amp FPP 5Gs 6 The user interface 6 1 Front panel The front panel of the device appears thus Back lighted 8 line LCD Activation keys for menus or buttons displayed onLCD LCD navigation key Keys Stop Numeric keypad Reset and Alarm stop and CANCEL and ENTER keys Direction keys FN DL FPP 5G Figure 4 Front panel 6 1 1 The LCD screen The front panel of the device therefore includes an 8 ine LCD which may be represented thus Retums one level B si calling for in the display hal ee hierarchy alphanumeric value Next display matory gt Sense mm ee gt Menu activated by key immediately below see Figure 5 General operation of display and menus Figure 4 On either side of this display two keys make it possible to travel up and down the hierarchy of screens activate the NEXT SCREEN and PREVIOUS SCREEN keys see Figure 3 In the lower part of the display there are four keys by means of which the menus displayed on the display can be activated 6 1 2 Backlight setting The LCD screen backlight is set by a combination of the ENTER Key and the high DIRECTI
45. IMS Use the adapter supplied see the Packing List it has two RS 485 connectors on one side which have to be connected simultaneously to the Analyzer s Alan input and output and on the other side an RS 232C connector to be connected to the PC Note The RS 232C communication mode has to be parameterized Refer to the Part 2 section 9 7 1 Setting up the RS232C link the RS232 menu page 2 70 Refer to the Appendix B RS232 link features on FPP 5G s page 85 for the link characteristics the description of the communication protocol and the meaning of the messages and 4 3 5 3 The SERVICE port The FPP 5G s has a serial SERVICE port as a standard fitting with which with the help of the ISL UDS maintenance software supplied software updates can be downloaded via a PC and the contents of the memory such as the internal parameters and results can be saved for subsequent reloading refer to the Part 2 section 9 9 4 File upload download commands the UDS menu page 2 73 FPP 5G amp 5Gs User Manual DOCV211A001 D General 5 Description of the device The FPP 5G s consists broadly speaking of two major parts e The user interface e The filtration bank and the electronic and mechanical parts linked to it The user interface will be the subject of the next paragraph As regards the filtration bank we will here only deal with the parts handled by an operator in the context of an CFPP test or one of the other fo
46. Instrumentation Scientifique de Laboratoire Aa zeg aS FPP 5G amp FPP 5Gs User manual Instrumentation Scientifique de Laboratoire BP 70285 14653 CARPIQUET CEDEX FRANCE Phone 33 2 31 26 43 00 Fax 33 2 31 26 62 93 Web htfp www isl france com Page 2 FPP 5G amp 5Gs User Manual DOCV211A001 D z Revisions historical j concemed Modification descriptive Date A Creation 00 04 01 Part 2 6 2 7 4 7 5 Software update to version 2 3 Jacket temperature checking procedure B 89 Quality menu addition of a memory resetting key Configuration menu spare 02 06 18 parts list adding General 6 2 Welcome screen language selection at power on Part 1 2 4 2 Assisted edition function Part 2 4 6 Printer configuration menu Part2 5 Program parameters configuration menu detection parameters for up and C down time added 03 07 11 Part288 Alarms treatment with historical Part 289 1 Configuration menu of power on parameters Appendix A Printout examples updated Appendix B Description of the communication protocol of the RS 232C link D Part 1 2 5 Modification of the Jacket Preparation menu 03 11 06 Appendix D Manual mode available DOCV211A001 D FPP 5G amp 5Gs User Manual Page 3 ISL C copyright The FPP5G s Analyzers and this manual are protected by copyright Reproduction of the unit will result in prosecution All rights to the
47. LS 5 TRANSMITTED DATA 5 1 MESSAGE FORMAT 5 2 RESULT MESSAGES 5 3 CONTEXT MESSAGE 5 4 PROGRAM MESSAGE 5 5 COOLING PROFILE MESSAGE 5 6 VACUUM PROFILE MESSAGE 5 7 RS 232C LINK CHECK MESSAGE 6 RS232 COST APPENDIX C DIAGRAMS 1 TEST LAUNCH DIAGRAM 2 ACTION CHART APPENDIX D MANUAL MODE 1 PREPARING THE TEST 2 TEST RUNNING IN MANUAL MODE INDEX SPARE PARTS LIST Page 10 FPP 5G amp 5Gs User Manual 2 63 2 63 2 63 2 63 2 64 2 65 2 66 2 66 2 66 2 67 2 70 2 70 2 70 2 72 2 72 2 76 2 77 102 103 104 DOCV211X200 DOCV211A001 D General Page intentionally blank Page 12 FPP 5G amp 5Gs User Manual DOCV211A001 D General 1 Introduction 1 1 ISL company profile We would like to take this opportunity to thank you for choosing ISL product We are confident that you will be completely satisfied with your new Analyzer and we hope that you continue to call on us for all of your laboratory s petroleum testing needs Before you begin we ask you to take a few minutes to become acquainted with ISL and its history ISL s beginnings go back to 1975 when a group of engineers and scientists from the heart of the Northem France s petrochemical industry began seeking ways to automate petroleum testing The neighboring industry served as an excellent research and development proving ground for their new equipment By the end of 70 s several quality instruments had been dev
48. ON KEY for less contrast and low DIRECTION KEY for more contrast refer to the next section FE Note The intensity of the backlight can change according to the ambient temperature Page 20 FPP 5G amp 5Gs User Manual DOCV211A001 D General 6 1 3 The control keys The lower left hand side of the front panel is taken up by three keys namely STOPITEST To stop a test or any other operation If the LED is lit up this means that a test is in progress STOP Ss RESET To cancel and go up through the display menu hierarchy Interrupts the audible alarm signal ALARM STOP N If the LED is lit up this means that a problem has arisen Pressing on this button will give the error message content The rest of the front panel is occupied by a numeric keypad equipped with a CANCEL KEY and an ENTER key lea ENTER key validate an input of variables DE To CANCEL characters Finally in the lower left hand section there are four direction keys used to move around a text field and select characters to enter variables e g name of sample DIRECTION keys Scrolling of test result suctions 6 2 Welcome display and language choice When the analyzer is switched on the welcome screen is displayed If it does not first check the backlight settings see section 6 1 2 on the previous page This screen provides information about ISL and two menus offering the choice of language I SL
49. Pa Name Unit Vacuum Profile menu Display 1 Segment 1 Vacuum profile No 2 Simul Kal 10 s Pset pt gto be reached 1n Vacuum Profile menu Display 2 1 2 Table7 Vacuum profile displays N 2 DOCV211A001 D End of profile FPP 5G amp 5Gs User Manual Name name of profile Unit unit of vacuum measurement Linear variation vacuum Set pt First vacuum limit value to be reached in time in seconds before moving to second vacuum limit value The display above is followed by two displays corresponding to segment 2 and segment 3 of the vacuum profile 13 50 KPa to be attained in 26s 15 50 KPa to be attained in 60s Advanced use of the FPP 5G 5Gs Field values String mmH20 Kpa mbar Next display 0 gt 1600 mmH20 0 gt 16 Kpa 0 gt 160 mbar 1 gt 180 s Page 2 51 FPP 5G amp FPP 5Gs 4 s w i w 6 Measurement and diagnostics the Service menu FPP 5G S N 212 FPP 5G S N 212 FPP 5G S N 212 Software V 2 4 2 4 C ISL 1999 lt H gt Software v 2 4 2 4 O ISL 1999 Software V 2 4 2 4 ISL 1999 Start i I Display RTS Program _J Service _ Quality _ Diagram 6 The Service menu Service is Diagnostics The Service menu is in great part dedicated to maintenance With this menu it is possible to e Display measures e Slave the main parts of the device Activating the Service menu calls up the fo
50. Results menu Test results are stored in a dedicated memory The FPP 5G can store up to 50 test results this depends on the number of suctions per test When the memory is full the FPP 5G automatically compresses the first results recorded The results can be sent to a PC by the ALAN or the RS232C link see 9 7 FPP5G s PC communication the PC Link and RS232 on page 2 70 To display the results the following procedure should be followed Procedure 1 Press the button for the Results menu this calls up the display allowing access to all the results saved which are shown as follows Res 3 28 CFPP 18 0 C Samp Diesel No 001 Prog 1CFPP C 12 05 1999 09 40 Ri Print MS 9 Next ETEN 1 Figure 24 Ecran 1 du menu Results e Res number of the result displayed over the number of results stored in memory An asterisk appears in front of the result number if the test has been carried out despite the date of the adjustment of the sample temperature measurement circuit was exceeded refer to the section 7 2 page 2 58 e CFPP __ Limit temperature of sample filterability and the type of blockage this information cannot be displayed See Display Print detection parameters Table 3 program on page 44 e Samp Identifying name of the sample e No Sample number e Prog The program chosen for the test e Date and time of the end of the test To access the desired result press as many times as necessary o
51. STALLING THE FPP 5GS UNLOCKING THE SHOCK ABSORBER 4 3 CONNECTIONS 5 DESCRIPTION OF THE DEVICE 6 THE USER INTERFACE 6 1 FRONT PANEL 6 2 WELCOME DISPLAY AND LANGUAGE CHOICE PART 1 USE OF THE FPP 5G S WITH PRE INSTALLED PROGRAMS 1 INTRODUCTION 2 THE FIRST TEST 2 1 PREPARING A SAMPLE 2 2 ASSEMBLING THE FILTRATION AND MEASURING ASSEMBLY 2 3 CHARACTERIZATION OF THE SAMPLE 2 4 TEXT ENTRY DISPLAY 2 5 PREPARING THE JACKET 2 6 INITIATING THE TEST 2 7 CLEANING THE EQUIPMENT PART 2 ADVANCED USE OF THE FPP 5G 5GS 1 INTRODUCTION 2 SCREENS OF THE MAIN MENU 3 DISPLAYING RESULTS THE RESULTS MENU 4 PRINTING OUT THE PRINT MENU 4 1 PRINTING OUT RESULTS 4 2 PRINTING TEST AND CLEANING PROGRAM PARAMETERS 4 3 PRINTING OUT THE CALIBRATION TICKET 4 4 PRINTING OUT MEASUREMENTS IN PROGRESS 4 5 PRINTOUT TEST 4 6 PRINTER CONFIGURATION 5 CHOOSING A PROGRAM AND DISPLAY FOR THESE PARAMETERS THE PROGRAM MENU 5 1 COOLING PROFILE THE COOLING PROFILE MENU 5 2 VACUUM PROFILE THE VACUUM PROFILE MENU 6 MEASUREMENT AND DIAGNOSTICS THE SERVICE MENU 6 1 MEASUREMENT AND DIAGNOSTIC ON THE FPP 5G ANALYZER 6 2 MEASUREMENT AND DIAGNOSTIC ON THE FPP 5GS ANALYZER 7 ADJUSTMENT AND CALIBRATION THE QUALITY MENU 7 1 SAMPLE PROBE CORRECTION TABLE THE CORRECT TABLE MENU 7 2 CALIBRATION OF SAMPLE TEMPERATURE MEASUREMENT THE SAMP T CALIB MENU 7 3 CALIBRATION OF JACKET TEMPERATURE MEASUREMENT THE JACK T CALIB MENU 7 4
52. The temperature setpoint is then displayed in the Jacket setup field and the real jacket temperature appears in the Tmp field It is possible to go directly to the following step by pressing the STEP key only after the first step was applied If the cooling profile does not include a jacket step you will have to enter the desired temperature Press the VALUE key of the Next setpoint menu Enter the temperature value of the desired step using the numeric keypad and validate with the ENTER key 3 Initiate preparation of the jacket by activating the APPLY button Otherwise activate the PREVIOUS LEVEL button the arrow on the left bottom The effect of both these actions is to re establish display 1 of the FPP Run Start menu see Figure 10 page 1 28 Do not forget to place the cover on the jacket so as to avoid condensation of water vapor inside it When the jacket has reached the set temperature an audible signal is given If for any reason the preparation of the jacket must be stopped simply press on the SToP TEST button on the front panel of the device The control software will ask for confirmation of the command on the following display FPP 5G amp 5Gs User Manual DOCV211A001 D Use of the FPP 5G s with pre installed programs Jacket preparation Do you really want to stop ae Te Figure 15 Confirmation that jacket preparation is to be cancelled Confirm or cancel the command by activating the Yes or No butt
53. VERSON LEN 2 31 26 62 93 FRANCE Francais FPP 5G S N 212 FPP 5G S N 212 FPP 5G S N 212 Software V 2 4 2 4 C ISL 1999 lt H gt Software v 2 4 2 4 C ISL 1999 lt gt Software v 2 4 2 4 C a 1999 Main menu A Sample No Sample No Prog 1 CFPP C Op La gt Prog 1 CFPP C Op now im Diagram 2 Access to the main display level The main level display is the highest hierarchically speaking It is not directly accessible when the device is switched on To access it after switching the device on and pressing on any button it is necessary to go up one display level Diagram 2 above shows how access to this level operates gt If the user has operator access a very simple menu is available to him amp The user can run and follow a test The user can display and print a result gt If the user has Laboratory Labo or Maintenance Maint access the complete menu is available 0 0 0 DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 37 DL FPP 5G amp FPP 5Gs FPP 5G S N 212 Software V 2 4 2 4 C ISL 1999 FPP Run o Start PILEN FPP 5G S N 212 Software V 2 4 2 4 C ISL 1999 o U Banal HIE ES MAN hl FPP 5G S N 212 Software V 2 4 2 4 C ISL 1999 o O ESTE Karrie Figure 23 The three displays of the main level with access level 1 or more The main display level includes the following components respectively f
54. Zi Verson ww isl france com 14790 VERSON Tel 33 2 31 26 43 O0 FRANCE Fax 433 2 31 26 62 93 English Frangais Figure 6 Welcome display This display remains active until the key corresponding to the language of your choice is pressed Doing this activates the display 1 of the CFPP Run Start menu see Diagram 1 page 1 25 Note You can disable the language choice as part of the startup parameters refer to the Part 2 section 9 1 page 2 66 If the choice is locked press any key on the front panel DOCV211A001 D FPP 5G amp 5Gs User Manual Page 21 DL FPP 5G amp FPP 5Gs Page intentionally blank Page 22 FPP 5G amp 5Gs User Manual DOCV211A001 D Part I Use of the FPP 5G s with pre installed programs Page intentionally blank Page 1 24 FPP 5G amp 5Gs User Manual DOCV211A001 D Use of the FPP 5G s with pre installed programs 1 Introduction The multi functional nature of the FPP 5G s is shown as discussed previously by the fact that it is possible to carry out over and above tests complying with the current standard in this case standard NF EN 116 a personalized test programs based on specific inputs In this part we will focus on a standard test i e the CFPP test This test is along with four others pre installed at ISL They are saved in a memory that is very easily updated e g to change a name by downloading from a PC via the ALAN network 2 The first test In this chapter we wil
55. ame PIDDMMYY NVM This way the latest version of the internal parameters will be saved to a file AID converter fault Permanent check made for absence of dialogue with converter Inhibits testing and stops a current test Upper optical fork fault Check made at the end of light slaving Stops a current test For the TLF slaving is made before each suction Fault condition if transmission is strong and reception is weak or if transmission is weak and reception is strong Thresholds are not programmable Alarm stopped each time a testis run Lower optical fork fault Check made at the end of light slaving Stops a current test For the TLF slaving is made before each suction Fault condition if transmission is strong and reception is weak or if transmission is weak and reception is strong Thresholds are not programmable Alarm stopped each time a testis run DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 67 FPP 5G amp FPP 5Gs Ambient light too strong Vacuum circuit fault Cooling circuit fault Heating circuit fault Sample temperature fault Jacket temperature fault Refrigerant temperature fault Jacket preparation impossible Test refused Page 2 68 Permanent check on light received outside transmission period Stop a current test One alarm for both upper and lower detectors Two programmable thresholds Average threshold time to be taken into account gt alarm and stop test Strong threshold with immed
56. art whatever the field is consisting of an alphabetic table from which the characters to be entered are selected and three buttons OK Delete and Insert Sample ID ABCDEFGHIJKLMNOPQRSTUVWXYZ HON Q J Ax abcdefghijkImnopqrstuvwxyz lt gt Figure 13 Text entry screen The field concemed is the sample identifying name sample ID The characters are entered in the following way 1 On the entry display a black rectangle flashes on the first letter of the table A To select a letter use the direction keys on the front panel Press the key as often as necessary or keep the finger pressed on it to indicate the direction of the character sought 2 When the flashing rectangle is positioned on the character sought press the ENTER key on the numeric keypad If the character is incorrect cancel it with the CANCEL key 3 If there is a mistake in the string of characters entered use the direction keys and the Insert and Delete buttons to remedy it 4 Finally validate with the OK button DOCV211A001 D FPP 5G amp 5Gs User Manual Page 1 29 FPP 5G amp FPP 5Gs Proceed in similar way for the operator name After validating by means of the OK button in the text entry display the initial display retums automatically to the display 1 of the Run menu see Figure 10 page 1 28 The same is true at each entry of text variables by means of the text entry display 2 4 2 Assisted edition To speed up test s
57. ax 120s stopping the test Os means that there is no detection on descent the sample is considered to have gone down Next display Detection Display Print type of detection Yes No displayed or not 18 C At filling up see Program No 1 Display Print Anomalies Figure 24 page 2 39 YES 0 0 Anomalies indicating the anomalieson Oto 100 nd ot tes Down t the up and down times printed with the 0 no check Detection Del ta Delta result and indicated by a waming alam at Program menu display 5 the end of test The up and down times are compared each others if delta T time interval between each suction decreases a waming alarm is triggered at the end of test and a message will be printed with the result The time reduction allowed is a percentage of the previous suction time if the interval in time of the suction N 1 time of the suction N gt to the interval programmed in an anomaly is detected at the suction N tr ta Interval in x 100 with t time of the suction N 1 amp time of the suction N Next display Cooling profile choice of cooling profile 10r2 Program No 1 pre heating option Vacuum profile choice of vacuum profile 1 or 2 Detailed in Table4 and Table 5 1 CFPP 1 CFPP Program menu display 6 Table3 Program menu displays Without the necessary authorizations passwords it is not possible to change the field values of the Program men
58. ays Vacuum Calib menu Vacuum measure calibration mmH20 MESEN SL MU LE Vacuum Calib menu Display 1 Vacuum meas calibration at 200 mmH20 lt Name gt lt Ref gt Vacuum Calib menu Display 2 Vacuum meas calibration at 200 mmH20 Connect a manometer able to measure 250 mmH20 then press OK Ok Vacuum Calib menu Display 3 Vacuum meas calibration at 200 mmH20 Calibration at 0 mmH20 waiting 12s Vacuum Calib menu Display 4 Vacuum meas calibration at 200 mmH20 Wait for circuit depressure 10 s Vacuum Calib menu Display 5 Ajust the depressure with or enter the read value Meaning of different menus Field values Going from left to right and from top to bottom Vacuum calibration Exit operation cancel 200 mmH20 1600 mmH20 Unit KPa mmH20 mbar Next display Vacuum calibration at 200 mmH20 Operator operator name String Calib Reference calibration reference String Next display At the end of the vacuum tube attach a manometer able to measure 2 50 KPa Validate by activating the OK button Next display Presetup at 0 KPa resetting of A D converter waiting time necessary for resetting Next display Wait for circuit depressure time necessary to 10s attain vacuum level desired 2 00 or 16 00 KPa gt 200mmH20 30s Cancel stops calibration gt 1600mmH20 Next display OK validates calibration Set pt entry of val
59. bolts in place FPP 5Gs Figure 2 Rear panels and connections DOCV211A001 D FPP 5G amp 5Gs User Manual Page 17 FPP 5G amp FPP 5Gs Page 18 4 3 4 Sample temperature probe connection 1 Connect the sample temperature probe DIN plug to the corresponding socket on the front panel of the device 2 Insert the probe in the probe holder on the upper part of the device Probe holder Sample temperature probe socket Figure 3 Sample temperature probe connection 4 3 5 FPP 5G s PC link The FPP 5G s Analyzer is fitted with an RS232C interface and an RS485 interface as standard 4 3 5 1 Connection to the Alan network RS 485 link The Alan network allows among others one or more devices to be run by a PC using software specially developed by ISL The connection to the Alan network is done by means of two ports input output in the back side of the Analyzer see Figure 2 page 17 LI Refer to Alan Software installation manual and follow on line help available Note The RS 485 communication mode has to be parameterized Refer to the Part 2 section 9 7 2 Setting up the PC link PC Link menu page 2 71 FE 4 3 5 2 RS 232 C link The Alan network input output ports may be connected via a special adapter supplied with the analyzer to form an RS 232 C serial link enabling results to be collected to the delimited ASCII format on a PC or on any other computer system and for transmission to a L
60. c ISL 1999 J K gt software v 2 4 2 4 ISL 1999 UT Start EEN A FPP Run Start menu display 1 et 2 Sample No Sample No Prog 1 CFPP C Op Prog 1 CFPP C Op Jacket tart C tart Prepar U mato mare mes BE Status idle mode Jacket setup 25 0 C Tmp 25 0 C 34 0 C Next setpoint Step Value Diagram 9 Access to the Jacket Preparation menu The cooling bath insulating of the FPP 5G s originally predicted for CFPP tests has not been provided for long term tests at low temperature below 70 C Ice should form around the bath in the analyzer and cause damages by melting DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix D 101 DL FPP 5G amp FPP 5Gs CAUTION The manual mode for measuring the cloud pour point should not be used more than 4 or 5 times a year for tests at low temperatures below 70 C The test should not exceed 4 hours and the jacket temperature should not lower under 90 C Ee Note Beyond the number of test advised if an insulating problem appears the warranty could not be taken into account after the opinion of the Customer Service 1 Preparing the test Prepare the sample and the analyzer e Prepare the sample following recommendations of the standard method used for the manual test e Install the different elements necessary for carrying out the test in the FPP 5G s analyzer bath in accordance with the recommendations
61. drical seal holder and the second O ring before introducing the assembly into the strainer body and tightening Assemble the rest of the filtration assembly as per Figure 9 on page 1 27 3 Put the filtration assembly into the testing tube having previously filled it 4 Carefully push the filtration assembly pipette stopper assembly into the testing assembly until they clip together To remove the stopper push in the direction opposite to that used to achieve mounting Make sure that the filtration assembly is right at the end of the testing tube 5 Fix the vacuum pump tube at the free end of the pipette 6 Place the measuring assembly consisting of the pipette the stopper and the filtration assembly into the receptacle intended for this purpose to the right of the jacket and called the Measuring Head Port DOCV211A001 D FPP 5G amp 5Gs User Manual Page 1 27 DL FPP 5G amp FPP 5Gs 2 3 Characterization of the sample When the device is switched on the welcome display per Figure 6 page 21 is displayed By pressing on the STOPITEST key on the front of the device the following display appears thus ID Ech Prog 1 CFPP C Start Jacket Oo Mel Figure 10 Display 1 of the FPP Run Start menu There are two points to be made in this respect gt After switching on the device the display of the FPP Run Start menu above is obtained after the language has been chosen or by pressing any key on the front panel if the lang
62. e The FPP 5G an extemal cooling analyzer e The FPP 5Gs a built in cooling analyzer The two models are similar and will be described as one FPP 5G s throughout the manual However the special characteristics of each model will be explained where necessary 2 Type of analyzer The FPP 5G makes it possible to determine the filterability limit temperature of medium distillates including those containing fluidification agents and other additives It will be recalled that the filterability limit temperature or CFPP is the highest temperature at which a given device when it is subjected to cooling in standard conditions ref NF EN 116 The special feature of the present device is that it is very multi functional in that all its parameters can be re set It can thus over and above the program govemed by the NF EN 116 standard standard pre installed CFPP test as well as four other programs run programs based on the personalized parameters and linked to the needs of the user This major trump card allows the device to be used not only for the usual tests but also in the R amp D area What is more this multi functionality has not been achieved at the expense of ease of use Indeed as we shall see in the following chapters the multi functionality of the device is equaled only by ease of use Finally it should be noted that the device has an electronic vacuum regulation system which significantly improves the accuracy of the tests and con
63. ed and controlled from a PC e Bymeans of the RS 232 C link the FPP 5G s can send test results to a PC e The service port The parameters linked to each of the communication modes are set out below 9 7 1 Setting up the RS232C link the RS232 menu If the RS 232 C link is chosen as means of communication it is necessary to have the requisite adapter supplied with the device This has a series port on one side while connecting simultaneously to the inlet and outlet of the ALAN network When the adapter is connected the device automatically detects the presence of an RS 232 C link If the RS 232 C adapter is not detected then e The RS 485 PC link is declared detected e The RS 232 link is declared not detected The parameters of this link are presented in the table below Displays Meaning of different menus Field values menu RS 232 Going from left to right and from top to bottom Link on line link established Yes No RS232 Link setup lt Detected not det gt Check sending ofa link check frame lt ISL ON OFF FPP 5G DB gt No OFF n ne Ed RS 232 menu Display 1 Next display Page 2 70 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs RS232 Link setup Transmitted data with the result NO NO Condition of rung Program RS 232 menu Display 2 RS232 Link setup 1 NO 0 Automatic validation RS 232 menu Display 3 RS232 Link setup 9600 bds 8
64. ed by the host computer which must protocol is send a ENQ enquiry character Any message must be acknowledged detailed by the host computer by sending a ACK character below Note There is no need to define a time between messages because the message sequencing keeps pace with the ENQs sent by the host computer Appendix B 88 FPP 5G amp 5Gs User Manual DOCV211A001 D RS232 link features on FPP 5G s 4 ENQ ACK protocol details All messages from the analyzer must be acknowledged by the host computer Should communication fail only the host computer can decide whether or not to abort transmission Analyzer response time on receiving ENQ lt 100 ms Waiting time for message acknowledgment 2 sec Results transfer delay after end of test delay for ENQ not limited Number of transmission of the same result message on receiving NAK not limited end with ACK or EOT reception Request reception and acknowledgement of results The host computer uses the ENQ code 05H to ask the analyzer if any results are ready to be sent If the analyzer has no results to send it replies ACK 06H the host computer does not have to reply to this ACK ANALYZER HOST COMPUTER No result available lt ENQ No resut ACK If the analyzer has results it starts their transmission On receiving the message the host computer must check it checksum and must reply ACK 06H or NAK 15H depending on whether the message was correct or not
65. eing done by means of the extemal calibrated thermometer In this case it will wait for a reference value to be entered before moving from one stage to the next Procedure 1 Follow the indications on the displays set out in the following table Displays Jack T Calib menu Jacket temp measurement calibration lt Name gt lt Ref gt IK motto gcalib Reterence Jack T Calib menu Display 1 Jacket temp measurement calibration Fill the jacket up to the mark and immerse the reference probe Jack T Calib menu Display 2 Jacket temp measurement calibration Set point 10 0 C waiting 6 min Jacket 29 8 C Sample 29 0 C Jack T Calib menu Display 3 Jacket temp measurement calibration Jacket 10 0 C Sample 10 0 C Waiting 10 min C Jack T Calib menu Display 4 Do the same for the second stage 34 0 C End of jacket temperature calibration wait until the jacket is reheated before draining it Jacket 15 C Meaning of different menus From left to right and from top to bottom Operator name of the operator for the jacket temperature probe calibration Calib Reference calibration reference Next display Fill the jacket up to the mark visible on the intemal wall of the jacket with the same liquid as that used in the cooling circuit Selection of two setting temperatures Setpt 10 34 C or Setpt 34 51 C cooling stages Continue
66. eloped and were being marketed in Europe under ATPEM Trademark The most famous of these new instruments was the CPP 97 Automatic Cloud and Pour Point Analyzer Introduced in the early 1980 s its successor the CPP97 6 revolutionized cold flow testing enabling up to six tests automatically and simultaneously Adding new automatic instruments each year ATPEM soon became a world wide leader in automatic petroleum test instrumentation In 1986 they expanded operations reorganizing into the company now knows as ISL Striving to maintain close contact with customers in over 75 countries ISL has since grown founded Sales amp Service branches on each continent With design marketing service and support operating together under the ISL roof the company reached a new dimension in 1993 by obtaining ISO 9002 certification from the BVQI Working hard to extend our quality assurance program we received ISO 9001 certification in 1995 Though best known for distillation viscosity testing cold behavior instrumentation flash point evaporation loss oxidation and asphalt testing equipment ISL s contributions to automated petroleum testing continue to grow With more than 10 patents to date ISL s constant research into new technologies buttresses our precedent for ultimate precision performance and safety The company now offers over 20 Automatic Analyzers for different applications giving incontestable benefits to its users in increasing of te
67. ent buzzer A release stops the buzzer and turns off the LED Indications Complementary information End of test with CFPP Result storedCFPP xx x Indication stopped each time a test is run End of test with CFPP at Result storedCFPP xx x end of first suction Indication stopped each time a testis run End of test on Stop The sample temperature has exceeded the Stop temperature set in the test program temperature Result storedStop on Stop temperature xx x Indication stopped each time a test is run End of cleaning Indication at the end of cleaning cycles Sample temperature Comparison of sample temperature with alarm temperature set in the test program reached Indication when sample temperature is low apart from preheating Indication stopped each time a test is run Jacket ready Indication during jacket preparation when jacket temperature reaches requested level 0 25 C 0 45 F Indication stopped each time a test is run Anomaly detected on Two parameters of FPP programs let the up and down times to be verified refer to the Table3 up down times page 2 47 If the time between two suctions decreases this waming alarm is set off at the end of test and a message will be printed with the result Table20 List of indications DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 69 amp DL FPP 5G amp FPP 5Gs 9 5 Personalization and access authorization to level 1 the Labo menu The FPP 5G s can be personali
68. erent extensions need to be connected and it should be plugged into different networks and circuits Regarding the connection of the FPP 5G s to the mains it should be noted that the device is built to operate from 90 to 130 Volts and from 180 to 250 Volts at 50 or 60 Hz in accordance with the majority of countries where the device is marketed The power cable corresponding to the country of sale is supplied with the device 4 3 2 Connecting the analyzer to the cooling circuit FPP 5G There are two nozzles for this purpose at the rear of the device see the photograph in Figure 2 page 17 When connecting pay attention to the inlet and outlet markings indicated on the nozzle support LU Refer to the ISL specifications for further details of the characteristics of the coolingunit Page 16 FPP 5G amp 5Gs User Manual DOCV211A001 D General 4 3 3 Connecting the printer A parallel port is provided at the back of the analyzer for connecting a printer compatible with the Analyzer using ESC P language with which to print out test results among other things Caution The Analyzer and peripherals must be switched off before connecting any new peripherals Service Port Parallel port Printer ALAN network inlet and outlet Cooling circuit inlet and outlet Logic card ventilator Mains switch and socket Cooling unit ventilator Shock absorber fixing panel with the two blocking
69. ersion Print printing of three displays Next display DOCV211A001 D Advanced use of the FPP 5G 5Gs Upper opt det Receiver Opts Receiver Opts Emitter Opts Emitter Opts Lower opt det Measures menu Display 3 Optical sensors reading noted Table8 Measures menu displays Upper optical detector Receiver number of points received Emitter number of points emitted Lower optical detector Receiver number of points received Emitter number of points emitted The Diagnostics menu can be accessed with the level 2 access authorization maintenance Displays Diagnostics menu Samp 30 4 C 111 85 A D DEDE Jack 29 2 C 111 38 o A D BE17 Refr 31 C 0 0 0 0 3 Diagnostics menu Display 1 Pressure 1 mmH20 A D r Pump i O mmH20 D A a a mH20 Su OFF se cars menu Display 2 Diag 200 mmH20 Pump gt Suct SV ON OFF gt AirSV OFF Upper opt det Receiver Opts Receiver Emitter Opts Emitter emit Emit Lower opt det Diagnostics menu Display 3 Table 9 Diagnostics menu displays DOCV211A001 D FPP 5G amp 5Gs User Manual Meaning of different menus Field values Going from left to right and from top to bottom For upper part of display see Table8 Cool percentage of cooling entry Heat percentage of heating entry Next display For upper part of display see Table8 200 1600 mmH2O Diag vacuum settin
70. esult searched is the operability cca Pre or temperature of the previous Kul analys Temperature plugging test Check Test Carrying out or not a suction atthe Yes No Program menu display 3 beginning of the test so as to check the device status First test temperature temperature 0 of the first test 1 If tmp of cloud point unknown gt Enter 6 1 Fixed 0 Min 70 C Max 50 C 2 If tmp of cloud point known gt 2 X 0 cloud X Min 0 C Max 50 C Next display Page 2 46 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs Alarm alarm at the moment a noteworthy Min 70 C Program No 1 temperature is reached Max 50 C Stop adjustment of the end of test sample Min 51 C 55 0 C 51 0 C Os temperature The last test will be carried out Max 50 C Kal Down Maximum up time adjustment of the Min 1s Program menu display 4 GEPF maximum duration of suction before the Max 120s test is stopped 60s is the duration required by NF EN 116 Program Na amp ifthe test type is CFPP Min Os 55 0 C 51 0 C Os Allowed down t time allowed for the Max 120s R verd mum sample to go back down the testing tube If oe Down the temp of the next suction is achieved Program menu display 4 Simul before this time has elapsed the test will not be stopped If the test type is Simul Maximum Down t maximum time for the Min Os sample to go back down the tube before M
71. etting for final re heating if Type 1 or preparation for a new test if Type 2 Stage 6 End of profile display common to all the profiles Meaning of different menus Going from left to right and from top to bottom Cooling profile 2 Name selection of profile name Unit selection of temperature measurement unit Stage 1 Sample cooling rate Set point setting of jacket cooling rate Limit limit sample temperature for moving to next stage Stage 2 Tests suction Frequency setting of interval between two suctions Intervals are expressed either in minutes or in degrees C F 1 Interval in minutes 2 Interval in C F Ti F1 3 Stage 3 Cooling Prof ile No See Cooling Profile menu Display 10 No 1 Step 2 Final Jacket Temperature Heating 25 0 C Cooling Profile menu Display 5 No 2 End of profile Table 5 Cooling profile N 2 FPP 5G amp 5Gs User Manual Min 20 C 68 F Max 30 C 86 F Next display Field values Next display Min 0 5 C h 1 F h Max 60 C h 108 F h Next display Yes No If Tests Yes Min 2 min Max 60 min Min 1 C 2 F Max 5 C 10 F Next display Page 2 49 FPP 5G amp FPP 5Gs 5 2 Vacuum profile the Vacuum profile menu vacuum profile is composed of segments Each segment is defined by the following elements e A type non modifiable e Asetting e Acondition for moving to the next stage if necessary After
72. formed at the analyzer level The transmission is possible after the validation automatic validation can be set in the RS232 Link setup The transmission is possible as soon as the distillation run ends 5 1 Message format Messages are transmitted in ASCII code Character strings are enclosed within double quotes They start with an opening bracket They finish witha closing bracket 2 characters CK and the characters CR LF and EOT CK 2 characters checksum the 2 least significant digits expressed in ASCII of the result of the hexadecimal sum of all the preceding characters including the brackets CR 1 non printable character Carriage Return ODh LF 1 non printable character Line Feed OAh EOT 1 non printable character End Of Transmission character programmable in the RS232 configuration menu if 0 there is no end of transmission character Appendix B 90 FPP 5G amp 5Gs User Manual DOCV211A001 D RS232 link features on FPP 5G s 5 2 Result messages The CFPP result is sent using the R message Example 1 R ISL 3419 E8 N 05 1 99 0 15 0 32 0 9999 9 9999 9 9999 9 1 69 Meaning of result message fields from left to right R message Field name Format Number of Field value Example characters Analyzer no from 00 to 99 2 1 Message type string 2 R result R Sample ID string 12 ISL 3419 Sample no string 12 E8 N 05 Test program no from 00 to 99 2 1 Reserve 99 2 99
73. g I 2 16 Kpa 20 160 mbar Pump manual pump start ON OFF Suct SV open shut suction solenoid valve ON OFF AirSV open shut leak solenoid valve ON OFF Diag 1600 mmH20 Pump ON gt Suct SV ON or OFF set before pump start gt AirSV ON Next display Optical detector Emitter number of points emitted 0 pts no light emitted 4095 pts maximum light emitted Receiver number of points received 0 pts no light received 4095 pts maximum light received Auto automatic control of emitter to obtain a given no of points on the receiver 2000 pts Emit manual entry of number of points to be emitted 0 gt 4095 pts 0 gt 4095 pts max emission Page 2 53 FPP 5G amp FPP 5Gs 6 2 Measurement and diagnostic on the FPP 5Gs analyzer The Measures menu in the Service menu gives access to the following information organized into three displays Displays Measures menu Samp 22 7 C 108 840 A D D8DE Jack 27 9 C 110 860 A D BD33 Cooling unit 0 Heat 0 00000001 0 0 0 0 LI Measures menu Display 1 Sample jacket and refrigerant temperatures taken Pressure 1 mmH20 A D F97 pump O mmH20 D A 0 Measures menu Display 2 Pressure measured and pump command noted Upper opt det Lower opt det Receiver Opts Receiver Opts Emitter Opts Emitter Opts Measures menu Display 3 Optical sensors reading noted Table 10 Measures menu displays Meaning
74. g profile for the standard CFPP test 2 Cooling profile for the Simul C test Cooling profile N 1 Displays Meaning of different menus Field values Cooling Profile menu No 1 Going from left to right and from top to bottom The cooling profile is number 1 Cooling Profile No 1 permanent field Name selection of profile name String Unit selection of temperature measurement CPF unit CFPP c 3 Name B unit Cooling Profile menu Display 1 No 1 Next display Step 1 Cooling Profile No 1 Pre heating of sample Step 1 Set point Sample pre heating temperature Min 30 C Sample Preheating for setting Max 50 C at 45 0 C 0 min Limit duration of pre heating expressed in Min O min Kal Set point mf minutes once the setting has been reached Max 60 min Cooling Profile menu Display 2 No 1 0 min indicates that there is no pre heating Next display Step 1 Cooling Profile No 1 Tests there can be no suction during the pre No step 1 heating stage No tests Cooling Profile menu Display 3 No 1 Next display Step 2 Cooling Profile No 1 First cooling stage in the CFPP test Step 2 Set point temperature setting of the jacket Jacket level Until sample cooling stage at Ep 0 C lt 20 0 C Limit limit sample temperature for moving to eS O next stage of jacket cooling Cooling Profile menu Display 4 No 1 Next display Page 2 48 FPP 5G amp 5Gs User Man
75. ge ISL FPP 5G DB 6 RS232 cost There is neither option nor extra fee for RS232 software and hardware including the RS232 cable adapter which is provided as standard DOCV211A001 D FPP 5G amp 5Gs User Manual Appendix B 93 DL FPP 5G amp FPP 5Gs Page intentionally blank Appendix B 94 FPP 5G amp 5Gs User Manual DOCV211A001 D Appendix C Diagrams Page intentionally blank Appendix C 96 FPP 5G amp 5Gs User Manual DOCV211A001 D Diagrams 1 Test launch diagram ISL Zi verson 14790 FPP 56 SN 212 FPP 5G HE 22 S N 212 Software V 2 4 2 4 ISL 1998 oyl software v 2 HE 240 Software V 2 4 2 4 FPP Run Start Display RS ECTS a F P P R n Main Menu saple No sample ND Prog 1PP CO Op Prog 1FP CO Op Va Ke ET RSS tes Operator ABCDEFGHIKLVNDPORSTOMANVZ ANTOL abcdefghi jklmopqrstuwxyz gt 0 Select a progran No Name PP CO unit C ECS 5 ID Sample tep 17 5 C Status Running o Time Durat Up Don Temp EH Test 10 gt t thet co Jack 34 0 C 2 6 0 C 40 4L 3 46 a 9 15 7 8 12 05 1999 14 12 Up s Dan s Ka Test 287 28 at 17 C net BT Sample ID gt ABDEFGHTSIKLNOPORSTUMIXYZ FEXT L A abcdefghi jklmopgrstumyr gt 0 Jacket preparation Jacket temperature
76. gt Software v 2 4 2 4 ISL 1999 K gt Software V 2 4 2 4 O ISL 1999 ee Start _ fisplay ACCESS Access Current Access Level 2 Labo Service Levei 1 air dd Level 0 Diagram 1 The Access menu If entry to a protected level is attempted the following message is displayed indicating the current level and the access level requested The access codes can be entered by means of two buttons Levelf and Level2 see the Config Labo menu for configuring the access code for level 1 laboratory Also see the Config Maint menu for the definition of the access code for level 2 maintenance Access Denied Current Access Level 0 Required 1 Labo Service 3 me Fer Figure 46 Access to level refused message indicating that the level is write protected The main display of the Access menu shown below enables access to a given level or if necessary to zero level Current Access Level 0 Labo Service 3 me KE Figure 47 Access menu display The digital access code is entered through the numeric segment If the code is correct access is achieved validation with the ENTRY key Page 2 76 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 11 Cleaning programs the Clean menu FPP 5G S N 212 FPP 5G HE 212 FPP 5G S N 212 Software V 2 34 2 4 ISL 1999 Software V 2 HE 2 4 ISL 1999 gt Software v 2 4 2 4 ISL 1999 sg Start Displa
77. he Correct Table menu The Correct Table menu makes it possible to enter a correction table for the sample temperature measurement probe The sample temperature displayed takes this table into account at rest during testing and during calibration The sample probe is a Pt100 platinum probe compliant with standard IEC 51 Class A It is S supplied with an ISL Quality Certificate stating the value of the temperature discrepancy at 40 C discrepancy Value reference t C On activating the Correct Table menu the following display appears Sample probe correction table Correction Probe value reference o K ms trees unit 5 Figure 38 Correct Table menu Display 1 This display allows the name of the correction table to be entered and the table s unit of temperature to be selected On a series of displays similar to the display below the correction values can be entered correction value value indicated by the probe reference value for temperatures from 100 C 148 F to 90 C 194 F with an increment of 10 C Sample probe correction table Correction Probe value reference 0 0 0 0 0 0 0 0 100 c sifre e t mira Figure 39 Correct Table menu Display 2 5 correction value entry display 7 2 Calibration of sample temperature measurement the Samp T Calib menu Page 2 58 Calibration of the sample temperature measurement is done through the Samp T Calib menu The sample
78. he C Unit menu DOCV211A001 D Advanced use of the FPP 5G 5Gs 7 Adjustment and calibration the Quality menu FPP 5G S N 212 FPP 5G S N 212 FPP 5G S N 212 Software V 2 4 2 4 ISL 1999 lt H gt Software v 2 4 2 4 ISL 1999 K gt Software v 2 4 2 4 ISL 1999 FPP Run Start __ fisplay Service Jj Quality quality Quality gt correc amp T ack T Vacuum alib ticke SG Table CULCE UD Kst Printing Diagram 7 The Quality menu The FPP 5G measurement instrumentation sometimes requires calibration How often depends on the user but it is recommended that all the measurement instruments be adjusted at least once a year The Quality menu has a series of menus dealing with the following adjustments these are grouped in the display below Quality LI Table Calib f Calib J calib Figure 36 Quality menu display 1 e The Correct Table menu sample temperature measurement correction table e The Samp T Calib menu calibration of sample temperature measurement e The Jack T Calib menu calibration of jacket temperature measurement e The Vaccum Calib menu vacuum circuit calibration Adjustments carried out in this way can be printed out using the Calib ticket Printing menu Quality Calib ticket Printing Figure 37 Quality menu display 2 DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 57 FPP 5G amp FPP 5Gs 7 1 Sample probe correction table t
79. he FPP 5G memory This makes it possible to carry out a test in strict compliance with the current standard e g line 1 table 2 but also all kinds of combinations provided one has the necessary access authorizations All the parameters of a program are visible but can only be modified if one has the level 1 access authorization laboratory To access the associated programs and profiles proceed as follows Procedure 1 Activate the Program menu of main level display 1 see Diagram 5 The Program menu on page2 45 The following display then appears Program No 1 Name CFPP C Unit C LS Figure 32 Display 1 of level 2 Program menu With the Next button the factory pre installed programs can be scrolled and selected In Figure 32 the program selected is number 1 2 Todisplay the program parameters press on the Details button These are the displays which appear Display Meaning of different menus Field values Program menu Going from left to right and from top to bottom Current program is N 1 permanent display Program No 1 Name selection of program name The program name in this case is CFPP String Unit selection of temperature measurement CFPP C unit The temperature is here measured in C 3 Name mire CF Program menu display 2 Next display Type of test choice of test type CFPP Simul P Re ram No 1 CFPP plugging temperature result search o r na oud or ae Simul r
80. iate recognition gt alarm and stop test Threshold limits 0 to 4095 points Time 0 to 120 seconds By default Threshold 1 1500pts after 5 seconds Threshold 2 2000pts Alarm stopped each time a test is run Check made on testing and cleaning Stops a current test Fault if pressure measured is outside limits Two thresholds programmable in relative to the instructions Lower threshold ve and upper threshold ve recognition time Limits Threshold ve 0 to 100 cs Threshold ve 0 to 100 csg Time 0 to 120 seconds By default Threshold ve 20 Threshold ve 20 Time 10 seconds Alarm stopped each time a testis run During cleaning only the Upper threshold exceeded test is made Checking is continuous Does not stop a test in Fault condition if jacket temperature does not vary at least 1 C after 10 progress minutes for an SV cold command of 100 Thresholds not programmable Alarm is stopped each time a test is run Checking is continuous Cuts the heat command Fault condition if jacket temperature does not vary at least 1 C after 8 and stops a test being minutes for an SV heat command of 100 run Thresholds not programmable Alarm is stopped each time a test is run Check made during test Stops a test currently Fault condition if sample temperature is outside limits after recognition time running Two thresholds programmable in C Lower threshold ve and upper threshold ve recognition time
81. l deal with a CFPP standard test carried out with the FPP 5G stage by stage We will however only describe the menus that are strictly necessary for the successful operation of the test We will further assume that the operator has taken due note of the care that needs to be taken with the substances tested and of cleaning products I SL Zi verson www ist 14790 VERSON 2 89 FRANCE Sample No Sample No Prog 1 CFPP C Op Prog 1 CFPP C Op acke ar c ar EG oe Bo fem Cloud Operator 7 ABCDEFGHIJKLMNOPQRSTUVWXYZ amp A abcdefghijkimnopqrstuvwxyz lt gt 0 Select a program No Name CFPP C Unit C le ID Sample temp 17 5 C Status Running 0 Time Durat Up Down Temp H t H Test 26 0 C p tot t l lt gt t s s CO Jack 34 0 C 40 41 3 46 41 9 15 7 80 12 05 1999 14 12 Up s Dwn s k Test 28 at 17 C Next 18 C Sample ID en p 7 abcdefghijkimnopqrstuvwxyz lt gt 0Q Status idle mode Jacket setup 25 0 C Tmp 25 0 C 34 0 C ext setpoin Step Value Apply Diagram 1 Starting a test DOCV211A001 D FPP 5G amp 5Gs User Manual Page 1 25 DL FPP 5G amp FPP 5Gs 2 1 Preparing a sample Before initiating the test phase a sample must be prepared It will be remembered that the FPP 5G s is intended fo
82. llowing display Service LI Measures Diagnostics Figure 35 Service menu displays The Measurements and Diagnostics menus lead to a series of screens The series of screens for the FPP 5G differs from those for the FPP 5Gs In fact on the FPP 5Gs the menus allow a builtin cooling compressor diagnostic to be made if necessary 6 1 Measurement and diagnostic on the FPP 5G analyzer The Measures menu in the Service menu gives access to the following information organized into three displays Displays Measures menu Samp 30 4 C 111 859 A D DEDE Jack 29 2 C 111 38 A D BE17 Refr 31 C USE Print Cool 0 0 Heat Measures menu Display 1 Sample jacket and refrigerant temperatures taken Pressure 1 mmH20 A D F97 Pump O mmH20 D A 0 Measures menu Display 2 Pressure measured and pump command noted Page 2 52 FPP 5G amp 5Gs User Manual Meaning of different menus Field values Going from left to right and from top to bottom Samp sample temperature C resistance of sample probe Q Jack jacket temperature C resistance of jacket probe Q AD analog digital conversion Refr cooling circuit entry temperature Cool percentage cooling Heat percentage heating Print printing of three displays Next display Pressure measured depression value AD analog digital conversion Pump vacuum value imposed on pump D A digital analog conv
83. m ENQ ACK protocol Acknowledgement 2 63 RS 232 89 Activated De activated 2 66 Entry Defauttalam_ 263 Access code 2 76 Modulation 2G Calibration values 2 72 2 73 Wamingalam 263 Optical detection parameters 2 72 Alarms Optical detection values 2 75 Historical 264 Regulation parameters 2 72 2 73 Listofh 267 Text Numerical values 1 29 Processing 2 63 Analyzer 2 70 2 71 F address 2 71 Filtration assembly 1 26 Filterability 14 1 29 2 39 2 40 2 45 Assembly Format Filtration 19 1 26 1 33 DateTime 272 Insulating 1 31 Measuring 1 31 1 33 I Slem near de Insulating assembly 19 Emitter 2 53 2 55 Insulatingring 49 Vee ee ae PB 101 B ISL 13 14 16 18 19 21 1 25 2 58 2 70 90 91 803016 101 Button Check 2 43 J Cloud 1 29 Cycles 1 34 Jacket 19 1 30 1 31 1 32 2 43 2 49 2 60 Delete 129 Jacket End 134 Cover 1 31 EE ee Jacket Prepar 1 30 level LEE S 276 Jacket Prepar 1 30 102 Measures 2 43 Modulation 2 66 K Oneres 2 42 Ke Setup 244 EE 21 ET CANCEL 21 G Control 21 Calibration 2 57 a our Jacket probe 2 60 NNN Sample probe 2 58 Bae Vacuum circuit 2 57 Stop lest_ 1 30 Vacuum pump calibration 261 Up Down YLE 2 40 Care un en Cleaning products 1 25 L Unpacking 16 CFPP14 19 1 25 1 29 1 30 1 32 2 40 2 46 2 47 2 48 Link 2 50 90 91 92 93 RS 232C 2 70 CFPP F 2 45 Cleaning M elg ORTEN Er lini Mode 99 Cleaning program enu Change 2 77 7 ons Cleaning 1 33 oint of 1 29 Clock 2 72 Connecting Cloud 1 28 ALAN EE
84. manual are reserved Reproduction in any form including in the form of excerpts shall require written permission from the copyright holder ISL FPP5G s Software 1999 ISL This software is owned by ISL and is registered under the registration number IDDN FR 001 250006 02 R P 1999 000 30000 at the Agence pour la Protection des Programmes 119 Avenue de Flandre 75019 Paris It is protected in France by the Code de Propri t Intellectuelle laws and intemationally by intemational treaty provisions and all other applicable national laws It must not be copied reproduced adapted translated rented or disassembled This also applies to the accompanying manuals INFORMATION Information in this document is subject to change without notice and does not represent a commitment on the part of ISL ISL provides this document as is without warranty of any kind either expressed or implied including but not limited to the particular purpose ISL may make improvements and or changes in this manual or in the product s and or the program s described in this manual at any time This product could include technical inaccuracies or typographical errors Changes are periodically made to the information herein these changes may be incorporated in new editions of the publication Reproduction of any part of this manual without express written permission is forbidden Translation in foreign local language other than French or English Translation in
85. means of the numeric keypad In fact if the cloud point temperature is known the test could start with that plus x C x being a program parameter x gt 5 C for a standard CFPP test The Prog button gives a choice of factory pre installed programs Activating the Prog menu displays the following screen Select a program No Name CFPP C Unit C LS a NS Figure 12 Display 1 of the Prog menu To select the desired program activate the Next button as many times as necessary When the desired program is displayed activate the OK button The FPP 5G s has 5 programs pre installed at the factory These programs are CFPP C Standard CFPP test Unit of temperature measurement C Simul C Filterability test with constant rate of cooling of jacket Unit of temperature measurement C CFPP F Filterability test Unit of temperature measurement F Simul F Filterability test with constant rate of cooling of jacket Unit of temperature measurement F 5 CFPP C Memory area for priority use for downloading programs from a PC N 9 All these programs are entirely modifiable provided there is the necessary authority to do so 2 4 Text entry display 2 4 1 Text entry This display is typical of text entry displays It is found at all points and is essentially made up of two parts e A variable part on the upper part of the display which is the name of the field e Arecurrent p
86. n the Prev and Next buttons Press the Print button to print out the result previously selected with the Prev and Next buttons Press the Transm button to validate a result so as to send it to the RS323C link or to the ALAN network When the desired result is achieved details of the result may be viewed by pressing on the NEXT DISPLAY button which gives the following display Res 2 28 CFPP tO gt t t l lt gt t S C S 42 30 4 30 60 14 2 50 LI Test 15 15at Figure 25 Display 2 of the Results menu ARON DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 39 FPP 5G amp FPP 5Gs Page 2 40 This screen similar to the one in Figure 19 on page 26 differs from it in the following respects gt Upper part of screen above table e Res _ __ sample ranking e g result of test n 2 out of 28 carried out gt Res 2 28 e CFPP limit temperature of filterability of the sample gt Lower part of screen below table e Test at C Number of the suction displayed over the total number and the temperature at which they were carried out 6 Press on the UP or Down keys on the front panel to display the details of each suction The duration of the rise the descent tH can be visualized in seconds or in one tenth seconds see section 9 page 2 65 for the configuration FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 4 Printing out the Print menu FPP 5G S N
87. n the course of cleaning e Pressure reduction applied for suction of the solvent This field may also be modified directly in the course of cleaning to allow the height of the solvent rise to be adjusted and the filtration assembly only to be cleaned or the whole measuring assembly by further reducing the pressure e With the End button the current cleaning stage can be definitively ended At the end of this stage the display in Figure 20 on page 1 34 appears For solvent 2 exactly the same procedure is followed At the end of each stage of the cleaning process an intermittent alarm tells the operator that the operation has finished A second program is available This may be useful if there is a change in the type of sample for example which might imply the use of different solvents and so a different number of cycles Page 1 34 FPP 5G amp 5Gs User Manual DOCV211A001 D Part 2 Advanced use of the FPP 5G 5Gs Page intentionally blank Page 2 36 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 1 Introduction This part deals with the advanced use of the FPP 5G i e the setting of the device according to the needs of the user As previously indicated this presupposes that the user is familiar with the techniques of plugging tests The FPP 5G settings are accessible from the main display see following paragraph 2 Screens of the main menu Ise BP 40 re 2 a1 56 B00 el 14790
88. nly quit when a connection has been made to the computer In the second case it is preferable not to try to quit download mode Downloading causes memory loss If an error is made it is better to let the downloading continue and then download again If the operator stops the analyzer during downloading the next time the analyzer is powered up it will automatically detect that a transfer is necessary DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 73 aa FPP 5G amp FPP 5Gs Page 2 74 9 9 4 1 Transfer procedure The analyzer goes into download mode either automatically or requested by the user It waits for a PC transmission When the downloading software is run on the PC it sends a specific message to the analyzer In replying to this message the analyzer indicates the type of downloading required followed by a safety sequence The PC then sends data which is processed by the analyzer When the PC software considers the downloading finished it validates this with a signal to the analyzer 9 9 4 2 Installation and start up of the downloading program See instructions in Read me file 9 9 4 3 User requested transfer Preparation Power down the PC and the analyzer and plug the cable into the serial connection on the back of the analyzer and the serial port of the PC ePower up the PC and the analyzer Analyzer Select the software downloading menu eSelect the required functions The transfer will be to the PC
89. o o oe st Cooling Profile 2 48 Coolingeireut 16 Correct Table 2 57 2 58 Mains NE NE Diagnostics 2 53 2 55 Control Display 1 33 Leak solenoid valve 2 53 2 55 Jack T Calib 2 57 Solenoid 2 53 2 55 Jack T Caib 260 DOCV211A001 D FPP 5G amp 5Gs User Manual Page index 1 iL FPP 5G amp FPP 5Gs Jacket Prepar 1 28 Selection 2 46 Measures 2 52 2 54 Test 2 42 No1 28 Oper 1 28 R PC Link 2 71 Print 2 42 Request and reception of results prog 1 28 RS 232 89 Program 2 46 Results Pwr on 2 66 Displays 2 39 Quality 2 43 2 57 Printing 2 42 Regul 2 43 Send to a PC or a LIMS 18 Regul 2 73 Storage 2 39 Results 242 Ring wedges 19 Al Cap ka RS 232 C link 2 70 amp T Cali a Samp T Calib 2 58 ed 87 Sample 1 28 Interface 87 Service 2 52 2 72 Start 1 31 S Start now 1 28 Vaccum Calib 2 57 Sample Vacuum Calib 2 61 Filtering 1 26 Vacuum Profile 2 50 Preparation 1 26 Menu Sceen Labo 2 70 LCD 20 Screen N Main level 2 37 Network Lee F Analyzer address name 2 71 Setpoint Jacket 1 30 0 Setup Optical detector Alams 2 66 upper lower 2 53 2 55 Solenoid valve 2 53 2 55 Stop P Jacket preparation 1 30 Pipette 19 Stopper 19 1 26 Preparation T Jacket 1 30 Printer Temperature Citizen 2 44 Jacket 1 31 EPSON 2 41 2 44 Temperature Sensor 19 Setup 2 44 Test Printing CFPP C 2 45 Calibration ticket 2 43 2 57 Launch 1 25 Check 2 43 Simul C 245 Program parameters 2 42 Simul F 2 45 Probe Testing tube 19 Jacket calibrati
90. oes automatically into download mode so that the contents of the RAM memory saved can be restored by loading a backup file from a PC For this purpose a diskette containing the internal parameter factory settings necessary if memory has not been recently uploaded and a PC up download program are shipped with the standard version of the Analyzer Refer to the section 9 9 4 page 2 730n how to load the Analyzer parameters Note So as to have an up to date copy of the Analyzer s internal parameters always to hand it is advised to upload the internal parameters to the PC during routine maintenance operations Use a new file name each time this operation is performed Do not use the intemal parameter file name on the original diskette supplied with the Analyzer Battery fault Permanent check The battery is used while the machine is stopped for the dock and to save parameters stored in RAM If the failure is reported Do not switch off the Analyzer as this will delete any stored data Print or upload to a PC file the Analyzer parameters contained in the non volatile back up memory the NVRAM see the section 9 9 4 page 2 73 Switch off the Analyzer and call a qualified technician to replace the battery Download Analyzer intemal parameters or enter them Note Regular uploading of the internal parameters must be programmed as part of the analyzer maintenance procedure Use a new filename e g with the current date in the n
91. of the standard method e Then using the Program menu of the FPP Run Start menu display 2 refer to the User Manual Part 1 section 2 3 Characterization of the sample select a prestored program on the analyzer to which a cooling profile with steps complying with the standard method is associated refer to the Part 2 in the User Manual section 5 1 Cooling profile the Cooling profile menu to visualize the parameters of a program Appendix D 102 FPP 5G amp 5Gs User Manual DOCV211A001 D Manual Mode You can use gt A prestored cooling profile by selecting a program to which it is associated gt A cooling profile specially created using ISL Alan Software and downloaded into the analyzer gt A prestored cooling profile in which the desired values will be entered this profile will be used as a base the values of steps entered will not be registered You also can modify a prestored cooling profile refer to the User Manual Part 2 section 5 1 Cooling profile the Cooling profile menu if it contains enough number of step Enter the cooling temperature of the bath indicated in the standard method used for each step It is even possible to program the analyzer to reheating the sample at the end of test 2 Test running in manual mode e Activate the FPP Run Start menu of the main menu screen 1 see Diagram 9 on the previous page Note The display of the FPP Run Start menu is obtained at switching on the device or as
92. on 2 57 2 60 Sample calibration 2 57 2 58 U Sample correction table 2 57 2 58 Profile Upload download 2 75 Cooling 2 48 Vacuum 2 50 yV Program14 1 25 1 29 1 30 1 34 2 38 2 39 2 41 2 42 2 44 2 45 2 46 2 47 2 48 2 65 2 66 2 71 2 78 91 92 Vacuum regulator 19 Cleaning 1 33 2 42 2 77 Vacuum Source 19 Elements 2 45 Number 1 34 W Parameters displa 2 46 Parameters kor 2 42 Welcome screen 21 Printing 2 42 Page index 2 FPP 5G amp 5Gs User Manual DOCV211A001 D
93. ons respectively To gain time the Jacket preparation stage can be carried out first before even preparing the sample and assembling the filtration assembly FE 2 6 Initiating the test After the audible signal for the end of the preparation of the jacket is sounded carry out following operations Procedure 1 Remove the Jacket cover 2 Place the insulating assembly at the bottom of the Jacket 3 Remove the measuring assembly from the receptacle and place it in the Jacket 4 Activate the Start now menu If all the stages have been carried out correctly the display below will appear Status Running ID O fest 260 C Jack 34 0 C 12 05 1999 14 12 Dwn s Figure 16 Display 1 Start now menu This display camies the following information e ID Sample identification name e Status Operation under way on this case the test is running e Test During the test this field indicates the temperature of the sample at which the forthcoming suction will be carried out e Jack Jacket temperature e Current date and time e In large characters The sample temperature given by the probe This screen gives access by means of the Next Display button to another display on which the progress and details of the current test may be followed in real time Sample temp 26 0 C Time Durat Up Down Temp H t H tO gt t t 1 lt gt t Cs Cs COQ Cs pr LJ Test O Oat Figure 17 Display 2 Start now
94. play below DOCV211A001 D FPP 5G amp 5Gs User Manual Page 1 33 DL FPP 5G amp FPP 5Gs Cleaning No 1 lt Name gt Select the next step Done Figure 20 Display 1 of the Cleaning menu This display includes in its upper part the number of the automatic cleaning program in progress Here it is program N 1 In the lower part of the display two buttons give access to the two stages of cleaning and a third Select allows a Cleaning program to be selected and displayed Completion of each stage will be indicated by Done 5 Immerse the measurement assembly in the container of the first solvent and validate by activating the OK button of the display below Otherwise exit by means of the Exit button Cleaning No 1 lt Name gt Solvent 1 Immerse the pipette into the solvent lt Message gt O OK Figure 21 Display 1 of the Solv 1 menu Modification of the lt Message gt and lt Name gt fields are dealt with in Part 2 section 11 Cleaning programs the Clean menu page 2 77 FE After validating the following screen appears Cleaning No 1 lt Name gt Solvent 1 Status Cleaning 0 5 150 mmH20 gt Ed Figure 22 Display 2 of the Solv 1 menu This display includes the following components e The number of the current program permanent field e The current stage e The status cleaning in progress e The number of cycles this field may be modified directly by activating the Cycles button i
95. r medium distillates and is not suitable for other hydrocarbons Procedure 1 By means of a non fluffy paper filter products certified with reference number standard NF EN 116 about 50ml of the sample at the laboratory s ambient temperature but in any case not below 15 C ref Standard NF EN 116 2 Pour the sample thus filtered into the empty testing tube as far as the permanent level marking a volume equivalent to 45ml 2 2 Assembling the filtration and measuring assembly The filtration and measuring assembly is assembled as follows Procedure 1 Insert the pipette into the stopper as shown in Figure 7 and Figure 8 see above Vent Space for the pipette 9 Space for the sample Figure 7 Stopper 3D view and view from above Figure 8 Positioning of the Pipette on the stopper Page 1 26 FPP 5G amp 5Gs User Manual DOCV211A001 D Use of the FPP 5G s with pre installed programs Pipette Upper wheel nut Conical seal holder O ring Cylindrical seal holder O ring Strainer body Er EN Strainer filter Web support Filter tightening nut Figure 9 Assembly of filtration assembly with parts list 2 When the pipette is introduced into the stopper insert into it The upper wheel nut the conical seal holder the first O ring the cylin
96. r a download the red LED will flash every second A downloading in progress is indicated by rapid flashing which is related to the rate of data transfer FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs The download and data transfer commands are accessible from the following displays Displays UDS menu Meaning of different menus Going from left to right and from top to bottom Transfer download Upload DownLoad Download u Download Download Program amp Text Download control software and text fields download Text Download download of control software text fields UDS menu Display 1 Next display Upload DownLoad Internal parameters Down 0a0 rom Upload to PC PC ALAN Internal parameters Download from PC ALAN download from ALAN network Upload to PC data transfer to a PC UDS menu Display 2 Table26 UDS menu display 9 9 5 Entering optical detection values the Detect menu The optical detection values can be entered on the following display Refer to the list of parameters supplied with the device Optical detection parameters 3 nos melo us eel Figure 45 Detect menu display DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 75 DL FPP 5G amp FPP 5Gs 10 Access levels and password the Access menu FPP 5G S N 212 FPP 5G S N 212 FPP 5G S N 212 Software V 2 4 2 4 C ISL 1999 lt
97. rom top to bottom and from left to right e The name of the analyzer e The serial number of the analyzer e The version of the control software and dialog boxes The menus of the main level are FPP Run Start amp FPP Run Display Results Print Program Service Quality Setup Access and Clean These menus will be dealt with in detail in the paragraphs following It should be noted however that the FPP Run Start and Display menu was covered almost in its entirety in Part 1 In the following we shall assume that the access level is level 1 Labo level This level allows access to the settings associated with tests making it possible to modify them and thus design personalized programs that respond to specific needs The access levels will be dealt with through the Setup menu Page 2 38 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 3 Displaying results The Results menu FPP Run FPP 5G S N 212 FPP 5G S N 212 FPP 5G S N 212 Software V 2 4 2 4 _ ISL 1999 H gt Software v 2 4 2 4 ISL 1999 Software V 2 4 2 4 ISL 1999 start Display results U ETES clean _ Res 2 28 CFPP 18 C at filling up Res 2 28 CFPP 18 C at filling up y Time Durat Up Doun Temp H t H Samp Diesel No 001 t0 gt t t 1 lt gt t 9 G CO G Prog 1CFPP C 12 05 1999 09 40 42 30 4 30 60 14 2 50 Test 15 15 at 18 0 C Diagram 3 The
98. s displaying screen Print To print the complete alarms review Details To display the detailed alarm message Display 1 of the Review menu Press the Details key to access to the detail displaying screen of the alarm selected Next Display Date date at which the failure occurs Src state of the analyzer when the alarm occurs Status Idle aes i Running Jacket Def Def alarm message displayed preparation Cleaning Diagnostic Details display the Review menu Exit to go back to the alarm displaying screen Table 17 Screens of Review menu of the alarms displaying screen Page 2 64 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the FPP 5G 5Gs 9 Configuration the Setup menu FPP 5G S N 212 FPP 5G Fe 212 FPP 5G S N 212 Software V 2 4 2 4 ISL 1999 Software V 2 Fe 2 4 ISL 1999 lt gt Software v 2 4 2 4 ISL 1999 ZET Start Displa Kal Print Program Service CES O setup FPP 5G S N 212 FPP 5G S N 212 FPP 5G S N 212 gt Analyser setup Analyser setup Analyser setup Labo Diagram 8 Setup menu The FPP G5j s working environment can be completely configured Thus the testing and cleaning programs in place when the device is switched on can be re set The triggering or stopping of an alarm can also be set for when a given error occurs and in other conditions set out below The configuration of the FPP 5G s is carried out b
99. siderably reduces the weight fragility and complexity of the device ISL has taken great care with the design and manufacture of this device and hopes it will give you every satisfaction FPP 5G amp 5Gs User Manual DOCV211A001 D Page 14 General 3 Care in use 3 1 Meaning of symbols Ce Note Important comment ATTENTION Call for particular care Raa Referral Referral to a particular document Standards or to another manual 3 2 Care in the use of testing and cleaning equipment It is supposed that operators are familiar with the handling of hydrocarbon products and that they are thus aware of the dangers and risks that attach to them 3 3 Precautions to take when using built in cooling analyzers Built in cooling analyzers comprise a cooling compressor that necessitates several special precautions to be respected for the long life of the analyzer and its optimum performance eAvoid using the analyzer on a vibrating surface Surface vibrations can enter into resonance with those of the compressor and cause damage to the analyzer eThe optimal operating temperature for the analyzer is around 20 C To avoid harmful overheating of the unit 1 Keep the rear of the unit clear to allow heat to escape easily 2 Keep the ventilation holes in the side of the unit clear They must be regularly blown clear of dust to avoid Clogging and possible blocking DOCV211A001 D FPP 5G amp 5Gs User Manual Page 15
100. ss authorization With this menu all the regulation data linked to the following functions can be collected and sent to a printer see Appendix A section 6 80 column test printout page A 84 or another peripheral PC e Jacket probe e Vacuum pump e Optical detectors 4 5 Printout test The Check button see Figure 27 page 2 41 allows a test to be printed out to check the printer lt gt FPP 5G s link see Appendix A section 6 80 column test printout page Appendix A 84 Moreover this makes it possible to check the printing quality of certain special characters e g the degree symbol which may not be printing properly because of incorrect adjustment DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 43 FPP 5G amp FPP 5Gs 4 6 Printer configuration Page 2 44 The printer is configured by means of the Setup button see Figure 27 on page 2 41 Configuration can also be carried out by means of the Printer menu of the Setup menu The following displays can be called up by activating the Setup button on the Print menu Display Meaning of different menus Field values Print Setup menu Going from left to right and from top to bottom Printer setting Printer setup Automatic result printing Automatic printing Yes No of results at end of test if a printer is connected YES to the device Automatic Chec Check Printer test printout fs ele Setup menu display 1 Next display
101. st precision by elimination of operator subjectivity and human errors while increasing productivity and reduce operator time with highest level of safety A worldwide distribution network supports our customers with quick efficient service and our highly knowledgeable service staff buttresses this relationship providing solutions to product or application challenges Please visit our web site for more information http Awww isl france com DOCV211A001 D FPP 5G amp 5Gs User Manual Page 13 FPP 5G amp FPP 5Gs 1 2 Typographical conventions Convention Meaning Bold Important words or phrases Bold Italics Menus or buttons on the LCD Bold SMALL CAPITALS Keys on the front panel of the device 1 3 About this manual This manual is made up of two main parts entitled 1 Part 1 Using the FPP 5G with the pre installed program 2 Part 2 Advanced use of the FPP 5G The first part allows the operator to carry out an initial plugging test with the FPP 5G in a few stages confidently and with no particular prior knowledge The second part on the other hand makes it possible to use the FPP 5G s potential to the full It is therefore intended for the knowledgeable user who is familiar with low temperature plugging tests In any case the sensitive parts of the FPP 5G control software those linked to the test parameters can be read amp write protected by a system of passwords chosen by the user There are two FPP models
102. t temperature measured by the analyzer Sample sample temperature measured by the sample temperature probe Set point jacket set point temperature Waiting near the set point temperature 0 25 C or 0 45 F a countdown is activated before the temperature is stable 15 mn after the set point temperature is reached the analyzer displays the jacket temperature and the temperature read by the sample temperature probe These ones must be similar Perform a jacket temperature calibration if necessary see section Part 01 1 of this part page 2 60 Jacket temperature checking wait for the jacket reheating Before draining it Jacket 15 C Jacket Temperature checking Display 4 Table 16 Jacket temperature checking menu displays FPP 5G amp 5Gs User Manual Next screen Jacket temperature checking permanent field At the end of the checking procedure the FPP 5G s reheats the jacket up to 25 C to allow to drain the jacket OK validate the procedure and retum to the Quality menu DOCV211A001 D Advanced use of the FPP 5G 5Gs 8 Alarm treatment 8 1 Types of alarm 8 1 1 Failure alarms The failure alarms wam the operator in the event of a malfunction Failure alarm detection has at least one of the following consequences e A test cannot be started e A test in progress is stopped These failures set off a continuous audio alarm and the red LED of the ALARM STOP key lights up on the keypad see the section 6
103. tarting the text entry screen enjoys a semi automatic input feature the latest text inputs are stored in memory so that the operator only needs to enter the first two or three characters for the whole to be displayed If the function Auto Edition is activated the Analyzer proposes a suite when characters are entered according to prior enters This function is intended for accelerate test initiating and it can be configured or deactivated refer to the Part 2 section 9 1 page 2 66 2 5 Preparing the Jacket Page 1 30 As indicated previously in the FPP 5G the jacket is of a piece with the cooling bath Preparation of the jacket consists of lowering the temperature to the first step of the cooling profile adopted e g fora standard CFPP test ref standard NF EN 116 this step is at the temperature of 34 0 5 C The jacket can also be re heated if necessary up to a maximum of 50 C Procedure 1 From the display 1 of the FPP Run Start menu see Figure 10 page 1 28 activate the Jacket Prepar menu The following display then appears Status idle mode Jacket setup 25 0 c Tmp 25 0 C 34 0 C Next setpoint Step Value Figure 14 Jacket Prepar menu display 2 The control program searches in the cooling profile of the program previously selected see section 2 3 page 1 28 for the first step jacket setting and displays it If the setpoint displayed meets the requirement of the tests press the APPLY key
104. tays on for as long as the default persists even if the alarm has been acknowledged Review to display the alarm historical 8 3 Alarm processing Certain alarm cases present a danger This is why most default settings switch the Analyzer into idle status thus the cooling unit is cut out and the heating is stopped However this is not to say that this type of analyzer is hazard free or that if the Analyzer fails to go into idle status the operator and or Analyzer are not in danger It is important always to check what is going on whenever an alarm is triggered A For example owing to a faulty component an alarm that normally should place the analyzer in idle mode fails to do so In that case the operator must intervene by switching off the Analyzer Attention Generally when the alarm buzzer is triggered the operator must display the cause and ensure that everything is working correctly DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 63 amp DL FPP 5G amp FPP 5Gs 8 4 Alarms historical The FPP 5G s can register up to 16 alarm messages Activate the Review menu from the alarm displaying screen see Figure 40 page 2 63 the following screens appear Displays Meaning of different menus Field values Review menu of the Alarm displaying screen Going from left to right and from top to bottom Faults review permanent field Faults review ace Time Message registered Exit To go back to the alarm
105. the Vacuum Profile menu has been activated the following display appears Vacuum profile No 1 Name CFPP ae MS Figure 34 Vacuum Profile menu Display 1 CFPP Unit mmH20 Details This display allows one of the two pre installed vacuum profiles to be chosen by activation of the Next button and validation with OK the necessary authorization having been received The following displays show the parameters for each stage of the profiles 1 Vacuum profile for the standardized CFPP test 2 Vacuum profile for the Simul C test Vacuum profile N 1 Displays Vacuum Profile menu Vacuum profile No 1 CFPP Meaning of different menus Field values Going from left to right and from top to bottom Vacuum profile N 1 CFPP perm field Name profile name Charac Unit unit of vacuum measurement mmH20 CFPP mmH20 ies a name Unit Vacuum Profile menu Display 1 Next display Segment 1 Vacuum profile No 1 CFPP Constant Vacuum 150250 Segment 1 Set pt setting of vacuum value mmH O 15 25 Constant 200 mmH20 a rset pt 15 0250 Vacuum Profile menu Display 2 mbar End of profile Table 6 Vacuum profile displays N 1 Page 2 50 FPP 5G amp 5Gs User Manual DOCV211A001 D Vacuum profile N 2 Displays Vacuum Profile menu Meaning of different menus Going from left to right and from top to bottom Vacuum profile N 2 Simul perm field Vacuum profile No 2 Simul K
106. the printer parameters e The Stop button to stop printing in progress DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 41 DL FPP 5G amp FPP 5Gs 4 1 Printing out results The FPP 5G s can print in different ways with or without details with or without program and as required the results of the last test of any test or of all the previous tests see Examples of printout types page Appendix A 79 Results can be printed out at two levels 1 From the Results menu by activating the Print menu At this level the desired result can be printed out by selecting it by means of the Next or Prev buttons 2 From the Print menu see Figure 23 on page 2 38 When the Results menu is activated the following display appears Results Printing Figure 28 Results menu Display 1 Print menu From this display the following can be printed out e Any result Activating the One res button calls up the display in Figure 24 on page 2 39 At this level the printout mode is that described in 1 of this paragraph It should be noted that a printout of a result can be set Thus in the printout result it is possible to include the test program used and or details of the suctions See 4 6 Printer configuration on page 2 44 e All the results in the memory In this latter case neither the programs used for the tests nor details of the suctions are printed out 4 2 Printing test and cleaning program parameters With the FPP 5G it is
107. tly on to the display below without prior adjustment Modify calibration values LS ENG BEGGS REC Figure 44 Calib menu display 9 9 3 Modifying sample temperature adjustment values High and low reference resistance values are related to the adjustment of the sample temperature They are calculated by automatic adjustment and do not normally need modifying If these values are modified manually this is indicated by an asterisk on the display and on the results print out 9 9 4 File upload download commands the UDS menu The basic analyzer is delivered with a PC program for downloading intemal parameters of a PC to the analyzer and for receiving intemal parameters of the non volatile back up memory Downloading Reception is made via the analyzer s standard RS 232C interface It is also possible to update analyzer program code and software texts using an update diskette An external connection cable is standard equipment for data flow between PC and analyzer During downloading modem signal management is not assured Downloading via the modem is made in two stages 1 Distant downloading PC PC via a modem 2 Local downloading PC analyzer without a modem Downloading Reception is a function special to this analyzer The analyzer is in this mode either eby automatic detection of a download request or eby an explicit request made via the analyzer s keyboard In the first case once the analyzer is in this mode it can o
108. u displays This requires authorization at Access 1 level The Cooling Profile and Vacuum Profile menus give access in their turn to another display level that allows the cooling and vacuum profiles to be seen or set Each pre installed program has its own vacuum and cooling profiles which can be set as desired A cooling profile can be displayed following the procedure below parameter setting change of values is subject to the necessary access authorization for level 1 DOCV211A001 D FPP 5G amp 5Gs User Manual Page 247 amp DL FPP 5G amp FPP 5Gs 5 1 Cooling profile the Cooling profile menu A cooling profile is made up of several stages Each stage is defined by the following elements e A type not modifiable on the device e ASet point e A condition for passage to the next stage Only the stages that have already been programmed may be modified To personalize the profiles it is necessary to go the PC software After the Cooling Profile menu has been activated the following display appears Cooling profile No 1 Name CFPP Unit C LS BROSSE Sa Figure 33 Cooling profile menu Display 1 With this display a cooling profile can be chosen from among the five pre installed by activating the Next button as often as necessary and validating with OK having received the necessary authorization On the following displays the parameters for each profile stage can be seen Taking as examples two profiles 1 Coolin
109. uage Auto Edition characters number neededto 99 activate the auto edition 0 inhibits the function Table 18 Power on parameters menu displays 9 2 Configuring results display the Display menu Up and Down times and temp H can be displayed printed in seconds or in tenths of seconds Example Format 99 seconds gt time in seconds 99 9 seconds gt time in tenths of a second A tenths of a second display is only possible with results obtained with version 1 5 of the control software and displayed in the Results Menu If the time is greater than 99 9 seconds the display automatically switches to seconds A test which is running will always be displayed in seconds 9 3 Configuring alarms the Alarm menu With this menu an audible alarm can be activated or de activated for a given fault or indication Activation of this menu Calls up the following display Alarms set up ET 20 en Modulation Figure 42 Alarms menu Display 1 With this menu the alarm can be activated or de activated as a waming system without however preventing the LED of the ALARM STOP lighting up Reminder pressing on this button reveals the error message content The intermittence of discontinuous alarms can be adjusted by means of the Modulation button 100 continuous alarm 0 alarm mute Warnings alarms and their corresponding messages are presented as follows Page 2 66 FPP 5G amp 5Gs User Manual DOCV211A001 D Advanced use of the
110. uage has been locked FE gt This screen is not placed hierarchically after the Welcome display The arrow on the left bottom of the display the PREVIOUS LEVEL key refer to the section 6 1 1 page 20 allows backing up on the main screens level refer to the Diagram 2 page 2 37 These measures have been taken to accelerate access to test related menus Display 1 of the FPP Run Start menu contains the following information e Sample identifying name of the sample e No sample number e Prog the program being used and the unit used for temperature measurement e Op name of the operator e The following menus and buttons gt Jacket Prepar jacket preparation menu gt Sample Sample ID entry button gt No Sample number entry button gt Start now Start test button Display 2 of the FPP Run Start menu accessible via the next display button has in its upper part the same fields as the previous screen and these buttons in its lower part gt Cloud Button for cloud point entry gt Prog Program selection menu gt Oper Operator name entry button gt Start now Start test menu ID ch Prog 1 CFPP C mC Start T macs me anses DS Figure 11 Screen 2 of FPP Run start menu Page 1 28 FPP 5G amp 5Gs User Manual DOCV211A001 D Use of the FPP 5G s with pre installed programs With the Cloud button in display 2 of the FPP Run Start menu the sample cloud point temperature can be entered directly by
111. ual DOCV211A001 D DOCV211A001 D Cooling Profile No 1 Step 2 Temp Interval 1 0 C Yes A Cooling Profile menu Display 5 No 1 Advanced use of the FPP 5G 5Gs Step 2 Tests suction or not during the first jacket cooling stage Frequency setting of interval between two suctions Intervals are expressed either in minutes or in degrees C F 1 Interval in minutes 2 Interval in C F Yes No If Tests Yes Min 2 min Max 60 min Min 1 C 2 F Max 5 C 10 F The above display is followed by four displays which correspond to the two jacket cooling stages described in standard NF EN 116 Cooling Profile No 1 Step 5 Final Jacket temperature Heating 25 0 C O tests Mm Setpoint Cooling Profile menu Display 10 No 5 Cooling Profile No 1 Step 6 End of profile Cooling Profile menu Display 11 No 1 Table4 Cooling profile N 1 Cooling profile N 2 Displays Cooling Profile menu No 2 Cooling Profile No 2 Simul Ke 3 tr fra Cooling Profile menu Display 1 No 2 Cooling Profile No 2 Step 1 Jacket Cooling Until sample rate at 40 0 C h lt 70 0 C Cooling Profile menu Display 2 No 2 Cooling Profile No 2 Step 1 Temp Interval 0 C eee Cooling Profile menu Display 5 No 2 Step 5 Type 1 Final jacket re heating 2 Preparation of jacket for next test Set point Jacket temperature s
112. ue read on manometer adjustment of vacuum as read on reference 200 H20 D A 2E0 manometer EA EE Vacuum Calib menu Display 6 Table 15 Vacuum Calib menu displays FPP 5G amp 5Gs User Manual Page 2 61 DOCV211A001 D FPP 5G amp FPP 5Gs 7 5 Jacket temperature checking procedure Page 2 62 To access to the jacket temperature checking procedure press the Jack T check button of the Quality menu see second screen Diagram 7 page 2 57 Proc dure Displays Jacket temperature checking menu Jacket temperature checking Fill the jacket up to the mark and Immerse the reference probe Jacket Temperature checking Display 1 Jacket temperature checking Jacket Set Point Jacket Temperature checking Display 2 J Jacket temperature checking Jacket 22 2 C Sample 21 9 C Set point 34 C Waiting min Jacket Temperature checking Display 3 Meaning of different menus Going from left to right and from top to bottom Jacket temperature checking permanent field Continue fill the jacket with methanol position the probe inside then press the Continue key to go on Next screen Jacket temperature checking permanent field Jacket Set point enter a set point temperature for the jacket Press the Enter key on the keyboard to validate Start Start the jacket temperature checking procedure Next screen Jacket temperature checking permanent field Jacket jacke
113. ur tests pre installed in the device memory at the factory The equipment necessary for a CFPP test in direct contact with the sample is strictly compliant with the current standard The FPP 5G s consists of 1 A cylindrical flat bottomed transparent glass Testing tube with a permanent mark corresponding to a volume of 45 ml designed to contain the sample 2 A flat bottomed brass cylinder forming a sealed air bath called in compliance with the standard a Jacket designed to contain the Testing tube so as to heat and cool it In the case of the FPP 5G s the Jacket is of a piece with the Cooling bath To maintain this bath at the desired temperature the FPP 5G must be linked to a coolingunit in order to keep to the requirements of the current standard 3 So as to insulate the Tube from the Jacket since the temperature change must occur across the air bath and not by contact there is a one piece assembly consisting from bottom to top of an Insulating ring and two Ring wedges The insulating assembly is made of an oil resistant plastic material the different parts are held together by stainless steel rods 4 A Stopper adapted to the testing tube by means of clips ISL improvement It is made of an oil resistant plastic material see Figure 7 on page 1 26 5 Apipette and filtration assembly strictly compliant with the current standard see Figure 9 on page 1 27 6 A standardized and calibrated Temperature probe N
114. y means of the Setup menu at the main display level see Figure 23 on page 2 38 After the Setup menu is activated the following display appears FPP 5G S N 212 Analyser setup Pwr on DAGEN Alarms HETH FPP 5G S N 212 Analyser setup Printer RS lt 32 GDS Clock FPP 5G Analyser setup service iSt _ Figure 41 Setup menu displays The above displays allows access to the configuration parameters set out below DOCV211A001 D FPP 5G amp 5Gs User Manual Page 2 65 amp DL FPP 5G amp FPP 5Gs 9 1 Power on parameters the Pwr on menu The Power on parameters menu allows choice of the test program the cleaning program and the access level in place when the device is switched on Displays Meaning of different menus Field values Power on parameters menu Going from left to right and from top to bottom Power on parameters Power on parameters Program Test program choice 135 Cleaning Cleaning program choice 132 1 CFPP C PD OED EEE Display 1 of the Pwr on menu Next display Access level choice of default access level 0 1 or 2 Power on parameters when the device is switched on 7 It should be noted that only the current 0 Selection access level or lower access level can be past ten aa level Edition Country language choice of language Selection English Display 2 of the Pwr on menu selected by default locked Selection allows Fran ais the operator to choose the lang
115. zed and so bear the name of the laboratory that acquires it together with the name of the head of the laboratory He or she can restrict access to write protect certain parameters e g the parameters associated with a standard The following displays can be called up by activating the Labo menu Displays Meaning of different menus Field values Labo menu Going from left to right and from top to bottom Access Code access code to level 1 32768 gt Laboratory setup 32767 Lab Name name of laboratory using FPP 5G s String ISB Access Code E Lab name Labo menu Display 1 Next display Manager name of laboratory manager String Laboratory setup Title title of laboratory manager String Manager title Labo menu Display 2 Table 21 Labo menu displays 9 6 Printer configuration the Printer menu Printing configuration has been dealt with the section 4 Printing out the Print menu on page 2 41 of the current part 9 7 FPP 5G s PC communication the PC Link and RS232 menus The FPP 5G s is an open device in more than one respect Not only can it be completely parameterized it can communicate with a PC through e the ALAN network whose inlet and outlet ports are at the back of the device e the RS 232 C link e the service port on the rear panel Each of these communication modes is specialized Thus e The ALAN allows if necessary several FPP 5G s analyzers to be interconnect

FPP 5G & FPP 5Gs User manual

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FPP 5G &amp; FPP 5Gs User manual

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FPP 5G & FPP 5Gs User manual