Manual - Boeco
Contents
1. 4 Rotation blocking knob which is placed on the rotary casing head set to the Lock position marking by red point for easier locking try to turn the casing a little Insert suck pipe in to the rotary casing until the sitting touches the plastic collar Than tighten the nut on the rotating casing Finally Unlock the blocking knob marking by green point 5 The opposite side of the head with the rotary casing contains a fixed housing with a nut Unscrew the nut fig 3 pos 2 put it on the fitted part of the ball adapter fig 3 pos 1 insert the bead type securing ring fig 3 pos 3 in such a way that it can latch behind the fitted part of the ball adapter Check that the gufero sealing treated with silicone Vaseline has been inserted inside the fitted part fig 3 pos 4 its open side should face out of the fitting Check that the flat sealing fig 3 pos 5 has been inserted in the casing and put carefully the ball adapter with gufero and nut on the suck pipe fig 3 pos 6 push the ball adapter until it stops and tighten the nut properly fig 3 pos 2 The spherical joint of the ball adapter faces down 6 Do not forget to apply silicone Vaseline to all glass parts joints 7 Install the condenser into the joint in the upper part of the ball adapter The upper outlet of the condenser serves for the connection of the vacuum source Connect the outlet of the condenser to the socket for the measurement of vacuum marke2. LA BOECO Germany ROTARY VACUUM EVAPORATOR RVO 400 SD User manual Boeckel Co GmbH Co Kg Roedingsmarkt 33 20459 Hamburg Germany Phone 49 40 325627 0 Fax 49 40 425627 41 E mail info boeco com Web http www boeco com BOECKEL CO GMBH CO KG Page 1 1 INTRODUCTION Innovated Rotary vacuum evaporator BOECO RVO 400 SD is new advanced model with system designed for the control and communication by PC with the possibility to data entry of pre set values and date processing while evaporating Is noted for affability value in use and compact construction Innovated design offer users comfort and safety using the remote control and safety bath cover Optional is possible to equip RVO 400 SD with the regulation in accordance by steam temperature 1 1 Apparatus use and specifications Rotary vacuum evaporator RVO 400 SD is designed for low pressure evaporation at the pre set value of the heating bath temperature and at the pre defined constant mixing process ofthe solution to be vaporised The vapours exhausted condense in a vertical or diagonal cooler and are collected into a flask The apparatus is fitted with a digital vacuum control and measuring system Vacuum ratio is driven by diaphragm vacuum pump control User comfort assure heating bath eguipped with motorized lift and manually tilted rotary casing head Rotation of the evaporating flask height of the heating bath steam temperature the
3. Vapor temperature sensor Remote control BOECKEL CO GMBH CO KG Page 19 ASKLO005 4SKLO020 GL14 3x 4SKL0026 Sn me 4SKL0002 3x 4SKL0027 4SKLOOOI VR 4SKL0021 50m 4SKL0025 1001 NZ45 40 ASKLO022 250 NZ14 23 mead 55 NZ14 23 4SKL0023 500mi 3xGL14 RO 3212 y RO I gt FA 989 NZ29 32 35 20 4SKL0004 1000m 535 20 250ml 4SKL0024 500ml ASKLO006 1000mi RO 4810 4SKL0034 2000ml NZ45 40 NZ14 23 ASKL0003 2000mi ASKLOO 2 4000mI Pr ASKLOOIS 3xNZ14 23 4SKLO010 250mi NZ14 23 535 20 SKLOOI8 XNZ14 23 EA ASKLOOII KND 100ml i xNZ14 23 TD 6 20ml aa RO 1041 ASKL0035 NZ14 23 ASKLOOTA LE Re 4 23 ASKLOOIS R 32 BOECKEL CO GMBH CO KG Page 20 Fig 8 Glass accessories overview 8 CONCLUSION 8 1 Carrying out of repairs All warranty and after warranty repairs shall be carried out by the manufacturer or by the organization authorized by them If the delivery note does not state otherwise contact the distributor for any repair requirements 8 2 Warranty The product is covered by the manufacturer s warranty lasting for one year from the day of the handing over to the customer of the product The apparatus can only be used in the way specified in these instructions The apparatus cannot be used in any other way than as provided for in these instructions otherwise the operation safety could be interf
4. vacuum ratio and length of evaporation can be digitally set and controlled using the Keyboard or PC All controlled values can be stored in memories Standard glass assembly can be adapt or enlarged on reguest 1 2 Technical characteristics Evaporating flasks iimenmenmeeneennenneni 20 4000 ml Rotation speed mrnreenentenenennenennenet 0 10 up to 280 rpm Bath temperature emnennenmeeneennenneni max 100 C for water filling max 180 C for oil filling Regulation accuracy meittmereneene 1 C up to 100 C 3 C up to 180 C Pressure measurement nenreeneeee absolute Pressure difference ereemeemennenneennennenna adjustable 1 500 mbar Power SUPPLY Linden diett 230V 10 50Hz Pow t Input ss an dhat kka a max 2000 W excluding vacuum pump Weight without glass oeer 20 kg Dimensions wx hx d mme 650 x 900 x 360 mm including glass 1 3 Symbol Explanation hot surface BOECKEL CO GMBH CO KG Page2 2 TECHNICAL DESCRIPTION Individual parts of the evaporator and their location can be seen on fig 1 G gt E 2 C2 CO CG 1 Stand 9 Filling pipe with valve 2 Rotary casing head 10 Fixed clip 3 Heating bath 11 Head tilt stick 4 Suck pipe 12 Lift top position stopper screw 5 Ball adapter 13 Keyboard see Fig 6 6 Condenser 7 Receiving flask 1000 ball
5. 3 3 2 Temperature setting In case the regulation is set according to the solution temperature Tac in the MENU position Heat pressing the HEATING button once displays the solution temperature setting by the arrows pressing it once more the solution heating is started Pressing the button still once more switches the heating off Pressing then the DISPLAY or ESC buttons returns the device into the initial display mode Press HEATING once more and temperature setting displays again and another pressing the button switches the heating off Correct function is indicated by top right corner of the button lighting in case of a failure the light starts flashing If the vapor sensor is installed and in the MENU mode in Heat the regulation is set according to Tvap and the display is in the temperature setting mode then the Tvap vapor temperature setting optional changes and the cooler temperature Tsol optional is only indicated If any of the sensors is not installed for the corresponding temperature NO is displayed Note the solution temperature Tac must be set accordingly higher than the reguired vapor temperature Tvap 3 3 3 Vacuum setting Pressing the VACUUM button once displays the vacuum value setting arrows pressing it twice starts vacuum control if the vacuum pump is installed see fig 5 Pressing it once more switches the vacuum control off Pressing then the DISPLAY or ESC buttons returns the device into the initial display mode
6. 82 Warranty ussssarasssmamimiadavudrkresmeasin E E E E E 22 8 3 Waste disposal eriseeria EE Sun D EEE Ge ea DEEE TE SEAE 22 9 TABLE OF CONTENTS Ea ER aR E a A 23 BOECKEL CO GMBH CO KG Page 22 Ole Listof pictures nd tables ars eres ser bede aa da katedraal kuts 9 1 List of pictures and tables Fig 1 Location of individual parts ofRVO mmseerernnernrrrrneenernevnsnernersesenssnernervevrensrnrsrenssnesnesvessensensee 5 FIS CONNSCtOrS aese aaret 6 Fig 3 Ball adapter sealing section view a D snnrnnnrnnrrnrrnnvnnnvnrnennrenrenreneenesresvenrenesnenssnesvesvesvenssnesne 7 Fig 4 Tube connection scheme Launsuetung ean niin eh natu aate Sa tause 9 Fig 5 Connection plan for vacuum control verreeenneeneeeneee ene enne ne eee een nants 10 Fig 6 Keyboard yria uenoi i noe ees ise iach ela edie woe eae ee eee wae 11 Fig 7 Remote Kontrol oriras aca evieees idan cscs made dawns koa dt al yes lei ele i s es 14 Fig 8 Monitor PO sur srussstesters bades vevd bea eee ed eee aN va Se nde eae uned eee da v ja ek chia 15 Fig 8 Glass accessories Overview sagnene ennen elser 21 BOECKEL CO GMBH CO KG Page23
7. KS 35 20 8 Round bottom flask 1000 and 2000 ml NS 29 32 Fig 1 Location of individual parts of RVO For complete list of basic accessories see paragraph 7 2 1 BOECKEL CO GMBH CO KG Page3 3 STARTING OF OPERATION 3 1 Unpacking of the apparatus Unpack the apparatus from the transport package check the evaporator s surface and check all items according to the delivery note If the apparatus is damaged or if an item is missing contact your supplier or the manufacturer Caution apply silicone Vaseline to the all joints of the glass assembly 3 2 Apparatus assembly 1 Keyboard can be hanged on the left fourpod leg of the stand apparatus or can be laid beside it Plug connection cable in to the keyboard and to the socket at the back of apparatus marked KEYBOARD fig 2 2 Place the heating bath on the lift table fig 1 insert the bath cable into the socket under the mains switch fig 2 pos 10 and plug the connector of the bath temperature sensor into the socket fig 2 pos 3 marked TAC THERMOMETER 3 Pour approximately I I of liquid into the heating bath Keyboard connector PC connector Vapour temperature sensor connector Vacuum sensor connectlon Bath temperature sensor connector Fuse TO 5A Main fuse TIOA Vacuum pump fuse T3 15A Main swith Vacuum pump socket Mains connection Bath connection Fig 2 Connectors BOECKEL CO GMBH CO KG Page4
8. control the lift movement and setting the values of the display The upward movement of the solution is limited by an adjustable limit switch placed on the right side of the device stand see fig I pos 12 It is operated by means of a black knob The downward movement of the solution is limited by a fixed limit switch CAUTION During upward movements of the warming solution make sure that the solution does not overflow or that the glass parts do not get damaged t o 1 E E D rr VACUUM HEATING DISPLAY MEN lt Fig 6 Keyboard 3 3 1 RPM setup Pressing the ROTATION button once displays RPM setting on the display by arrows and pressing it twice starts the rotation Pressing it once more the rotation stops Pressing then the DISPLAY or ESC buttons returns the device into the initial display mode Another pressing the ROTATION button displays again the RPM setup and one more pressing it stops the rotation Correct operation is indicated by top right corner of the button lighting Always make sure that the button of rotation blocking is in the position UNLOCKED If you start rotation with the blocking button in the LOCKED position the case with the tube does not start rotating just starts rotation lighting will flash The apparatus enables you to set both directions of the rotation The opposite direction of the rotation is indicated with the minus sign BOECKEL CO GMBH CO KG Page 10
9. the device switches off setting the heating regulation mode according Tac solution temperature or Tvap vapor temperature reading 4 device setups the memory content is copied into the actual setup storing 4 device setups writing the actual setup into the memory These parameters are stored Pac Tac Tvap Tac Tvap regulation type RPM timer Delta P AtmosfP Setting setting the pressure hysteretic for regulation within I to 500 mBar setting the difference between switching the vacuum pump of and off ifthe absolute sensor is installed optional it shows the absolute pressure it may not be edited if absolute sensor is not installed the ambient pressure may be set manually according to a calibrated barometer If 0 is set the display shows the absolute value of the relative pressure Setting parameters for the display module units lighting contrast beep and return to factory setup The values are stored directly in the display module and are valid for the specific module ENTER selection confirmation ESC return After the device is switched on or when switching memory rotation and heating the warming solution is switched off for safety reasons We recommend controlling the RPM value set before you start the rotation BOECKEL CO GMBH CO KG Page 12 3 3 7 Remote control optional LIFT HEATING ROTATION VACUUM AS A RVO 400 Fig 7 Remote control The LI
10. the instrument using PC The changed parameters by PC will be rewritten also by display of keyboard and reversaly PC requirements Windows office seri l port or USB converter seri l port 3 3 9 Vacuum evaporating report by PC accessories by request Select under PC program mode of evaporating run select name and enter After push button operation START the program is runing For the each one data jogging you can create new datab ze or select primary and the data are storaged as continuation storaged data before The rekord consist of instrument setting and recording at selected scaning intervals Getting of storrings Flask rotation Bath temperature Heating temperat Vapour tempera Temperatureof coolers vapour Vacuum Vacuum settingiii Bath and vzpour temperature setting Pressure diference setting between ON and OFF of vacuum pump Parameters r Yacu Create Time like database interval of scaning FIRYO 400 3 01 Lift operating memories1 4 o n min Stop p Vacuum Timer Start 0 mbar Write 00 00 00 ca m Heating Start Tac 0 OC C Tvap o C 2 lei x Error Database j Record reporting and Scan 60 sec Bank fil Load deletion r E write enable Save Rotatid r Eldvator Alarm 289 E neers nomen maniar Start vi F Rotat
11. FT button activates the arrows for lift movement after a longer standby time it is necessary to activate them again The ROTATION button displays RPM setting by arrows upon the 1 pressing upon the 2 it starts rotation If pressed once more the rotation stops Correct operation is indicated by top right corner of the ROTATION button lighting located on the keyboard with the display The HEATING button displays a keyboard for temperatures Tac and Tvap setting on the monitor by arrows according to the regulation time set in MENU upon the 1 pressing The 2 pressing switches on the heating If pressed once more the heating is switched off Correct operation is indicated by top right corner of the HEATING button lighting located on the keyboard with the display The VACUUM button displays vacuum value setting by arrows upon the 1 pressing upon the 2 it starts vacuum control if the vacuum pump is installed see fig 5 If pressed once more the vacuum control is switched off Correct operation is indicated by top right corner of the VACUUM button lighting located on the keyboard with the display The Display after some 10 idle seconds switches to the initial readings BOECKEL CO GMBH CO KG Page 13 3 3 8 Operating by PC accessories by request Install the program from CD to PC first Interconnect PC and RVO 400 SD by the delivered link cabel seri l port Start program and now you can kontrol
12. Pressing the VACUUM button again the display will show vacuum value setting again and another pressing the button shall switch the vacuum control off Correct operation is indicated by top right corner ofthe button lighting 3 3 4 ENTER button function In all modes apart frem MENU pressing the corresponding button switches ROTATION HEATING VACUUM on off After recalling memory LOAD 1 4 functions of ROTATION HEATING VACUUM and TIME switch on off ENTER in the MENU meode is the selection confirmation 3 3 5 DISPLAY button function Pressing the button cyclically changes the display mode and the arrows are active as lift movement controls 1 Tac Pac 2 Tvap Tsol if installed 3 Timer Pressing the DISPLAY button also overrides other display readings Rotation Vacuum Heating BOECKEL CO GMBH CO KG Page11 3 3 6 MENU ESC button function MENU Menu items Timer Heat regulation Load Memo Save Memo Timer Heat Tac Tvap Load memo Load 1 Load 2 Load 3 Load 4 Save memo Save 1 Save 2 Save 3 Save 4 Delta P Atmosf P Setting Pressure units Torr mBar Temperature units C K Beep on off Default yes no setting time countdown Ifthe time 00 00 is set the operation time is not limited When the time set is reached the heating switches off the solution moves down rotation stops and also the vacuum pump is switched off In case of failure or stopping of the rotation or heating
13. cified by the manufacturer This situation will be signaled by the flashing of the LED for heating BOECKEL CO GMBH CO KG Page 16 6 2 Operation conditions The apparatus is designed for the work under ordinary laboratory conditions at temperatures of 10 to 30 C and air humidity up to 80 The power supply is 230 V 10 A 50 Hz The inlet cord should be connected into a socket circuit featuring protection from 10 A or 16 A diaphragm vacuum pump connected The inlet cord cannot be in contact with the heating bath The socket designed for the connection of the heating bath is designed exclusively for this bath Oil used in the bath must be designed for a temperature of at least 180 C The bath volume shall not exceed 2 I It is forbidden to handle any bath which has been heated to a temperature exceeding 40 C in any other way than by using the apparatus lift If you want to fill the liquid into the heating bath always switch the vaporized sample rotation OFF For temperatures up to 100 C use water as the filling of the heating bath with regard to its higher thermal capacity Caution If you are replacing the round bottom flask after the vaporized solution has become thicker pay particular attention and if it is not possible to remove the flask easily from the cone carry out any other handling only after the cooling of the bath Caution If you use oil as the filling of the heating bath the heating bath must be properly dri
14. d VACUUM and to the vacuum source with the help of a T union Other outlets serve for connection of cooling water 8 Attach the receiving flask with ball joint to the ball adapter with the help of a fixed clip tighten properly 9 Put the round bottom flask on the pipe and secure it with a wire combi clip 10 Insert the filing pipe with a valve valve closed into the ball adapter BOECKEL CO GMBH CO KG Page 5 DJ gt w 1 Ball adapter Bo is 2 Nut 6 Housing 3 Bead type securing ring 7 Suck pipe 4 PTFE sealing Fig 3c Ball adapter sealing chemical resistant BOECKEL CO GMBH CO KG Page6 RON gt TKS G ES 4 by KI NO Ball adapter 5 Flat sealing Nut 6 Housing Bead type securing ring 7 Suck pipe Gufero sealing 35 22 10 Fig 3a Sectional assembly view low chemical resistant BOECKEL CO GMBH CO KG Page 1 Cooling water outlet 3 T tube connection 2 Cooling water inlet 4 Vacuum connection Fig 4 Tube connection scheme 11 Connect the main cord fig 2 12 Lift the heating bath using the lift to its working position At the bath top position adjust the lift stopper and fill in the liquid in the heating bath in such a way that the round bottom flask can be sufficiently immersed in the liquid The maximum liquid level is approximately 20 mm below the edge of the heating bath Flask can be immerse and emerg
15. e by tilt the rotary casing head For tilt use stick on the left side of the apparatus When tilt the head move stick carefully pay attention to glass equipment 13 When removing the round bottom flask release the vacuum first e g use the filling pipe valve For easier manipulation use the rotation blocking knob to lock the rotation Carefully unscrew the wire combi clip until the flask is released During the flask removing work with caution 14 When the vacuum control is desired connect the mains cable of vacuum pump into the socket on the back side of the apparatus In this case connection between condenser vacuum outlet and vacuum measurement socket has to be established BOECKEL CO GMBH CO KG Page8 1 Cooling water outlet 4 Controlled vacuum pump plug socket 2 Cooling water inlet 5 T union 3 Vacuum sensor connection 6 Vacuum pump Fig 5 Connection plan for vacuum control Caution It is not possible to use the glass part if it features visible scratches or any other defects W hen controlling the vacuum only the diaphragm vacuum pump with maximum input 650 W can be plugged in the evaporator BOECKEL CO GMBH CO KG Page9 3 3 Apparatus control The device is started up by switching the mains switch on Upon startup the display is lighted temperature Tac and pressure Pac is displayed By repeated pressing the DISPLAY button the initial reading changes to Time Button and w
16. ed before its being filled Caution If you are working with oil heated above 100 C you must ensure that no water can enter into the oil If you are replacing the round bottom flask pay particular attention that no water drops shall enter into the oil While working use personal protection equipment goggles gloves coat and shoes BOECKEL CO GMBH CO KG Page 17 7 ACCESSORIES AND SPARE PARTS 7 1 Basic accessories comes with evaporator Inlet cord Glass assembly Round bottom flask 1000 and 2000 NZ29 32 Receiving flask 1000 o ml KS 35 20 Suck pipe Ball adapter Vertical condenser Filling pipe with a valve 3 pieces of GL14 connection fitting Sealing gufero sealing 35 22 10 Fig 3a pos 4 flat sealing Fig 3 pos 5 or gufero sealing 35 22 7 Fig 3b pos 4 with scraper ring Fixed clip Keyboard Adaptor Keyboard Cables 0 4 and 2m Tubing coupler PA vacuum tubing 100 110 a 150cm Main inlet cord 7 2 Other accessories 7 2 1 Glass accessories Fig 7 4SKL0021 4SKL0025 4SKL0022 4SKL0023 4SKL0004 4SKL0003 4SKL0012 4SKL0017 4SKL0024 4SKL0006 4SKL0034 4SKL0005 4SKL0033 4SKL0020 4SKL0001 4SKL0002 4SKL0008 RO4810 RO3212 Evaporating flask 50 ml joint NZ29 32 Evaporating flask 100 ml joint NZ29 32 Evaporating flask 250 ml joint NZ29 32 Evaporating flask 500 ml joint NZ29 32 Evaporating flask 1000 ml joint NZ29 32 Evaporating flask 2000 ml joint NZ29 32 Evap
17. ered If the conditions of these instructions are not met the manufacturer will not be liable for damages which could arise 8 3 Waste disposal When the instruments operating life is over dispose it in respect to valid regulations also it can be returned to the vendor or producer for liguidation Warning Instrument contains parts PCB s which are rated as hazardous waste BOECKEL CO GMBH CO KG Page21 9 TABLE OF CONTENTS ly INTRODUCTION aner naaede aan an seed AE 3 1 1 Apparatus use and specifications teninreeneeenenneeneennenneeneenneenennenneennennennennet 3 12 Technical chatacteristics en reen agerede bes kult puha ea a ara ng 3 1 3 Symbol Explanation rr ar rage ae heel asic anda ere taa ANE 3 TECHNICAL DESCRIPTION ai beast aksept gester 4 3 STARTING OF OPERATION dreiende eeii ete i E EE sita ita oli 5 3 1 Unpacking of the apparatus sseeerrrrrrrrrrrrrrrrrrnrnrrrrrrnrrrrrrernrrnnernernnrnernnensenernsensesnernsensesnennee 5 3 2 Apparatus assembly seiis oai naia ra aa aeaa a i eaa 5 3 3 Apparat s Control vista e e a a A E Gre tee ghd AREE Aa 11 23L RPMsetup 1443vsvsikat RESENS aea a bcd ies kad k nd E EEG eda ika a 11 3 3 2 Temperature Setting 2 agesseaom orka ankom oktett rn 12 33 30 Vacuum SEIM iil ss 12 3 34 Enter button function eier ease 12 3 3 5 Display button function meererrerrrnrrrrrrnrrrrrrnenrrrrernrrnrrrrernnrnernernnrnernernsessern
18. he ball adapter and carefully remove the actual adapter Release the gufero sealing clean the ball adapter slightly apply silicone Vaseline onto the new sealing and mount it into the ball adapter The sealing cavity faces out of the ball adapter If necessary replace also the flat sealing between the ball adapter and the head fitted with a rotary casing Perform the assembly according to the point 3 2 Apply a light layer of silicone Vaseline to the gufero sealing approximately after 80 operation hours more often if necessary 5 DEFECTS AND TROUBLESHOOTING 5 1 Leakage The main cause of leakage is usually an incorrect sealing assembly At first you should check that all joints have been installed correctly If it is the case disassemble the glass and verify the condition of the ball adapter sealing and flat sealing if necessary replace them Carefully assemble according to the instructions switch the rotation ON and start the vacuum pressure up BOECKEL CO GMBH CO KG Page 15 5 2 Other failures The apparatus does not respond when you switch it ON Check fuses possibly replace with new ones featuring the same parameters fig 2 T 0 5A and T 10A The window of the rotation key is flashing rotating parts are not moving Ensure that Rotation blocking knob is set to Unlock and than press rotation key again The window of the rotation key is flashing Check that there is not anything which could impede the flask from i
19. ion I Temp START STOP setting mbar delta P 0 P atmospher sett 0 P atmgaf Read er actual Setting of run time Static pressure setting in case without absolute sensor Static pressure No Senzore arn t detected other way are displayed current values E After setting required values enter Write Fig 8 Monitor PC Communication port selection Err Communication error OK free and clear Program termination BOECKEL CO GMBH CO KG Page 14 4 MAINTENANCE 4 1 Apparatus maintenance Do not leave the evaporator surface contaminated from corrosive substances It could damage the evaporator coating Clean the contamined surface with a clean soft cloth The cloth may be moistened but not wet It is also possible to use ordinary washing means for cleaning purposes It is forbidden to clean the heating bath with the means which could spoil its smooth surface In case of sediments of turning impurities particulates of water rusts use the cleaning compounds for cleaning of furning or mellow solution of HCL In process of cleaning use the protective means recommended by producer of applied cleaning compounds Caution Disconnect the apparatus from the network while cleaning it with a wet cloth 4 2 Sealing replacement Disassemble the condenser remove the releasing pipe with the valve remove the ball and socket ground joint flask release the nut of t
20. orating flask 4000 ml joint NZ29 32 only RVO400 Receiving flask 250 ml joint KS35 20 Receiving flask 500 ml joint KS35 20 Receiving flask 1000 ml joint KS35 20 Receiving flask 2000 ml joint KS35 20 Vertical condenser Diagonal condenser Dry ice trap Filling pipe with a valve short Filling pipe with a valve long Ball adapter Ball adapter including steam temperature sensor Suck pipe BOECKEL CO GMBH CO KG Page 18 4SKL0016 4SKL0009 4SKL0010 4SKL0019 4SKL0018 4SKL0011 4SKL0014 4SKL0015 4SKL0035 Test tube 20 ml joint NZ14 23 Flask 100 ml joint NZ14 23 Flask 250 ml joint NZ14 23 Spider with 3 sleeves NZ14 23 max flask 250ml Spider with 5 sleeves NZ14 23 max flask 100ml Spider with 6 sleeves NZ14 23 max flask 20ml Foam trap NZ29 32 NZ14 23 Foam trap NZ29 32 NZ29 32 Adapter NZ29 32 NZ14 23 7 2 2 Spare parts other accessories BOE 8090005 1TOO0007 1TG24524 1TOO0009 1TOO0010 ITOOOO1 I RO1080 RO1041 4SKL0026 4SKL0027 90000013 5HAD0003 BOE 8834000 BOE 8090006 3V0D0003 Fuses5x20mm RO4810 Safety bath shield Gufero sealing 35 22 10 Fig 3a Flat sealing Gufero sealing 35 22 7 Fig 3b Scraper ring Sealing PTFE Fig 3c Fixed clip for KS32 20 Elastic clip for NZ14 23 Straight fitting GL 14 Cap nut GL 14 Tubing coupler PA Vacuum tubing BOECO C 410 Chemical resistant vacuum pump CD with programm RVO400 Inlet cord T10A T3 15 A T0 5 A
21. sessesnesnn 12 3 3 6 MENU ESC button function rrerrreeeneenee nee cnet ene nene nene 13 33 7 Remote control aoee rnond Aa e dm aa fersk done eee 14 33 8 Controlling by PC uses agai es wanes kne 15 3 3 9 Recording the vaporization course on PC mrreeenen enne nen neee 15 4 MAINTENANCE sagnene sen erne GAGN 16 4 1 Apparatus maintenance mmrrrrrrererrrrrrrrrernrrnrrnrrnrrererneessrsnernnrnnernersernernnensesnernsssnesnernesnnensenn 16 4 2 Se lmgr pl tement ss aan rarere san A EA E EN EE EES 16 5 DEFECTS AND TROUBLESHOOTING imimiememeneemeneenenenenenenennenennenenannenenneneenenet 16 51 Leakage SS RE 16 5 2 Other Taures ieie tegtek e desduliecteee drekk 17 6 SAFETY AND OPERATION CONDITIONS rorrrrevvrnrenrrrsreneenernenesnessenresrrsrenesnernessensrnesssnesnenne 17 61 OPETALIOMISATELYE sideordnede 17 62 Opera ton conditons AAA ST 18 7 ACCESSORIES AND SPARE PARTS imimimiiteteneetesnenenenenneneneeneneeeenennneneneneanenee 19 7 1 Basic accessories comes with evaporator rnnennnenennenerenene 19 72 Other accessories inienn iea ia stevnene end 19 TZ Gl ss ccess ries nanandasnnen s paid ites keen ovat e ues 19 7 2 2 Spare parts other accessories ecesesceceesceseeseeeceeceeseeseeseceseeaeeeeeeeeseeseeaeeeenseeaeeats 20 8 7 CONCBUSTON pkt 22 Sil Carrying out Of repairs Kader Alert Da 22
22. ts rotation manually switch the mains switch OFF and ON and press the rotation key again The window of the temperature key is flashing This indicates that the temperature sensor have been connected incorrectly Check the sensor connection quantity of liquid in the heating bath and switch the main switch OFF and ON and press the temperature key again Controlled vacuum pump is not running even the pump mains cable is correctly plug in the rear of evaporator as well as vacuum connecting hose Check the vacuum pump fuse possibly replace it with new one featuring the same parameters fig 2 T3 15A 6 SAFETY AND OPERATION CONDITIONS 6 1 Operation safety Ensuring of rotation of the sample to be vaporized Current protection of the driving motor If the resistance against rotation has increased above the prespecified limit the driving motor voltage will be disconnected This situation will be signaled by the flashing of the rotation LED Protection of the heating bath lift Friction coupling between the driving motor and lifting equipment In the case of an increase in resistance during the lifting of the bath above the specified limit the friction coupling could slip Protection of bath heating Electronically by means of a thermal protection Against overheating There will not be any heating if the incorporated sensor of the heating bath has been connected or if the difference of temperatures between sensors rises above the limit pre spe
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