Vial Selection Guide
Contents
1. 477 1227 410 381 1227 Fax 410 381 1222 URL www ssi shimadzu com Webstore URL store shimadzu com Company names product service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation and its affiliates whether or not they are used with trademark symbol TM or Third party trademarks and trade names may be used in this publication to refer to either the entities or their products services Shimadzu disclaims any proprietary interest in trademarks and trade names other than its own For Research Use Only Not for use in diagnostic procedures The contents of this publication are provided to you as is without warranty of any kind and are subject to change without notice Shimadzu does not assume any responsibility or liability for any damage whether direct or indirect relating to the use of this publication SIVIA D1dH2. Adsorption glass vials are made from pharmaceutical Type borosilicate glass by a unique process that yields a surface chemistry with significantly reduced sample interactions without the use of a coating This results in extremely low compound loss through adsorption or catalytic degradation Our glass vials have very low reactivity pH shift and leaching characteristics Extra Low Adsorption vials are a must have for MS users or when working with micromolar concentrations and or low sample volumes where the surface to volume effects are much more pronounced The 12x32mm 1 5mL clear and amber vials are also available with silanized glass which is a conventional way to lower adsorption of polar compounds by chemically modifying the glass with permanently bonded hydrophobic groups via multi step gas phase deactivation to make the surfaces inert Shop online store shimadzu com or call Shimadzu at 800 477 1227 HPLC Vials Consult your user manual for recommended needle stroke settings prior to starting your analysis Compatible Systems Vials 1mL Clear Plug Cap 1mL Amber Plug Cap Part Number 220 91521 06 220 91521 07 x SIL 30AC SIL 30ACMP SIL 20ACXR SIL 20ACHT SIL 20AC SIL HTA HTC SIL 10A Ai AF AP LC 2030 2040 LC 2010AC HT default needle stroke a aaa Inserts gt LC Vial Selection Guide HPLC Vials Consult your user manual for recommended needle stroke settings prior to starting your analysis Comp
3. CD SHIMADZU SSI LCV 11 2015 Excellence in Science High Performance Liquid Chromatography Vial Selection Guide SHIMADZU Vial selection for an HPLC system is an important but often overlooked step Several characteristics of vials and septa are critical for optimum performance in an HPLC run The following guide will assist you in making the best selection for your specific analysis S Vial Mouth Opening A 6mm opening for the 1 5mL vial provides a better target for the autosampler needle and makes __ filling easier and cleaner especially with automatic pipettors LabTotal vials have a 9mm opening for maximum sample retrieval via pipette Glass Thickness Uniformity of the vial bottom thickness ensures consistent needle _ depth from run to run and is one of 14 strictly controlled manufac turing points Septa Quality The 1 5 and 4mL vials use a PTFE silicone septum and its cleanliness is suitable for everyday applications as well as the most discriminating LCMS analyses The septum is press fit inside the cap without any bonding agents which could potentially contaminate samples It also prevents the needle from pushing the septum into the vial A pre slit version is also available One Twist Cap For high throughput labs our single twist cap allows fast and easy sample preparation We also offer a 1 5mL 7 snap cap vial for extra convenience Low Adsorption Glass Shimadzu Low and Extra Low
4. L uL For additional assistance in filtering we offer the Filter Vial Toggle Press This Press provides the extra force re quired to filter very viscous and or particulate laden samples 220 91521 56 Filter Vial Toggle Press N ra S gt S LC Vial Selection Guide Important This publication may not be reproduced in whole or part without written permission from Shimadzu Corporation Since Shimadzu products are frequently upgraded and im proved information in this publication is subject to change without notice Please read the instruction manual included with all products before use The replacement and maintenance periods listed in the guide are presented only as guidelines and not as a guarantee Routine maintenance and inspection will vary de pending on usage conditions J a a A Should you have questions on items listed in this guide please contact your nearest Shi madzu representative Links Shimadzu Scientific Instruments U S Webstore http store shimadzu com Shimadzu Nexera Virtual Advisor https nexerava ssi shimadzu com Shimadzu Prominence Virtual Advisor https prominenceva ssi shimadzu com 6 SHIMADZU SHIMADZU CORPORATION International Marketing Division 3 Kanda Nishikicho 1 chome Chiyoda ku Tokyo 101 8448 Japan Phone 81 3 3219 5641 Fax 81 3 3219 5710 URL www shimadzu com SHIMADZU SCIENTIFIC INSTRUMENTS 7102 Riverwood Drive Columbia Maryland 21046 U S A Phone 800
5. atible Systems 1 5mL 1 5mL 1 5mL 1 5mL 1 5mL 1 5mL 1 5mL Clear w Amber WI Clear w Clear Amber WI Amber Clear w Snap Cap Snap Cap Screw Cap _ Silanized Screw Cap Silanized Screw Cap w Screw w Screw Pre Slit Cap Cap Septa 220 91498 00 220 91521 17 228 45450 91 228 45451 91 228 45452 91 228 45453 91 220 91521 18 x x x x X Part Number SIL 30AC SIL 30ACMP SIL 20ACXR SIL 20ACHT SIL 20AC SIL HTA HTC SIL 10A Ai AF AP LC 2030 2040 LC 2010AC HT Recommended Fill 1 5mL 1 5mL Volume Residual Volume 185uL 185uL default needle stroke Glass Adsorption N A Low Adsorption Type Replacement Cap Part Number 220 91521 22 nonslit 228 45454 91 nonslit 220 91521 16 pre slit 220 91521 23 pre slit 220 91521 16 septumless Inserts Shop online store shimadzu com or call Shimadzu at 800 477 1227 HPLC Vials Consult your user manual for recommended needle stroke settings prior to starting your analysis Compatible Systems 1 5mL MT 1 5mL MT 1 5mL MT 1 5mL 200uL 200uL 300uL IT Clear IT Amber IT Clear Certified Q sertTM Q sertTM Polypro Center Center Center LabTotal fused fused in pylene w Draining Draining Draining Vial for MS insert w sert w Snap Screw cap w Screw w Screw w o Caps w Screw Screw cap cap Cap Cap Cap zoar J x x x x x _ fsuzoac_ x x x x _ cerae x x x x x su towavariae x x x x x czo x
6. p 220 91521 14 nonslit 220 91521 24 pre slit Inserts Part Number 228 21284 91 w spring n a 228 21285 91 insert only D X X Shop online store shimadzu com or call Shimadzu at 800 477 1227 Autosampler Racks Consult your user manual for recommended needle stroke settings prior to starting your analysis Nexera Prominence Integrated Systems Compatible Systems 1ImL 175 position Rack 1 5mL 105 position Rack 1 5mL 105 position cooled Rack sIL30AC 7 SIL 30ACMP n a n a n a Compatible Systems 1 5mL 70 position cooled 1 5mL 54 position Vial Tray 4mL 50 position Rack Rack SIL 30AC 228 50830 92 set of 2 SIL 30ACMP SIL20ACXR sl 20ACHT SIL20AC SEI 228 50830 92 set of 2 LC 2030 2040 ETO 228 50830 92 set of 2 1 Use cooled racks in SILs with cooling 2 Racks sold as set of 2 3 Also comes as set of 12 220 91532 00 LOSE EE Rack Type Part Number 1 5mL vials 13mL vials eee a I n OOo p coers Jsa fx Sid SSCS SSS TET H H HS E H H SS Cd SSCS E H H H HS 4 requires Universal Sample Tray 499 00206 91 LC Vial Selection Guide Filter Vials Our filter vials offer a single sample filtration system all performed in an autosampler ready vial The filter vial consists of two parts a filter vial shell and a plunger which includes a filter on one end and a vial cap on the other end Samples are filtered by pipetting the sample into the filter vial shell inserting the plunger into
7. the shell and then pushing the plunger into the shell For Shimadzu autosamplers needle stroke needs to be set to no more than 49mm for the 1 5mL vial rack For non Shimadzu autosamplers needle stroke needs to be set to 5mm from the bottom of the filter vial Consult your user manual for instructions on how to change needle stroke settings Filter vials are available in a variety of filter membranes and pore sizes and come with pre slit septa Vials are 12 x 32mm and come 100 pack Membrane Material Aqueous Organic Low Protein Samples Samples Binding Samples Bn HH HH H men Membrane Material Explanations PTFE polytetrafluoroethylene hydrophobic membrane for use for samples containing gt 50 organic solvents membrane for hydrophilic samples PVDF polyvinylidene difluoride low protein binding membrane for use with samples containing lt 50 organic solvents including proteins peptides and E coli PES polyethersulfone low protein binding membrane for aqueous samples mostly used for mammalian cell culture antibodies and proteins Pore Size Cells Cell Debris in LC Column LC Column Sample Particle Size lt 3um Particle Size gt 3um oam Cd SSCS D H HE S Shop online store shimadzu com or call Shimadzu at 800 477 1227 Filter Vials 0 2um Pore Membrane Max Fill Volume Dead Volume Recommended for Size uL uL E SS eee eee 0 45um Pore Membrane Max Fill Volume Dead Volume Recommended for Size u
8. x x x x x jucaioacnt x x x x 12 x 32mm 12 x 32mm 12 x 32mm 12 x 32mm Recommended Fill 1 2mL 1 5mL 200uL 290uL Volume Residual Volume BUL 185uL BUL 8uL default needle stroke Glass Adsorption Extra Low Adsorption Extra Low Low Adsorption N A Type Adsorption Replacement Cap Part Number 228 45454 91 nonslit N A 228 45454 91 nonslit 220 91521 16 pre slit 220 91521 16 pre slit 220 91521 12 septumless 220 91521 12 septumless Quantity 1000 1000 Inserts Includes inspection certificate for integrity of multiple manufacturing points as well as residual compounds for LCMS and GCMS analysis LC Vial Selection Guide HPLC Vials Consult your user manual for recommended needle stroke settings prior to starting your analysis Compatible Systems AmL Clear 4mL Amber AmL Clear 4mL MT IT AmL MT IT 13mL Clear w Screw Cap w Screw Cap w Screw Clear Center Amber w Screw Cap Cap Pre Slit Draining Center Septa w Screw Cap Draining w Screw Cap 220 91521 08 220 91521 09 220 91521 20 220 91521 10 220 91521 11 228 21280 92 x x x X Part Number SIL 30AC SIL 30ACMP SIL 20ACXR SIL 20ACHT SIL 20AC SIL HTA HTC SIL 10A Ai AF AP LC 2030 2040 LC 2010AC HT 15 x 45mm 15 x 45mm 23 x 45mm Recommended Fill 3 5mL 3 0mL 12 5mL Volume Residual Volume 342uL 12uL 500uL default needle stroke Glass Adsorption Low Adsorption Extra Low Adsorption Type Replacement Ca
Download Pdf Manuals
Related Search