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User`s Manual

1. Catalog RapidVap Description 79000 00 RapidVap Vacuum System 115V 79000 01 RapidVap Vacuum System 230V 79000 02 RapidVap Vacuum System 115V with lid heater 79000 03 RapidVap Vacuum System 230V with lid heater 79000 10 RapidVap Vacuum System 115V with RS 232 Interface 79000 11 RapidVap Vacuum System 230V with RS 232 Interface 79000 12 RapidVap Vacuum System 115V with lid heater with RS 232 Interface 79000 13 RapidVap Vacuum System 230V with lid heater with RS 232 Interface Plus the Following Part Component Description 78286 04 Hose Vacuum 14888 00 Two 2 Clamps 13364 00 Power Cord 115V or 13365 00 Power Cord 230V 19116 00 Washer 3 19092 21 Acorn Nut 3 12556 00 Heat Transfer Grease 74901 00 User s Manual 74848 00 Cable Assembly RS232 Models 79000 10 11 12 13 Since users preference of sample size varies the sample holding block is not included with the RapidVap Vacuum System or the RapidVap N2 48 Evaporation System The correct size block must be selected and ordered separately Refer to Appendix D RapidVap Accessories for block selection Catalog RapidVap Description 79100 00 RapidVap N Evaporation System 115V 79100 01 RapidVap N Evaporation System 230V 79100 10 RapidVap N Evaporation System 115V with RS 232 Interface 79100 11 RapidVap N Evaporation System 230V with RS 232 Interface Plus the Following Part Component Description 79131 01 Exha
2. is sent the RapidVap will respond 0 1 or 2 S Xxx Selects the vortex speed of program 9 from 0 or 12 to 100 will get a xxx yyy n response for confirmation xxx speed setpoint yyy actual speed T xxx Selects the HEAT TEMPERATURE SET POINT of program 9 from 30 to 100 C will get a xxx yyy n response for confirmation xxx temperature setpoint yyy actual temperature by entering TO the heat will be set to OFF t XxXxx Selects the TIME SET POINT of program 9 from 1 to 999 minutes and 1000 for no stopping will run continuously will get a xxxx yyyy n response for confirmation xxxx time setpoint yyyy time left V xxxx Selects the VACUUM SET POINT if the RapidVap is a Vacuum model of program 9 from to 1000 mBar will get a XXxXx yyyy n response for confirmation xxxx vacuum setpoint yyyy actual vacuum 42 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap Selects the PRE HEAT SET POINT of program 9 from 30 to 100 C will get a xxx yyy n response for confirmation xxx pre heat setpoint yyy actual temperature KEY LOCKED when x 1 and UNLOCKED when x 0 will get a x n response for confirmation elects the N2 VALVES if the RapidVap is an Nz model of program 9 from 0 2 4 6 8 will get a x n response for confirmation x will mute the audio alarm x 0 will allow the audio alarm to work normally T
3. ODNOJAVI SN SEER PE over s dYAQIdYY OJNOJAVI a airi N a vb FIRAD Ja T HIMOTH EH OREHE Wd Duva HILI nep s ix a li ji TAER na nm Wa CEs wig Je pEi anG WARD vama 14000 Da ikiga vun k i g PETU 05 diwa ODO AV Lite O O ee hu ig wA sO ONAY dlm 30 F s z OxH Z LOODE Nid eran iid aoe TTT N a DBD JJV dag LNI BOSI IKOLYHIANJI GO GO OCEKL Wd EN HITIDHIMOI to OO GTOrI N d DWE HITIOHIMOJ 65 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C RapidVap Specitications Wiring Diagram 230V Models TEMPERATURE Bor To TEMPERATURE JLM umi LABCONCO WIRING DIAGRAM RAPIOVAP EVAPORATION SYSTEM 230V 50 60 HZ P N 7490300 SA BU BA BAN REV E 4 HARNESS P M 74905 ra z z bas a m z 4 r 3 v VACUUN CONTROL 24Vdc 7A mit si ice 2 05 VAC SENSOR P N 74918 CONTROLLER BASIC P N 74858 00 04 CONTROLLER N2 P N 74838 03 INTERFACE CABLE P N 74599 P N 7908001 SWITCH BOARD P N 7483802 1X 6 CO P N 4503700 MAGNETIC LID Sw LABCONCO RAPIDVAP 66 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C RapidVap Specifications Evaporation Rates RapidVap Vacuum Models The following tables show the approximate time to evaporate various solvents in 75mm and 16mm sample tubes when the sample block is
4. 89 339 Glassware Used 0 5 ml PN 79259 00 77 in 1 9 cm Long Stem 1 5 ml PN 79139 00 1 37 in 3 5 cm Long Stem 2 0 ml PN 79137 00 1 62 in 4 1 cm Long Stem 3 0 ml PN 79135 00 2 25 in 5 7 cm Long Stem 11 Appendix C RapidVap Specitications 12 RapidVap N 48 Models The following tables show the approximate time to Li evaporate various solvents in 12mm and 20mm sample tubes when the sample block is fully loaded Other sample blocks are available for different size tubes If they are used or if a different number of samples is run at one time the evaporation times can be estimated from these charts or determined experimentally Evaporation rates may vary from tube to tube Evaporation Time RapidVap N gt 48 Models 12 mm Sample Tubes Time in Minutes Methylene Toluene Acetonitrile Methanol Hexane Hexane Solvent Chloride Ethyl Acetate Ethyl Acetate 75 25 50 50 Block Preheat amp Block Set Point Temp 40 C 80 C eae 40 C 40 C 40 C Starting Volume 2 ml 6 8 8 18 5 5 Number of samples 48 Vortex speed 100 Nitrogen pressure 8 psi Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C RapidVap Specifications Evaporation Time RapidVap N gt 48 Models 20 ml Sample Tubes Time in Minutes Methylene Toluene Acetonitrile Methanol Hexane Hexane Solvent Chloride Ethyl Acetate Ethyl Acetate 13 29 50 50 Block Preheat amp Block Set Point T
5. Sensor Lower 22 Temperature Sensor Upper 23 Vacuum Sensor 24 Spring Latch 25 Latch 26 Washer Latch 27 Knob Latch 28 Nut Block 29 Washer Block 30 Stud Block 31 Trim Ring 32 Hose Exhaust 33 Shield Lid 34 Lid 34A Lid With Heater 35 Thermal Fuse 36 Valve Vacuum 37 PCB Display Control 38 Label Control Panel 39 l Fuse Main Vacuum PCB 2A Type T Slow Blow Not Shown 56 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix A RapidVap Vacuum and RapidVap N Components Product Service Domestic 1 800 522 7658 International 816 333 8811 57 Appendix A RapidVap Vacuum and RapidVap N2 Components RapidVap N and RapidVap N 48 Components 55 6 1927105 Washer Latch o Z o o o o oo y O 06060 Il 74845 00 Lid RapidVap N3 60A 1 7913101 Hose Exhaust Short AA l i 61 2 63 64 74920 02 PCB Display Control 7 74922 00 Label Control Panel 79759 01 Thermal Fuse 13444 03 Fuse Exhaust Blower 4A Type T Slow Blow Not Shown 6 58 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix A RapidVap Vacuum and RapidVap N gt Components Product Service Domestic 1 800 522 7658 International 816 333 8811 59 Appendix A RapidVap Vacuum and RapidVap N Components 60 Product Service Domestic 1 800 522 7658 International 816 333 8811 APPENDIX B RaPpiD VAP DIMENSIONS RapidV
6. Starting Volume 450 ml 58 56 33 68 75 420 400 53 48 29 61 63 352 350 48 40 24 54 52 321 300 41 35 21 47 45 266 250 35 31 19 43 40 230 200 30 26 16 38 35 193 150 25 22 14 34 28 153 100 19 17 11 29 22 120 50 10 9 7 16 15 68 Number of samples 8 Nitrogen pressure 10 psi at volumes 0 thru 300 ml see Note 1 5 psi at volumes above 300 thru 350 ml 4 psi at volumes above 350 thru 400 ml 2 psi at volumes above 400 thru 450 ml Vortex speed 70 at volumes 0 thru 300 ml see Note 1 36 at volumes above 300 thru 450 ml Sample tubes Not covered with caps 70 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C RapidVap Specifications KI Table C Evaporation Rate in Cool Zone Stem 600 ml Sample Tubes Time in Minutes Methylene Solvent Chloride Block Preheat k Block Set Point Temp 40 C Ending Glassware Volume 0 5 ml Stem 0 5 4 Dry 10 1 5 ml Stem 1 5 4 1 0 9 0 5 17 Dry 31 2 0 ml Stem 2 0 3 1 0 17 Dry 64 3 0 ml Stem 3 0 4 2 0 20 1 0 ST Dry 128 Number of samples 8 Vortex speed 70 Nitrogen pressure 10 psi Sample tubes Covered or not covered with caps Product Service Domestic 1 800 522 7658 International 816 333 8811 Ethyl Acetate Hexanes Acetone Toluene Water TS 70 C SC 100 C 95 C 4 3 4 5 42 9 7 9 10 78 4 2 3 5 23 7 5 7 9 43 13 8 12 15 75 24 16 22 26 120 3 2 3 4 28 11 8 15 14 80 34 26 47 30 201 4 3 3 5 34 12 10 16 17 76 34 25 50 40 170 81 52 108
7. begun Do not use the RapidVap in a manner not specified by the manufacturer refer to Appendix C RapidVap Specifications The electrical protection properties of the RapidVap may be impaired if the RapidVap is used inappropriately Product Service Domestic 1 800 522 7658 International 816 333 8811 23 Chapter 4 Using Your RapidVap 24 Planning Thoroughly understand procedures and the eguipment operation prior to beginning work The unigue performance of the RapidVap Vacuum is dependent upon the proper balance of heat vacuum and vortexing action If the proper balance is not established it is possible to damage or lose a portion of the sample Therefore if you are unfamiliar with the RapidVap or are attempting a new protocol it may be helpful to make a trial run that is void of the sample you are attempting to concentrate Select the size of the sample tube so it is compatible with the block Tubes should not be loose in the block Blocks are available with holes for various size tubes Refer to Appendix D RapidVap Accessories for available block sizes and pages 19 and 20 for recommended usable tube volumes and vortex speeds The unigue performance of the RapidVap N 1s dependent upon the proper balance of heat gas flow and vortexing action If the proper balance is not established it is possible to damage or lose a portion of the sample Therefore if you are unfamiliar with the RapidVap N gt or are attempting a
8. bottom of the chamber Position the block over the three studs in the chamber Install the flat washers and either nuts or guide rods Tighten securely Product Service Domestic 1 800 522 7658 International 816 333 8811 15 Chapter 3 Getting Started Never lift the lid if the block is moving Samples may splash out Never operate the RapidVap without the sample block securely fastened in place Excessive vibration will occur Never attempt to reach into the chamber if the block is moving Nut or guide rods 3 required Washer 3 required Mounting stud Temperature sensor Apply heat transfer grease Nitrogen Gas Connection for a 1 4 I D hose into the out port of the regulator Clamp securely Alternately a compression fitting may be used that is suitable for a hose with a 3 8 O D and 1 4 I D THE NITROGEN PRESSURE MUST Ce NEVER BE ALLOWED TO EXCEED 20 PSI 103 KPA nj Turn the gas supply off Install a barb fitting suitable 16 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 3 Getting Started Exhaust Port If the RapidVap N is not located in a fume hood attach one end of the two inch diameter venting hose that is NI supplied with the RapidVap to the exhaust port on the right side of the unit Clamp securely Route the other end to a fume hood or other laboratory ventilation device Electrical Connection Plug the power cord
9. fully loaded Other sample blocks are available for different size tubes If they are used or if a different number of samples is run at one time the evaporation times can be estimated from these charts or determined experimentally Evaporation Time 75 mm dia Sample Tube Time in Minutes Methylene Solvent Chloride Toluene Acetonitrile Water Block Preheat amp Block Set Point 50 C 80 C 75 C 80 C Temperature Vacuum 250 mbar 133 mbar 167 mbar 133 mbar Starting Volume 300ml 62 90 102 402 250 56 72 84 345 200 49 66 71 289 150 42 57 60 239 100 36 33 49 189 50 22 40 37 95 Number of samples 8 Vortex speed 28 Vacuum pump Labconco model 79249 00 Rated free air flow 88 L min Max attainable vacuum 31 mbar Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C RapidVap Specifications 68 Evaporation Time 16 mm dia Sample Tube Time in Minutes Methylene Solvent Chloride Toluene Acetonitrile Water Block Preheat amp Block Set Point 50 C 80 C 75 C 80 C Temperature Vacuum 200 mbar 200 mbar 330 mbar 133 mbar Starting Volume 10 ml 18 25 25 119 8 14 20 22 101 6 10 14 17 72 4 8 12 13 50 2 4 6 7 26 Number of samples 69 Vortex speed 95 Vacuum pump Labconco model 79249 00 Rated free air flow 88 L min Max attainable vacuum 31 mbar RapidVap N Models The following tables indicate the approximate time required to evaporate vario
10. into the receptacle on the back of the RapidVap and plug the other end into a suitable wall power receptacle Calibrate the Vacuum Sensor The vacuum sensor can be calibrated to room ambient atmospheric pressure To do this determine the atmospheric pressure using a known reference device such as a mercury barometer Press and hold the vacuum release button on the RapidVap while turning on the RapidVap power switch Use the increase or decrease buttons to make the vacuum display agree with the reference pressure Press run to store the calibration In memory Chemical Attack on RapidVap Components Your RapidVap Evaporation System is designed to be chemical resistant to most compounds that are commonly used in the concentration processes that are performed in it However by necessity the RapidVap is comprised of a number of different materials some of which may be attacked and degraded by certain chemicals The degree of degradation is obviously dependent on the concentration and duration of exposure Some of the major components of the RapidVap that are susceptible to degradation are as follows Product Service Domestic 1 800 522 7658 International 816 333 8811 17 Chapter 3 Getting Started s O N O lt Oo D O lt COMPONENT MATERIAL Manifold N2 48 Exhaust Elbow N2 Polyamid Nylon D Blower Fan N2 Polyamid Nylon D Exhaust Hose N2 Polyethylene Vacuum Fittings Polypropylene
11. lid Reposition sample tubes Tighten all three mounting screws Install sample block Redirect hose to fume hood Replace blower Product Service Domestic 1 800 522 7658 International 816 333 8811 PROBLEM Sample in bottom of chamber Poor recovery rates Evaporation rate is reduced No vacuum poor vacuum RapidVap Vacuum Product Service Domestic 1 800 522 7658 International 816 333 8811 CAUSE Gas pressure too high RapidVap N2 Vortex speed too high Condensation forming inside lid RapidVap Vacuum Sample going to dryness RapidVap N gt Sample sloshing out of tube Heat setting is too high Gas supply depleted RapidVap N2 Heater inoperable Vacuum pump failure RapidVap Vacuum Pump not on Control valve open Leaks in lines or connectors Foreign material on lid gasket Vacuum pump oil low Excessive contamination in vacuum pump oil Pump not connected to RapidVap Chapter 7 Troubleshooting CORRECTIVE ACTION Reduce pressure Reduce speed Install lid heater See page 36 Program RapidVap N to prevent dryness Decrease vortex speed Decrease heat Replenish gas Contact Labconco Check pump Turn on pump Check control valve Locate and repair Clean gasket and lid Add oil Replace oil Connect hose and power cord 51 Chapter 7 Troubleshooting PROBLEM CAUSE No gas flow Gas depleted Rapi
12. proper balance of the machine Therefore if less than a full load of samples is run it is important to load samples into the RapidVap in a fairly uniform manner 26 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap distributing the weight of the samples and glassware evenly in the sample block IN ORDER TO MAXIMIZE THE PERFORMANCE OF THE RAPIDVAP IT IS IMPORTANT THAT SOME OF THE SAMPLES ARE CLUSTERED AROUND THE FRONT LEFT HAND BLOCK MOUNTING STUD THE BLOCK TEMPERATURE SENSOR IS LOCATED ADJACENT TO THIS BLOCK MOUNTING STUD BY POSITIONING THE SAMPLE NEAR THE SENSOR THE SENSOR WILL DETECT THE COOLING EFFECT OF THE EVAPORATING SAMPLES AND SIGNAL THE CONTROLS TO SUPPLY MORE HEAT TO THE SAMPLE BLOCK The best evaporation rate is achieved under conditions that maximize sample surface area These include using the largest tube possible and using the highest vortex speed possible When less than 8 samples are run in the RapidVap N2 or less than 48 samples are run in the RapidVap N 48 nitrogen flow can be directed to 2 4 or 6 positions It is important to position glassware properly in the RapidVap N when less than a full block is run to ensure that nitrogen gas 1s directed downward where the sample is located Note the label on the hub in the center of the chamber This indicates which nozzles on a RapidVap N or nozzle clusters on a RapidVap N gt 48 will be activated I
13. resume operation at the same set point parameters and the timer will continue to count down from the time at which the RapidVap was stopped End Alarms The RapidVap has two means to signal the completion ofa run The first method is determined by the operator when the run time is set as described in the previous paragraph Time Setting Guidelines In the second method the RapidVap will automatically sense when an evaporation process is nearly complete by comparing temperatures in the unit When the RapidVap detects end point it will sound an alarm and the LED next to the PREHEAT END ALARM button will flash This alerts the operator to closely monitor the run s completion This method performs best when large samples are processed at high temperatures When small samples or low temperatures are used the alarm may signal prior to the end of evaporation The audible alarm may be canceled by pressing the PREHEAT END ALARM button The LED will continue to flash until the STOP button is pressed If the button is pressed again the audible alarm will become active again RS 232 Communications Some RapidVaps are equipped with RS 232 communications capabilities This hardware and software allows a user to perform all the front panel functions from a standard RS 232 link Communications will be at 4800 baud no parity 8 bit word stop bit and a 3 wire interface TXD RXD and circuit common The RS 232 link will be duplex
14. set point To change the speed set point parameter press the set point select button directly under the word SPEED Arrows will point to the present set point The speed may be altered from 0 to 100 by pressing the increase or decrease buttons The last entered set point will be stored in memory Product Service Domestic 1 800 522 7658 International 816 333 8811 37 Chapter 4 Using Your RapidVap 38 It is suggested that the user set the vortex speed at a low percentage and gradually increase it after the run is started This will minimize the possibility of samples sloshing out of the tubes Reruns of the same protocol may start at the speed determined by previous runs Change heat set point To change the heat set point press the set point select button under the word HEAT Arrows will point to the present set point which can be changed from OFF up to 99 by pressing the increase or decrease buttons The set point is 100 C if the display shows HI The last entered set point will be stored in memory Change time set point To change the time set point press the set point select button under the word TIME Arrows will point to the present set point which can be changed from to 999 minutes by pressing the increase or decrease buttons If it is desired to have the RapidVap run continuously without alarming at the end of a time period press the increase button until the display says RUN The last
15. side of the graph 3 Draw a straight line linking these two points Product Service Domestic 1 800 522 7658 International 816 333 8811 29 Chapter 4 Using Your RapidVap 4 Find Constant b for the solvent on the top of the grid Follow that line until it intersects with the line as drawn between the two points This point represents the boiling point at the given pressure and the temperature is read off the left or right side of the grid 0 250 C To determine the operating pressure necessary to achieve a siven boiling point 1 Find the boiling point at normal atmospheric pressure 1 Bar on the left side of the graph 2 Find the Constant b and follow this line to the desired boiling point on the grid 0 250 C 3 Draw a straight line linking these two points and extrapolate on the right hand scale to find the operating pressure 30 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap Physical constants HEAT OF VACUUM FOR BOILING DENSITY VAPORIZATION BOILING POINT SOLVENT PT C g cm Kcal Kg CONSTANT b AT 40 C MBAR ON EEN a Na ee Acetylene tetrachloride Tetrachloroethane Toluene TN 0867 86 202 AAA Product Service Domestic 1 800 522 7658 International 816 333 8811 31 Chapter 4 Using Your RapidVap Determination of Operating Conditions Applied Vacuum Boiling Point DETERMINATION OF OPERATING CON
16. to bump In the RapidVap Vacuum models generally the evaporation rate will be optimized with the block temperature set and preheated 20 to 40 C above the boiling point of the solvent at the operating pressure 28 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap For example methanol which boils at 65 C at atmospheric pressure boils at 5 C at pressure of 53 mBar Under these vacuum conditions the block temperature should be set between 25 to 45 C The nomogram and equation to follow will help in this determination Calculating the boiling point The operating pressure corresponding to the desired boiling point temperature may be calculated for any solvent using the following formula log P 2 8811 Ta T b T Where P Vacuum mm Hg Ta Boiling Point Temperature at Atmospheric Pressure K T Desired Boiling Point Temperature K b Constant from Table Useful conversion factors mBar 75 mm Hg K O 273 Using the nomogram To use this graph three facts must be known about a given solvent 1 Boiling point at normal atmospheric pressure 1 Bar 2 Constant b 3 Either operating temperature or operating pressure To determine the desired boiling point at a given pressure 1 Find the boiling point at normal atmospheric pressure 1 Bar on the left side of the graph page 32 2 Find the operating pressure on the right
17. tube when vacuum is applied to the chamber of the vacuum model GLASS VIALS USED IN THE RAPIDVAP eS SHOULD BE OF THE STYLE THAT DO NOT V HAVE THE BEAD OR LIP ON THE TOP EDGE IF VIALS WITH BEADS ARE USED THE BEADS COULD HIT EACH OTHER AND BREAK THE GLASS Several different size sample blocks are available for the RapidVap Vacuum model The maximum recommended sample volumes and vortex speeds are as follows TUBE SAMPLE VORTEX SIZE VOLUME SPEED 12 x 75 mm 6 ml 3 ml 95 13 x 100 mm 10 ml 5 ml 95 16 x 150 mm 23 ml 12 ml 95 15 ml centrifuge 7 5 ml 66 28 mm 46 ml 23 ml 48 600 ml 30 ml 45 100 ml 45 200 ml 38 300 ml 29 400 ml 20 450 ml 18 Product Service Domestic 1 800 522 7658 International 816 333 8811 25 Chapter 4 Using Your RapidVap TUBE SAMPLE VORTEX SIZE VOLUME SPEED 170 ml 50 ml 50 75 ml 47 100 ml 42 125 ml 35 Two sample blocks are available for the RapidVap No NI Recommended speeds are as follows TUBE SAMPLE VORTEX SIZE VOLUME SPEED 600 ml 50 ml 90 100 ml 90 200 ml 76 300 ml 58 400 ml 40 450 ml 36 170 ml 50 ml 100 75 ml 95 100 ml 85 125 ml 70 Four sample blocks are available for the RapidVap N 48 Recommended speeds are as follows TUBE SAMPLE VORTEX SIZE VOLUME SPEED 12 mm 6 ml 3 ml 100 13 mm 10 ml 5 ml 100 16 mm 23 ml 12 ml 100 20 mm 35 ml 18 ml 100 Loading Glassware Into the RapidVap Smooth operation of the RapidVap is dependent upon
18. vane pump the oil in the pump should be checked often It must be changed 1f it is cloudy shows particles or is discolored The useful life of vacuum pump oil can be extended if the vacuum pump is operated for an extended period of time after the RapidVap run is over This allows contaminants to be purged from the hot oil This must be done with the inlet to the pump blocked off to prevent air from free flowing through the pump If the pump is operated at an elevated vacuum level oil will be expelled from the pump and damage will occur With prudent maintenance your RapidVap will provide years of service Warranty on the effected parts will be void if maintenance has obviously been neglected If you have questions about using specific compounds in your RapidVap contact Labconco Technical Service at 1 800 821 5525 or 816 333 8811 or e mail labconco labconco com Solvent Safety Precautions The RapidVap is not classified as explosion proof It has been designed with safety as a primary consideration and should be used in a prudent manner using good laboratory practices It has been designed for use with compounds as described in the United States National Electrical Code Class I Group D The block that holds the sample tubes may be programmed to run as hot as 100 C however the heater element may normally run at 110 C A thermal fuse limits the heater to a maximum temperature of 130 C Itis important that the solvents used a
19. 0 VAC 50 60 Hz 3 4 amps single phase 195 liters per minute 2 x 10 mbar max vacuum For use with non flammable solvents only Vacuum Pump Two stage direct drive pump 220 208 230 VAC 50 60 Hz 3 4 amps single phase 117 liters per minute 2 x 10 mbar max vacuum For use with non flammable solvents only Vacuum Pump Two stage direct pump 115 VAC 60 Hz 6 8 amps single phase 117 liters per minute 2 x 10 mbar max vacuum For use with non flammable solvents only Secondary Trap Canister Includes stand and fittings Requires an insert suitable for the application Acid Trap Insert Installs inside secondary trap canister Contains acid neutralizing desiccant Moisture Trap Insert Installs inside secondary trap canister Contains desiccant 77 Appendix D RapidVap Accessories 18 PART DESCRIPTION 78150 00 Radioisotope Trap Insert Installs inside secondary trap canister Contains activated charcoal 78152 00 Solvent Trap Insert Installs inside secondary trap canister Contains molecular sieve 75380 00 Secondary Vacuum Trap 9 Ya h x 7 7 8 diameter with Ya vacuum connections Volume of inner pot holds 2 85 liters of dry ice and alcohol Ice trapping capacity is over 900 ml Shipping weight 9 Ibs 75382 00 Secondary Vacuum Trap 9 Ya h x 7 7 8 diameter with 1 2 vacuum connections Volume of inner pot holds 2 85 liters of dry ice and alcohol Ice trapping capacity is over 900 ml Shipping w
20. 1 63 Appendix C RapidVap Specifications 64 Environmental Conditions e Indoor use only e Maximum altitude 6562 feet 2000 meters e Ambient temperature range 41 to 104 F 5 to 40 C e Maximum relative humidity 80 for temperatures up to 88 F 31 C decreasing linearly to 50 relative humidity at 104 F 40 C e Main supply voltage fluctuations not to exceed 10 of the nominal voltage e Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary voltage spikes on the AC input line that may be as high as 1500V for 115V models and 2500V for 230V models are allowed e Used in an environment of Pollution degrees 2 1 e where normally only non conductive atmospheres are present Occasionally however a temporary conductivity caused by condensation must be expected in accordance with IEC 664 N Nitrogen Consumption e Gas flow RapidVap N with 8 active nozzles 0 55 SCFM 12 psi 0 41 SCFM 6 psi e Gas flow RapidVap N gt 48with 48 active nozzles 3 5 SCFM 20 psi 2 5 SCFM 10 psi Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C RapidVap Specifications Diagram 115V Models iring W a AJY DOBIE N d SSIKEVH JAWA EW O 4 O Om N a s MEZA COrOBRE Nd i ULF TT e m i ZH 09 05 ASI NJISAS NOILYHOAYAJ dYAJidYH i pi 1 TOMIMOJ MANOVA it WYHOVIO ONIMIM ZIM z rt ledt i See 7 ami
21. 5 C Starting Volume 450 ml 9 82 54 90 109 623 400 80 65 52 75 80 531 350 69 56 33 64 69 437 300 59 48 29 54 60 379 250 SI 40 22 45 50 323 200 43 33 19 38 41 270 150 36 26 16 31 32 221 100 28 19 11 23 23 173 50 18 12 7 14 13 106 Number of samples 8 Nitrogen pressure 10 psi at volumes 0 thru 300 ml see Note 1 3 psi at volumes above 300 thru 350 ml 4 psi at volumes above 350 thru 400 ml 2 psi at volumes above 400 thru 450 ml Vortex speed 70 at volumes 0 thru 300 ml see Note 1 36 at volumes above 300 thru 450 ml Sample tubes covered with caps Note 1 Even though the RapidVap N is capable of processing starting volumes as high as 450 ml using the 600 ml sample vial its optimum volume is 300 ml Above Product Service Domestic 1 800 522 7658 International 816 333 8811 69 Appendix C RapidVap Specitications 300 ml the vortex speed must be reduced and the nitrogen pressure must be decreased to prevent the sample from splashing out This data for starting volumes over 300 ml was generated by starting the evaporation at reduced levels of nitrogen pressure and vortex speed As the solvent evaporated the nitrogen pressure and vortex speed were increased NY Table B Evaporation Time in Upper Portion of Sample Vial 600 ml Sample Tubes Time in Minutes Methylene Ethyl Solvent Chloride Acetate Hexanes Acetone Toluene Water Block Preheat amp Block Set Point Temperature 40 C 75 C 70 C 5320 100 C 95 C
22. 800 522 7658 International 816 333 8811 83
23. 8811 CHAPTER 2 PREREQUISITES Before you install your RapidVap you need to prepare your site for installation Carefully examine the location where you intend to install your RapidVap You must be certain that the area is level and of solid construction In addition an exhaust means must be provided and a source of nitrogen must be available for the RapidVap N2 An electrical source must be located near the installation site Carefully read this chapter to learn e the electrical supply requirements e the exhaust requirements e the nitrogen supply requirements for the RapidVap N2 e the vacuum pump requirements for the RapidVap Vacuum Refer to Appendix C RapidVap Specifications for complete RapidVap electrical and environmental conditions specifications and requirements Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 2 Prerequisites Electrical Requirements If your RapidVap is a Vacuum model a dedicated electrical outlet is required This outlet requires a 20 Amp circuit breaker or fuse for models rated at 115V 60 Hz A 10 Amp circuit breaker or fuse is required for models rated at 230V 50 60 Hz 115V models are equipped with a 20 Amp NEMA 5 20P plug 230V models are equipped with a 16 Amp CEE 7 7 plug It may be necessary to remove the plug and install a different plug to match the available receptacle If your RapidVap is a Nitrogen model a dedicated electrical outlet is r
24. Blower Housing N2 Polyeropylene J PMG 5 7 Vacuum Hose PVC Trim Ring Bromyl Butyl O Rings Neoprene Block Hardware Stainless Steel Nozzle N2 Stainless Steel Vacuum Sensor Stainless Steel Solvents Chloroform Ethyl Acetate Hexanes Toluene v O Si gt gt sim z 5 2 O E s lt CiC DIDID jc joy DIDIDID ID D fc tty D DID D D D jc tt A je f f JE fe Cc Jelc tot tt teh Ki Jo C Moderate Degradation Ouestionable Use D Severe Degradation Infreguent use recommended immediate thorough cleaning required e Ifarotary vane vacuum pump is used most compounds used in the RapidVap will degrade the oil if allowed to enter the pump Generally a rotary vane pump is not suitable for use with the RapidVap e Diaphragm vacuum pumps sold by Labconco have wetted parts either made from Teflon or protected by Teflon coatings and are suitable for nearly all procedures e Glass lids are suitable for use with all common compounds When using compounds in the RapidVap that are hostile to the materials of construction it is imperative that the equipment is properly maintained 18 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 3 Getting Started e After each run clean up all residues spills and materials that might have splashed in the chamber using agents suitable for the substance involved e When using a rotary
25. DITIONS APPLIED VACUUM BOILING POINT Constant b Boiling point at normal atmospheric pressure ts C 250 ts Boiling point at 1 bar normal pressure t Boiling point at P mbar operating pressure p Operating pressure in mbar Example methyl alcohol 1 Boiling point at normal 1 bar atmospheric pressure 65 C 2 Constant b 0 160 3 Operating pressure 130 mBar 4 Boiling point at 130 mBar pressure 24 C 32 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap Aliphatic halogenated hydrocarbons 0 195 Aromatic hydrocarbons Aromatic halogenated hydrocarbons Ketones Ethers Nitriles Heterocyclic compounds Esters Time Setting Guidelines before the solvent is entirely evaporated This is accomplished by using glassware that has a small diameter stem on the bottom and using the Time function to shut off the process after a predetermined interval of time It is often desirable to stop the concentration process N The Cool Zone feature is available on the RapidVap N with 8 places and is not available on the RapidVap N with 48 places The design of the RapidVap N gt causes the evaporation to proceed quickly when the sample is in the larger upper chamber of the sample tubes When the solvent evaporates sufficiently to drop the level into the smaller stem the evaporation rate decreases significantly This phenomenon al
26. Repair connection Replace bottom sensor assembly Repair connection Replace sensor assembly Repair connection Close lid Replace switch Repair connection Product Service Domestic 1 800 522 7658 International 816 333 8811 49 Chapter 7 Troubleshooting 50 DISPLAY ERROR CODE Mem Fail Push Prog Motor Error CAUSE Memory failure New memory IC chip Bad memory IC chip Stalled condition Excessive speed detected 1 e gt 120 Defective motor CORRECTIVE ACTION Push program button Push program button Call Labconco Replace IC chip or control PCB Turn power off Try to restart after one minute Call Labconco if error message remains Turn power off Try to restart after one minute Call Labconco if error message remains Turn power off Try to restart after one minute Call Labconco if error message remains Other corrective actions for potential problems are as follows PROBLEM Unit will not operate Excessive vibration Sample odor in lab CAUSE Unit not connected to electrical power Circuit breaker blown Lid open Sample tubes not located symmetrically in block Sample block loose Sample block not installed Vent hose exhausting into lab area Inoperable blower RapidVap N gt CORRECTIVE ACTION Connect unit to proper electrical receptacle Correct electrical problem and reset circuit breaker by pressing button Close
27. Under normal operation the RapidVap requires little maintenance The following maintenance schedule is recommended As needed 1 Clean up all spills remove liquids from chamber 2 Clean lid and gasket using soft cloth sponge or chamois and a mild non abrasive soap or detergent Weekly 1 Ifthe vacuum pump contains oil check the V condition and level If the oil level is low add oil If the oil contains excessive amounts of moisture detected by a cloudiness in the oil it will be necessary to change the oil For further information regarding procedures for changing the vacuum pump oil refer to the vacuum pump manufacturer s instructions To expel small amounts of water that may have accumulated in the pump oil periodically operate the vacuum pump against a dry leak tight system The gas ballast must be open Product Service Domestic 1 800 522 7658 International 816 333 8811 45 Chapter 5 Maintaining Your RapidVap Monthly l The rubber components on the RapidVap may eventually deteriorate and require replacement The effective life of rubber parts depends upon both their usage and the surrounding environment Check all rubber hoses and gaskets and replace any that show signs of hardening permanent set or deterioration Using a soft cloth sponge or chamois and a mild non abrasive soap or detergent clean the glass lid Using a soft cloth sponge or chamois and a mild non abrasive soap or detergent cle
28. User s Manual RapidVap Vacuum N2 amp N2 48 Evaporation Systems Models 7900000 7900001 7900002 7900003 7900010 7900011 7900012 7900013 7910000 7910001 7910010 7910011 7910012 7910013 7910014 7910015 To receive important product updates complete your product registration card online at register labconco com Protecting you _ laboratory environment er KR Z LABCONCO Labconco Corporation 8811 Prospect Avenue Kansas City MO 64132 2696 800 821 5525 816 333 8811 FAX 816 363 0130 E MAIL labconco labconco com HOME PAGE www labconco com Please read the User s Manual before operating the equipment Copyright O 1999 2007 Labconco Corporation All rights reserved The information contained in this manual and the accompanying products are copyrighted and all rights reserved by Labconco Corporation Labconco Corporation reserves the right to make periodic design changes without obligation to notify any person or entity of such change Warranty Labconco provides a warranty on all parts and factory workmanship The warranty includes areas of defective material and workmanship provided such defect results from normal and proper use of the eguipment The warranty for all Labconco products will expire one year from date of installation or two years from date of shipment from Labconco whichever is sooner except the following e Purifier Delta Series Biological Safety Cabinets and PuriCare L
29. ab Animal Research Stations carry a three year warranty from date of installation or four years from date of shipment from Labconco whichever is sooner SteamScrubber FlaskScrubber Glassware Washers carry a two year warranty from date of installation or three years from date of shipment from Labconco whichever is sooner Blood Drawing Chairs carry a ten year warranty Carts carry a lifetime warranty Glassware is not warranted from breakage when dropped or mishandled This limited warranty covers parts and labor but not transportation and insurance charges In the event of a warranty claim contact Labconco Corporation or the dealer who sold you the product If the cause is determined to be a manufacturing fault the dealer or Labconco Corporation will repair or replace all defective parts to restore the unit to operation Under no circumstances shall Labconco Corporation be liable for indirect consequential or special damages of any kind This statement may be altered by a specific published amendment No individual has authorization to alter the provisions of this warranty policy or its amendments Lamps and filters are not covered by this warranty Damage due to corrosion or accidental breakage is not covered Returned or Damaged Goods Do not return goods without the prior authorization from Labconco Unauthorized returns will not be accepted If your shipment was damaged in transit you must file a claim directly with the freight
30. acity Package of eight 8 79139 00 Sample Tube End Point Volume 1 5 ml Borosilicate glass 600 ml capacity Package of one 1 Product Service Domestic 1 800 522 7658 International 816 333 8811 79 Appendix D RapidVap Accessories 80 PART DESCRIPTION 79140 08 Sample Tube End Point Volume 1 5 ml Borosilicate glass 600 ml capacity Package of eight 8 79137 00 Sample Tube End Point Volume 2 ml Borosilicate glass capacity Package of one 1 79138 08 Sample Tube End Point Volume 2 ml Borosilicate glass capacity Package of eight 8 79135 00 Sample Tube End Point Volume 3 ml Borosilicate glass capacity Package of one 1 79136 08 Sample Tube End Point Volume 3 ml Borosilicate glass capacity Package of eight 8 74876 00 Rack For 600 ml Sample Tubes Holds eight 8 tubes 74863 00 Rack For 170 ml Sample Tubes Holds eight 8 tubes 79254 08 Sample Tube Cap Teflon For 600 ml Sample Tubes Package of cight 8 79268 08 Sample Tube Cap Teflon For 170 ml Sample Tubes Package of cight 8 79265 08 Sample Tube Cap Polyethylene For 170 ml Sample Tubes Package of eight 8 79255 00 Sample Tube Cap Polyethylene For 600 ml Sample Tubes Package of one 1 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix D RapidVap Accessories The following accessories are available f
31. acuum Model Only When pressed and held the vacuum valve will open to break vacuum This is used to quickly decrease vacuum should bumping of the sample occur 36 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap Operating The RapidVap Controls Preheat To preheat the chamber press the preheat button The LED next to the button will illuminate and the display will show SP XXC ACT XXC Press increase or decrease buttons until the desired set point is displayed The actual block temperature will be displayed to the right When power is being supplied to the heaters a bar under the actual temperature will illuminate The block will continue to preheat until either the preheat button is pressed again or the run button is pressed Select existing program Operating parameters can be stored in memory so protocols can be repeated Nine programs can be stored To select a program press the set point select button directly under the word PROG An arrow will point to the current program number indicating that this set point can be altered To change the program number press the increase or decrease button until the desired program number is displayed When the program number is changed all its set points will change also to indicate the last entered parameters Pressing the PROG set point button will reset the timer to the previous set point time Change speed
32. an the exterior surfaces of the unit Liquid spray cleaners and polishes may be used on the exterior surfaces Do not use solvents to remove stains from the exterior surfaces as they may damage the finish 4 All weekly activities Product Service Domestic 1 800 522 7658 International 816 333 8811 CHAPTER 0 MoDiFyiNG YOUR RAPIDVAP The configuration of your RapidVap may need to be changed to accommodate your needs For example you may want to change the sample size you are running so you will need to change the block or you may want to add a lid heater to eliminate condensation inside the lid Read this chapter to learn how to e change blocks e install a lid with heater Changing the Sample Blocks If it is necessary to change from one sample size to another it may be necessary to change the block Refer to Appendix D RapidVap Accessories for available sample blocks First using a 7 16 socket RapidVap Vacuum and RapidVap N2 remove the three nuts and washers on the top of the existing block The RapidVap N gt 48 requires a 9 16 socket to remove the three manifold guides that secure the block Lift the block out of the chamber Note the asymmetric hole pattern of the three Product Service Domestic 1 800 522 7658 International 816 333 8811 47 Chapter 6 Moditying Your RapidVap Product Service Domestic 1 800 522 7658 International 816 333 8811 mounting holes Apply a small amount of heat trans
33. ap RapidVap Components Setting Up Your RapidVap Vacuum Pump Connection Sample Block Nitrogen Gas Connection Exhaust Port Electrical Connection Calibrate the Vacuum Sensor Chemical Attack on RapidVap Components Solvent Safety Precautions Your Next Step CHAPTER 4 USING YOUR RAPIDVAP Planning Glassware Selection and Speed Setting Guidelines Loading Glassware Into the RapidVap A WN mm N SO SO GO 00 AI ON ON MW Heat Setting Guidelines Time Setting Guidelines RapidVap Controls Operating the RapidVap Controls Operating The RapidVap Operational Notes Interrupting a Cycle After it Has Begun End Alarms RS 232 Communications RS 232 Programming Syntax RS 232 Hardware Required CHAPTER 5 MAINTAINING YOUR RAPIDVAP CHAPTER 6 MODIFYING YOUR RAPIDVAP Changing the Sample Blocks Installing the Optional Lid Heater CHAPTER 7 TROUBLESHOOTING APPENDIX A RAPIDVAP AND RAPIDVAP N COMPONENTS APPENDIX B RAPIDVAP DIMENSIONS APPENDIX C RAPIDVAP SPECIFICATIONS Wiring Diagram 115V Wiring Diagram 230V Evaporation Rates RapidVap Vacuum Models RapidVap N Models RapidVap N2 48 Models APPENDIX D RAPIDVAP ACCESSORIES RapidVap Vacuum Model Accessories RapidVap N Model Accessories RapidVap N2 48 Model Accessories DECLARATION OF CONFORMITY 45 47 47 48 49 CHAPTER 1 INTRODUCTION Congratulations on your purchase of a Labconco RapidVap Labconco manufactures two types of RapidVaps one utilizes vacuum and the oth
34. ap Vacuum INCH CENTIMETERS Product Service Domestic 1 800 522 7658 International 816 333 8811 61 Appendix B RapidVap Dimensions 62 RapidVap N INCH CENTIMETERS Product Service Domestic 1 800 522 7658 International 816 333 8811 APPENDIX C RAPIDVAP SPECIFICATIONS This Appendix contains technical information about the RapidVap including specifications environmental operations conditions wiring diagrams and evaporation rates Electrical Specifications e Nominal amperage for 115V RapidVap Vacuum model 79000 00 amp 79000 10 excluding vacuum pumps 8A Maximum amperage with vacuum pump 16A e Nominal amperage for 230V RapidVap Vacuum model 79000 01 amp 79000 11 excluding vacuum pumps 4A Maximum amperage with vacuum pump 8A e Nominal amperage for 115V RapidVap Vacuum model 79000 02 amp 79000 12 with Lid Heater excluding vacuum pump 8 6A Maximum amperage with vacuum pump 16A e Nominal amperage for 230V RapidVap Vacuum model 79000 03 amp 79000 13 with Lid Heater excluding vacuum pump 4 3A Maximum amperage with vacuum pump 8A e Nominal amperage for 115V RapidVap N model 79100 00 79100 10 79100 12 amp 79100 14 8A e Nominal amperage for 230V RapidVap N model 79100 01 79100 11 79100 13 amp 79100 15 4A Frequency all models 50 60 Hz Phase Single Heater power 1000 watts Lid heater power 40 watts Product Service Domestic 1 800 522 7658 International 816 333 881
35. carrier Labconco Corporation and its dealers are not responsible for shipping damages The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen 15 days of delivery Limitation of Liability The disposal and or emission of substances used in connection with this equipment may be governed by various federal state or local regulations All users of this equipment are required to become familiar with any regulations that apply in the user s area concerning the dumping of waste materials in or upon water land or air and to comply with such regulations Labconco Corporation is held harmless with respect to user s compliance with such regulations Contacting Labconco Corporation If you have questions that are not addressed in this manual or if you need technical assistance contact Labconco s Customer Service Department or Labconco s Product Service Department at 1 800 821 5525 or 1 816 333 8811 between the hours of 7 00 a m and 6 00 p m Central Standard Time Part 7490100 Rev G ECO E465 TABLE OF CONTENTS CHAPTER 1 INTRODUCTION About This Manual Typographical Conventions Your Next Step CHAPTER 2 PREREOUISITES Electrical Requirements Location and Exhaust Reguirements Vacuum Pump Requirements Vacuum Line Traps Nitrogen Supply Requirements Space Requirements Tools Required Your Next Step CHAPTER 3 GETTING STARTED Unpacking Your RapidV
36. dVap N Sample position not activated Nozzle clogged Valve inoperable Gas flows Valve inoperable continuously Control inoperable CORRECTIVE ACTION Install new supply of gas Activate position per page 30 Unplug nozzle with fine wire Contact Labconco Contact Labconco Contact Labconco 52 Product Service Domestic 1 800 522 7658 International 816 333 8811 APPENDIX A Rapid VAP VACUUM AND RaPiDVaP N COMPONENTS The following pages list components that are available for your RapidVap The parts shown are the most common replacement parts If other parts are required contact Product Service Product Service Domestic 1 800 522 7658 International 816 333 8811 53 Appendix A RapidVap Vacuum and RapidVap N Components RapidVap Vacuum and RapidVap N Components Switch Power Foot Fan Cooling PCB Main RapidVap Vacuum PCB Main RapidVap N amp RapidVap N gt 48 PCB Main RapidVap Vacuum w RS232 PCB Main RapidVap N amp RapidVap N 48 w RS232 Isolator Upper Isolator Lower Cord Power 115V Cord Power 230V Triac Diode Bridge Belt Motor 54 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix A RapidVap Vacuum and RapidVap N Components Product Service Domestic 1 800 522 7658 International 816 333 8811 55 Appendix A RapidVap Vacuum and RapidVap N Components RapidVap Vacuum Components 21 Temperature
37. e cross bar clockwise approximately 1 8 lift the lid and remove the samples 14 Any time the RapidVap is not in operation the power switch should be turned OFF This will prolong the life of the cooling fan and the blower in the RapidVap N2 Operational Notes The LCD display conveys various pieces of information When the RapidVap is turned on the RapidVap will return to the same mode RUN or STOP that it was in when the power was turned off If the RapidVap was in the RUN mode when the power was turned off when the power is turned on the RapidVap will attempt to return to the programmed set points If the previous run is to be duplicated it 1s important to press the program set point button prior to pressing run This will show all the set points for that program and will reset the timer back to the programmed set point Without pressing the program set point button the time will not be reset and will continue to count down from the time at which it was stopped Interrupting a Cycle After it Has Begun At any time during a run the cycle may be stopped by pressing the STOP button This shuts off all operating functions After the chamber stops oscillating the latches may be unlatched and the lid opened If it 1s necessary to re start the RapidVap close the lid and 40 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap secure the latches and press RUN The RapidVap will
38. eight 9 Ibs 75384 00 Secondary Vacuum Trap 7 7 8 h x 6 5 8 diameter with 1 2 vacuum connections Volume of inner pot holds 1 8 liters of dry ice and alcohol Ice trapping capacity is 200 ml Shipping weight 5 lbs 74865 00 Lid Heater Includes glass lid with heater attached 78734 00 Liquid Trap Capable of trapping 2 550 ml 79705 00 Liquid Trap Capable of trapping 240 ml Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix D RapidVap Accessories The following accessories are available for the RapidVap Li N PART DESCRIPTION Du 74864 00 Block 8 170 ml tubes Order tubes from Labconco 79270 00 Sample Tube Flat Bottom Borosilicate glass 170 ml capacity Package of one 1 79271 08 Sample Tube Flat Bottom Borosilicate glass 170 ml capacity Package of eight 8 79266 00 Sample Tube End Point Stem 1 5 ml Borosilicate glass 170 ml capacity Package of one l 79269 08 Sample Tube End Point Stem 1 5 ml Borosilicate glass 170 ml capacity Package of eight 8 79092 00 Sample Tube Flat Bottom Borosilicate glass 600 ml capacity Package of one 1 79134 08 Sample Tube Flat Bottom Borosilicate glass 600 ml capacity Package of eight 8 79259 00 Sample Tube End Point Volume 0 5 ml Borosilicate glass 600 ml capacity Package of one 1 79260 08 Sample Tube End Point Volume 0 5 ml Borosilicate glass 600 ml cap
39. emp 50 C 80 C DG 40 C 40 C 40 C Starting Volume 10 ml 17 23 24 49 18 20 8 14 21 21 6 11 18 18 4 9 15 14 2 5 9 8 Number of samples 48 Vortex speed 100 Nitrogen pressure 20 psi Product Service Domestic 1 800 522 7658 International 816 333 8811 13 Appendix C RapidVap Specifications 74 Product Service Domestic 1 800 522 7658 International 816 333 8811 ApPpenDix D RAPIDVAP Accessories This following accessories are available for the RapidVap Vacuum model PART DESCRIPTION 74913 00 Block 110 12 mm dia tubes 74858 00 Block 110 13 mm dia tubes 74914 00 Block 69 16 mm dia tubes 74963 00 Block 69 15 ml centrifuge tubes m re Package of one 1 Product Service Domestic 1 800 522 7658 International 816 333 8811 15 Appendix D RapidVap Accessories 76 PART DESCRIPTION 79134 08 79270 00 79271 08 Sample Tube Flat Bottom Borosilicate glass 600 ml capacity Package of eight 8 Sample Tube Flat Bottom Borosilicate glass 170 ml capacity Package of one 1 Sample Tube Flat Bottom Borosilicate glass 170 ml capacity Package of eight 8 Vacuum Pump Diaphragm pump corrosion resistant 115V 60 Hz 3 3 amps single phase 42 liters per minute 207 mbar max vacuum For use with non flammable solvents only Vacuum Pump Diaphragm pump corrosion resistant 220V 50 Hz 1 5 amps single phase 36 liters per minute 207 mbar
40. entered set point will be stored in memory To reset the timer to the previous set point time the PROG set point button must be pressed Change the Vacuum set point Vacuum model only To change the vacuum set point press the set point select button directly under the word VACUUM An arrow will point to the last entered vacuum set point The vacuum level may be set between 0 to 999 mBar by pressing the increase or decrease buttons Above 999 mBar the display will show HI With a HI setting the vacuum pump will not operate The last entered set point will be stored in memory Keep in mind that even though a deep vacuum set point may be entered the actual vacuum level that the RapidVap will Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap try to maintain can be no deeper than the vacuum level that the vacuum pump can maintain Select the number of samples that will be run RapidVap N only Press the set point select button under the word SAMPLE An arrow will point to the last entered set Li point By pressing the increase or decrease button the number of samples or clusters may be changed from 2 to 4 to 6 to 8 When running less than eight samples in the RapidVap Nz or 48 samples in the RapidVap N2 48 be sure to position them as described in the previous paragraph Loading Glassware Into the RapidVap Operating The RapidVap Never lift the l
41. equired This outlet requires a 15 Amp circuit breaker or fuse for models rated at 115V 60 Hz or an 8 Amp circuit breaker or fuse 1s required for 230V 50 60 Hz models 115V models are equipped with a 20 Amp NEMA 5 20P plug 230V models are equipped with a 16 Amp CEE 7 7 plug It may be necessary to remove the plug and install a different plug to match the available receptacle Location and Exhaust Requirements The RapidVap Vacuum Evaporation System should be located within a fume hood if hazardous or flammable solvents are used In all cases regardless of the solvent used it is strongly recommended that the vacuum pump is located and vented in a fume hood The RapidVap N Evaporation System should be located within a fume hood if hazardous or flammable solvents are used In all cases regardless of the solvent used it is recommended that the exhaust hose is vented into a fume hood or other laboratory ventilation device 6 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 2 Prerequisites Vacuum Pump Requirements A vacuum pump must be provided by the user For most applications it is recommended that the vacuum pump is capable of a free air flow of 88 L min and 29 0 inch Hg 31 mbar vacuum although in some applications other pumps may be satisfactory or be required The inlet fitting on the vacuum pump must be suitable for 0 50 I D hose Biological samples for example are often dissolved
42. er utilizes nitrogen as an aid to evaporation Each model is available for operation on 115V or 230V Superior evaporation rates are achieved by the unique blending of several gentle forces on the sample Samples are subjected to a gyrating motion causing the liquid to form a vortex configuration which greatly increases the surface area and hence the ability to evaporate A precisely controlled amount of thermal energy can be supplied to the sample to heat it In the vacuum model the sample can be subjected to a decreased pressure by the application of a regulated vacuum In summary the vacuum model RapidVap performance is maximized by increasing the sample s surface area increasing temperature and decreasing pressure In the RapidVap No a stream of nitrogen or dry gas is directed downward onto the surface of the sample This reduces the partial pressure directly over the liquid to speed evaporation and helps remove the solvent as it evaporates In summary the RapidVap N gt performance is maximized by increasing the sample s surface area increasing temperature and directing gas over the sample Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 1 Introduction The gyrating motion imparted to the sample causes other more subtle effects to occur Excellent mixing of the components in the liquid sample is obtained Also as the liguid forms the vortex shape a centrifugal force is established which forc
43. es the liguid outward against the tube walls This helps prevent bumping and in turn allows the evaporation rate to be optimized The microprocessor which controls the operation of the heater and the motor provides excellent regulation and reproducibility of protocols The end of the run can be signaled by the automatic end point system or by a manually preset timer Nine different protocols can be stored in memory so exact test parameters can be easily repeated About This Manual This manual is designed to help you learn how to install use and maintain your RapidVap Instructions for performing routine maintenance and making minor modifications to your RapidVap are also included Chapter I Introduction provides a brief overview of the RapidVap explains the organization of the manual and defines the typographical conventions used in the manual Chapter 2 Prerequisites explains what you need to do to prepare your site before you install your RapidVap Electrical and exhaust reguirements are discussed as well as vacuum pump or nitrogen requirements Chapter 3 Getting Started contains the information you need to properly unpack inspect install and test your RapidVap Chapter 4 Using Your RapidVap discusses the basic operation of your RapidVap Information on how to arrange the samples inside your RapidVap and select an operating cycle 1s included Chapter 5 Maintaining Your RapidVap explains how to perform routine mainte
44. f one or two positions are to be run samples must be positioned at locations identified 2 If three or four positions are to be run samples must be positioned at locations identified 4 If five or six positions are to be run samples must be positioned at locations identified 6 If seven or eight positions are to be run samples may be positioned at any of the locations When using the RapidVap N 48 glassware may be placed anywhere within the activated cluster of nozzles Product Service Domestic 1 800 522 7658 International 816 333 8811 KI 27 Chapter 4 Using Your RapidVap o 9 Q Q ACTIVE N POSITIONS QO e Heat Setting Guidelines The evaporation rate achieved by the RapidVap is dependent upon a variety of factors These include the nature of the solvent the temperature the pressure in the vacuum system or the flow of the nitrogen gas in the RapidVap N gt the volume of sample shape of tubes and vortex speed Because of the multiplicity of factors it is impossible to give typical performance data By design the RapidVap Vacuum model can be run at lower temperature settings than the RapidVap N2 model This is because the decrease in pressure will cause the sample to evaporate at a lower temperature As a general guideline to speed the evaporation process the RapidVap temperature should be set as high as possible as long as the temperature will not damage the sample or cause the sample
45. fer grease supplied with the RapidVap to the end of the temperature sensor probe that extends up from the bottom of the chamber Position the block over the three studs in the chamber Install the flat washers and nuts or manifold guide rods Tighten securely Installing the Optional Lid Heater If a Lid Heater is to be added by the user first disconnect the main power cord to the RapidVap Then remove the existing lid by removing the two screws that hold either the RH or LH hinge pivot support bracket Remove the bracket and then slide the lid assembly off of the other bracket Install the new lid with the heater attached by reversing the process Plug the jack attached to the lid heater into the receptacle on the back of the RapidVap The lid heater will operate any time the main power switch is on CHAPTER 7 TROUBLESHOOTING Refer to the following if your RapidVap fails to operate properly If the suggested corrective actions do not solve your problem contact Labconco for additional assistance The following failure codes may appear on the display when problems are sensed by the internal self check routine DISPLAY CAUSE ERROR CODE Top Temp Sensor Top sensor failure Connection failure Bottom Temp Bottom sensor Sensor failure Connection failure Vacuum Sensor Sensor failure Connection failure Lid Opened Lid open Switch failure Connection failure CORRECTIVE ACTION Replace top sensor assembly
46. he RapidVap will respond to this command with a pev numeric value as follows indicates an endpoint has been reached 0 endpoint has not been reached The RapidVap will respond to this command with a numeric value as follows O lt all functions are normal 1 lid is open 2 communication problem 3 and later numbers will be established later as specific error messages Note When controlling the RapidVap using the RS 232 link all control parameters will be entered into program 9 Note All of the above commands can be sent with no numeric value that is command without value to read out the setpoint and actual value without changing the setpoint Note There is no command for the vacuum release button on the front panel since this button is momentary in nature the V0000 command will bleed the vacuum chamber to atmospheric pressure Note The above commands can be sent at a maximum rate of one command per second Product Service Domestic 1 800 522 7658 International 816 333 8811 43 Chapter 4 Using Your RapidVap RS 232 Hardware Required The connecting cable Labconco 7484800 is supplied with the unit and is wired as shown below COMPUTER r TITT Lot RAPIDAV AP TERMINAL SCHEMATIC NOTE CONNECTOR VIEWS ARE FROM FRONT CONTACT SIDE 44 Product Service Domestic 1 800 522 7658 International 816 333 8811 CHAPTER B MAINTAINING YOUR RAPIDVAP
47. id if the block is moving Samples may splash out Never attempt to reach into the chamber if the block is moving 1 Turn the power switch ON 2 Select a program or set the set point parameters 3 Turn on the nitrogen RapidVap N gt only 4 Preheat the block if desired 3 Place samples in vials Normally the vials should be no more than half full 6 Load sample vials in the chamber 7 Close the lid On RapidVap N gt 48 models press down and rotate the cross bar on the top of the lid counter clockwise approximately 1 8 8 Swing both latches over the lid and tighten both knobs Do not over tighten 9 Press RUN If the display was showing set point parameters it will change to show actual parameters Press RUN again The S STOP in the display will change to R RUN 10 Set point parameters can be altered at any time during a run by first selecting the parameter using the appropriate set point select button and then pressing the Increase or Decrease switch Product Service Domestic 1 800 522 7658 International 816 333 8811 39 Chapter 4 Using Your RapidVap 11 If the time set point is used at the end of the set time an alarm will sound All operating functions will cease 12 Press STOP to terminate operation if the RapidVap has not already stopped itself 13 When the evaporation is complete allow the chamber to stop moving unlatch the latches on the RapidVap N2 48 models rotate th
48. in water a high boiling point solvent and are often heat liable Such samples require the high vacuum achievable with a mechanical vacuum pump usually with an ultimate vacuum of 1 3 x 107 mBar to achieve a good evaporation rate On the other hand samples dissolved in methylene chloride a low boiling point solvent can be efficiently concentrated using a water aspirator The nomograms in Chapter 4 Using Your RapidVap will help determine the boiling point of a solvent at pressures below atmospheric This can serve as a guide to the appropriate vacuum source TO INSURE THAT AGGRESSIVE SAMPLES USED IN THE RAPIDVAP DO NOT DAMAGE THE VACUUM PUMP IT IS RECOMMENDED THAT ALL INTERNAL WETTED PARTS ARE TEFLON OR TEFLON COATED TO PREVENT A HAZARDOUS CONDITION THE PUMP MUST BE SUITABLE FOR HANDLING THE VAPORS FROM THE SOLVENTS THAT WILL BE EVAPORATED IN THE RAPIDVAP Product Service Domestic 1 800 522 7658 International 816 333 8811 7 Chapter 2 Prerequisites 8 Product Service Domestic 1 800 522 7658 International 816 333 8811 CAUTION When selecting the HU vacuum pump it is very important to consider the flammability of the solvents that will be used If the solvents are flammable an explosion proof vacuum pump is recommended Vacuum Line Traps When using a mechanical pump which is not corrosion resistant a trap must be used in the vacuum line to prevent damage from solvent vapors This is most often a condense
49. l times must be determined by the user The RapidVap can be set to alarm after a preset period of operation When the time expires the RapidVap will give an audible alarm and turn off all functions RapidVap Controls The control panel for the RapidVap vacuum model and the RapidVap Nz are shown below with a description about their function RapidVap Vacuum Model C MINUTES PROG SPEED HEAT TIME S ma me O INCR DECR RUN STOP VACUUM RELEASE ii a am Product Service Domestic 1 800 522 7658 International 816 333 8811 35 Chapter 4 Using Your RapidVap RapidVap N Model C MINUTES PROG SPEED HEAT TIME SAMPLE om INCR DECR RUN STOP 3 PRE HEAT 1 Display The liquid crystal display LCD shows set point parameters and actual measured conditions 2 Set Point Select Button To select a parameter to change press the set point select button directly below the parameter 3 Run Stop Button Used to start or stop a run 4 Decrease Button When pressed the last selected set point will decrease 5 Increase Button When pressed the last selected set point will increase 6 Preheat Button Used to turn on the heaters to preheat the sample block prior to loading samples When pressed during a run it will switch the end point alarm from audible to muted or back to audible The audible alarm is the default mode when the RapidVap is powered up 7 Vacuum Release V
50. llow safe lifting guidelines Product Service Domestic 1 800 522 7658 International 816 333 8811 11 Chapter 3 Getting Started The United States Interstate Commerce Commission rules reguire that claims be filed with the delivery carrier within fifteen 15 days of delivery Unpacking Your RapidVap Carefully unpack your RapidVap and inspect it for damage that may have occurred in transit If your RapidVap is damaged notify the delivery carrier immediately and retain the entire shipment intact for inspection by the carrier DO NOT RETURN GOODS WITHOUT THE PRIOR AUTHORIZATION OF LABCONCO UNAUTHORIZED RETURNS WILL NOT BE ACCEPTED IF YOUR RAPIDVAP WAS DAMAGED IN TRANSIT YOU MUST FILE A CLAIM DIRECTLY WITH THE FREIGHT CARRIER LABCONCO CORPORATION AND ITS DEALERS ARE NOT RESPONSIBLE FOR SHIPPING DAMAGES Do not discard the carton or packing material for your RapidVap until you have checked all of the components and installed and tested the RapidVap RapidVap Components As previously mentioned Labconco manufactures two types of RapidVap the Vacuum and the Nitrogen models Each model is available in 115V or 230V The different RapidVap models require different assembly components Locate the model of RapidVap you received in the following tables Verify that the components listed are present and undamaged 12 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 3 Getting Started
51. lows the solvent in all sample tubes to evaporate out of the large upper chamber before any of the small chambers are completely evaporated dry providing that all sample tubes are filled with nearly the same starting volumes Product Service Domestic 1 800 522 7658 International 816 333 8811 33 Chapter 4 Using Your RapidVap UNSCONCO 450ml b in lo Cool Zone When it is necessary to end the concentration process with the sample still dissolved in a small amount of solvent the time function should be activated and the process time set to allow the solvent sufficient time to evaporate completely out of the large upper portion of the sample tube and into the small lower portion Cool Zone This time can be approximated by knowing the starting sample size the desired end point volume the stem size of the sample tube used and the solvent The tables in Appendix C RapidVap Specifications indicate the approximate time required to evaporate various common solvents Actual times must be determined by the user When the set time has expired the RapidVap N will give an audible alarm and turn off all RapidVap functions un sla ead Bal I I I i i 34 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap The tables in Appendix C RapidVap Specifications indicate approximate times reguired to evaporate various common solvents Actua
52. max vacuum For use with non flammable solvents only Vacuum Pump Diaphragm pump corrosion resistant 115V 60 Hz 10 8 amps single phase 88 liters per minute 31 mbar max vacuum For use with non flammable solvents only Vacuum Pump Diaphragm pump corrosion resistant 230V 50 Hz 4 0 amps single phase 74 liters per minute 31 mbar max vacuum For use with non flammable solvents only Vacuum Pump Diaphragm pump corrosion resistant explosion proof 120V 60 Hz 5 8 amps single phase 42 liters per minute 207 mbar max vacuum Vacuum Pump Diaphragm pump corrosion resistant explosion proof 220V 50 Hz 3 1 amps single phase 36 liters per minute 207 mbar max vacuum Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix D RapidVap Accessories PART DESCRIPTION 14721 00 78153 00 78148 00 78149 00 Product Service Domestic 1 800 522 7658 International 816 333 8811 Vacuum Pump Diaphragm pump corrosion resistant explosion proof 115V 60 Hz 5 8 amps single phase 88 liters per minute 31 mbar max vacuum Vacuum Pump Diaphragm pump corrosion resistant explosion proof 220V 50 Hz 3 1 amps single phase 74 liters per minute 31 mbar max vacuum Vacuum Pump Two stage direct drive pump 115 VAC 60 Hz 6 8 amps single phase 195 liters per minute 2 x 10 mbar max vacuum For use with non flammable solvents only Vacuum Pump Two stage direct drive pump 220 208 23
53. n with this eguipment may be governed by various Federal State or local regulations All users of this eguipment are urged to become familiar with any regulations that apply in the user s area concerning the dumping of waste materials in or upon water land or air and to comply with such regulations Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 3 Getting Started Your Next Step The installation and setup of your RapidVap is now complete To learn how to load and operate your RapidVap proceed to Chapter 4 Using Your RapidVap To make a modification to the configuration of your RapidVap proceed to Chapter 6 Modifying your RapidVap To perform additional diagnostics on your RapidVap proceed to Chapter 7 Troubleshooting To learn about the maintenance reguirements for your RapidVap proceed to Chapter 5 Maintaining Your RapidVap Product Service Domestic 1 800 522 7658 International 816 333 8811 21 Chapter 3 Getting Started 22 Product Service Domestic 1 800 522 7658 International 816 333 8811 CHAPTER 4 Using YOUR RAPID VAP After your RapidVap has been installed as detailed in Chapter 3 Getting Started you are ready to begin using your RapidVap Read this chapter to learn how to e set operating parameters e operate the controls e properly select and position glassware inside your RapidVap e understand the display e interrupt a cycle after it has
54. nance on your RapidVap 2 Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 1 Introduction Chapter 6 Modifying Your RapidVap describes how to install other blocks and the optional lid heater Chapter 7 Troubleshooting contains a table of problems you may encounter while using your RapidVap including the probable causes of the problems and suggested corrective actions Appendix A RapidVap and RapidVap Nz Components contains labeled diagrams of the components of the RapidVaps Appendix B RapidVap Dimensions contains comprehensive diagrams showing the dimensions for the RapidVap and RapidVap No Appendix C RapidVap Specifications contains product specifications Wiring diagrams for both the 115V and 230V RapidVaps are also included Appendix D RapidVap Accessories lists the part numbers and descriptions of all of the accessories available for your RapidVap Typographical Conventions Recognizing the following typographical conventions will help you understand and use this manual e Book chapter and section titles are shown in italic type e g Chapter 3 Getting Started e Steps required to perform a task are presented in a numbered format e Comments located in the margins provide suggestions reminders and references e Critical information is presented in boldface type in paragraphs that are preceded by the exclamation HU icon Failure to comply with the information following an e
55. new protocol it may me helpful to make a trial run that is void of the sample you are attempting to concentrate Determine if the sample which 1s to be processed will be allowed to go to dryness or whether the evaporation is to cease prior to dryness If the process should not go to dryness the proper sample tubes must be selected to allow the desired amount of solvent to remain in the tubes Sample tubes are available for various end point volumes Refer to Appendix D Accessories for available sample tubes Any style ground glass tube may be used if the sample is to go to dryness however flat bottom tubes evaporate the quickest Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 4 Using Your RapidVap Glassware Selection and Speed Setting Guidelines The speed at which the sample block should oscillate 1s dependent on the sample tube size and the sample volume Generally the tube should be no more than half full The faster the speed the higher the sample will vortex giving a maximum surface area and therefore a maximum evaporation rate However if the speed is too fast samples will raise above the top of the tube and be lost Smaller tubes can be run faster than larger tubes The following table gives recommended safe speeds for tubes loaded with water Experimentation with the specific sample may determine faster speeds When setting the speed keep in mind that the sample will raise up slightly in the
56. or two way that is it will allow the RapidVap Basic and N models to be controlled externally incoming commands as well as provide status information coming out of the RapidVap outgoing status All communications will be done in standard ASCII format using the programming syntax below Product Service Domestic 1 800 522 7658 International 816 333 8811 41 Chapter 4 Using Your RapidVap RS 232 Programming Syntax The RapidVap only responds to commands sent by the connected computer or terminal it does not send out commands on its own The programming syntax has two forms 1 command abbreviation letter value when the command requires a numeric value 2 command abbreviation letter when the command does not require a numeric value When the programming syntax contains a numeric value it will change the operation of the RapidVap When the programming syntax does not contain a numeric value the RapidVap will respond with its current status for that command value Note that the lead in character is while the brackets are shown only to separate parameters for ease of understanding These brackets will not be used in the actual ASCII command string Finally the is used to indicate the end of acommand Also note that An indicates a newline character R x x 0 for stop x 1 for run and x 2 for pre heat will get a x n response for confirmation when a R with no x
57. or the RapidVap NI N 48 PART DESCRIPTION 74821 00 Block 48 12 x 75 mm tubes 74822 00 Block 48 13 x 100 mm tubes 74823 00 Block 48 16 x 150 mm tubes Product Service Domestic 1 800 522 7658 International 816 333 8811 81 Appendix D RapidVap Accessories 82 Product Service Domestic 1 800 522 7658 International 816 333 8811 DECLARATION OF CONFORMITY Application Council Directive s 73 23 EEC 89 336 EEC 2002 95 EC ROHS 2002 96 EC WEEE 2004 108 EC Standard s to which conformity is declared EN61010 1 EN61326 1 EN55022 EN61000 3 2 3 Manufacturer s Name Labconco Corporation Manufacturer s Address 8811 Prospect Avenue Kansas City MO 64132 USA Importer s Name See Shipping Customs Documents Importer s Address See Shipping Customs Documents for your equipment Type of Equipment Laboratory Equipment Sample Preparation Model No RapidVap N 79100 01 79100 13 79100 11 79100 15 RapidVap 79000 01 79000 11 79000 03 79000 13 Serial No Various See Individual Declaration Year of Manufacture 1996 and Subseguent I the undersigned hereby declare that the equipment specified above conforms to the above Directive s and Standard s See individual Declaration of Conformity which will be signed by the importer for your country Place Signature Date Full Name Position Labconco P N 36960 08 Rev C ECO E465 Product Service Domestic 1
58. r type trap chilled with dry ice acetone When evaporating acids it is advisable to include a soda lime acid trap in the vacuum line This adds additional protection for the pump Several components within the RapidVap are made from stainless steel and can be degraded if exposed to acids Before evaporating acids be sure to contact Labconco A moisture trap and radioisotope trap are also available When evaporating high boiling point solvents a liquid trap should be positioned between the RapidVap and the vacuum pump to prevent liquid from entering the pump Refer to Appendix D RapidVap Accessories for ordering information Nitrogen Supply Requirements The 1 4 I D hose on the rear of the RapidVap Nz must be attached to a source of nitrogen or other suitable gas Pressure must NOT exceed 20 psi A regulator must be supplied by the user The nitrogen supply must be capable of 0 6 CFM flow rate for the 8 place RapidVap Nz The RapidVap N2 48 requires a flow rate of 3 5 CFM A suitable barb or compression fitting must be supplied by the user Chapter 2 Prerequisites Space Requirements Refer to Appendix C RapidVap Specifications for dimensional drawings of the RapidVap Tools Required Common hand tools are required to set up the RapidVap A screwdriver or 5 16 socket is needed to attach hose clamps A tubing cutter or knife is needed to shorten exhaust hoses If the sample block must be installed or exchanged at
59. re compatible with these temperatures Do not evaporate solvents that have an autoignition temperature below 180 C Do not evaporate solvents that are classified as Group A B or C by the National Electrical Code Evaporate only non flammable or Group D solvents with autoignition temperatures 180 C or above Use of other compounds could cause an explosion Product Service Domestic 1 800 522 7658 International 816 333 8811 19 Chapter 3 Getting Started 20 Solvents used in the RapidVap may be flammable or hazardous Use extreme caution and keep sources of ignition away from the solvents When using flammable or hazardous solvents both the RapidVap and the vacuum pump should be operated inside a fume hood If a sample is spilled in the chamber it must immediately be cleaned up Hazardous materials such as strong acids or bases radioactive substances and volatile organics must be handled carefully and promptly cleaned up if spilled Several components of the RapidVap which are located inside the chamber are made of stainless steel which can be attacked by acids Use of acids such as trifluoroacetic acid can result in degradation of the product and the vacuum pump if the vacuum system is being used Use care when using aggressive liguids which can damage the RapidVap and thoroughly clean the RapidVap after each use Contact Labconco before evaporating acids WARNING The disposal of substances used in connectio
60. taching nuts on the RapidVap Vacuum and RapidVap N gt require a 7 16 socket The manifold guides which secure the block on the RapidVap N2 48 require a 9 16 socket Your Next Step After you have determined that the location for your RapidVap accommodates the installation and operational requirements you are ready to unpack and install your RapidVap Proceed to Chapter 3 Getting Started Product Service Domestic 1 800 522 7658 International 816 333 8811 9 Chapter 2 Prereguisites 10 Product Service Domestic 1 800 522 7658 International 816 333 8811 CHAPTER 3 GETTING STARTED Now that the site for your RapidVap is properly prepared you are ready to unpack inspect install and test your RapidVap Read this chapter to learn how to e unpack and move your RapidVap set up your RapidVap connect the vacuum pump or nitrogen source to your RapidVap e connect the electrical supply source to your RapidVap e properly exhaust your RapidVap calibrate the vacuum sensor solvent safety precautions Depending upon which model of RapidVap you are installing you will need common hand tools including a flat blade screw driver a 7 16 socket and an adjustable wrench to complete the instructions in this chapter The RapidVap weighs over 70 Ibs 33 Kg The carton allows for lifting with a mechanical lift truck or hand truck If you must lift the RapidVap manually use at least two 2 persons and fo
61. the hose to prevent kinks Clamp all connections securely Plug the pump into the pump receptacle on the back of the unit and turn the pump switch on if it is so equipped When evaporating high boiling point solvents a liquid trap should be positioned between the RapidVap and the vacuum pump to prevent liquid from entering the pump It is recommended that the vacuum pump is located inside a fume hood If that is not possible the exhaust of the Product Service Domestic 1 800 522 7658 International 816 333 8811 Chapter 3 Getting Started pump should be directed to a laboratory fume hood or other laboratory ventilation device Vacuum pump power connection Optional vacuum pump exhaust hose to ventilation device ys a FOG Vacuum pump x gt a A inlet fitting Vacuum hose Clamp all connections Optional liguid trap or chilled trap or secondary trap Sample Block If the Rapid Vap was not shipped with the sample block installed then it must be installed by the user The sample block must be securely attached to its mounting plate Note the asymmetric hole pattern of the three thru mounting holes Locate the three flat washers either nuts or manifold guides that were shipped with the RapidVap The RapidVap Vacuum uses nuts while the RapidVap N gt 48 uses guide rods Apply a small amount of heat transfer grease that was shipped with the RapidVap to the end of the temperature sensor probe that extends up from the
62. us common solvents Tables A and B show the average time required to evaporate 8 samples from the selected beginning volume to a level where the solvent is at the top of the Cool Zone stem Tables C shows the average time to evaporate various solvents in different length Cool Zone stems It shows the average time for solvents to evaporate from the top of the stem to the indicated remaining volume when 8 vials are run simultaneously The following example illustrates the use of the charts Assume that a starting volume of 300 ml methylene chloride 1s placed in a 600 ml sample vial with a 1 5 ml stem The vial is covered with a cap The desired endpoint volume is 0 5 ml From Table A the time to evaporate to the top of the stem is 59 minutes From Table C the time to Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C RapidVap Specifications evaporate from the top of the stem to 0 5 ml is 17 minutes Adding the two times together the total time to evaporate 300 ml of methylene chloride to 0 5 ml in a sample tube with a 1 5 ml stem is approximately 76 minutes If fewer than eight samples are run at a time the time to evaporate will become shorter Table A ki Evaporation Time in Upper Portion of Sample Vial 600 ml Sample Tubes Time in Minutes Methylene Ethyl Solvent Chloride Acetate Hexanes Acetone Toluene Water Block Preheat amp Block Set Point Temperature 40 C 75 C 70 C 59 C 100 C 9
63. ust Hose 19660 00 One 1 Clamp 79255 00 Eight 8 Sample Tube Caps 13364 00 Power Cord 115V or 13365 00 Power Cord 230V 12556 00 Heat Transfer Grease 74901 00 User s Manual 74848 00 Cable Assembly RS232 Models 79100 10 11 Product Service Domestic 1 800 522 7658 International 816 333 8811 13 Chapter 3 Getting Started 14 Catalog RapidVap Description 79100 12 RapidVap N 48 Evaporation System 115V 79100 13 RapidVap N 48 Evaporation System 230V 79100 14 RapidVap N 48 Evaporation System 115V with RS 232 Interface 79100 15 RapidVap N 48 Evaporation System 230V with RS 232 Interface Plus the Following Part Component Description 79131 01 Exhaust Hose 19660 00 One 1 Clamp 13364 00 Power Cord 115V OT 13365 00 Power Cord 230V 12556 00 Heat Transfer Grease 74901 00 User s Manual 74488 00 Manifold Guide 3 19116 00 Washer 3 74848 00 Cable Assembly RS232 Models 74100 14 15 If you do not receive one or more of the components listed for your RapidVap or if any of the components are damaged contact Labconco Corporation immediately for further instructions Setting Up Your RapidVap After you verify the RapidVap components move your RapidVap to the location where you want to install it Then follow the steps listed below Vacuum Pump Connection Connect the pump inlet to the fitting at the right hand rear corner of the RapidVap using the hose and clamps provided Route
64. xclamation icon may result in injury to the user or permanent damage to your RapidVap Product Service Domestic 1 800 522 7658 International 816 333 8811 3 Chapter 1 Introduction e Important information is presented in capitalized type in paragraphs that are preceded by the pointer icon It is imperative that the information contained in these paragraphs be thoroughly read and understood by the user e Information that is specific to a particular model of RapidVap is preceded by a letter icon The V icon indicates the text is specific to the Vacuum model The N icon indicates the text is specific to the RapidVap N gt model Your Next Step If your RapidVap needs to be installed proceed to Chapter 2 Prereguisites to ensure your installation site meets all of the reguirements Then go to Chapter 3 Getting Started for instructions on how to install your RapidVap and make all of the necessary connections For information on the operational characteristics of your RapidVap go to Chapter 4 Using Your RapidVap If your RapidVap is installed and you need to perform routine maintenance on the RapidVap proceed to Chapter 5 Maintaining Your RapidVap For information on making modifications to the configuration of your RapidVap go to Chapter 6 Modifying Your RapidVap Refer to Chapter 7 Troubleshooting if you are experiencing problems with your RapidVap 4 Product Service Domestic 1 800 522 7658 International 816 333

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