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MAINTENANCE AND USER`S MANUAL

1. Introduce the sample n N Type in the expected temperature Select method A or B or Test start Up Test parameter check out Gas flame ignition Tune up the spark intensity Atmospheric pressure introduction or if manual mode 760 mmHg Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC Bitumen method Sample preheating temperature introduction see 7 1 1 Test start Up Flame dipping or heating spark at expected temperature X 18 up to safety Flash point detection Yes YES Alarm Buzzer Acquisition buzzer End of the test Koehler Instrument Company Inc Automatic buzzer 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen
2. Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC VIII PRINTING RESULTS 8 1 TYPES OF PRINTERS e Ticket printer delivered with the instrument e All types of 80 column printers except laser printer 8 2 PRINTING CURRENT TEST RESULTS Automatic right after the end of test buzzer alarm 8 3 PRINTING PREVIOUS TEST RESULTS see chap VI Possibility of printing out results of the previous 100 tests when necessary 8 4 PRINTING TEMPERATURE SLOPE see chap VI software configuration see chap 11 2 9 Allows to follow up the sample temperature increase during the test print out every minute starting after 5 minutes 8 5 PRINT OUT EXAMPLES FLASH POINT PENSKY MARTENS ISO 2719 ASTM D 93 IP 34 85 App 3711 Date 1 12 1998 Time 15 36 Duration 48 08 Sample 236 Expected temperature 250 Method A Bar Corr 760 mmHg Nb of dips 32 Flash point 122 0 Corr Flash Point 122 1 C Flam Gas Flash NB OF DIPS gt 20 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Cu
3. lieler INSTRUMENT COMPANY INC Display of sample probe calibration values Allows to check up the conversion values of the probe calibration Point calibration In case of an unexpected loss of calibration values it s possible to type in a calibration by conversion point value Its also possible to type in a calibration value by conversion points previously edited on the lockbook A calibration through conversion points required for the low and high reference temperature to be entered 11 3 3 B BAROMETRIC PRESSURE see chap VI Physical calibration The physical calibration of the barometric pressure measurement system requires Either a device able to reach a 920 mbar pressure with a 1 mbar precision of 920 mbar 690 mmHg and a 1066 mbar see cap lll for connection Either a voltage generator able to provide a 4 345 V for 920 mbar and 4 877 for 1066 mbar see chap lll for connection A specific wire is also necessary Connect the pressure generator or the voltage one with the specific wire Apply a pressure equivalent to 920 mbar and press Enter key see figure 2 Apply a pressure equivalent to 1066 mbar and press Enter key see figure 2 A calibration refused message indicates a wrong calibration which has to be performed again Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 58
4. Buzzer Page 35 11 2 7 New software release Page 35 11 2 8 New password Page 35 11 2 9 Temperature slope print out Page 35 11 2 10 To guit the configuration process Page 35 11 3 Hardware configuration Page 36 11 3 1 Languages Page 36 11 3 2 Units Page 36 11 3 3 Calibration Page 36 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KEA INSTRUMENT COMPANY INC 11 3 3 A Sample probe Page 37 Physical calibration Page 38 Display probe calibration values Page 38 Point calibration Page 38 11 3 3 B Barometric pressure Page 38 Physical calibration Page 38 Display calibration value Page 39 Point calibration Page 39 11 3 3 C Pre test steps Page 39 Step calibration Page 39 Step display Page 39 11 3 3 D Electrical supply regulation Page 40 Physical calibration Page 40 Display of calibration point Page 40 Point calibration Page 40 11 3 4 Controls Page 41 11 3 4 A Analogic readings Page 41 11 3 4 B Logic I O checks Page 41 11 3 4 C Autodiagnostic Page 41 11 3 4 D Lock book print out Page 41
5. e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC IX SAFETY 9 1 PT100 PROBE ABSENCE When starting a test the instrument automatically checks out the presence or absence of the sample probe In case of absence the test can t be performed a warning message is displayed on the screen and a buzzer sounds 9 2 DEFAULT IN SAMPLE TEMPERATURE INCREASE The test automatically stops and a buzzer sounds when the recorded sample temperature remains unchanged after 10 min of test 9 3 ELECTRIC SAFETY An electric safety of the heating block is programmed in the factory at 550 C When the safety operates a sound alarm with the following displayed message High Safety appears To recover the normal functions of the tester it s necessary to switch off the instrument and to start it again If the problem keep on occurring the instrument has to be disconnected and the local distributor s maintenance department has to be contacted 9 4 SAMPLE TEMPERATURE SAFETY The sample temperature safety is determined by adding X degrees to the expected test temperature during the keyboard configuration procedure Limits are from 15 C to 99 C above the expected T A buzzer sounds when the sample temperature reaches 15 C under this limit It s then possible to modify the expected temperature to carry on the test
6. e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC KOEHLER INSTRUMENT COMPANY Cm mr E uer SO KH Le Ce HT KEY BOARD Cover START Ces rer SE CONG PREVIOUS UPLOADING N wem PREVIOUS OFFSET RESULT GASELECTR SE E sace rM sg LUCHOORRELA CONFIG SOFTE Lal L E im LL pewse EE ere CAURATON N BY KEYBOARD i UE BY KEY BOARD d a BY KEY BAORD E emm r BY KEY BOARD Key LIST ICHART Key SEARCH METHOD Lo a Note in any case except after entering data a pressure on NI key will provoke to return to the main screen or to the previous display Vil RUNNING A TEST FAN Handling liquid petroleum products or equivalent ones requires to wear protective gloves glasses and clothes Do not handle flammable products near a source or a flame Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KEA INSTRUMENT COMPANY INC 7 1 TESTING PROCESS Connect and switch on the instrument Prepare the sample cup and lid Set the stirring flexible See o
7. A buzzer sounds with a displayed message Safety Stop when this limit is reached acquisition by ACGBUZZER The test procedure is cancelled The programmed difference between the expected temperature and the safety temperature remains the same whatever the entered expected temperature Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC 9 5 GAS SAFETY Automatic cut off at the end of the test Message Gas Ignition with a sound alarm at the beginning of the test An optic flame detection operates during the test In case of flame absence during 30 sec the test is automatically stopped and a buzzer sounds Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC X INSTALLATION OF SOFTWARE UPDATE Switch on the instrument Enter the administration password in order to have access to new relea
8. INSTRUMENT COMPANY INC 7 1 1 Bitumen method e Aimed at viscous or thick samples at ambient temperature e_ Stirring and test will effectively start up when sample has reached the preheating temperature The stirring system can be severely damaged if the sample is not fluid enough or if the preheating temperature is too low 7 2 STARTING A TEST IN SEARCH MODE FOR A PRODUCT CORRESPONDING TO THE SPECIFICATIONS OF THE PENSKY MARTENS METHOD AND FOR WHICH THE FLASHPOINT IS UNKNOWN e Enter the expected T C e Enter a sample identification number by pushing on key e Start the test like in 7 1 The instrument carries on flame dipping as soon as the beginning of the test every 1 or 2 C The slope is automatically set up according to selected method Note for a larger search area without several selections of expected temperature it s possible to modify through keyboard the alarm and safety stop related to expected temperature 7 3 QUICK METHOD OUT OF STANDARD The method consists of performing tests with the A method on known samples with a temperature slope higher than 10 C min This method allows to rapidly approach the Flash Point value of the sample In order to get the correct value a second test with the standardized method is necessary Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800
9. Overflow in the cup emulsion 66 security flam ignition gas or electric 77 safety stop no detection 88 Flash on the first dip 99 Manual stop Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC XVII Chart of the functions ka jen 2 8 seess CALIB VIEW Lo ET BY KEY BOARD CALIBVIEW CES CAUBEY BATH BY KEY BOARD CALBVIEW Ex T E Es o 2 BY KEY BOARD ae if dur GER z o o ln o St si 8 S sel LL ERIE d amp lala HE T O IONSA T DET TCDETECT STIRRING 2 TESTFLAMTX LE TEST CONTINU SGASVALVE RACH 5 SPARKNGODL LW T PREVIOUS PRNTO_ OFFSET RESULT CET COOL STOPT Y CALIBRATION P L___ TESTS FEAT BLOCK FIRE SECURITY PR S BA RO MAINS VOLTAGE our 1 HEATING 2 EV WAT FAN PASSWORD PENSKY Vers on 47 EXIT BY r Key LIST CHART Key SEARCH METHOD Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www ko
10. XII INCIDENTS Page 42 XIII MAINTENANCE Page 43 13 1 Calibration Page 43 13 2 Controls Page 43 13 3 Cooling system scaling Page 43 XIV ACCESSORIES AND REFERENCES Page 44 14 1 Accessory parts Page 45 14 2 Optional accessories Page 45 XV KEY CONTACT Page 45 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen INSTRUMENT COMPANY INC I INTRODUCTION 1 1 SAFETY INSTRUCTIONS For any use of the instrument operators must have the following expertise e A good knowledge of manual petroleum testing methods and the experience of performing flash point tests e A good understanding of the risks associated with product and sample manipulation Manipulations of hot cup and cover are prohibited In case of absolute necessity manipulations have to be realized with utmost care In every case operators have to wear gloves glasses and protective safety clothes ___ 1 2 OPERATION INSTRUCTIONS Tests have to be exclusively performed e according to the methods described in the user s manual e with the accessories delivered and recommended in the user s manual e according the testing process and starting up proc
11. baths Wire for barometric pressure sensor Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC XVI YOUR KEY CONTACT Koehler Instrument Company 1595 Sycamore Avenue Bohemia NY 11716 Tel 1 631 589 3800 Fax 1 631 589 3815 info koehlerinstrument com Web http www koehlerinstrument com Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen INSTRUMENT COMPANY INC XV To put into service the electric ignition on the apparatus i e not using gas ignition KR Loosen the needle screw FT 4 Take off the ipe 21 om Put the electric ignition Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e
12. lower than 50 C and higher than 450 C are not acceptable 1 Connect the resistance box with the specific wire or in case of a complete calibration with two thermostatic baths connect the Pt 100 probe with the specific wire 2 Tune up the resistance box in order to get a low reference value i e 50 C see Figure 1 or dip the Pt 100 probe in a 40 C bath for example 3 Type in this low reference value in C and confirm with the enter key 4 Tune up the resistance box in order to get a high value i e 400 C see figure 1 or dip the Pt 100 probe in a 150 C bath for example 5 Type in this high reference value in C and confirm with the enter key A calibration refused message indicates a wrong calibration which has to be performed again Figure 1 C Ohms 0 100 50 119 4 100 138 5 150 157 32 200 175 84 250 194 08 300 212 03 350 229 69 400 247 06 To issue a lock book see chap VI and 11 3 4 D Information stored in the lock book could be used for a multiple point calibration in case of unexpected loss of calibration data Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing
13. power supply cable WARNING Connect the cooling system to a soft water supply or a drinking water supply Hard water may cause a premature limestone progressing In that case the cooling system efficiency is decreasing clean the cooling system with an anti limestone rinse vinegar anti limestone kettle Rinse the cooling system before using the tester Do not use acids since the pipes are made of copper Periodic preventive anti limestone treatments are recommended Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC 5 3 2 Front connections of the tester Connect the glass Pt100 probe the detection cable the lid mass spiral must correctly lean on the connector cable the thermocouple detection cable Use with electric ignition Set the electric spark in its stand The inserted ring is designed to correctly position the spark Connect the 2 spark wires with the 2 electrical supply given see schema Tune up the electrical supply potentiometer of the heating spark at 7 8 for the first run the heating spark is supplied with AC at low voltage Note A The use of the instrument with a heating spark absol
14. 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC 11 3 2 UNITS see chap VI Pressure and temperature units have to be selected on screen 11 3 3 CALIBRATIONS see chap VI Allow to calibrate temperature and barometric pressure measurement steps at the beginning of the test and the electric network image Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KEANE INSTRUMENT COMPANY INC 11 3 3 A SAMPLE PROBE see chap VI Physical calibration A resistance box simulating a Pt 100 probe 0 01 Q resolution and a specific cable to connect the instrument with the resistance box are necessary in order to perform the physical calibration of the sample temperature measurement In order to achieve a complete physical calibration of the sample temperature measurement probe included its required to successively put the Pt 100 probes in two thermostatic baths The temperature gradient between the two baths has to be at least 100 Temperatures
15. 7 240 to 260 RPM Ambient Natural rise At first degree 1 C 90 to 120 RPM or without stirring Bitumen 18 C before 1 C 110 Without stirring preheating B expected T 2 C 110 240 to 260 RPM Quick A Average 12 i 90 to 120 RPM C min then 5 to 6 C min at expected T 50 C Search of an AorB At first degree 1 C 110 C As per the unknown Flash or Bitumen 2 C 110 C method Point or Quick A Sample preheating at programmed t without stirring D g at prog with a method B slope Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing than test starts up with stirring at programmed T lieler INSTRUMENT COMPANY INC 5 3 STARTING UP 5 3 1 Rear panel connections For water cooling connect the inlets outlets with refrigerated water 5 psi maximum fasten the clamps switch on the water circuit and check that there is no leak For gas connection 50 mbar max connect the gas fasten the clamps the automatic valve is closed out of test check that the flame valves are closed switch on the gas and check that there is no leak connect the PC and or printer cables if necessary connect the
16. 9 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC Figure 2 Mbar mmHg mV 920 690 4345 1066 800 4877 To issue a lock book see chap VI and 11 3 4 D In case of an unexpected loss of calibration values it s possible to type in a calibration by conversion point value It s also possible to type in a calibration value by conversion points previously edited on the lockbook Display of the calibration values Allow to control the conversion point values of the sensor calibration Point calibration In case of an unexpected loss of barometric calibration values it s possible to type in a calibration by conversion point previously edited in the lockbook The point conversion calibration reguires to enter the high and low pressure corresponding to the conversion points Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KEANE INSTRUMENT COMPANY INC 11 3 3 C PRE TEST STEPS see chap VI 3 steps can be defined at the beginning of the test Those steps determin
17. ED WITH THE INSTRUMENT 1 power supply cable 1 cover and 1 Pensky Martens cup 1 container 1 detection cable 1 glass Pt 100 probe for the sample 2 tubings with clamp collars for connection to water supply 1 gas tubing with clamp collars 1 stirring flexible 1 RS232C cable 1 users manual 1 compliance certificate and quality control certificate 1 ticket printer with connection cables power supply for loading 1 electrical spark 1 detection thermocouple 4 1 OPTIONS e Removable gas cartridge with stand and connections Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen INSTRUMENT COMPANY INC 4 2 SET OF ACCESSORIES Paper for Printer POWER SUPPLY PRINTER PRINTER CABLE Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen INSTRUMENT COMPANY INC SET OF ACCESSORIES GANED Complete Lid e N 2 F
18. ES Aes H SL d a ae tt Tn e EE pc SS 1 AAA AE ooo o 54 Se dei za as ape mn Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC ORY E E v 5 FA Hi 8 Denis VAI Rondelle plastigue Montage Tour 386 Carte SBC104 PENSKY MARTENS 10F F Rondelle Plastique Rondelles Plastigues Y N KE o x lt Carte 001128 R f 10061N Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing INSTRUMENT COMPANY INC KEANE NC8VOC 494 6c 112 11 00 VOd ojjeuie4 owas Jnegoeuuo5 u Op Du NZt28C Jou S49 88 n 91 93 Ieixeoo ejgeo seiiosseooy sep seDe qe 381 v98S9 O3DO LZY LOL 8LL 0 971 N co0c e dnooouue uA woop 6uo1 N98v0c 31VW OW31 PP2V12 00 SOV44 eje oue Cie vi Fr oo al BIBI og
19. G jepurg Jnejoeuuo3 NGOLOZ 060v JON 8S wo 0 Duo euooijis neAn 4vN060pl uio 7 Duo epuos euog NLOSO uj 8 Duo 00LLd aan epuos NZZSOZ wo op Duo gpulig L L O age NOPZ8Z uo 00 1d 1g g W Jeputg Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing INSTRUMENT COMPANY INC cen ais aw c1 6OdOV eDe geo ON NV1d _ ANODVA Sue vd 3NISS30 WcV 6OdOV ALYVO 2000 L 20001 00000008 0000008 i BELSIpZ EN j cS Z n pn 22000000 Pn 2000000 MOL ESeN MOR sea oooooooosjooo0o00o000o6 oooooooooooooooooooe i GGOC8 Sn o wo 3U001 oooooooooooooooooooo o L I1 o Sorig al ooo i es un GA HIM roooooooesjcS3M 00000000 ef 4 oooooooooe 0000000008 TBreioHr yn i 88919H 2 cn vO LS 0000000000 0000000000 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing
20. LLATION INSTRUCTIONS The cooling circuit of the instrument must be connected to a max 5 psi pressure water supply The water connections must be done with the delivered tubes and clamp collars The gas circuit of the instrument must be connected to a max 50 mbar pressure gas supply with the tubes and clamp collars delivered in accessories or to a removable gas cartridge delivered in option with its connecting accessories The instrument has to be located on a stable and strong table or laboratory bench Electric supply has to be in accordance with the one described on the identification tag and the instrument has to be connected to the earth The instrument has to be located under a fume hood equipped with a vapor extractor and the working space has to be sufficiently ventilated 1 4 CHECK WHEN DELIVERED e Packaging should not be damaged If so the necessary claims have to be made to the carrier e Compare the content of the packing with the provided list of accessories e Control accessory identification and quality ll TECHNICAL FEATURES Determination of the Closed Cup Flash Point according to the following standards EN 22719 ISO 2719 ASTM D93 e P34 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Ana
21. OOLING SYSTEM SCALING The use of hard water in the cooling system can provoke a stopping in the pipes In that case a monthly scaling is recommended White vinegar or a dedicated scaling solution could circulate by gravity in the cooling system In order to improve the efficiency of the procedure the heating block can be heated a little In any case avoid using acid or strongly corrosive products because the cooling system pipes made of copper will be severely damaged Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC XIV ACCESSORIES ET REFERENCES 14 1 ACCESSORIES Designation Cup Complete cover Glass Pt 100 probe lonization detection wire Thermocouple detection Stirring spring Ticket printer Paper roll for ticket printer Ink ribbon for ticket printer Electric test spark Reinforced water pipe 10x16 minimum 5 meters Gas pipe back side connection 1 meter Gas tube for test flame minimum 2 meters 14 2 OPTIONAL ACCESSORIES Designation Wire for sample temperature calibration Extension wire for Pt 100 probe calibration with thermostatic
22. ch off Afterwards the new password is necessary in order to have access to it Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC 11 2 SOFTWARE CONFIGURATION see chap VI 11 2 1 RESULT CORRECTION see chap VI Possibility of making up results up to 9 9 C 9 9 F 11 2 2 STOP OF BLOCK COOLING see chap VI Programmable temperature of the stop of the block cooling after test between 0 C and 60 C 32 F to 140 F 11 2 3 SAFETY STOP see chap VI The instrument can be configured in order to stop the test as soon as the preset temperature is reached This temperature has to be between 15 C and 99 C 27 F 178 F 11 2 4 ENTER THE EXPECTED TEMPERATURE see chap VI Possibility of introducing a different expected temperature each time a new test is started associated with an automatic reset at the end of the test if requested 11 2 5 BAROMETRIC PRESSURE see chap VI Automatic determination of the barometric pressure or manual introduction status modification with gt If the manual barometric pressure setting is chosen the adaptable default value 760 mmHg or 1013 mba
23. creen Page 22 6 2 Access to functions Page 22 25 VII RUNNING A TEST Page 25 7 1 Test process included method for bitumen Page 25 28 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC 7 2 Unknown product quick search Page 27 7 3 Quick A Method Page 27 VIII PRINTING Page 28 8 1 Types of printer Page 28 8 2 Printing current results Page 28 8 3 Printing previous test results Page 28 8 4 Printing temperature slope Page 28 8 5 Print out examples Page 28 8 6 Lock book print out Page 29 IX SAFETIES Page 29 9 1 Pt 100 probe absence Page 30 9 2 Default in sample temperature increase Page 30 9 3 Electric safety Page 30 9 4 Sample temperature safety Page 30 9 5 Gas safety Page 31 X INSTALLATION OF SOFTWARE UPDATE Page 32 XI FEATURES Page 33 11 1 Password new password Page 33 11 2 Software options Page 34 11 2 1 Result correction Page 34 11 2 2 Stop of block cooling Page 34 11 2 3 Safety stop Page 34 11 2 4 Introduction of expected temperature Page 34 11 2 5 Barometric pressure Page 34 11 2 6
24. e Selection of the units C F mbar mm Hg Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KEANE INSTRUMENT COMPANY INC Calibration of the temperature measurement regulated bath or resistance box Obliteration or preservation of the presumed temperature after each test Buzzer continuous or 3 minutes Stop temperature of the cooling heating block Correction of temperature deviation on result 9 9 C Safety on sample from 15 C to 99 C above ambient temperature Alarm sounds at safety temperature 15 C Instrument piloting Waterproof tactile screen liquid Crystal backlit graphic display 256x128 pixels gt Printing of configuration report Printing of results 80 column printer or ticket printer supplied For logic UO Flash Eprom Through teleloading 270 x 550 x 550 20 kgs 115 or 230 V 10 50 60 HZ Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design am
25. e the 3 heating power during the first 5 minutes of the test in order to benefit from the optimum start conditions Electrical power variations are automatically compensated during the 5 first minutes see 11 3 3 D Step calibration Through keyboard enter the 3 percentages corresponding to the reguired heating power Step 1 controls the heating power for the first minute Step 2 between minute 1 and 3 and Step 3 between minute 3 and 5 Press ul after each data introduction Step display Allow to control steps values when starting the test 11 3 3 D ELECTRICAL SUPPLY REGULATION See chap VI The electrical supply regulation guarantees that for the first 5 minutes of the test any public electric supply variation will have no impact on the provided heating power during the 3 start up steps Physical calibration The physical calibration of the electrical supply regulation requires an auto variable transformer with a minimum operating range at least between 210 V and 245 V The electrical supply of the instrument through the auto transformer has to be maintained only during the calibration process The procedure is the following Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumen
26. edures described in the manual Testing processes have to be permanently watched The instrument has to be located under a fume hood equipped with a vapor extractor and the working space has to be sufficiently ventilated Water and gas supplies have to be controlled at least once a month in order to verify the good condition of pipes and fastenings Gas pipes have to be replaced prior to the expiration date If an incident occurs gas cut off overheating of the instrument leakage which could damage the instrument or components an internal and external check up has to be carried out by a person with the adequate technical level Only skilled technicians are allowed to perform maintenance on the instrument which has to be back at ambient T and unplugged from electric supply excepted for calibration purpose water and gas supplies Maintenance functions described as in the user s manual should only be performed by a qualified technician Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC Prior to using the instrument operators have to take knowledge of keyboard function keys described in the user s manual 1 3 INSTA
27. ehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cocher INSTRUMENT COMPANY INC XVIII ELECTRIC AND ELECTRONIC SCHEMES 3 3705738 REVIDATE DESSINE PAR 3 VAUDRY ur 59 Hie 20 ag e ES H ED EI s a Gan au 3D eu 425 nm RES4 BXIOK S E S ple OW ELO bl Eins E le Bao 6 UE amp ER S 2 so SE DE Bog Po AN AMENER NN np LE ES gc J ME 3 e R g eq E 4449 didddddddd dade ll ONES Gl MES ee WE ER E E GE Se l s T HE He SS As tee Poil 2 e e see sdsdss584 4 yy e percent Ey ey sim of d 3 E m 000000000000000000 oo0dobood8ooR a GR eis GE x S s BB SS XY wo nuo 2 EE ps a ME E D S lt 0000000000000000000000000000 E i gigi sii iei ajo da elelchdel dell Uae PF SS NBPREPIE na 2 Qe SCC EC IP Sls NU 5 Addo so LS PREE a G a gt 5 ipm a S S S SC SL
28. k press key 11 3 4 B LOGIC I O Allow to operate the Instrument e logic UO and to display the logic outputs to end task press s key 11 3 4 C AUTODIAGNOSTIC Automatic procedure to install an automatic control of some instruments components including a report print out 11 3 4 D LOCK BOOK PRINT OUT Print out of a lock book with the calibration safety and operation parameters Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC Model CONFIGURATION V1 2 App 3711 Date 8 4 1999 Stop safety at expected temper 20 C End of cold 040 C Write ET at each test No Flash by Gas Security Flam Ok No Atmo pressure calibration 690 mmHg 920 mbar gt 0101 pts 800 mmHg 1066 mbar gt 0211 pts Last calibration of Pressure 24 02 1999 Power Supply Calibration 210 V gt 0033 pts 245 V gt 0129 pts Last Calibration of supply 24 02 1999 Corrected result 0 0 C Start Param 080 060 032 Etalonnage Temperature 119 4 ohms gt 50 0 c gt 186796 pts 153 6 ohms gt 140 0 C gt 316873 pts Last temperature calibration 24 02 1999 Nb
29. lieler INSTRUMENT COMPANY INC MAINTENANCE AND USER S MANUAL PENSKY MARTENS FLASH POINT TESTER K87100 K87190 EN 22719 ISO 2719 ASTMD 93 IP 34 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen INSTRUMENT COMPANY INC Table of contents I INTRODUCTION Page 5 1 1 Safety instructions Page 5 1 2 Operation instructions Page 5 1 3 Installation instructions Page 6 1 4 Checks out when delivered Page 6 ll TECHNICAL FEATURES Page6 7 III INSTRUMENT DESCRIPTION Page 8 3 1 Presentation Page 8 3 1 1 Control Panel Page 8 3 1 2 Front side middle Page 8 3 1 3 Front side low Page 8 3 1 4 Back side Page 8 3 1 5 Working area Page 9 3 1 6 Right side Page 9 3 1 7 Schemas Page 10 11 IV SUPPLIED ACCESSORIES Page 13 4 1 Options Page 12 4 2 Accessories Page 14 17 V METHODS AND STARTING UP Page 18 5 1 Standards Page 18 5 2 Methods Page 19 5 3 Starting up Page 20 5 3 1 Rear panel connections Page 20 5 3 2 Front panel connections Page 21 5 3 3 Power supply connection Page 21 SOFTWARE DESCIPTION Page 22 6 1 Waiting s
30. lysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC Ambient working temperature 15 C to 30 C Working temperature range 20 C to 400 C Detection temperature range 70 C to 700 C Sample temperature measurement 4 wired glass Pt100 probe accuracy 0 1 C gt Flash point detection Flame dipping Automatic with gas or electrical Test electric spark Electrical supply potentiometric tune up Stirring 2 speeds 90 to 120 rpm 240 to 260 rpm Cooling of heating block Air ventilation and or refrigerant Gas supply Gas network 50 mbar max optional gas cartridge about 8H of autonomy Water supply Water network 5 psi max Connection ext diameter 12 5 mm Pilot and test flame Adjustable by valves Safety of heating Hard heating cut off at 550 C Measured in the heating block Independently of the microprocessor With sound alarm Safety on samples Cut off of on going test with sound alarm programmable safety from 15 C to 99 C above expected temperature Probe safety Faulty probe abnormal temperature reading Gas safety Optical detection of flame absence with sound alarm and automatic gas cut off after 30 and test termination Carte 386SX Programming through tactile keyboard with e Automatic barometric correction membrane with manual registration of the atmospheric pressure or by pressure transducer
31. mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen INSTRUMENT COMPANY INC 2 G S Wa e J we w Jam the electric ignition by the needle Plug the electric ignition Screw LU en Check the positioning of the filament It can not touch the edge of the lid Configure by keypad the electric ignition See the flow chart Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing Kleeder INSTRUMENT COMPANY INC KOEHLER INSTRUMENT COMPANY Ee pre IELELELEES EK d etam ae Een A SE PE EE Cem Een erar ee t Eee NU Key LIST CHART Key SEARCH METHOD 1 GASVALVE Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cana INSTRUMENT COMPANY INC XV Troubleshootin XVI Error codes Trouble code on the report 55
32. of test since last calibration 41 Nb of test since first uses 112 XII INCIDENTS A gas over pressure can provoke internal disconnection of pipes fastenings and valves In that case a check out by a gualified technician is mandatory prior to starting up the instrument An over heating can provoke damages to internal components pipes and valves A check out by a gualified technician is mandatory prior to starting up again the instrument Any sample leakage can provoke a fire inside the instrument A complete clean up by a gualified technician is mandatory Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC XIII MAINTENANCE 13 1 CALIBRATION Perform a calibration check out at least once a year 13 2 CONTROLS The user shall define a periodicity for an autodiagnostic The cleaning of the instrument has to be performed as often as possible in order to maintain adequate working conditions No drastic solvents An internal check out of the instrument will be performed depending on the number of achieved tests In case of intensive use the instrument should be checked by a duly appointed technician 13 3 C
33. p Manufacturing lieler INSTRUMENT COMPANY INC Ill INSTRUMENT DESCRIPTION 3 1 PRESENTATION 3 1 1 Control panel e 1 waterproof tactile keyboard 1 e 1 backlit liquid crystal graphic display 256x128 pixels 2 3 1 2 Front panel middle e thermocouple connector for the flash point detector 3 e cable connector for ionization detection 4 e sample Pt100 probe connector 5 e gas connections for the pilot 6 and the test flame 7 3 1 3 Front panel bottom e pilot flame needle valve 8 test flame needle valve 9 e light indicators for heating 10 and cooling 11 of the heating block e electrical supply potentiometer of the lighting spark 28 3 1 4 Rear panel e general power supply switch with fuses 12 e RS232 port for PC connection 13 e printer connector 14 e gasinlet 15 e inlet 16 and outlet 17 connections of the cooling circuit e gas cartridge fastenings 18 e pressure generator connection for pressure sensor calibration 19 e_ electrical regulator connection for pressure sensor calibration 30 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC 3 1 5 Wo
34. r appears at the beginning of the testing process Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KEANE INSTRUMENT COMPANY INC 11 2 6 BUZZER see chap VI Choice of the alarm buzzer mode continuous or 3 minutes 11 2 7 SOFTWARE NEW RELEASE see chap VI and chap X Up dating of the instrument software 11 2 8 NEW PASSWORD see chap VI Allow to change the password In order to validate the new password the instrument has to be switch off After a new start up the configuration panel can t be accessed anymore without the newly introduced password 11 2 9 PRINT OF THE TEMPERATURE SLOPE see chap VI Allow to print the temperature slope of the current test as well as the result at the end of it or if required only the final result at the end of the test status modification with A 11 2 10 TO ESCAPE FROM SOFTWARE CONFIGURATION PANEL Press except if an expected numerical data is entered 11 3 CONFIGURATION HARDWARE 11 3 1 LANGUAGE see chap VI A language has to be selected on screen Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free
35. rking space electrical spark connections 20 e cup container when no test is under way 21 e heating block 22 flame dipper 23 or electrical spark pilot flame 24 e arm for controlling the flame presentation traps 25 e connection axis of the stirring 26 flexible stirrer 27 3 1 6 Right side e Identification tag 29 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing cen INSTRUMENT COMPANY INC Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing aner Wieder COMPANY INC Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KECA INSTRUMENT COMPANY INC IV ACCESSORIES DELIVER
36. se in configuration configuration software Note the administration password is provided with the connection cable kit and the up dating diskette Follow the instructions displayed on the PC s screen Connect series port to the PC s COM 1 and restart the PC s with the up dating diskette boot included Follow instructions on PC s screen Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC XI FEATURES See chap VI This function allows the operator to have access to configuration control and maintenance functions This access can be protected by a password 11 1 PASSWORD Initially no password is necessary A simple validation of the original password allows to have access to the following functions In order to define a new password the following procedure has to be followed Press software configuration icon Use arrow keys in order to access to new password icon see chap VI Enter the new password and validate Confirm this new password and validate Switch off and restart the instrument after a few seconds Note The configuration menu remains available prior to any instrument swit
37. stom Design amp Manufacturing KEANE INSTRUMENT COMPANY INC 8 6 LOCK BOOK PRINT OUT Printing the lock book makes available the necessary pieces of information to follow up the instrument in terms of Quality Assurance FLASH POINT PENSKY MARTENS ISO 2719 ASTM D 93 IP 34 85 App 3711 Date 1 12 1998 Time 15 36 Duration 48 08 Sample 236 Expected temperature 250 Method A Bar Corr 760 mmHg Nb of dips 32 Flash point 122 0 Corr Flash Point 122 1 Flam Gas Flash NB OF DIPS gt 20 CONFIGURATION V1 2 App 3711 Date 8 4 1999 Stop safety at expected temper 20 End of cold 040 Write ET at each test No Flash by Gas Security Flam Ok No Atmo pressure calibration 690 mmHg 920 mbar gt 0101 pts 800 mmHg 1066 mbar gt 0211 pts Last calibration of Pressure 24 02 1999 Power Supply Calibration 210 V gt 0033 pts 245 V gt 0129 pts Last Calibration of supply 24 02 1999 Corrected result 0 0 C Start Param 080 060 032 Temperature 119 4 ohms gt 50 0 gt 186796 pts 153 6 ohms gt 140 0 gt 316873 pts Last temperature calibration 24 02 1999 Nb of test since last calibration 41 Nb of test since first uses 112 Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com
38. tation e Custom Design amp Manufacturing KEA INSTRUMENT COMPANY INC Apply a 210 V power supply wait for roughly 1 minute prior calibration Enter the value 210 and press enter key Apply a 245 V power supply wait for roughly 1 minute prior calibration Enter the value 245 and press enter key Issue a lock book see chap VI et 11 3 4 D The information contained in this lock book could be used afterwards for a point calibration in case of an unexpected loss of calibration data Electrical power supply regulation display Allow to control the calibration values of the electrical power supply regulation Point calibration In case of an unexpected loss of the electrical supply regulation calibration it is possible to enter point calibration values thank to the conversion points previously edited on the lock book Point calibration requires to enter the conversion point values corresponding to the voltage displayed on the screen Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KECA INSTRUMENT COMPANY INC 11 3 4 CONTROLS see chap VI 11 3 4 A ANALOGIC READINGS Display of the Instrument e analogic entries to end tas
39. ument conforms to the following standards EN22719 SO 2719 ASTMD93 P34 Determination of a closed cup Flash Point of fuels lubricating oils liguids with suspensions of solids and liguids that tends to form a surface film under test conditions A 75mL test specimen is heated at a slow constant rate with continual stirring in a brass test cup of specified dimensions with cover of specified dimensions An ignition source is directed into the test cup at regular intervals with simultaneous interruption of the stirring The flash point is the lowest liguid temperature at which application of the ignition source causes the vapor of the test specimen of the sample to ignite e Test range 0 to 400 C e Repeatability 1 Up to 104 C gt 2 C Above 104 C gt 5 5 C e Reproducibility 1 Up to 104 C 2 3 5 C Above 104 C gt 8 5 C Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing Ic chin INSTRUMENT COMPANY INC 5 2 METHODS METHOD SLOPE C MIN 17 FLAME SPEED STIRRING PRESENTATION A 5 to 6 C min 18 C before 1 C 110 C 90 to 120 RPM expected T 2 C 110 C B 1 to 1 5 C min Y
40. utely requires to disconnect gas supply on the rear panel 5 3 3 Power supply connection Check the voltage indicated of the instrument and be sure it is equivalent to the laboratory supply to be used Press the switch located on the rear panel of the tester During the central unit inititialization the screen remains empty After around 20 seconds the instrument is ready and the screen provides parameters and data Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC VI SOFTWARE DESCRIPTION 6 1 SCREEN The main screen has arrows and icons for making choices of programs to run 6 2 PROGRAM SCHEMAS Note Access to programs and options is provided with a click on the arrows located on the right of icons The screen is not a tactile one and a strong pressure on displayed icons could deteriorate the screen Each menu or sub menu is designated by an icon Their signification is summarized hereafter Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com
41. w 7 ST D Cog PD S mu cUBOeee LENS e Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 htto www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KOSME INSTRUMENT COMPANY INC SET OF ACCESSORIES DETECTION AMPLE THERMOCOUPLE EE DETECTION CABLE Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing KOSME INSTRUMENT COMPANY INC CARTIDGE CASE FOR GAS CARTRIDGE GAS OPTION WATER TUBING GAS TUBING COLLAR FOR COLLAR FOR GAS TUBING WATER SE 10 16 mm TUBBING 10 16 mm Koehler Instrument Company Inc 1595 Sycamore Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing amp Analysis Instrumentation e Custom Design amp Manufacturing lieler INSTRUMENT COMPANY INC V METHODS AND STARTING UP 5 1 STANDARDS The instr

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