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1. User Manual Edit Batch Options To edit batch options click on Edit Batch button Edit Batch dialog will appear Fdit Rateh General Calibration Samples Reporting Format Mote Batch ID EXAMPLE_BATCH Analysis Total Perroleum Hydrocarbons Analyte Mame TPH Method Mame Total Perroleurm Hydrocarbons by GC FID Reference EPA Instrument a FID 01 Calibration Date Sunday December 28 2014 Calibrated By Jhon Analysis Date Sunday December 28 2014 Snalvzed By Lewis Conc Unik mg L Response Unit Peak Area Batch Status Completed Approved Edit Batch dialog contains several tabs and below is the details of each General Tab Batch ID Analysis Analyte Name Method Name Reference Instrument Standard Solvent Sample Solution Calibration Date Calibrated By Analysis Date Analyzed By solns Conc Unit Response Unit Batch Status Rev 2 Description Unique batch ID in the database This field is read only It can t be changed after it has been created Analysis name which is performed in the lab e g Hydrocarbons Chloride Sulfate etc Name of the analyte to be analyzed The laboratory method name or standard operation procedure SOP Reference method number e g EPA ASTM ISO etc Instrument name or ID used to perform analysis and read analyte responses e g UV VIS HPLC GC ICP etc Solvent name used to dilute standard solutions Solvent name used to dilute sampl
2. Allow saving password Test Connection Rev 2 Page 11 of 28 A CHEMIASOFT Standard Curve User Manual Batches In Standard Curve software every collection of calibration standards and unknowns called a batch Create New Batch To create new batch from toolbar click New Batch button enter a unique name of the batch and press OK New Batch Enter new batch ID pT If the batch name is unique the name will be reserved in the database It is preferred to have unique naming system of all batches in lab For example use batch name derived from date of analysis like if a batch analyzed on Jan 8 2015 will be named as e g B20150108 A B means batch and A means first trial of analysis performed Be careful batch name is permanent and can not be changed after created Once you press OK Edit Batch Dialog will appear Edit Batch General Calibration Samples Reporting Format Mote Batch Batch ID EXAMPLE BATCH Analysis Total Perroleum Hydrocarbons Analyte Mame TPH Method Mame Total Perroleurm Hydrocarbons by GC FID Reference EPA Instrument tsC FID 01 Calibration Date Sunday December 28 2014 Calibrated By Jhon Analysis Date Sunday December 28 2014 Snalvzed By Lewis Conc Unik mg L Response Unit Peak Area Batch Status Completed Approved Fill batch information and press OK gt Rev 2 Page 12 of 28 A CHEMIASOFT Standard Curve
3. and press Save As button Save Batch As dialog will show up to enter new unique batch ID Also select if whether you want to copy calibration standards and samples to the new batch There are two options with available at the bottom of the dialog Copy calibration standards and Copy unknown samples save Batch As Eg Enter new batch ID Copy calibration standards Copy unknown samples CE Once you enter new batch ID click OK Then Edit Batch dialog will appear to make changes if there is any Click OK or press ENTER when you are done Rev 2 Page 20 of 28 A CHEMIASOFT Standard Curve User Manual Chemiasoft Standard Curve EXAMPLE_BATCH ae Edit Batch m afa General Calibration si p Open Batch New Batch Delete Batch Calibration Samples Reporting Format Note Batch Details EE Calibration Standards Batch ID EXAMPLE_COPY Batch Analysis Total Perroleum Hydrocarbons Batch ID EXAMPLE BATCH Total Perroleum Hydrocarbons Created On 12 28 2014 Analyte Mame TPH Created By USER Batch Status Completed Approve Last Updated 12 28 2014 Reference EPA Analysis Total Perroleum Hyg Instrument GC FID 01 Analyte Name TPH arlene farang Calibration Date Sunday December 28 2014 v Method Name Total Perroleum Hyd EEE EEE Instrument SC FID 01 Analysis Date Sunday December 28 2014 Conc Unit mg L Method Name Total Perroleum Hydrocarbons
4. 63CA Sa This version iz license To Mame r Activation Code aa Page 28 of 28
5. Min Not Detected Above Max Over Range Ox Calibration Tab Items Description Trend Line Fitting Type Fitting type there are six options available Linear Power Natural Logarithmic Logarithmic base 10 exponential and Quadratic Fitting Curve Options Force To Origin make fitting line pass through origin point 0 0 this option available only for quadratic and linear type Include Origin include origin point 0 0 to the calibration points Weighted Least Square Select Weight Least Square WLS option to enable weighted WLS calibration When this option is not selected Ordinary Least Square OLS will be used in calculations Method Detection Limit Calculate method detection limit MDL for batch calibration Enable this option when batch is conducted for MDL study MDL is calculated according to ISO 11843 2 Methodology in the linear calibration case also called Hubaux Vos MDL Refer to those methods online for more details on how to calculate MDL set K value MDL factor and Confidence Interval as per method requirement Calibration Two options are available here Concentration Range e When Report within Calibration Range is checked then only samples solutions concentration within calibration range will be reported If sample solution below calibration range it will be reported as Under Range or Over Range if exceed calibration range concentration The concentration range will be ident
6. by GC FID Analyzed By Lewis Response Unit Peak 4rea Final Conc Unit mg Kg Conc Unit mail Calibration Response Unit Peak Area Fitting Type Linear Batch Status Completed Approved Calibration Date 12 28 2014 Calibrated By Jhon Analysis Analysis Date 12 28 2014 Analyzed By Lewis Delete Existing Batch To delete existing batch open batch you want to delete Click Delete Batch button from toolbar A message will appear to confirm click Yes to proceed Restore Deleted Batch To restore deleted batch s go to menu Batch gt gt Restore Deleted Batch Restore Deleted Batch dialog will show up Select batch s you want to restore then click Restore Selection to proceed Rev 2 Page 21 of 28 A CHEMIASOFT Standard Curve User Manual Standards Add New Standard To add new standard to batch click button from standard table toolbar then Edit Standard dialog will show up de z Fill all information of the new standard Below table explain each part tem Description gt Z gt O Standard Name Name of the standard e g Standard One 25 ppm on this number one value only Responses Responses reading s from instruments used to run standard solution You can enter single or multiple reading separated by comma You may enter each ready in new line The software will calculate the average and relative standard deviation RSD of the readings Weight factor required when weighted calibration is se
7. dialog will show up Edit the sample information from the dialog and click OK Once you edit standard the software will do recalculate edited sample final concentration Delete sample To delete sample select sample you want to delete by mouse or by using keyboard arrows up down Click button from sample toolbar Delete Confirmation A Are you sure you want to delete selected Sample Recalculate Samples When recalculate sample the software will do all calculations for all samples it will take responses and calculate concentrations base on calibration equation From the toolbar click Recalculate Samples button Note This step will calculate all samples It will NOT do recalibration of batch standards If you want recalibration then see Recalibrate Batch Rev 2 Page 26 of 28 A CHEMIASOFT Standard Curve User Manual Report Batch report contains all batch details standards and samples Generate Report To generate batch report open batch you want to report as per Open Existing Batch section Click on Report button from toolbar report will be generated on screen Press Print button to print generated report E Preview SEAAMAQim QEBiE0AF K 4 of 3 gt Di Batch Details Batch ID EXAMPLE_BATCH Created On 12 28 2014 Analysis Total Perroleum Hydrocarbons Created By USER Analyte TPH Calibrated On 12 28 2014 Method Total Perroleum Hydrocarbons by GC FID Calibrated By Jhon Instrument GC FID 01 Analyze
8. 8496763754045 Std Err 0 46562234934166 0 999590587167821 Number of Points 5 Standa u rve Regression Std Error 33496 2446062566 Calibration Result Standard Curve Response Peak Area am a am a rm rm mo co Wy e Concentration mg L 7 On Calibration Standards tab screen become three parts Standards table at the top which list all calibration standard solutions Standard curve area at the left bottom shows the calibration curve On the bottom right area there is Calibration Result table which contains fitting type equations and other details related to calibration 8 On Standards table the first column Cal shows tick mark when the standard included in the calibration 9 On the Standards table double click on the standard 2 row The dialog will appear as follow Edit Standard Standard Mame Level Concentration 30 mgfL Responsels 1230 1200 Peak Area For mutiple values enter each value in separate line or separated by comma Remark cadmium chloride Include in calibration Ox Rev 2 Page 7 of 28 A CHEMIASOFT Standard Curve User Manual On Edit Standard dialog there are several input fields include standard name level remark concentration and responses The concentration must be single value but responses can accept several values by separate them with comma or enter each value in new line The software will calculate average of all entered response s and c
9. A CHEMIASOFT Standard Curve Software Manual Revision 2 January 19 2015 By CHEMIASOFT TEAM www chemiasoft com Note There might be some differences between this manual and the software due to continuous development For the latest version of this manual please refer to online version A CHEMIASOFT Standard Curve User Manual Table of Content PANDO aaah A aceasta eae elas ced alec deat deca deceased ceeeaeece 3 CANIN OS i E 4 Genting otare d srs E ne cect se sen venesecaseseeunseneseseeacevaunsasewccceaes 5 Data DaS Eai vada cece tecesiietenuccauteceedcetecuesnetecuwsasiecustaetenucsanteceecosteiesdecetss 11 BAONE S ar a mere armen enn acer ereer ner 12 Create INGW Bale M tevpssrcceviesearriisseevs serrata severe ee ei ae eae 12 EGit Bale ODUONS sscstetscacstetacas stots EEE EEE ETE EAE E E EEEE 13 PERE O E O ene te er tor eet ee en eee 19 Save Balch AS DING ent NAME sactvsncisctvondcscavansisvevacideddventiisevandehulvontuseivantisuadanidedeuaedacieunks 20 Delele ExisunG Balch eea E 21 Restore Deleted BION eseas E E 21 Standards osoen 22 POACHING W Standard renns aan A a E ees aciun uence aes en 22 OE EIS NC LN AN Ch 2s ess os sceanonaaconseeuanion EEEO 23 Delete Existing Standard seere E E A O eee 23 Recalibrate Batch otandardS saisaitia A Gate naceumielatnieloasbaianes 23 SAMPES aa AE a ae sehdwetse cue seideesiuuieccuencdsians 24 AJda Sample 10 Balae a A 24 Edit Sample do a A E a AEE LEA 25 DELIE SAMPIO ere ee
10. Sunday December 28 2014 Calibrated By Jhon Analysis Date Sunday December 28 2014 Analyzed By Lewis Conc Unik jrg l Response Unit Peak Area Batch Status Completed Approved rm D ri T D m Edit Batch dialog contains all information about the batch and calibration At the top there are several tabs you can switch between tabs and discover the details Make some changes and press OK button to see the effect That is all for now Please refer to the Table of Content page 2 and find out more details If you can t find answer of your question please contact us by sending an email to support chemiasoft com Rev 2 Page 10 of 28 A CHEMIASOFT Standard Curve User Manual Database Standard Curve software is database software It is supporting MS Access database Future versions will be developed to support other types of databases Like MySQL The default database is located in C Program Files Chemiasoft Standard Curve Database database mdb To change database properties go to menu File gt gt Database Properties Data Link Properties dialog will show up Change database properties or location then press OK B Data Link Properties Provider Connection Advanced All Specity the following to connect to Access data 1 Select or enter a database name ChemiasottStandard Curve D atabase database mdb Led 2 Enter information to log on to the database User name Admiri Blank password
11. a EE EEEE enea E 26 Recalcukte Samples ercan ei 26 FRO DONG s aeia aoai ori 27 Genar Ae RepON see a a 27 Save REDON rioei eie e EEEE eee 27 Rega Na E ee or ce wees E re ws cee ewe ee ee seen eee 28 Rev 2 Page 2 of 28 A CHEMIASOFT Standard Curve User Manual About Standard Curve is defined as the easiest way to graph calibration curve from standard solutions and identify unknown samples in laboratory There is no need to use MS Excel to make calculations and pain full process Standard Curve made it easy for you Calibration is at the heart of chemical analysis and is the process by which the response of an instrument in metrology called indication of the measuring instrument is related to the value of the concentration of the analyte A typical example in analytical chemistry is the calibration of a GC gas chromatography analysis The heights of GC peaks are measured as a function of the concentration of the analyte in a series of standard solutions calibration solutions and a linear equation fitted to the data Standard Curve is robust industrial productivity software It has been developed in real laboratory world Width Standard Curve laboratory routine work becomes easy In addition all data will be saved in local computer database and it can be backed up at anytime Start using Standard Curve today and make your life easy Rev 2 Page 3 of 28 A CHEMIASOFT Standard Curve User Manual Features R
12. alculate relative standard deviation RSD Weight value required when using weighted calibration WLS and manual entry of weight factor Include in calibration points to include or exclude standard from calibration curve Uncheck the box to exclude from calibration and press OK to see the effect Equation will be recalculated All samples also will be recalculated base on new fitting 10 Switch to Unknown Samples tab table contains all samples in the batch with their responses and calculated concentrations Chemiasoft Standard Curve EXAMPLE_BATCH File Batch Help A if amp amp E Open Batch Mew Batch Delete Batch Save 4s Edit Batch Report Refresh Close Batch Details E Calibration Standards Wl Unknown Samples SOLE No Sample Name Response Peak Area RSD Calc Conc mg L Total ol L Original Sample Wt Kg Dilutia A 1 Blank 445 000 0 000 0 055 O 1 0 05 zZ 2 Quality Control 50 mg L 432 000 0 000 49 911 1 1 1 3 Sample 1 3500500 Sore 76 709 O 1 0 1 2 ESEE 6317 500 147 416 E E Double click on any sample by left mouse click Edit Sample dialog will show up Rev 2 Page 8 of 28 A CHEMIASOFT Standard Curve User Manual Edit Sample Sample Detail Sample Name Sample Z Analyte Factors Analyte Response Responses 5595 6737 For mutiple values enter each value in separate line or separated by comma Sample Remark The dialog contains sample inp
13. d On 12 28 2014 Reference EPA Analyzed By Lewis Batch Status Completed Approved Last Updated On 12 28 2014 Calibration Standards Include Standard N Concentration Response ap Calc Conc z poe Calib ame mg L Peak Area mgA rror mor ma OO Ome smn SSO C E T E 3 True Standard 3 100 4600 000 0 0 104 309 4 309 4 309 Ec fete Sms SOCORRO Save Report To save report from report screen click on Save button and select the format you want to save You can save report in various formats e g PDF JPEG PNG MS Excel MS Word etc Rev 2 Page 27 of 28 A CHEMIASOFT Standard Curve User Manual Registration To register your copy Standard Curve do the following 1 2 3 Rev 2 On Standard Curve software go to menu Help gt gt Registration the Registration dialog will show up Copy Hardware ID Visit www chemiasoft com and place your order for Standard Curve Use the hardware ID while placing your order online you will be asked for your hardware ID Once you complete your order you will receive an email with the license information and registration code Copy the registration code from the email you received and paste it on the Registration dialog and click Register button Welcome message will appear Close and restart Standard Curve to complete registration Enjoy using Standard Curve with full features Registration Registration Information Activated Hardware Unique ID 3506 6E62 4635
14. e solutions Date of the calibration run of the standards Name of the analyst perform the calibration process Date of performing sample analysis Name of the person perform sample analysis Concentration of the solutions used in the analysis including both calibration solutions and samples solutions Response name from the instrument used to perform the analysis e g Peak Area Peak height Absorbance intensity etc Status of the batch e g Under process under review rejected approved etc Page 13 of 28 A CHEMIASOFT Standard Curve User Manual Edit Batch Ontions Fq i General Calibration Samples Reporting Format Mote a L Linear Logarithmic base 10 Exponential Natural Logarithmic Power Quadratic Linear and Quadratic Fitting Curve Options Force to origin Weighted Least Square WLS Weighted least square Auto calculate weight Factor Calibration Method Detection Limit MOL Only For Linear Fitting Calculate method detection limit MBL Number of preparations tk value 1 fdeFaulk 1 MDL Factor 2 default 2 MDL Confidence Interval t Skatistic default 95 99 95 99 5 97 5 i a5 39 9 C a9 g5 O a0 99 87 O 98 O a0 75 Calibration Concentration Range Calculate concentrations within calibration concentration range only Min Calibration Quantification Conc mg L Max Calibration Quantification Conc mgs Under
15. ere is no undo for this step Delete Confirmation A re you sure you want to delete selected standards Recalibrate Batch Standards When recalibrate batch the software will do all calculations for fitting equation will mTo recalibrate batch from toolbar click Recalibrate Standards button EOE Rev 2 Page 23 of 28 A CHEMIASOFT Standard Curve User Manual Samples Add Sample to Batch To add new sample to batch click button from sample table toolbar then Edit Sample dialog will show up Edit Sample Sample Detail Sample Name Sample 1 Analyte Factors Analyte Response Responses 3412 3589 For mutiple values enter each value in separate line or separated by comma Sample Remark Q Fill all information of the new sample Below table explain each part Analyte Tab Description gt O Sample Name Name of the sample Number Sequence order in the table Samples are sorted in the table base on this number Responses Responses reading s from instruments used to run sample solution You can enter single or multiple reading separated by comma You may enter each ready in new line The software will calculate the average and relative standard deviation RSD of the readings Remarks Note about the sample Rev 2 Page 24 of 28 A CHEMIASOFT Standard Curve User Manual E Edit Sample Seles Sample Detail Sample Name Sample 1 Analyte Factors Dilution Facto
16. escription Check this option to include dilution factor column in samples table This part is very essential when you have high concentrated samples and you want to make dilution before injected to the instrument Dilution factor is calculated using equation _ Final Volume mL Initial Volume mL For example if you take 5 mL from solution and diluted to 100 mL with solvent then dilution factor will be 100GnL 5 mL Check this option to include multiply factor column in samples table This will multiplied calculated concentration by this factor Mostly used when sample required preparation before analysis like digestion in trace metal analysis For example enter Total Volume L in the title field Check this option will include divide factor column in samples table This will divide calculated concentration by this factor Mostly used when sample required preparation before analysis like digestion in trace metal analysis For example enter Sample Weight Kg in the title field Page 16 of 28 A CHEMIASOFT Standard Curve User Manual Samples Tab Custom Factor Check this option to include custom multiply factor column in samples table This will multiplied calculated concentration by this factor This factor is considered as extra option Use it if you want to make correction factor of the calculated concentration For example conversion factor from Liter to milliliter etc Fdit Batch Ontian
17. ev 2 Easy to use and straight forward Support MS Access database Create unlimited number of batches Every batch includes calibration curve and unknown samples Graph and run calibration curve from standard solutions and identify unknowns several types of trend line fitting include Linear Quadratic Logarithmic base 10 Exponential Power and Natural Logarithmic Support both Ordinary Least Square OLS and Weighted Least Square WLS calibration methods Accept single or multiple measurement values like absorbance peak area or peak height and calculate average and RSD Include or exclude standards from calibration curve Graph calibration points and trend line Display calibration result in table like fitting equation standard errors for equation parameters coefficient of determination and standard regression error also called residual standard deviation Calculate concentration of unknown samples based on calibration curve Support several multiplication factors to finalize calculation in origin samples For example Dilution factor total volume and initial sample weight Calculate method detection limits MDL as per ISO 11843 2 Hubaux amp Vos and SEMI standard method set quantification limits and final reporting limits Generate professional batch report includes standards calibration curve and unknowns Export report as PDF MS Excel Image and Email and other formats Print and export graph as PDF and ima
18. ge Search batches using several inputs like batch ID analyte analysis method creation date and modification date Delete and restore batches Page 4 of 28 A CHEMIASOFT Standard Curve User Manual Getting Started 1 After installation of the software complete run Standard Curve from desktop icon or from start menu Once the software start it will connect to local default database and the main software screen will appear Chemiasoft Standard Curve File Batch Help Open Batch New Batch Database Connected No Batch Open 2 Once the main screen appeared it will show Database Connected If there is any problem with database then refer to Database section 3 Now press Open button on the main toolbar and search dialog will appear 4 Leave all fields empty and press Search bution List of all available batches will appear Rev 2 Page 5 of 28 A CHEMIASOFT F Chemi Search Batch To Open File Batchi Search Batch Detail Created On Batch ID Creation date range From Lizard Analyte Analysis a f rey Standard Curve User Manual Last Updated On Last update range Method sear Batch ID Analysis Analyte EXAMPLE BATCH Total Perroleum Hydrocarbons TPH 5 Double click on EXAMPLE_BATCH to open Method Total Perroleum Hydrocal 12 28 2014 6 After selected batch open main batch screen will appear Batch name will show at title bar of the software between two b
19. ified automatically by identify the maximum and minimum concentration in the calibration standards When uncheck Report within Calibration Range then you have to enter quantification concentration range Enter maximum and minimum calibration quantification Rev 2 Page 14 of 28 A CHEMIASOFT Standard Curve User Manual Calibration Tab Item concentration to be determined base on the equation Note Calibration range is different from Final reported range shown in Report tab Calibration range is defined as the analyte concentrations in solutions used during running instrument and take reading responses Final reported range is defined as the concentration of analyte in origin sample Reported concentration is calculated from solution concentration Rev 2 Page 15 of 28 A CHEMIASOFT Samples Tab Use dilution factor Multiply Factor Divide Factor Rev 2 Standard Curve User Manual Edit Batch General Calibration Samples Reporting Format Note j Final Calculation Options Use dilution Factor O F t Multiply Factor Multiply Concentration By Solution Total wolwe Use mutiply Factor colurnn Multiply Factor Tithe Total vol Ll Divide Concentration By Origin Sample volt Use divide Factor column Divide Factor Title Original Sample Wwe Kg Multiply Concentration By Custom Factor Use custom Factor column Custom Factor Tithe Custom Factor 5 D
20. lected in Batch Options There are manual and automatic calculations of weight points Click OK to proceed Once you add new standard the software will do recalibration and recalculate all samples Edit Standard Standard Name ame nl Response s 1230 Peak Orea 1200 For mutiple values enter each value in separate line or separated by camma Remark cadmium chloride Include in calibration E Rev 2 Page 22 of 28 A CHEMIASOFT Standard Curve User Manual Edit Existing Standard To edit existing standard double click standard you want to edit using left mouse button or select the standard using arrow up down and press ENTER Another way is to select standard and click on Edit Standard button from toolbar e of amp 2 Edit Standard dialog will show up Edit the standard information from the dialog and click OK Once you edit standard the software will do recalibration and recalculate all samples automatically Edit Standard Mame Standard Name Standard 6 Analyte 1 Value Analyte Y Values Response 23272 1889 159 Analyte For mutiple values enter each value in separate line or separated by comma Include in calibration points Ox Delete Existing Standard To delete standard select standard you want to delete by mouse or by using keyboard arrows up down Click button from standard table toolbar Lelde From confirmation message click Yes to proceed Note that th
21. r Dilution Factor 2 Total Vol L 0 Divide Factor Original Sample Wt Kg 0 Multiply Factor Ox Factors Tab tem Description gt Z gt O Dilution Factor Dilution factors means how many times sample is diluted more details about this factor in Edit Batch dialog Calculated concentration from calibration equation will be multiplied by this factor If the sample is not diluted then set this factor 1 Multiply Factor Usually its value is set to total sample solution volume in liter This factor will multiply with calculated concentration from calibration equation Factor name can be changed from Edit Batch dialog Divide Factor Usually its value is set to initial sample weight in Kg Calculated concentration from calibration equation will divide by this factor Factor name can be changed from Edit Batch dialog Factors can be removed from Edit Batch dialog Edit Sample To edit existing sample double click sample you want to edit using left mouse button or select the sample using arrow up down and press ENTER Another way is to select sample and click on Edit Sample button from toolbar e ohf Rev 2 Page 25 of 28 A CHEMIASOFT Standard Curve User Manual Edit Sample Seles Sample Detail Sample Name Sample 1 Analyte Factors Analyte Response Responses 3412 3589 For mutiple values enter each value in separate line or separated by comma Sample Remark Q Edit Sample
22. rackets EXAMPLE_BATCH Chemiasoft Standard Curve EXAMPLE_BATCH Open Batch New Batch Delete Batch Save As Edit Batch Report Refresh faa Calibration Standards fay Unknown Samples Batch ID EXSMPLE_BATCH Created On 12 78 7014 Created By USER Batch Status Completed Approved Last Updated 12 28 7014 Analysis Total Perroleum Hydrocarbons Analyte Name TPH Method Name Total Perraleum Hydrocarbons by GC FID Reference EPA Instrument GC FID 01 Conc Unit mg L Response Unit Peak Area Final Conc Unit mg Kg Calibration Fitting Type Linear Calibration Date 12 28 2014 Calibrated By Jhon Analysis Analysis Date 12 78 7014 Analyzed By Lewis Rev 2 Clase Batch Page 6 of 28 A CHEMIASOFT Standard Curve User Manual Batch screen contains three tabs Details Calibration Standards and Unknown Samples The Details tab contains information about the batch Now switch to Calibration Standards tab Chemiasoft Standard Curve EXAMPLE_BATCH File Batch Help LE Open Batch New Batch Delete Batch Save 4s Edit Batch Report Refresh Close Batch Details EA Calibration Standards iy Unknown Samples Cal No Standard Name Concentration mg L Response Peak Area RSD o Calc Conc mg L Error Error o J 1 Standard 1 af 2 Standard 2 50 2500 000 0 000 51 574 af 3 Standard 3 100 4600 000 0 000 104 272 Tee Stahdards Tabl Linear Y A XB 444 809870550162 Std Err 118 624962508291 39
23. s al a General Calibration Samples Reporting Format Note l Final Concentration Reporting Unit Report Concentration Unit maka Minimum Reporting Concentration Min Reporting Conc mgikg IF cocnentration below Min Reporting Conc then report as lt 5 Maximum Reporting Concentration Max Reporting Conc 5000 mgikg IF cocnentration above Max Reporting Conc then report as tem Description S O Reporting The final concentration unit after performing all calculations Concentration Unit Min Reporting Conc The minimum reporting concentration of the original sample If concentration below Enter the text to be reported if the final calculated concentration Min Reporting Conc below Min Reporting Conc Then report as If concentration above Enter the text to be reported if the final calculated concentration Max Reporting Conc above Max Reporting Conc Then report as Rev 2 Page 17 of 28 A CHEMIASOFT Standard Curve User Manual Edit Batch Options RSD Calculated Concentration Error Error b Samples Final Concentration o Format Tab In this tab set details of digital value format to display result in standards and samples tables as per your needs The following format specifiers are supported in the format result Digit place holder If the value being formatted has a digit in the position where the 0 appears in the format result then that digit is copied to the output re
24. sult Otherwise a 0 is stored in that position in the output string Digit placeholder If the value being formatted has a digit in the position where the appears in the format string then that digit is copied to the output string Otherwise nothing is stored in that position in the output string Decimal point The first dot character in the format string determines the location of the decimal separator in the formatted value any additional dot characters are ignored The actual character used as the decimal separator in the output string is determined by the DecimalSeparator global variable whose default value is specified in the Number Format of the International section in the Windows Control Panel Thousand separator If the format string contains one or more comma characters the output will have thousand separators inserted between each group of three digits to the left of the decimal point The placement and number of comma characters in the format string does not affect the output except to indicate that thousand separators are wanted The actual character used as the thousand separator in the output is determined by the ThousandSeparator global variable whose default value is specified in the Number Format of the International section in the Windows Control Panel Rev 2 Page 18 of 28 A CHEMIASOFT Standard Curve User Manual The following table shows some sample formats and the results produced when
25. the formats are applied to different values Format string 1234 and 0 5 0 1234 1 0 00 1234 00 0 50 Note Tab This tab is to enter user note for batch Open Existing Batch To open existing batch from toolbar click on Open Batch button Search Batch dialog will show up In Search Batch dialog enter search conditions like Batch ID Analysis name or creation date etc and press ENTER or click Search button to see the result list If search conditions have no result message will appear In the case you have to change search conditions Search Batch To Open Search Batch Detail Created On Last Updated On Batch ID Creation date range Last update range g DO l eem e ee a Batch ID Analysis Analyte Method SaESOMPLE BATCH Total Perroleum Hydrocarbons D i Cher To list all batches available in the database leave search fields empty and click Search button or press ENTER Rev 2 Page 19 of 28 A CHEMIASOFT Standard Curve User Manual Click on column header to sort the result Select batch you want and click Open button or press ENTER Search Batch To Open Search Batch Detail Created On Last Updated On Batch ID Creation date range Last update range Batch ID Analysis Analyte Method Created On A EZAMPLE_BATCH Total Perroleum Hydrocarbons Total Perroleum Hydrocal 12 28 2014 Save Batch As Different Name Save batch as different name is similar to copy batch First open the batch you want to copy
26. ut details like Sample name order number and responses similar to the standards dialog In addition it contains Factors tab click on factors tab to see the details E Edit Sample Sample Detail Sample Mame zEmm E Analyte Factors Dilution Factor rave Divide Factor Multiply Factor Different factors are appeared Dilution Factor how many times sample is diluted Total volume the total sample solution in liter Origin Sample Weight the amount of the sample in sample preparation process in kilograms The factors are very essential in lab calculations In this example calculated concentration from calibration curve in mg L will be multiplied by dilution factor and then multiplied by total volume of the sample solution The result will be divided by origin sample weight Kg in this example 100 g 0 1 Kg The final calculated value will be in mg kg which is the concentration of the analyte in origin sample i e the reported concentration Click OK or Cancel button to hide Edit Sample dialog 11 On the toolbar click on Edit Batch button Edit batch dialog will appear Rev 2 Page 9 of 28 A CHEMIASOFT Standard Curve User Manual Edit Batch General Calibration Samples Reporting Format Moke Batch Batch ID EXAMPLE BATCH Analysis Total Perroleum Hydrocarbons Analyte Mame TPH Method Mame Total Perroleum Hydrocarbons by GC FID Reference EPA Instrument a FID 01 Calibration Date

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