Hydra II AA Installation Guide
Contents
1. Processor Pentium Dual Core 2 3 GHz Networking One standard factory installed Ethernet connection if a Communication Ports network connection is desired One available USB port Additional Hardware CD ROM drive Printer with Windows compatible print driver PS 2 or Bus Mouse Internet Browser Microsoft Internet Explorer 4 or higher must be installed for the software Help to function 1 5 Choosing a Location NOTE Always position the equipment so that it is easy to disconnect the power cord The typical Hydra I mercury analyzer system includes the mercury analyzer autosampler PC standard desk top mini tower with monitor reagent and rinse bottles and possibly a printer located next to the instrument The system with a PC monitor and reagent bottles requires a minimum linear bench space of 120 cm 48 in Approximate spacial requirements for each component configuration are shown in Table 1 3 Hydra I Spacial Requirements Combine widths to estimate the total linear bench space required for your system configuration NOTE Allow an additional 5 cm 2 in behind the system for cable egress ventilation and access to power switches Hardware Software Requirements Hydra Il Mercury Analyzer Pre Installation Guide 47x TELEDYNE LEEMAN LABS a Everywhereyoulook Table 1 3 Hydra Il Spacial Requirements Configuration Hydra Iljq PC 49 5 cm 19 5 in 92 cm 36 in 49 5 cm 12. outlets are not available Certified Mercury Standard Solution 100 or 1000 ppm Hydrochloric acid Minimum grade Trace Metal specification 37 Recommended Mallinckrodt Macron 6 each 2 5 L AR Select Item 5587 46 Nitric acid trace metal grade 68 70 Recommended Mallinckrodt Macron 2 5 L AR ACS Item 2704 46 Stannous chloride crystals Di hydrate Recommended Mallinckrodt Macron ACS 500 g Item 8176 04 Potassium permanganate solid crystalline suitable for mercury analysis i e EPA 245 1 Recommended j t baker 500 g bottle Item 3227 1 Vapor Trap System PN 125 00143 1 The vapor trap system is designed to capture mercury vapor from the instrument exhaust The system includes activated charcoal flow through bottle quartz wool and tubing assemblies to connect to the instrument and external exhaust 2 Propanol High purity spectrophotometric grade 2 propanol will be used for cleaning the optical cells and cell windows Additional Chemical Compounds mw NOTE The sample preparation procedures of the intended analytical method may require additional chemical compounds Refer to published method specifications Necessary Supplies Hydra Il Mercury Analyzer Pre Installation Guide aA TELEDYNE LEEMAN LABS Everywhereyoulook 1 11 Recommended Supplies Volumetric Flasks 100 mL class A TC 12 each Volumetric Flasks 1000 mL class A TC 2 each Volumetric Flasks 2000 mL class A TC 1 ea
3. s manual 1 7 Gas Supply Requirements A source of ultra high purity dry research grade N or 99 999 purity Argon The recommended gas regulator must be an inert two stage design and provide 0 345 kPa 0 50 psi Teledyne Leeman Labs recommends PN 115 00032 The cylinder or dewar must be capable of delivering 172 kPa 25 psi The gas connection must be located within 3 m 10 feet of the Hydra I and must accept 6 35 mm 1 4 in OD 3 18 mm 1 8 in ID urethane tubing mw NOTE An inert two stage regulator is required to provide a stable input pressure 1 8 Ventilation Requirements z NOTE Ventilation is recommended but not required if the analyzer is equipped with an optional mercury trap to collect trace elemental mercury from system exhaust gases If connecting to a ventilation system the system must provide at least 11 8 L sec 25 CFM Ventilation should allow for connection of 6 35 mm 1 4 in OD urethane tubing The exhaust line may be clipped into existing hood Gas Supply Requirements Hydra Ila Mercury Analyzer Pre Installation Guide a TELEDYNE LEEMAN LABS Everywhereyoulook 1 9 Environmental Conditions 1 9 1 Temperature The recommended nominal or average laboratory temperature is 15 30 C 60 86 F 1 9 2 Temperature Variation The temperature rate of change in the laboratory should be limited to 2 C 3 6 F per hour with a maximum daily change of 10 C 18 F This temperature variation allo
4. 9 5 in 44 cm 17 in a 30cm x 30 cm 1 ft of floor space is required for the liquid waste receptacle The waste receptacle can be located directly below the analyzer or directly in front of the lab bench in line with the analyz er s peristaltic pump b PC width requirement can be reduced to 51 cm 20 in by placing the mini tower of the pc behind the monitor c Includes an additional 16 cm 6 in to allow the door to sit in the open position Figure 1 1 Dimensions of the Hydra Il yy 48 cm 19 in Additional 16 cm 6 in required for door to open SSCL 49 5 cm 19 5 in 49 5 cm 19 5 in The analyzer must be placed on a sturdy countertop or table 1 5 1 Work Surface Requirements Do not place the analyzer on a wheeled cart or folding table The work surface should be at least 61 cm 24 in deep Choosing a Location Hydra ll4a Mercury Analyzer Pre Installation Guide a TELEDYNE LEEMAN LABS Everywhereyoulook 1 6 Electrical Requirements mw NOTE Do not apply power to the power supply until ready to operate the analyzer Four electrical outlets 110 VAC 10 50 60Hz 15A or four electrical outlets 240 VAC 10 50 60Hz are required one each for the analyzer computer monitor and printer mw NOTE An AC surge protected power strip with six outlets is strongly recommended The analyzer is provided with a 2 29 m 7 5 ft power cord with a NEMA 5 15P male conne
5. a TELEDYNE LEEMAN LABS Everywhereyoulook Hydra AA Mercury Analyzer Pre Installation Guide Part Number 150 00316 Rev H May 2015 Copyright 2015 Teledyne Technologies Incorporated All rights reserved Reproduction adaptation or translation without permission is prohibited except as allowed under copy right laws Printed in the U S A Updated Information The information contained in this document is subject to change without notice Trademarks The companies indicated own the following trademarks None All other brands or product names are trademarks or registered trademarks of their respective owners Teledyne Leeman Labs 110 Lowell Road Hudson NH 03051 U S A www teledyneleemanlabs com Sales Support 800 634 9942 Technical Support 800 533 6267 Main 603 886 8400 Fax 603 886 4322 a TELEDYNE LEEMAN LABS Everywhereyoulook Hydra llaa Mercury Analyzer Pre Installation Guide 1 1 Introduction Thank you for purchasing a Teledyne Leeman Lab s Hydra II CVAA mercury analyzer The purpose of this guide is to assist new users in the preparation of their laboratory prior to the installation of the Hydra II mercury analyzer If there is any doubt about the information provided please contact your local Service Representative or Teledyne Leeman Labs using information in Section 1 13 Contact Information In preparation for the installation of your analyzer please review this pre install
6. ation guide to ensure that your laboratory is prepared After the installation please retain a copy of this guide for your records 1 2 Receiving the Instrument If your analyzer will be installed by a Teledyne Leeman Lab s Service Engineer please do not unpack any boxes without consulting the Teledyne Leeman Lab s Customer Support Department see Section 1 13 Contact Information if necessary The Service Engineer will be responsible for reviewing the shipment against the packing list The Service Engineer cannot be responsible for this task nor can Leeman Labs be responsible for any missing items if boxes have been opened or removed before the arrival of the installation engineer The Service Engineer is a skilled professional who will install your equipment verify that it is operating to specifications and train your personnel in its basic operation Your preparation enables you to use his her visit to the best advantage The connection of the Hydra llaa mercury analyzer to your company s internal communication network server is not part of the normal installation process and is best left to a trained Information Technology IT professional Introduction Hydra Il Mercury Analyzer Pre Installation Guide 494 TELEDYNE LEEMAN LABS 9 Everywhereyoulook 1 3 Pre Installation Requirements This section summarizes the site requirements necessary for proper installation of the Hydra Iaa mercury analyzer Specific detai
7. ch Precision adjustable air displacement pipettes 10 to 100 ul TD 200 to 1000 ul TD 400 to 2000 ul TD 1000 to 5000 pl TD 2000 to 10000 pl TD Replacement Tips for micropipettes Disposable Plastic Pipette Droppers Graduated Cylinders 10 and 100 mL Kimwipes Polypropylene or Polyethylene Bottle with Cap 1 L Weighing Balance top loading 0 1 g readability or better capacity gt 200 g Laboratory Scoopula and Large Spatula Stopwatch for measuring liquid uptake rates Stirring Rod Powder Funnel wide bore stem small overall size Wrenches adjustable 12 in 6 in and 4 in Screw Drivers e 1 Small Phillips Head e 1 Medium Phillips Head e 1 Long Shank Medium Flat Head e 1 Small Thin Flat Head Flow Meter 0 1500 mL min calibrated to user s choice of carrier gas with 1 mL readability Used to confirm gas flows for troubleshooting gas leaks after optical cell maintenance Deionized Water 1 12 Preparedness Statement Failure to meet one or more of the pre installation requirements may prevent your instrument from operating properly During installation if an installation engineer determines that one or more of the pre installation requirements have not been met the company reserves the right to delay installation until all requirements are satisfactorily met Any time lost during installation caused by failure to meet the pre installation requirements will be billed to your account If you have any questions r
8. ctor and an IEC 320 C13 female connector as shown in Figure 1 2 NEMA 5 15P Plug and IEC 320 C13 Receptacle Figure 1 2 NEMA 5 15P Plug and IEC 320 C13 Receptacle 1 NEMA 5 15P IEC 320 C13 For locations outside of North America where this NEMA 5 15P male connector is not common or desired the power cord can be replaced or the plug male connector may be replaced with a suitable connector Wiring connections should be made as denoted in Figure 1 2 and Table 1 4 IEC 320 C13 Wiring Connections Table 1 4 IEC 320 C13 Wiring Connections Neutral Blue wire Earth Ground Green wire with yellow strip Line Brown wire The Hydra H44 mercury analyzer uses a power brick that accepts AC input from 100 240 VAC 10 50 60Hz The specifications are shown in Table 1 5 Voltage and Power Requirements Table 1 5 Voltage and Power Requirements Hydra Il Mercury Analyzer 1 4A 120 VAC 10 0 7A 240 VAC 10 50 60 Hz 15 VDC Electrical Requirements Hydra Il Mercury Analyzer Pre Installation Guide 47x TELEDYNE LEEMAN LABS a Everywhereyoulook This equipment is designed for connection to a grounded earthed outlet The grounding type plug is an important safety feature For continued protection against electrical shock or damage to the instrument do not disable this feature The power requirements for the computer can be found on the label affixed to the bottom of the computer or in the computer user
9. egarding these requirements please contact Teledyne Leeman Labs using Section 1 13 Contact Information Recommended Supplies Hydra Il Mercury Analyzer Pre Installation Guide 4945 TELEDYNE LEEMAN LABS a Everywhereyoulook 1 13 Contact Information Teledyne Leeman Labs encourages you to contact us for any questions or concerns regarding your installation or to order accessories and consumables Please use the appropriate means of contact listed below for the most efficient service 1 13 1 Teledyne Leeman Labs 110 Lowell Road Hudson NH 03051 U S A Main 603 886 8400 Fax 603 886 4322 www teledyneleemanlabs com 1 13 2 Sales US and International 1 800 634 9942 or 1 603 886 8400 US and International Fax 1 603 886 4322 E mail salesinfo teledyne com Visit our website at www teledyneleemanlabs com for a complete list of US and International Sales Representatives 1 13 3 Technical Support US 1 800 533 6267 1 800 Leemans International 1 603 886 8400 E mail service teledyne com 1 13 4 Replacement Parts and Consumables US and International 1 800 533 6267 E mail service teledyne com Contact Information 19 Hydra ll4a Mercury Analyzer Pre Installation Guide 1 TELEDYNE LEEMAN LABS Everywhereyoulook 1 14 Your Installation is Our Highest Priority Streamlining the installation of your new Hydra I mercury analyzer system is our highest priority Teledyne Leeman Labs would like to thank you in adva
10. ls of these requirements are included in the sections which follow Dimensions Ventilation Width Base 49 5 cm 19 5 in Rate 11 8 L sec 25 CFM Depth Base 49 5 cm 19 5 in Connection 6 35 mm 1 4 in OD Urethane Tubing Height 47 cm 19 in Waste Drain Weight 18 4 Kg 40 6 lbs Waste Respectable 2 Lor more of acidic waste Electrical Requirements Environmental Conditions Four Grounded Electrical 110V 15A 60Hz or Temperature 15 30 C 60 86 F Outlets 220V 10A 50Hz Gas Supply Max Temperature Variation 2 C hr 3 6 F hr 10 C day 18 F day Type Argon or Nitrogen Relative Humidity 20 80 non condensing Purity 99 999 Inert Gas Regulator Two Stage Recommended Pressure 0 345 kPa 0 50 psi Range Max Distance to Instrument 3 m 10 ft Connection size 6 35 mm 1 4 in OD 3 18 mm 1 8 in ID a Requires an additional 17 cm 6 5 in to allow the door to sit in the open position Pre Installation Requirements Hydra Il Mercury Analyzer Pre Installation Guide a TELEDYNE LEEMAN LABS Everywhereyoulook 1 4 Hardware Software Requirements NOTE Skip this section if your Teledyne Leeman Lab s Hydra llaa mercury analysis system was purchased with a PC from Teledyne Leeman Labs Table 1 2 Minimum PC Hardware Software Requirements Operating System Microsoft Windows 7 32 and 64 bit and 8 1 64 bit Random Access Memory RAM 2 GB
11. nce for the preparation of your laboratory Your attention to detail will assist in the installation of your new instrument If you have any questions or concerns we encourage you to contact us directly He 16s BL Mla Jeff Forsberg Bob McCarthy Teledyne Leeman Labs Teledyne Leeman Labs Mercury Product Manager Director Customer Support jeff forsberg teledyne com bob mccarthy teledyne com 402 733 2829 603 521 3267 Your Installation is Our Highest Priority Hydra Il Mercury Analyzer Pre Installation Guide a TELEDYNE LEEMAN LABS Everywhereyoulook Your Installation is Our Highest Priority 12 Hydra Ila Mercury Analyzer Pre Installation Guide
12. ws for the most stable operation of the instrument Greater temperature variations will affect instrument stability Causes of temperature shifts including heat adjustments to the laboratory from morning to night increase in room temperature due to direct sunlight automatic air conditioner adjustments as well as positioning the analyzer near or beneath a heating cooling vent should be avoided Protection such as blinds from direct sunlight via windows is necessary due to optical heating from direct sunlight 1 9 3 Relative Humidity Humidity plus heat plays a major role in operating stability Humidity may vary between 20 and 80 but must be a non condensing environment The laboratory humidity range should be monitored to determine if additional climate controls are needed to prevent conductivity changes on detector assemblies Environmental Conditions Hydra Il Mercury Analyzer Pre Installation Guide 47x TELEDYNE LEEMAN LABS a Everywhereyoulook 1 10 Necessary Supplies UHP Nitrogen or Argon Cylinder or Dewar Ultra high purity dry research grade N or 99 999 purity Argon Inert Gas Regulator Inert 2 stage 0 345 kPa recommended range 0 50 psi secondary pressure gauge PN 115 00032 with a coupling for either a cylinder or dewar capable of delivering 172 kPa 25 psi The Hydra Ila should be located within 3 m 10 ft of the gas source AC Power Strip surge protected with six outlets if sufficient wall
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