Storm Water Test Kit - Fondriest Environmental
Contents
1. Refer to Free and Total Copper 0 4 mg L test procedure on page 8 English 9 Replacement items Note Product and Article numbers may vary for some selling regions Contact the appropriate distributor or refer to the company website for contact information Description Item no Color comparator box 1 173200 Color viewing tubes with caps 6 pkg 173006 Copper color disc 1 9263300 Free Copper Reagent Powder Pillow 100 pkg 2182369 Hydrosulfite Reagent Powder Pillow 100 pkg 2118869 Stoppers for viewing tubes 6 pkg 173106 Optional items Description Item no Copper Standard Solution 10 mg L 100 mL MDB 12932 Formaldehyde Solution 100 mL SCBD 205932 10 English Detergents Test preparation e Assemble the color comparator Put the Detergents color disc on the center pin with the lettering facing out Use sunlight or a fluorescent light source to compare colors e Rinse all viewing tubes with the sample water before testing and between tests e Ifthe disc becomes wet carefully open the plastic case Dry the case and the color insert with a soft cloth Assemble the case when the parts are completely dry Filter the chloroform layer If the water sample is turbid filter the chloroform layer at step 13 1 Puta small ball about the size of a large pea of glass wool in the filter thimble 2 Use the draw off pipet to remove the chloroform Filter the chloroform through the glass wool and into an unused glass2. 6 minutes for full color development p z 3 Fill a second color viewing tube to the lower edge of the frosted area 5 mL mark with the water sample 7 Put the tube into the right opening on the top of the comparator Hold the comparator in front of a light source Turn the disc to find a color match 4 Add the contents of one DPD Total Chlorine Reagent Powder Pillow y H x 8 Read the mg L total chlorine Cl gt from the scale window Ifthe result is between two values use the value halfway between the two printed numbers Note Product and Article numbers may vary for some selling regions Contact the appropriate distributor or refer to the company website for contact information Description Color comparator box Color viewing tubes with caps DPD Chlorine disc 0 3 4 mg L 6 English 173200 4660004 990200 Description Item no DPD Total Chlorine Reagent Powder Pillows 100 pkg 1407699 Caps for color viewing tubes 4 pkg 4660014 English 7 Total Copper Test preparation This test procedure identifies the concentration of free or complexed copper Free copper refers to any free or weakly chelated copper on in solution Complexed chelated copper is tightly bound as in Cu EDTA Free copper plus complexed copper gives the total dissolved copper e Assemble the color comparator Put the copper color disc on the center pin with the lettering facing out Use sun
3. LD DOC326 97 00024 Storm Water Test Kit 11 2013 Edition 1 User Manual Table of Contents General information ensure 3 ate informato s ll lt eege 3 Use of hazard information occcoccccoccnococnconnncnncnnoncnconnnnnnonnnnnnonnnnnnnnnonnnncnnnnnnncnos 3 Precautionary labels sun a un 3 Steiere et 3 Produc compone MS ee ooo 5 A EE 6 Test preparalon a nee sein 6 Total Chlorine 0 3 4 mg L test procedure u ssssssneenneennnnnknnkkkn kr kr kkrnnnee 6 Replacement EE 6 TOA CODO iaa 8 Re e Mi Ree ee oe aie eee 8 Free and Total Copper 0 4 mg L test procedure u sssssssssneeeneeennnnkknnnnne 8 LLCO CCS An 9 tee le Leer 9 Selen al eee lacio tec tal escitas 10 Opina EMS ars ae ol ae e do a 10 A A A re Fine ee 11 RR gel e SE 11 Detergents 0 1 2 mg L test procedure ocoooooccncccccccccconcoconocononnncnnnononcnnononenononaninnnnos 11 Replacement temsa ic a e dae ad e ao 12 A A AA 14 e a e CNE o eee 14 Test preparation ara ee en 14 Phenols 0 4 mg L test procedure nenne nenne nenne ERR EL ES 19 Replacementltens astra ie een 15 Opona Saca een 16 Table of Contents General information In no event will the manufacturer be liable for direct indirect special incidental or consequential damages resulting from any defect or omission in this manual The manufacturer reserves the right to make changes in this manual and the products it describes at any time without notice or obligat
4. eionized water Use the dropper to add 1 mL of the water sample to the tube Replacement items 01 00 12 Do not touch the tube for 1 minute to let the chloroform separate 11 Put the stopper in the tube Shake vigorously for 30 seconds O 15 Fill a second test 16 Put the deionized tube with deionized water tube into the left water opening on the top of the comparator Hold the comparator in front of a light source Turn the disc to find a color match O gt 19 Add deionized water to the upper mark 20 mL 20 Do steps 2 17 and multiply the results by 20 Note Product and Article numbers may vary for some selling regions Contact the appropriate distributor or refer to the company website for contact information 12 English Description Bulb for draw off pipette Color comparator box Color viewing tubes with caps 5 mL and 20 mL marks Chloroform ACS grade approximately 100 tests Detergents color disc 0 1 2 mg L Detergents reagent Dropper 0 5 mL and 1 0 mL marks Filtering thimble Glass tube for draw off pipette Glass wool Test tube Wash Water Buffer approximately 32 tests Quantity 100 mL MDB 5 pkg 1 1 5g Item no 178600 173200 173606 1445849 9265700 105932 1419700 51200 221800 252074 56510 99949 English 13 pH Refer to the documentation supplied with the Pocket Pro pH tester to do a pH measurement Phenols Test preparati
5. els and tags attached to the instrument Personal injury or damage to the instrument could occur if not observed A symbol on the instrument is referenced in the manual with a precautionary statement Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August of 2005 In conformity with European local and national regulations EU Directive 2002 96 EC European electrical equipment users Must now return old or end of life equipment to the Producer for disposal at no charge to the user Note For return for recycling please contact the equipment producer or supplier for instructions on how to return end of life equipment producer supplied electrical accessories and all auxiliary items for proper disposal Product overview Chemical exposure hazard Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled Refer to the current safety data sheets MSDS SDS for safety protocols English 3 Environmental Protection Agency EPA studies show that storm water runoff carries pollutants to nearby lakes rivers and streams To protect receiving waters the EPA issued regulations in November 1990 which apply to both municipalities and industrial storm water discharges Part 1 of the NPDES National Pollutant Discharge Elimination System application requires municipalities to do field screening with grab sample
6. er Pillows e Color viewing tubes with caps 4x e Hydrosulfite Reagent Powder Pillows e Color comparator box e Free Copper Reagent Powder Pillows e Carrying case EDTA Reagent Powder Pillows e Chloroform ACS grade e DPD Total Chlorine Reagent Powder Pillows e Detergents Test Solution e Potassium Persulfate Powder Pillows e Wash Water Buffer 2x e pH 7 0 SINGLET buffer solution packs e Hardness 1 Buffer Solution e Dropper e Filtering thimble e Beaker 100 mL e Test tube 10 mL 2x e Demineralizer bottle e Draw off pipet e Glass wool for detergents test English 5 Total Chlorine Test preparation e Assemble the color comparator Put the DPD Chlorine color disc on the center pin with the lettering facing out Use sunlight or a fluorescent light source to compare colors e Rinse all viewing tubes with the sample water before testing and between tests e Accuracy is not affected by undissolved powder e If the disc becomes wet carefully open the plastic case Dry the case and the color insert with a soft cloth Assemble the case when the parts are completely dry Total Chlorine 0 3 4 mg L test procedure ye ea 1 Fill one color viewing tube to the lower edge of the frosted area 5 mL mark with clear water ID 5 Swirl to mix Replacement items 2 Put the tube into the left opening on the top of the comparator 03 00 6 A color will develop if chlorine is present in the sample Wait 3
7. ion Revised editions are found on the manufacturer s website Safety information NOTICE The manufacturer is not responsible for any damages due to misapplication or misuse of this product including without limitation direct incidental and consequential damages and disclaims such damages to the full extent permitted under applicable law The user is solely responsible to identify critical application risks and install appropriate mechanisms to protect processes during a possible equipment malfunction Please read this entire manual before unpacking setting up or operating this equipment Pay attention to all danger and caution statements Failure to do so could result in serious injury to the operator or damage to the equipment Make sure that the protection provided by this equipment is not impaired Do not use or install this equipment in any manner other than that specified in this manual Use of hazard information ADAN GER Indicates a potentially or imminently hazardous situation which if not avoided will result in death or serious injury Indicates a potentially or imminently hazardous situation which if not avoided could result in death or serious injury Indicates a potentially hazardous situation that may result in minor or moderate injury NOTICE Indicates a situation which if not avoided may cause damage to the instrument Information that requires special emphasis Precautionary labels Read all lab
8. light or a fluorescent light source to compare colors e Rinse all viewing tubes with the sample water before testing and between tests e Accuracy is not affected by undissolved powder e Refer to Table 2 on page 9 for interfering substances e If the disc becomes wet carefully open the plastic case Dry the case and the color insert with a soft cloth Assemble the case when the parts are completely dry Free and Total Copper 0 4 mg L test procedure E 1 Fill two color viewing tubes to the lower edge of the frosted area 5 mL mark with the water sample 2 Add the contents of one Free Copper Reagent Powder Pillow to one of the tubes 5 Put the untreated sample tube into the left opening on the top of the comparator 8 English 6 Put the prepared sample tube into the right opening on the top of the comparator Hold the comparator in front of a light source Turn the disc to find a color match 3 Puta stopper in the tube with the powder Invert the tube several times to mix y H x 7 Read the mg L free copper Cu from the scale window Ifthe result is between two values use the value halfway between the two printed numbers 02 00 4 A purple color will develop if free copper is present in the sample Wait 2 minutes for full color development 8 To identify the concentration of total dissolved copper present add the contents of one Hydrosulfite Reagent Powder Pillo
9. low to each tube 6 Put one of the tubes into the left opening on the top of the comparator ID 10 Put the cap on the tube and swirl until the powder is dissolved 3 Put the cap on each tube and swirl until the powder is dissolved 7 Add the contents of one Phenol Reagent Powder Pillow for non extraction method to the second tube 11 Put the second tube into the right opening on the top of the comparator Hold the comparator in front of a light source Turn the disc to find a color match 4 Add 15 drops of Hardness 1 Buffer Solution to each tube gt 8 Putthe cap on the tube and swirl until the powder is dissolved y H x 12 Read the result in mg L from the scale window Ifthe result is between two values use the value halfway between the two printed numbers Note Product and Article numbers may vary for some selling regions Contact the appropriate distributor or refer to the company website for contact information Description Color comparator box Color viewing tubes Quantity Item no 173200 4660004 English 15 Description Clippers for powder pillows EDTA Reagent Powder Pillows Hardness 1 Buffer Solution Phenol Reagent Powder Pillows nonextraction Potassium Persulfate Powder Pillows for Phosphonate Optional items Description Filter discs 25 mm 45 micron Filter holder for Luer Lok Syringe 30 cc Luer Lok tip 16 English Qua
10. ntity 1 50 pkg 50 mL 100 pkg 100 pkg Quantity Item no 93600 700599 42426 2481569 2084769 2209525 246800 2225800 0 8 HACH COMPANY World Headquarters HACH LANGE GMBH P O Box 389 Loveland CO 80539 0389 U S A WillstatterstraRe 11 Tel 970 669 3050 D 40549 Dusseldorf Germany 800 227 4224 U S A only Tel 49 0 2 11 52 88 320 Fax 970 669 2932 Fax 49 0 2 11 52 88 210 orders hach com info hach lange de www hach com www hach lange de Hach Company Hach Lange GmbH 2013 All rights reserved Printed in U S A HACH LANGE Sarl 6 route de Compois 1222 V senaz SWITZERLAND Tel 41 22 594 6400 Fax 41 22 594 6499
11. on e Assemble the color comparator Put the Phenols color disc on the center pin with the lettering facing out Use sunlight or a fluorescent light source to compare colors e Rinse all viewing tubes with the sample water before testing and between tests e Ifthe disc becomes wet carefully open the plastic case Dry the case and the color insert with a soft cloth Assemble the case when the parts are completely dry Filter the sample If the sample is turbid it may be necessary to filter the sample 1 Install a 0 45 micron filter disc in the filter holder Refer to Figure 2 Make sure that the holder is closed tight after the disc is installed 2 Fill the 30 cc syringe with the turbid sample 3 Attach the filter holder to the syringe with a twisting motion 4 Filter the sample directly into the viewing tubes from the syringe Use the filtered sample in the test procedure Figure 2 Assemble the filter assembly a cc ee RA fe es ae I l I I I I I I I I I I I I I I I I I I I I I I I l 1 Filter disc 14 English Phenols 0 4 mg L test procedure 1 Fill two color viewing tubes to the upper mark 20 mL with water sample ID 5 Put the cap on each tube and swirl 9 Add the contents of one Potassium Persulfate Powder Pillow for Phosphonate to the second tube Replacement items X Kc O D Ose oe cee 2 Add the contents of one EDTA Reagent Powder Pil
12. s collected from dry weather flows These samples will be analyzed for pH total chlorine total phenols total copper and detergents Use this test kit on site or in a laboratory to identify the pH level and the concentrations of total chlorine total phenols total copper and detergents in storm sewer outflow and industrial discharge Refer to Table 1 for the test kit parameters A color comparator box and color discs are used to identify the concentration of total chlorine total phenols total copper and detergents Refer to Figure 1 The Pocket Pro pH tester is used to identify the pH level Table 1 Test kit parameters Parameter Number of tests Type of test Sensitivity H Refer to packaging lon selective electrode Refer to packaging Copper free and total 0 4 mg L 100 Bicinchoninate Hydrosulfite 0 1 mg L reduction Phenol 4 aminoantipyrine 0 1 mg L Detergents 0 1 2 mg L Toluidine Blue O 0 05 mg L Figure 1 Color comparator box 1 Color matching windows 4 Scale window 2 Opening for tube with untreated sample 5 Color disc A Opening for tube with prepared sample Federal Register November 16 1990 4 English Product components Make sure that all components have been received Refer to the list that follows If any items are missing or damaged contact the manufacturer or a sales representative immediately e Pocket Pro pH tester e Stopper for color viewing tubes e Color discs 4x e Phenol Reagent Powd
13. test tube Detergents 0 1 2 mg L test procedure 1 Fill one test tube to the upper mark 20 mL with the water sample 5 Put the stopper in the tube Shake vigorously for 30 seconds N 2 Add 12 drops of Detergent Test Solution 01 00 6 Do not touch the tube for 1 minute to let the chloroform separate 3 Put the stopper in the tube Shake to mix 7 Use the draw off pipet to remove the water from the tube Discard the water y 4m 4 Add chloroform to the lowest mark 5 mL Chloroform is heavier than water and will go to the bottom of the tube LA 8 Add Wash Water Buffer to the upper mark 20 mL English 11 9 Use the draw off pipet to remove the Wash Water Buffer Discard the buffer Note This step washes away the remaining water sample 13 If the water sample is turbid filter the chloroform layer y H x 17 Read the ppm Detergents LAS and or ABS from the scale window If the result is between two values use the value halfway between the two printed numbers If the color is darker than the highest reading on the color disc do steps 18 20 to make a 20 to 1 dilution LA 10 Add Wash Water Buffer to the upper mark 20 mL 14 Put the prepared sample tube into the right opening on the top of the comparator Lo OA 18 Discard the contents of the prepared sample tube in the right opening Rinse the tube with d
14. w clear pillow to the tube 9 Puta stopper in the tube Remove the tube from the comparator Invert the tube several 02 00 10 Wait 2 minutes for full color development 11 Put the prepared sample tube back into the right opening on the top of the comparator y H x 12 Read the mg L total dissolved copper free copper and complexed copper from the scale window If the result is between two values use the value halfway between the two printed numbers times to mix Hold the comparator in front of a light source Turn the disc to find a color match LC ENEREBEN 13 To identify the concentration of complexed copper present in the sample subtract the amount of free copper from the amount of total dissolved copper Interferences Table 2 Interfering substances Interfering substance Interference level Cyanide More than 2 mg L inhibits color development Add three drops of Formaldehyde Solution before the viewing tube is put into the comparator box Wait 3 minutes and then read the mg L free copper Accuracy check Periodically identify the reagent accuracy with a reliable standard such as Copper Standard Solution 10 mg L 1 Prepare a2 mg L free copper solution a Carefully measure 1 mL of Copper Standard Solution 10 mg L into a sample tube b Add deionized water to the sample tube to the 5 mL mark 2 Identify the concentration of copper that is present in the standard
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