- User Manual
Contents
1. RS doc sal Signature gt Service report lt O Installation O End of warranty visit O Warranty O Repair O Maintenance O Out of warranty System description ee TT NE eee eee Module C ICS CO EE ES TE E E ec itte vo EEE utacaess painterchim 211 bis avenue J F Kennedy T l 33 4 70 03 88 55 BP 1140 03100 Montlu on Fax 33 4 70 03 82 60 Hotline 33 4 70 03 73 01 E mail interfinedinterchim fr Not contractual pictures2. gt S sd E r i i cl a i m a 1 i d i Lk a i P i M INN INTERFINE CHEMICALS ANALYTICAL SCIENCES BIOCHROMATOGRAPHY BIOSCIENCE INNOVATION MINI 4 P d 7 4 El User MENT ET ITM 2012 10 12 The most economical and efficient solution for all your routine purifications mg up to hundreds of gram Lor ue P d CIVIL OK 17 250 ml min up to 7 bar INTERFINE CHEMICALS a Ir 211 bis avenue JF Kennedy ea nte e h m BP 1140 03100 Montlu on Hotline 33 4 70 03 73 01 interfine interchim fr Fax 33 4 70 03 82 60 IUBS OK 33 4 70 03 73 01 Summary 1 gt Packing list page A 3 2 gt Technical Data page A 3 a Technical Data Overview b Hydraulic connection 3 gt Care amp Use Instructions page A 4 4 gt Functions description page A 4 a Manuel mode b External mode 5 gt Protocol of Communication page A 6 a General Description b Transmission Parameters c Task List 6 gt Minibox cleaning procedure page A 8 7 gt Warranty page A 9 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE Takaa re 33 4 70 03 88 55 Fax 33 4 70 03 82 60 wwwinterchim com User Manual 1 gt Packing list v PU LASH APUNTS ON Mf v Tubing Kit P N JO2550 option Flow rate Pressure documentation Care amp Use Instructions interfine interchim fr 2 gt Technical Data a Technical Data Overvi
3. professionals and within the technical characteristics compatible with the functions defined in the user manual Terms and conditions of the guarantee Y The device is only guaranteed if installed by a service provider approved by Interchim Y The guarantee covers the supply of parts found defective by Interchim free of charge as a minimum within the limits of the parts The device must have been used in normal operating conditions and in accordance with the instructions The device must have been used with the consumables recommended by Interchim Il Guarantee exclusions The guarantee will not cover devices installed by the customer or by a service provider not approved by Interchim The guarantee will not cover equipment used in a manner which is non compliant with the provisions in the instructions The guarantee will not cover equipment subject to interventions repairs or modifications by personnel without Interchim approval The guarantee will not cover parts modified or changed by the customer or the service provider without Interchim s approval parts damaged by this modification parts not recommended by Interchim parts subject to wear and consumables The guarantee will not cover electrical and or electronic and or IT incidents caused by external factors The guarantee will not cover damage caused to the software or hardware due to contamination by an IT virus The guarantee will not cover damage or failure
4. the pump The pump is intolerant of solids 4 gt Functions description a Manuel mode To switch on the pump Press the power button at the back side of the pump To prime the pump Adjust manually the white dot of the potentiometer on the P value Press the Run Stop button to start the priming When the priming is done press again the Run Stop button To start the run Adjust manually the potentiometer to the consign value to set the flow rate Press the Run Stop button to start the run the green led light To modify the flow rate during the run just adapt a new consign value To stop the run Press the Run Stop button the red led light After each run clean the pump by flushing with isopropanol If you didn t use the pump remove the inlet and outlet tubing and put the plug 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE Takaa re 33 4 70 03 88 55 Fax 33 4 70 03 82 60 wwwinterchim com User Manual interfine interchim fr 3 Digital Display Priming Value Potentiometer Green Led Run Button Run Stop Red Led St ed Led Stop b External mode RS232 Communication Port Stop OUT Start OUT Start IN Stop IN Reverse IN Start In Command the start of the pump by contact in the 2 pins Stop In Command the stop of the pump by contact in the 2 pins v Reverse In Command the start stop of the pump by contact in the 2 pins If the pump is in the running mode the
5. R otherwise S in ASCII External control status in ASCII code if Start In return 1 if Stop In return 2 if Start Out return 4 if Stop Out return 8 FlowRate Percent Consign from 0 to 100 in ASCII characters 6 Minibox cleanin rocedure Switch On the pump and prim it with hot demineralized water 2 If the pump doesn t work remove the tubing and introduce three times omL of hot water with a syringe directly into the pump 3 Put the tubing and test a new priming 4 Relaunch step 2 and 3 if needed 5 Switch on the pump and run during 30 minutes with hot water in closed board put the suction tube at the top of the bottle and the oulet tube at the down to not re pump the particles 6 Clean the pump with isopropanol 7 Plugged Inlet amp Outlet when the pump is stored 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE Takaa re 33 4 70 03 88 55 Fax 33 4 70 03 82 60 wwwinterchim com User Manual 7 gt Warranty Interchim guarantees the PGe L SH MIMSOX Mf for one year for parts and labour at the discretion of Interchim in normal conditions of use and installation from the date of signing of the installation report by the service provider approved by Interchim to install the machine and by the customer interfine interchim fr The PURI LASH MINOR M device is guaranteed against material and manufacturing defaults in normal conditions of use by approved
6. command is Stop and if the pump is in stop mode the command is Run Start Out closing contact signal is send when the pump start to Run Stop Out A closing contact signal is send when the pump just Stop v RS232 Communication Port We can also control the pump by RS232 communication see explanation in chapter Protocol Communication ee Ll 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE MCCAIN re 33 4 70 03 88 55 Fax 33 4 70 03 82 60 www interchim com 5 PL OK 33 4 70 03 73 01 5 gt Protocol Communication a General Description During the dialog between a pump and the central system the central system is always master and pumps are slaves Orders are transmitted via a RS 232 serial communication Data transmission is protected by a checksum longitudinal parity and uses 2 ASCII bytes For each order the sequence is Data emission from host STX Pump number M in hexadecimal A letter giving task type None or one or many parameters according to the task ETX Checksum excluding STX in 2 bytes MSB first CR Answer from the addressed pump The answer is an acknowledgement or an information about the pump state The sequence is STX Pump Address M in hexadecimal Task type A message depending of the task v ACK if the order is accepted v NAK if the order is unaccepted or impossible or not understanding An information on pump state ETX Checksum excluding STX
7. entiometer Possible reason of refused command Enable Disable isn t O or 1 ASCII characters Run R Description Start the engine with existing parameters The Start Out signal is send during 2 seconds Frame STX Pump Address R EX Checksum Checksum CR Possible reason of refused command Command can t be refused Stop S Description Stop the engine The Stop Out signal is send during 2 seconds Frame Possible reason of refused command Command can t be refused Read X Mersion Number N Description The answer to this command allows to read the version number of the software load in the electronic board It can be usefull for service Frame Send this to the pump Pump Address Ll 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE MCE T l 33 4 70 03 88 55 Fax 33 4 70 03 82 60 www interchim com ITUS OR M 33 4 70 03 73 01 Pump answer Version Version Version Version Version number in 4 ASCII characters v Read Stat U Description The answer to this command allows to read Status of the pump Start In Stop In Start Out Stop Out value Flowrate Percent Frame Send this to the pump Pump answer Start In Stop STX Pump Address U ETX Run Stop IN Start Out Flow Rate Flow Rate Flow Rate State Stop Out Percent Percent Percent Run Stop state if pump is in running mode it s return
8. ew Dimensions W x H x D 4 1 x 2 77 x 5 17 16 x 10 8 x 22 5cm Weight 2 5Kg Connection Voltage 100 240 VAC 15 Power consumption max 100 W Frequency 50 60 Hz Pressure range 0 100 psi Flow Rate at 100 psi 0 250 ml min Material in contact with solvent 316L stainless steel peek Teflon Kalrez Minibox Il FlowRate Pressure with distilled water at RT 20 psi emu 100 psi FlowRate ml min Ll 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE CGT re 33 4 70 03 88 55 Fax 33 4 70 03 82 60 www interchim com 33 4 70 03 73 01 PL OR P b Hydraulic connection Inlet Outlet 3 16 OD 3 2mm ID 1 8 OD 2 4mm ID 3 gt Care amp Use Instructions v PURIFL ASH MINISOX IM must be stored in Isopropanol v Pump inlet and outlet must be plugged during storage Never start the PURI LASH MINMBZOX U pump without liquid v Without solvent heat build up may occur v Avoid any chemicals products Solvent Compatibility All standard solvents for chromatography can be used with the PURI LASH MINISOX I ex Cyclohexan Ethyl Acetate DCM Chloroform Acetonitrile Methanol THF Water v PH range stability 6 lt pH lt 7 5 The longer is the exposure to acids and or bases the more damage it cause v Buffers and salts are acceptable as long as they stay dissolved in solution To prevent the system from crystallization use lukewarm water to rinse
9. in 2 bytes MSB first CR b Transmission Parameters Data transmission is 9600 bauds with 8 bits without parity 1 stop bit half duplex c Task List Complete Control Table With the ASCII convention STX 02H ETX 03H 2 a ases ACK 06H NAK 15H N Version Number CR ODH P Set Potentiometer R Run S Stop U Read State Command List Data transmission is 9600 bauds with 8 bits without parity 1 stop bit half duplex v Consigne Value D Description This command allows to enter a consigne of the flow rate in percent If potentiometer is enable this command disable it 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE Takaa re 33 4 70 03 88 55 Fax 33 4 70 03 82 60 wwwinterchim com User Manual interfine interchim fr Frame Pump Address cm Flow Rate Flow Rate Flow Rate The Flow Rate format is in percent in 3 ASCII characters hundred tens units Possible reason of refused command The Flow Rate percent isn t in the scale 0 100 v Set Potentiometer P Description This command allow to enable disable the use of the potentiometer You must disable the potentiometer when you control the pump with a computer and enable the potentiometer for control the flowrate with the potentiometer manually Frame Pump Address PJ Enable Disable Enable Disable 0 ASCII characters Disable Potentiometer 1 ASCII characters Enable Pot
10. k of surveillance by the customer or due to non compliance with safety rules v The guarantee will not cover damage if the maintenance procedures recommended by the manufacturer are not complied with v Interchim will not guarantee the results of the use of the PURIFLEASH PINEOX ff Ll 211 bis avenue JF Kennedy BP 1140 03100 Montlu on FRANCE Duell T l 33 4 70 03 88 55 Fax 33 4 70 03 82 60 www interchim com so gt Service report lt O Installation O End of warranty visit O Warranty O Repair O Maintenance O Out of warranty Systemi description esis r o Sh PEE eee eee Module AC ne moe ee E E eee ere P N and description of defective spare DAC scnnnunsetweeudoterneadntaduetlegiateusunciadegsknvauvena adacyernntyenculausiedemevnseieadecheents Any further action required Leia ce senos Una rax ret thus repo dta Ne mu rax uet Rn etasu s vectutuxssateeentdanebesancesvseanternectsaxtevendnersieenedebaredy Bru ne hop Signature gt Service report lt O Installation O End of warranty visit O Warranty O Repair O Maintenance O Out of warranty System CES CITES ns teens ae ea da ete ea ea ie et ne 71 REN Module eese eese CS CONS MC T P N and description of defective spare part 28 22 horae Py teca rue esie ere pia ne edes sh aesa e tis e pec immensitat Any fur
11. s caused by impact and or bad weather The guarantee will be cancelled in case of damage caused by abnormal mechanical forces applied to the device and exceeding the limits defined in the user guide The guarantee will be cancelled in case of corrosion to the device due to solvent leakage or samples The guarantee will be cancelled in case of corrosion to electronic components caused by highly corrosive gas The guarantee will not cover damage or failures caused by assembly dismantling modification or transport after initial installation The guarantee will be cancelled in case of failure or damage due to non compliance with the closing and shutdown procedure for the device The guarantee will be cancelled in case of failure or damage due to wrong installation The guarantee will be cancelled in case of failure or damage due to wrong AC power supply v The guarantee will be cancelled in case of failure or damage due to mechanical force to the unit v The guarantee will be cancelled in case of failure or damage due to acts of nature v The guarantee will be cancelled in case of failure or damage due to non compliance with safety procedures v The customer is liable for transport risks In case of damage during transport the beneficiary must issue all reserves to the transport firm before accepting the delivery of the device v The guarantee will not cover damage caused in accidents external events contingencies or force majeure due to negligence or a lac
12. ther action required RER RER ES DATE ones wiirnsehieanitann utes IANS RS doc sal Signature gt Service report lt O Installation End of warranty visit O Warranty O Repair O Maintenance O Out of warranty System description ee TT NE eee eee Module C ICS CO EE ES TE E E ec itte vo EEE utacaess gt Service report lt O Installation O End of warranty visit O Warranty O Repair O Maintenance O Out of warranty Systemi description esis r o Sh PEE eee eee Module AC ne moe ee E E eee ere P N and description of defective spare DAC scnnnunsetweeudoterneadntaduetlegiateusunciadegsknvauvena adacyernntyenculausiedemevnseieadecheents Any further action required Leia ce senos Una rax ret thus repo dta Ne mu rax uet Rn etasu s vectutuxssateeentdanebesancesvseanternectsaxtevendnersieenedebaredy Bru ne hop Signature gt Service report lt O Installation O End of warranty visit O Warranty O Repair O Maintenance O Out of warranty System CES CIO ns teens seen da et ea ea ie ee 71 RER Module ACTOR MC T P N and description of defective spare part 28 22 horae Py teca rue esie ere pia ne edes sh aesa e tis e pec immensitat Any further action required RER RER ES DATE ones E utes IANS
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