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Operating Instructions Calibry 5.0 Pipette

1. 16 2 1 Calibration settings Calibration Settings for test methods Settings for methods Min readings for as found The minimum number of As Found measurements Calibry accepts when defining a method chapter 7 factory setting 0 Default readings for as found The number of As Found measurements Calibry suggests when defining a method factory set ting 4 Min readings for as returned The minimum number of As Returned measurements Calibry accepts when defining a method factory setting 2 Default readings for as returned The number of As Returned measurements Calibry suggests when defining a method factory setting 4 Settings for calibration procedure Settings for calibration Max number of undo s The maximum number of invalid measurement values you can delete during a calibration setting range 0 10 factory setting 10 Volumes proceed order If you select Ascending factory setting the smallest volume appears at the top of the list of calibration volumes If you select Descending the list of calibration volumes starts with the largest volume Reference number required If you select this option entering a reference number before calibration is mandatory otherwise calibration cannot be started Compensate for evaporation If you activate this setting the Enable evaporation option will always be selected in th
2. Tasks Contacts Reports and History Click on the desired tab to load the associated list e g the pipette list or contact list Underneath the list is a row of command buttons for the displayed list e g Add or Delete 3 2 List options Various options are available for the lists displayed under the six tabs You can change the pre set order of the columns in Calibry by clicking on a column header and moving it to the new position If you drag a column header into the area marked Drag a column header here to group by that column the entries in the list are grouped according to the selected column header for example If you group the pipette list by the column header Number Of Channels the entries are grouped according to the number of pipette channels and you can see at a glance which 8 channel pipettes are available To undo the grouping simply drag the column header back to its original position at the top of the list Pipette Serial Number Renee You can filter lists quickly by clicking the small gray arrow symbol that appears when the scom f f f d 414K022 D D glans cursor is placed over a column header A window appears showing all the entries in the stots won Blanks column Select the required entry or enter a character string Only entries that begin with rer 42467892 this character string are then displayed in the list To remove the f
3. In the list mark the fault correction measures which were per formed Click on OK to save the inputs and close the window The calibration dialog appears The calibration procedure is identical to that for a simple calibration chapter 9 2 When all the measurements have been preformed click on the Finish button to complete the calibration Calibration Reports 52 10 Calibration Reports Calibry produces a detailed report for each calibration that has been completed including all data that is relevant to the calibration and the ambient conditions p Calibry File Users Balances amp Devices Options Help i Pipettes A Contacta A Reports Methods Tasks A ee ee Drag a column header here to group by that column Method Name Is Printed TSO type A Mul PHO TsQ type A Mul RH ISO type A Mul Q FHRH Rainin Pipet Lit cS FY ne RY Rainin Pipet Lit CRFHRH Rainin Pipet Lit O FHR Rainin Pipet Lit aF HFH Manufacturer ll SA FH RH al Manufacturer Mode FH Calibratio b 17 05 2011 18 414K022 D 17 05 2011 16 414K022 D 14 05 2008 19 414K022 D 13 05 2008 16 42467892 _ 13 05 2008 13 76564363 13 05 2008 13 76564363 13 05 2008 13 76564363 13 05 2008 13 76564363 13 05 2008 13 42467892 13 05 2008 12 42467892 07 05 2008 13 AR444 K 07 05 2008 13 AR444 K 25 04 2008 18 TEP1 O Q
4. gt Open Formula Editor Calibry provides separate equation editors for the Z factor and the measurement uncertainty Below you will find some information on how to use the equation editors The example is based on the equation editor for the Z factor but these basic explanations apply to the equation editor for the measurement uncertainty as well Edit formula for 7 Factor ulimeg Equations f constants System values O00 E400 pavp bil patpi Air temperature C 8000 Water temperature C aO al theta ty Aaa tw stad ty Pressure in hPa hPa 999 55306 Hurmidity 3 6 32693 10 2 Alpha c for pipette 71 C 6 5235829 1 0 3 Evaporation pl 6 9435246 710 5 uncertainty of evaporation pl 3 621216 10 7 kl P H ko tatksitattal 273 15 0 34644 0 00252 0 020582 Operator Addition Subtraction Multiplication Division Power Open paranthesiz Closing paranthesis Description At the left side of the window in the Equations constants section you will find the formula for the Z factor listed at the very top Always define this formula first Below the formula you will find the definitions of the various components Note that all components used in the formula must be defined they are evaluated when the formula is calculated The available system variables and operators are listed on the right side of the window If you wish to change the formula or a particular component highlight the re
5. 0 Rag Rainin Pipet Plus R20 Rainin Pipet Lite 8ch 20 200 ul Add Edit Delete 6 1 Defining a new pipette j Quick Access To define a new pipette click on the Add button at bottom left in the main Pipet window This starts the Pipette Assistant Note When working with the RFID Option the pipette assistant will start automatically if you import the RFID of a pipette which is not yet available in Calibry Further information on the RFID option can be found in chapter 17 Add pipette Step 1 3 M Pipette Identification according to your needs Add pipette Serial Number 468 KRS1_A 2nd ID Laboa The Serial Number has to be unique and should be writen on your pipette t cannot be changed later The 2nd ID is for your own internal use and can be edited 1 This pipette SM is already assigned to another pipette Step 1 Enter pipette serial number and ID In the first window of the Pipette Assistant you are prompted to enter the serial number of the pipette This entry is mandatory and the serial number must be unique Carefully check your entry as it cannot be changed later on Optionally you may enter a second identification for the pipette 2nd ID such as an internal designation The second ID does not need to be unique thus you may assign the same ID to several pipettes Notes lf you use a serial number which currently exists in the pipette list the error message
6. Ho D So 3 2 Ho l 2 4 4 J 6 7 5 13 Channels 200 jul Systematic Error 1 6 So 0 o 1 6 Ve 1 Z a 4 z 6 T 5 Channels Generated with Calibry 5 0 17 30468 Printed with Calibry 5 0 17 0 Certificate number 1113800231 0 R1 Sample Corp Research Cat Fritz 3 Vol 4 Meas 20 100 200ul 100 ul Systematic Error 3 2 4 4 a Channels 6 Page 2 10 Calibration Reports 56 10 2 Report options When a report is displayed you can use the buttons at the bottom of your screen to activate the following options Report preview a Oss ty A Select language gt Close Print Quick PDF File ene Print eee See 2 Lan English German French Italian Spanish Japanese Pipeti Pipe E3 VIEW Print Save as POF Export to ML he Export bo Microsoft Office Delete VIEW Print Save as PDF Export to ML Export bo Microsoft Office he Delete File Balances amp Devices Ls Print Preview be Print Strg P Export Exit Report preview EER Close Print Quick PDF File Print Select language z Po Document _ Signing Selecting the report language select the language that is to be used to display or print out the report The languages available are English French German Italian Japanese and Spanish For other languages please contact METTLER TOLEDO Note Depe
7. If you wish you can automate the data backup process The Windows Control Panel contains a scheduled tasks function Add a new task specify the path to the program Calibry DBMaintenance exe in the same directory as Calibry Then specify the time intervals for the data backup and set up a password In the advanced settings you then need to enter the backup parameter which instructs Calibry DB Maintenance to perform the data backup function for example C Program Files METTLER TOLEDO Calibry5 0 CalibryDBMaintenance exe backup Now specify the location and name under which the backed up data should be saved for example D Calibry Backups mybackup bak backup Load a backup copy of a database Restore This option allows you to load data records from a backup copy into the current database Note This replaces all data in the current database with the data from the backup copy Initialize database Initialize This option deletes all data records in the current database We therefore recommend that you create a backup copy first Installing the Software and launching Calibry 11 2 4 Starting the application and selecting the required Calibry edition start Calibry from the shortcut to the Windows desktop via the Windows start menu or by double clicking the file Calibry 5 0 exe in the METTLER TOLEDO file in the Windows program directory Welcome to Calibry 5 0 Welcome to Calibry 5 0 Beta H
8. Midt Fl mont 000111222 18 02 2006 25 04 2008 26 04 2008 26 04 2008 27 04 2008 30 04 2008 amp 30 04 2008 amp 27 05 2008 RF Ry 13 07 2008 amp F PRY Dete Calibrate external Calibrate method chapter 7 If you specified q calibration interval instead of a particular date the date for the next calibration will be calculated automatically and inserted in the Task Due Date column based on the interval specified If neither a date nor an interval is specified the Due Date column remains empty BSE S ESE DS P Legend Status and Schedule The Status and Schedule columns con tain information in the form of symbols Calibration status epei a From the Help menu you can open the As found Fly Fy legend shown at left which briefly explains As returned Rig RL the symbols npa P In the upper part of the legend you will find Information about the symbols which are ee used in the Status column In the middle Sota QE Overdue part of the legend the symbols of the sy oe Inactive Schedule column are explained Method settings Quick check As return calibration only Visual inspection and as returned calibration Visual inspection as found and as returned calibrations The Tasks List 40 et RY A RY A Fg Rig Jo R LORY BO The symbols in the Status column indicate
9. Undo AFUndo Reasons for cancelling As Found measurements plain text AsFoundPossible Indicates whether or not the As Found measurement was carried out Yes or NextDueDate Next adjustment date scheduled for the pipette ReviewerName Name of the user who counter signed the report Notice Note on calibration InspectionCount Number of pipette defects selected Inspection Pipette defects selected plain text CorrectionCount umber of measures taken for defect elimination Correction easures for defect elimination selected plain text OrderNumber eference number of calibration ARVol_ChX_VolY_MZ esult of As Returned measurement as volume value pl ARW_ChX_VolY_MZ esult of As Returned measurement as weight value g ARBal_ChxX_VolY_MZ alance used for the As Returned measurement serial number AFVol_ChxX_VolY_MZ esult of As Found measurement as volume value Ul AFW_ChX_VolY_MZ Result of As Found measurement as weight value g AFBal_Chx_VolY_MZ Balance used for the As Found measurement serial number No 7J O X Number of pipette channel or H for Horizontal or V for Vertical respectively Y Number of volume or H for Horizontal or V for Vertical respectively Z Number of measurement or H for Horizontal or V for Vertical respectively CertificateNumber Certificate number Statistical data AFMean_ChX_VolY Mean value of As
10. s i Enlarges the display size of the document Instructions for Using Calibry 19 3 5 The optional menu If you position the cursor in the current list and click with the right mouse button an additional menu appears giving you quick access to particular functions The contents of this optional menu depend on the list currently displayed Specifying Managing and Adjusting Balances and Peripheral Devices 20 4 Specifying Managing and Adjusting Balances and Peripheral Devices Upon startup Calibry automatically detects and recognizes most balances by METTLERTOLEDO hence you do not need to define such balances manually However balances supporting uni directional communication only cannot be recognized automatically and you will have to add such balances to Calibry manually The menu described hereafter lets you define balances manually and you may change or make up the settings of balances already known to Calibry In addition you may configure peripheral instruments such as thermometers barometers and hygrometers Launch the Balances amp Devices Management menu Balance amp Device Management bad In the left part of the window there IS q list BE pee containing the available types of devices Device ist ey er balances barometers hygrometers and evi ai ZEEE thermometers while the right part shows all Barometer rar enone instruments known to Calibry The Required MCP105 1126243149 i ee Feat ce MCP105 1119
11. Defining Pipettes 28 6 Defining Pipettes To make defining new pipettes easy Calibry has a pipette assistant which guides you step by step through all the necessary inputs Options Help 7 CA f Reports Pipettes Methods A Tasks a Contacts ay History Click onthe Pipettes tab to open the menu for defining pipettes DER Yes iy METTLER TOLEDO In the example at left some pipettes are Drag a column header here to group by that column Pipette Serial Number Pipette Type Description Pipette Second ID Rain Plpet Lite 6ch 20 2000 uf 42467892 Rainin Pipet Lite Sch 20 200 ul 65577888844 Rainin EDP PLUS EP 10 3K338 76564363 Rainin Pipet Lite 8ch 2 20 ul 7864767 Rainin Pipet Lite 12ch 20 200 ul _ 9087436 Rainin Pipet Plus R20 9954324 Rainin Pipet Lite 8ch 20 200 ul a0500089a Rainin Pipet Lite 8ch 20 200 ul AR444 K Biohit E Pet El 100 S000ul DTR777444 DT Pipet 8ch 20 200 ul 206207B Rainin Pipet Plus R20 302062078 MRM878999 Rainin Pipet Lite 8ch 20 200 ul Pipette Type Rainin Pipetite Sch 20 200 ul Rainin Pipet Lite 8ch 20 200 ul Rainin EDP PLUS EP 10 Rainin Pipet Lite 8ch 2 20 ul Rainin Pipet Lite 12ch 20 200 ul Rainin Pipet Plus R20 Rainin Pipet Lite amp ch 20 200 ul Rainin Pipet Lite 8ch 20 200 ul Pipette Number of Channels already defined Number of pipettes displayed 14 Biohit E Pet El 100 5000ul DT20 200 ul ma 0 f0 N
12. MCP1O5 MCP1O5 surement is necessary or just being performed If a reference measurement is necessary start it on the balance If the reference measurement was started automatically by Calibry wait until it has finished When the reference mea surement has been successfully completed the green balance symbol is 1126300064 displayed al rails Yellow The calibration proceeds and Calibry receives the measurement values from the balance Calibrating Pipettes 46 Underneath the result window you will find the following additional settings Bh Stele sesserstie Enable evaporation If this option is activated the measure Eoo oon m ment values are corrected for the evaporation value which you specified in the environmental parameters Environment gt Evaporation Tare between readings Activate this option if you wish to tare the balance manually after each measurement Note Both the above options are not available if the calibration is carried out on several MCP systems Accept low values Calibry automatically discards measured values which are below 65 of the expected value Activate this option if you want Calibry to accept these values as well When the green balance symbol appears you can select the volume you want to pipette first from the list above the balance symbol the sequence of volumes can be freely chosen Pipette the selected v
13. Owner OwnerCity OwnerPhone OwnerFax OwnerEMail DelClientNumber DelCompany Company name Delivery DelLastname DelFirstname First name Delivery DeiDepartement DelAddress Address Delivery DelState DelZIPCode ZIP code Delivery DelCity DelPhone DelFax City Delivery hone number Delivery Fax number Delivery DelEMail E mail address Delivery FactClientNumber Client number Invoice FactCompany Company name Invoice FactLastname Family name Invoice FactFirstname First name Invoice FactDepartement Department Invoice FactAddress ddress Invoice FactState tate Invoice FactZlPCode IP code Invoice gt N Advanced Options Field name Description FactCity City Invoice FactPhone Phone number Invoice FactFax Fax number Invoice FactEMail E mail address Invoice Pipette PipetteSerieNumber serial number of the pipette PipetteName Pipette name PipetteSndlD PipetteRangeMax PipetteRangeMin PipetteDescription PipetteManufacturer PipetteChannelCount PipettelSOClass g9 cond identification of the pipette aximum volume of the pipette in microliters inimum volume of the pipette in microliters ipette type ipette manufacturer Number of pipette channels ISO Class of the pipette 0 unknown 1 ISOPistonTypeA 2 ISOPistonTypeD1 3 SOPistonTypeD2 4 IS
14. Type name Description Manufacturer een D D SR Channels Name for the new pipette type Description for the new pipette type Enter the manufacturer of this pipette type Mh NE E Ern D b F b F Bette bae Vorme i p fto x a Number of channels of this pipette type Range From the list select the volume range which applies to the new pipette type If no suitable range is available click on the Range editor button to define a new range ae 4 Click on the Add button In the min and ni 40n max fields enter the minimum and maximum 10nl 100 nl _ 2ni 200i volumes of the respective pipette type and the 0 1pl 0 2yl l l a corresponding unit pene uN here Click on Save to save the new range 200 nl 2 pl Quit the Range Editor and the new range is now available in the Manage pipette type window ISO Class ISO Class Piston pipettes types A Class according to ISO 8655 for the current Piston pipettes types A Piston pipettes types D1 __ Piston pipettes types D2 Hand driven burettes Motor driven piston burettes Unknown pipette type If the pipette type does not match an ISO class or if you do not know the class select Unknown Defining Pipettes 30 F Add pipette Step 3 3 Contact Information Contact Mettler Toledo Lab vVeighing Solutionsi Merini Milay ka Select a contact for th
15. and Level in the same way as you would when you define a new user chapter 13 1 Note For the active user and the administrator only the user name can be changed Once all changes have been completed click on Save to save the modified user data In the user list highlight the user that is to be deleted and then click on the Delete button One of the following messages will appear If you answer yes to the prompt the user is deleted However the name of the deleted user will still appear on existing calibration reports If you try to delete the user which is currently active the following message appears The active user cannot be deleted Note If you really want to delete this user you must log onto Windows using a different user account for which a corresponding user has to available in Calibry Audit Trail 64 14 Audit Trail Calibry records data relevant operations in a so called audit trail see also chapter 20 This makes it possible to find out at any time which user worked with Calibry when and what actions they performed Options Calibration Setup Configuration Unscheduled Calibration Methods View audit details pos detail Date amp Time User Computer Action type Action Upar MICA edited beret ieri Lowel Lave aided evel Lewet4 removed liner ML creoted Peete SN ALU Aled t Damwrder ho postte SN 41402 Romario l gt gpette 4140001 D4 O At
16. fields are also available for the As Found status check assuming you have selected the Calibration with inspection and As found mode Usually the status check is automatically based on the same tolerances as the actual calibration For special cases you may modify the tolerances for the status check by entering appropriate factors for the systematic error and the random error Important The Factor fields are available only if you have selected the User setting see above i e you do not calibrate the pipette according to manufacturer s specifications or ISO standards Saving a test method Once you have defined all parameters of the new method click on the Save bution to save the new test method G Saye Calibration Method iethothname ari descrietion Enter an appropriate name for the method The method will Hame Custom 8x 200p appear with this name in the list of methods Note If the selected he oe ee tolerance values are based on the ISO standard Calibry suggests BS CrIRMON uN n j SEE RE RTE R ERA a method name starting with ISO If the tolerances are based on the manufacturer s specification Calibry suggests Manufacturer You are about to save anew method Please check the name and i description then click OK instead If you have defined your own values Calibry will suggest Fr Custom as a name In the Description field you may enter a de
17. 11138300 Setting up Calibry Balance properties Usually Calibry will detect the MCP automatically otherwise add the MCP as a new boal ance as shown in the example to the left see chapter 4 Balance into Communication Name Fic Catreton Sen oo The settings marked with a red dot are mandatory while the other settings may be modi Seretrumber freaasog2 fied to match your local conditions Internal ID 4 Balance line MCP aa pais In the Options Configuration Balance MCP balances menu see chapter 16 set the Locatin X Process adapter parameter to Off In the same menu you may define further settings ee G for the MCP as needed you may even advise Calibry to inform you when the instrument oo Le is due for adjustment The number of pipette channels to be calibrated 1 is defined when setting up a pipette type chapter 6 Notes on operation Baud rate ee The measured values are transmitted to Calibry when the Start key of the MCP is pressed ne The entire pipette calibration workflow is controlled by Calibry Handshake Hardware Configuration 101 19 5 Calibry and XP precision balances This chapter provides information on how to use Calibry in conjunction with the XP precision balance by METTLER TOLEDO The XP standard equipment includes a serial RS232C interface optional interfaces are available on request The balance interface is to be connected to the C
18. 16 2 8 Database settings Database These settings are defined when Calibry is installed and can only be changed using the Calibry DBMaintenance program The follow ing information is displayed SQL server instance Instance of the SQL server on which the Calibry database is running Database name Name of the Calibry database Version Version number of the Calibry database 16 2 9 Options for experts Advanced In this group of settings experts may further customize Calibry This may be mandatory for customers working to particular standards that require the documentation of the values described below Note The values described hereafter appear only in the exported records and basically Calibry does not perform any calculation based on these values except if you are using one of these values in the equation editor for calculating the Z factor or the measurement uncertainty see chapter 18 With the factory settings none of these options are activated Set uncertainty value for evaporation You may set up Calibry to display an additional field for entering the measurement uncer tainty of the evaporation value when defining the environmental parameters Set cubic expansion coefficient for pipettes You may set up Calibry to display an additional field for the entry of the cubic expansion coefficient when defining a new pipette In this case there will also be a second field for the measureme
19. B of the water temperature thermometer used at the end of the As Returned measurements of the As Returned measurements measurements Serial number of the barometer used at start of the As Found measurements Last adjustment date of the barometer used at start of the As Found measurements Error mode for adjustment values of the barometer used at start of the As Found measurements G disabled none SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the barometer used at start of the As Found measurements 2nd coefficient for adjustment errors Beta or RE of the barometer used at start of the As Found measurements 3rd coefficient for adjustment errors A of the barometer used at start of the As Found mea surements Ath coefficient for adjustment errors B of the barometer used at start of the As Found mea surements Number of the adjustment certificate of the barometer used at start of the As Found measure ments Note on adjustment for the barometer used at start of the As Found measurements Serial number of the barometer used at the end of the As Found measurements Last adjustment date of the barometer used at the end of the As Found measurements Error mode for adjustment values of the barometer used at the end of the As Found measure ments disabled none
20. Chart damaged the status check As found and pass directly to the window for selecting the measures taken to correct the fault The next window is identical to the window for a calibration with inspection and fault correction as described inthe previous chapter Make the necessary inputs chapters 9 2 and 9 3 and then click on Calibrate Calibration for pipette 414K022 D Rainin Pipet Lite ch 20 200 ul M Calibration Settings Tip AS found tips ki Add Balance Emo i Use MCP 1 System Reference number MRF 54 22 Environmental parameters Air temperature eae Vater temperature i Hurmidity 30 Z Factor 1 0039 pling Pressure 900 hPa Evaporation 0 plicycle Failed to get the environmentals Ect Physical Inspection Corrective Action Invalidate Pipette Calibrate Cancel As found l s onthe balance s Print key to scare the calibration Lo ume 20 pl 414K022 D Rainin Pipet Lite Sch 20 200 ul 8 channel s Method Brand New 8x 200p1 3 Vol 4 4 Meas 20 100 200p 20pl 100p 200p1 8 channel s Current volume Volume 20 pl Measurements 4 Environmental conditions Pressure Humidity Air temp Vater temp Z Factor Evaporation 900 hPa 30 Fase Fea 1 0039 pling 0 plicycle Total progress Status 204i 100p 200p Status 20ul 100pl Systematic Error Random Error Systematic Error Ri T25 1 0 8 0 ch 1 ch 2 ch 3 Ch 4 Ch 5
21. Column Chooser Displays a list of all other available columns If you wish to add a column select it from the list and drag it to the required position Best Fit Selects the optimum width for the selected column and auto matically adjusts the width of the other columns Best Fit all columns Optimizes the width of all columns with the aim of displaying as many of the selected columns as possible Clear Filter This option only appears if a column has been filtered using the filter editor as described below Filter Editor Opens the filter editor allowing you to filter the entries by selected criteria The filter editor is described below You can use the filter editor to specify which information is to be displayed in the selected column The column to which the filter is to be applied is shown in square brackets and blue font By default Calibry displays the column from which you started up the filter editor When you click the entry a list of all available columns in the list appears and you can select the desired column The mathematical operator is shown in green You can click through the following to select the operator you require Equals Does not contain Does not equal Begins with Is greater than Ends with ls greater than or equal to Is like Is less than Is not like Is less than or equal to Is blank Is between Is not blank Is not between Is any of Contains Is none of
22. Instructions for Using Calibry 16 Depending on the selected operator one several or no gray lt enter a value gt fields ap pear Click on the field to enter the required value If you wish to use more than one filter criteria click the symbol at the top right of the filter editor amp Filter Editor This menu also contains the option Add Group which you can use to define a subgroup i for the filter Opposite is an example for filtering with a subgroup In this example after E Aa a filtering only pipettes whose serial number begins with 123 or which have 8 or 12 PEEP EnA channels are displayed in the list Number OF Channels Equals 12 1 Cancel After you have established the filter criteria click OK The column is now filtered and only entries which meet the defined criteria are displayed Once a column has been filtered the Clear Filter option becomes available in the menu allowing you to remove the filter Notes When quitting Calibry the filter settings will be maintained i e the lists will still be filtered when launching the application the next time All printing and export functions relate to the contents of the current list If you want to print or export the complete list make sure it is not filtered 3 3 The menu line Calibry File Balances amp Devices Users Options Help pea Pipettes nw Fa r A Tasks A contacts f Repor
23. Range editor button to define a new range Click onthe Add button Inthe min and max a fields enterthe minimum and maximum volumes aE mE 7 and the corresponding unit pomu ET o ee p MRIJ Click on Save to save the new range and to ozu zori 20000 quit the Range Editor 0 2 pl 10 1pl 0 2pl Tosu 50 nl 500 nl 1 yl 100 nl 1 pl tl tul ipl i 2ul 0 1pl 2pl 2y 200 nl 2 pl r Range editor Yolume Range min 25 jul aa max 250 ul hd m gesa Defining Test Methods 33 Channels Number of channels of the pipette s needing to be calibrated with the new test method ISO Class Piston pipettes types A ISO Class Class according to ISO 8655 for the pipette s aie which are to be calibrated with the new test iston pipettes types D1 Piston pipettes types D2 method If the pipette type does not match an Hand driven burettes ae Ase eee ISO class or if you do not know the class select Unknown Unknown Click on OK in the Method Editor to continue defining the new testing method Method Editor Mode Channel selection C Quick check Calibration dododeddod od Jojo BU FO i 2 23 3S a Se Se Oe aA 2 C Calibration with inspection Calibration with inspection and As found data conventional balance only With a MCP balance all channels are ch FH FH proceeded Set tolerances Tolerances e W Enabled I Enabled W Enab
24. SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the barometer used at the end of the As Found measurements 2nd coefficient for adjustment errors Beta or RE of the barometer used at the end of the As Found measurements 3rd coefficient for adjustment errors A of the barometer used at the end of the As Found measurements Ath coefficient for adjustment errors B of the barometer used at the end of the As Found measurements Number of the adjustment certificate of the barometer used at the end of the As Found measurements Note on adjustment for the barometer used at the end of the As Found measurements Serial number of the barometer used at start of the As Returned measurements Last adjustment date of the barometer used at start of the As Returned measurements Error mode for adjustment values of the barometer used at start of the As Returned measure ments disabled none SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the barometer used at start of the As Returned measurements 2nd coefficient for adjustment errors Beta or RE of the barometer used at start of the As Returned measurements 3rd coefficient for adjustment errors A of the barometer used at start of the As Returned measurements Advanced Options
25. to demonstrate the program or for training or testing purposes For these situations demo mode has the following advantages You do not need a balance to perform simulated calibrations Since no real measurement values are recorded calibrations run much faster You can input random measurement values e g for testing In principle you can work with Calibry in demo mode exactly the same as in normal working mode The only difference is the procedure for calibration which is explained below Note Calibry does not distinguish between data which is input or determined in demo mode or in normal working mode It always uses the same database All settings calibrations etc that you make in demo mode are handled exactly the same as those you make in normal working mode however they are not added to the history Reports of calibrations you perform in demo mode are marked with DEMO Calibration for pipette 414K022 D Rainin Pipet Lite Bch 20 200 ul When yon start a calibration the window at left OPE Cals example If you wish to work in demo mode select Demo in the balance section M Calibration Settings Note If Calibry did not find a balance at startup only the Demo E up Else z setting will be available and Calibry automatically runs in demo Balance mode Reference number Select the appropriate parameters in this window see chapter 9 then start calibration M Environmental parame
26. AN MAUMA DOING OG ieee ee ee er eee Eo aeaa ee a et ee ee 105 Calibry and AT MT UMT balances c ccc ccccccsccccceseeeeceseeeeeceeseeeeeeeeeeeeeesceeeeeeeceseeeeeeeesaeeesseeseeeesensaaaeseesseaeeessenaeeeseees 106 calib and AG DAINO YS cisnienia sn anes exiandub anon beige RAEO AEE AES tn iis 107 CATHIE TOUS AO ONC GS cic cocina oara etry grees etl en increased ota ed rr te ayn E adenoid neato 108 Cae PAOR ILOa Ae AA E ener reve ee meee ee ee ee eee ee 109 Colibry and genen af 0 p cots eee ee mm rnee ite ne ee ner er am ete ts Sere en et net ee nee en nT ee eer ne eee Ae ee 110 PR Ne aise acc alle otc ree ct ate tance EEO 111 Information about time MANAGEMENT iN COLIDIY cece ceeesccessesseeeesceseeesseesseeeeeeeeeeeeseeeeeeeecseeesesasaeessseaseesesenaaass 111 Formulae used in in Calibry 9 0 cee ecceeccccecesseeseeeeeseeseeeeeseeeeeceseeeeecesseeeesEHGASESSEEEIAESSSDEAEEESSSDAEEEASSSHASGEESESeAGHAE ER EErEE 113 Formulae ii decordance WiN IOO GOOI eee eee ee eee eet ee ee ee eee eee eee eee 113 Form le TN accordance Wih ISO R 2040 ccc cscs siaaarceier peasonctx oessien nn wa diveons e i vesteecued E diane 115 Entenng OF CalCUIATING TOIEYANCES S DECI COTONS escaissar kaasa a iee a iaiiaeeeai esia 116 Using measurement values and rounding in Calibry sss nsesnnreerrrsserrserrrrenrrrenrrrssrrrssrrrserrserrnnrrrsnrnrnnrrrssnrrsserersnne 117 Calculating measurement uncertainty in accordance with ISO TR 20461 sssnsssesnnrssssr
27. Bits Handshake Hardware Configuration 104 19 8 Calibry and XS WX balances This chapter provides information on how to use Calibry in conjunction with the XS analytical and precision balances and the WX bal ances by METTLER TOLEDO The XS and WX standard equipment includes a serial RS232C interface optional interfaces are available on request The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and the balance are switched off Connection RS9 RS9 cable 1 1 m f 11101051 Setting up the XS WX balance set the Host interface to the following values Baud rate 9600 Baud Bit Parity 8 Bit none Stop Bits 1 Handshake XON XOFF End of line character lt CR gt lt LF gt and Character set ANSI WINDOWS Setting up Calibry Usually Calibry will detect the XS WX balance automatically otherwise add the XP WX as a new balance as shown in the example to the left See chapter 4 Balance info Communication oe parr The settings marked with a red dot are mandatory while the other settings may be modi Serial number fasga5066 lt sS fied to match your local conditions m am Internal ID Balance line Moas In the Options Configuration Balance Other XS XA balances menu you may advise eee Calibry to inform you when the balance is due for adjustment Location On this computer Yes Door mode N
28. Ch 6 ch 7 ch 8 FE Tare between readings Accel Calibration for pipette 414K0272 0 Rainin Pipet Lite Gch 20 200 ul E Corrective Action Description Broken shaft Electronics changed New Friction Ring Mew plunger Mew rod New Seal New Shaft New Tip Ejector C Ot of order _ Recalibrated Calibrating Pipettes 5 After the initial inspection of the pipette you may carry out a status check As Found Basically this is similar to the normal calibration but the values which are determined are used only for the status check In contrast to the real calibration the status check usually involves a reduced number of measurements The number of measurements for the status check can be specified when defining the test method chapter 7 Perform the measurements necessary for the status check Conclu sion of all measurements is confirmed in the Instructions section of the window Click on the Finish button to conclude the status check Note Should the status check end prematurely you can end the measurements at any time using the Finish button If inspection of the pipette Physical Inspection atthe very begin ning of the calibration procedure revealed faults and these were marked in the list the Corrective action window opens for input of fault correction measures which were performed otherwise the calibration dialog opens immediately
29. Comment optional i should be serviced asap calibration p Cancel Calibrating Pipettes 42 9 Calibrating Pipettes The instructions in this chapter assume that all previously necessary operations have already been completed see previous chapter 9 1 Starting the calibration dialog You can launch the calibration dialog from the Tasks list by selecting the pipette you alibrate l na ae A wish to calibrate and then clicking on the Calibrate button You can also select the pipette in the Pipette list click the Quick Access button see chapter 12 choose the test method to be used and start the calibration with the Calibrate button The procedure for the calibration depends on the calibration mode you have selected with or without checking for faults additional status check etc see chapter 7 The individual calibration modes are described separately below 9 2 Simple calibration of a multi channel pipette Fij With these calibration methods Calibration and Quick check the pipette is only calibrated no check for faults and no status check is made However please still read this chapter even if you do not want to work with these calibration methods since it contains instructions and information which also apply to the other calibration methods e g selection of the pipette tips or specification of the environmental conditions Calibration for pipette 906 436 Rainin Pipet Plus R
30. Date on which the performance of a pipette is checked between official calibration dates in order to check conformity to required tolerances Notes about the Task list In the program specifications timeframes for monitoring pipettes can be established in the Tasks list Options Calibration Setup schedule From there you can also specify whether tasks should be created automatically The following applies to the creation of tasks Atask is created automatically if the calibration date entered or calculated corresponds to the timeframe of the Task list and auto matic task creation is activated see above A task is created manually by clicking the Add to Tasks button When a calibration is started a task is always created Appendix 112 Calculating the next calibration date After a successful calibration Calibry calculates the next calibration date based on the specifications If this is not possible for example because a specific calibration date has been set or because a period of limited validity was set for an interval and this has expired a user with the correct authorization needs to set new calibration schedules If no calibration date was set None the user will not be prompted to set new schedules following a successful calibration i e the pipette will no longer be monitored by Calibry After an unsuccessful calibration Calibry does not calculate a new calibration dat
31. FHR 25 04 2008 15 TEPL 1 View Print Delete Pipette Seria Rainin Pipet Lit 150 Bch 2 20 ul Rainin Pipet Lit testo Tepip_Calib_Only Balance Used Demo Demo Demo Calibrated By SPI SPI Devenport Jsir spr Spr SPI SPI SPI amp pu Admin KEk History Number of reports displayed 52 a Calibrated 6 Balance Seri Fal Admin Fi Admin Fil Devenport amp Fy SF lAdmin Status Pipette Seca MERT 262 MERT 262 MERT 262 7 RFU BRD admin RB RF Rg Admin Sid Rll admin as Paii Admin R Admin RAV BAU amn Fig Admin Export as XML Export to Microsott Office Click on the Reports tab to open the calibration report menu This menu contains the calibration reports for all pipettes Alternatively you can click on Reports in the Quick Access dialog to view the calibration reports for the selected pipette Most columns of the report list contain information which you are already familiar with test method types of pipettes and pipette serial number etc The two columns Calibration Date and Is Printed provide information on the creation date of the relevant report and whether it has already been printed out Calibration Reports 53 10 1 The contents of the reports YEW Highlight the desired report in the report list and then c
32. Name Biling Compa Calibration User Calibration Co Mettler Toledo Owner Zip Code Owner City Owner State Misty Millage virtual Town Owner Company Name Owner First Name Owner Phone Owner Address 13 Calibration User z i Nightway Calibration Co Miller 01 123 456 Ocean Side 41 44 944 2211 Im Langacher Greifensee Mettler Toledo Merini Add Edit Delete 5 1 Defining a new contact To define a new contact click on the Add button at bottom left in the main Contact window A window opens for entering the cus tomer data 7 Add contact Copy contact information from WTE Delivery Billing Company Client Department Last name First name Address City f State Zip Phone Fax 45678 98 765 432 azes Use owner address also for E delivery address E biling address Enter the owner data see example at left Note using the scroll list Copy contact information from you can copy an existing entry into the window and edit this if required If you wish to use the same data for shipping Delivery and or invoicing Billing check the respective boxes at the bottom of the window This automatically copies the owner data to the respective entry masks If you wish to enter different data for shipping Delivery and or invoicing Billing click on Next or on the respective tab at the top of the window The entry masks fo
33. adjustment Error mode for adjustment values ErrorMode 0 none 1 Random Error and YE Enor 2 2AB Ist coefficient for adjustment errors Alpho SE Beta RE SU 3rd coefficient for adjustment errors A SS 2 __Aheosfienforagusimentora 8 Ath coefficient for adjusiment errors B Thermometer 2 blocks of data for As Found and As Returned Pp measurement the thermo meter was used for As Returned or As Found ee a y Internal ee oe of the unit Advanced Options 86 Group Subgroup 1 Subgroup 2 Subgroup 3 _ Subgroup4 XMLelement Description a SN Serial number of the thermometer Serial number of the thermometer _ of the thermometer ue e of last adjustment Error mode for adjustment values ErrorMode 0 none 1 Random Error and se Error 2 2AB o aa Ist coefficient for adjustment errors Alpho SE oe ee ee eee co Ese _ D e AA po S S OalCertificate Number of adjustment certificate oo T S o OO fCaotice Note on adjustment __ Barometer 2 blocks of dota for As Found and As Retumed Type of measurement the barometer was used for As Returned or As ee CT ID Internal identification of the unit _ Internal identification of the unit _ of the unit a SN _ Serial number of the barometer eS CalDate Date of last adjustment Error mode for adjustment values ErrorMode 0 none 1 Random Error a
34. c Measurement uncertainty values from a data sheet d Measurement uncertainty from the calibration certificate 4 The formula required to calculate the expanded measurement uncertainty is created in the equation editor There the measure ment instrument parameters previously entered can be used together with the variables listed in the following table to perform the calculation Appendix 119 Measuring device Calibration error mode SEand RE 2B Equation editor Export to MS Office Balance SE Alpha dBAlpha AFBalanceAlpha ARBalanceAlpha RE Beta dBBeta AFBalanceBeta a ee ee N A A dBA AFBalanceA ha a N A dBB AFBalanceB SS i ie With regard to the measurement instrument parameters for the environmental conditions a distinction must be made according to whether the measurements are entered automatically via the Calibry Capture Tool or manually Calibry Capture Tool Similarly to the balance the measurement instrument parameters can be entered into Balances amp Devices Management and used directly as a variable Measuring device Calibration error mode SE and RE Export to MS Office Water thermometer SE Aloha dtwAlpha AFSWaterThermAlpha AFEWaterThermAlpha ARSWaterThermAloha AREWaterThermAlpha RE Beta dtwBeta AFSWaterThermBeta AFEWaterThermBeta ARSWaterThermBeta AREWaterThermBeta N A A diwA AFSWaterThermA AFEWaterThermA ARSWaterThermA AREWaterThermA N A diwB AFSWaterThermB AFEWaterThermB ARSWat
35. calibration method Steps which are identical to those of a simple calibration chapter 9 2 are not described again pr Physical inspection Physical Inspection Corroded piston _ Electronics broken Froition ring is missing or cracked Micrometer out of phase Mo movement possible Gut of Specification Plunger bent Seal leaks Shatt damaged Description Calibration for pipette 414K0272 0 Rainin Pipet Lite Gch 20 200 ul Ea Corrective Action C Broken shatt Electronics changed New Friction Ring Mew plunger Mew rod New Seal Description Mew Shatt C New Tip Ejector Out of order _ Recalibrated Reference number MRF 54 Ze Environmental parameters Air temperature 25 70 Vater temperature 257 C Humidity 30 Factor 1 0039 pling Pressure S00 hPa Evaporation 0 plicycle Failed to get the environmentals Edit Physical Inspection Corrective Action Invalidate Pipette Calibrate Cancel When the calibration dialog is started chapter 9 1 the window Physical inspection for checking the pipette for possible faults first opens The list installed at the factory contains a selection of the most common faults Note In the Options Calibration Setup menu you can edit the list of the most common faults or if desired translate them into your own language see chapter 16 Inspect the pipette and mark any faults in the list of detected faults Click on OK to
36. calibration results that are included in the reports and the respective data will no longer be available to Calibry Make sure that you really do not need this data or that you have already exported or printed it out Pipette History 58 11 Pipette History Calibry runs a so called History for each pipette with the results of all calibrations that have been carried out Entries in the history cannot be changed or deleted F Calibry SAE Click on the History tab to open the his File Balances PEFEA Options Help t O ry m enu l METTLER TOLEDO The columns of the history list contain infor OF a E a A e E crate OF evans aly Hoy mation which you are already familiar with COO pipette serial number and type of pipette rag a colann header here to toup by that can contact etc Pipette Serial Number Pipette Type Pipette Second ID Pipette Type Manufact Owner Company Name Owner Last Name Owner First Name 76564363 Rainin Pipet Lite ch 2 20 ul Rainin Sample Corp Fritz N ot e Yo u c q n c h q n g e th e q 0 0 e q r q n C e 7864767 Rainin Pipet Lite 12ch 20 Rainin Sample Corp Cat Fritz 1 Biohit Proline 1ch 10 100 ul Biohit Calibration Co Miller Max a0500089a Rainin Pipet Lite Sch 20 2 Rainin Calibration Co Miller Max of th e h Sto ry St to SU it YO Ur OWN S pec ifi C 302062076 Rainin Pipet Plus R20 Rainin Calibration Co Miller Max 42467892 Rainin Pipet Lite amp
37. environmental data to Calibry see chapter 18 the connected measuring instruments are recognized and added to the list automatically If you wish to add a new device manually highlight the appropriate type barometer hygrometer air temperature thermometer or water temperature thermometer in the list and then click on the Add button Specifying Managing and Adjusting Balances and Peripheral Devices 25 Make sure the desired type of device barometer hygrometer air temperature thermometer or water temperature thermometer ap Device type and serial number pears in the Type field then enter the serial number of the new device Click on the OK button to add the new device to the list Type were Brewery Note If the new device does not show up in the list select Refresh from the File menu item to update the list Add new device omen If you wish to enter the adjustment data of a barometer hygro meter or thermometer select the respective device from the list Calibration result and then click on the Calibrate button The window shown at left appears and you may enter the result of the adjustment Pass or Fail In addition you may enter the number of the certificate as well as a notice Note In the Options Configurations menu chapter 16 you may Certificate No e a select additional fields for the entry of measurement errors to show Opti
38. for As Found measurements Serial number of balance used for As Found measurements Location of the balance used for As Found measurements eadability of the balance used for As Found measurements ast adjustment date of the balance used for As Found measurements umber of the adjustment certificate of the balance used for As Found measurements ote on adjustment for the balance used for As Found measurements Error mode for adjustment values of the balance used for As Found measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB 1st coefficient for adjustment errors Alpha or SE of the balance used for As Found measure ments 2nd coefficient for adjustment errors Beta or RE of the balance used for As Found measure ments 3rd coefficient for adjustment errors A of the balance used for As Found measurements Ath coefficient for adjustment errors B of the balance used for As Found measurements Type of balance used for As Returned measurements serial number of balance used for As Returned measurements ocation of the balance used for As Returned measurements eadability of the balance used for As Returned measurements ast adjustment date of the balance used for As Returned measurements umber of the adjustment certificate of the balance used for As Returned measurements ote on adjustment for the balance use
39. for the current Pipette PC NB Clause Number of pipette defects selected Advanced Options 84 Group Subgroup 1 Subgroup2 Subgroup3 Subgroup 4 XML element Description _ o S d S d Cioase l blockofdataperpipetiedefect po fC tuseNo Number of the pipette defect po ext Description of the pipette defect E eee NBClause Number of measures taken for defect elimination 1 block of data per measure taken defect elimination Number of the measure taken for defect elimination Description of the measure taken for Text ers S Sanne elimination m 2 a of data ae As Found As Returned RT measurement As Returned o type or As Found Reference number of the calibra OrderNumber tion same for As Found and As Returned Pipette tip Cubic expansion coefficient of the e Ree EGS Date Date and time of calibration Name of the user who carried out the measurement BFactor Z factor pl mg SS a Evaporation factor ul measuring cycle EvaporationError Uncertainty of the evaporation factor ul measuring cycle Measurements cancelled Undo The particular cheers a separated by tabs 1st digit Number of the volume 2nd and 3rd digit Number of the measurement followed by the reason for a 2 blocks of data a before oa o Emone Saft caiion a whether the e data Time has been acquired or entered before or after calibration i Pressure B
40. import a Microsoft Access database from an earlier version of Calibry Import Selecting an existing Calibry 5 0 database or creating a new database Click the Configure button in the database utility program select the SQL server instance to be used all existing SQL server instances are displayed If you wish to use an existing database with Calibry select it from the list all available databases for the selected SQL server instance are displayed If you wish to create a new database enter its new name Confirm by clicking OK If you have entered anew name the utility program will ask whether you wish to create a new database Click Yes to this prompt Importing an older Calibry database First configure a Calibry database as described above The data from the older Microsoft Access database is imported into this database Installing the Software and launching Calibry 10 Click the Import bution in the utility program and locate the database whose content you wish to import Calibry DB Maintenance ea The warning opposite alerts you to the fact that the import operation DD Reprctonnt peste extr data yar clr database Ths opeatn stevertiewthut a backup will replace all data in the current database with the imported data If you still need this data you should first back up the current database sie uae by clicking Yes This starts the backup dialog see below After successfully backi
41. is recalculated based on the schedule External calibrations The Tasks list contains the Calibrate external button chapter 8 This allows tasks to be defined as being carried out externally and the relevant data calibration date certificate number calibration result optional comments to be entered In terms of scheduling external calibrations are treated in exactly the same way as those carried out in Calibry i e the next calibration date is calculated on the basis of the established schedules RFID data additional RFID option After successful calibration if pipettes are equipped with an RFID chip the information calculated for the next calibration is recorded on the chip after confirmation from the user For Quick check calibrations the quick check date is updated on the chip For normal calibrations without additional status checks Calibration the next calibration date is recorded on the chip For calibrations with additional status checks Calibration with inspection the last and next service dates are updated on the chip Appendix 113 20 2 Formulae used in in Calibry 5 0 20 2 1 Formulae in accordance with ISO 8655 The following formulae in accordance with ISO 8655 6 2002 are used in Calibry 5 0 Mass of the pipetted water m m mM m Mass of the pipetted water measured by the balance mg m Mass of the weighing vessel before pipetting measured by the balanc
42. setting the calibration values are displayed with the unit otherwise the measurement values are displayed without a unit 16 2 2 Settings for the environmental conditions Environmentals Ask for environmental conditions after calibration If you activate this option you may enter the environmental parameters again after calibration this does not recalculate the Z factor The new values appear on exported reports only Factory setting option not activated Disable air and water temperature editing If you activate this option the water and air temperature values cannot be changed in the calibration dialog which may be useful if you are working in a climate controlled room with a constant temperature Factory setting option not activated Use water temperature as air temperature If you activate this option factory setting Calibry assumes that water and air tempera ture are the same otherwise the environmental parameters window will show an additional field for entering the air temperature Disable editing for pressure If you activate this option the current barometric pressure part of the environmental parameters of the calibration menu cannot be changed before you do the calibration Factory setting option not activated Disable editing for humidity If you activate this option the current air humidity setting part of the environmental parameters of the calibration menu cannot be changed befo
43. shown at left appears lf you enter the serial number of an earlier pipette that has undergone at least one calibration and was then deleted you are asked whether you wish to reactivate the deleted pipette Click on the Next button to call up the next window of the Pipette Assistant Defining Pipettes 29 Step 2 Defining the pipette type Inthe second window of the pipette assistant you define the pipette type Click on the arrow next to the type designation to display a list of all available pipette types The fields below the type designation contain additional information about the selected pipette type F Add pipette Step 2 3 gt Type information Type name WRainin Pipet Lite amp ch 20 200 ul Description Rainn Petite 60n 202004 If the desired pipette type is available in the database and all displayed information is correct you may click on Next to load Manufacturer Rann SCSC lt 7S SS the third window of the pipette assistant Channel Bb o However if none of the available pipette types correspond to your Range Fon zop new pipette click on the Add button to create a new pipette type Previous a Cancel as explained below Creating a new pipette type select from the list a pipette type which is as near as possible to the new type you want to create and then click on the Add button The parameters of the selected type can be edited in the lower part of the window
44. software portal or create a new user account directly in Calibry using your user data You can then activate Calibry from the software portal lf you select manual activation your license key is saved locally You can then send this file lic to your Mettler Toledo representative or transfer it to the METTLER TOLEDO software portal via the link provided requires internet access and a browser In both cases you will receive an activation file which you can load in Calibry Installing the Software and launching Calibry 13 2 Software update procedure Calibry is under continuous development and METTLER TOLEDO provides the latest versions of the application to their registered customers Please note the following before starting an update procedure For all pipettes that have already undergone a status check As found measurement make sure the calibration procedure has been completed i e the As returned measurement must have been carried out Verify this in the Tasks list and carry out the measurements that are probably missing Back up your database before starting the update procedure see chapter 2 3 Quit Calibry if your are working on a network quit the application on all workstations Please proceed as follows when updating Calibry Install the new version of Calibry see chapter 2 2 Update your previous database using the database utility program Calibry DB Maintenance see cha
45. the balance are switched off Connection Serial Data I O Cable 00210493 Setting up the AT MT UMT balance Set the balance interface to the following values Data transfer mode Stb Baud rate 2400 bd Parity E Handshake HS soft and End of line character crLF Except for special applications we recommend to disable the door management function of Calibry see below and to set up the bal ance accordingly Select DoorAuto if you wish to use the automatic door function otherwise disable the automatic door function Setting up Calibry Usually Calibry will detect the AT MT or UMT balance automatically otherwise add it as a new balance as shown in the example to the left see chapter 4 The settings marked with a red dot are mandatory while the other settings may be modi fied to match your local conditions Balance into Communication Name aT John Meyers Serial number 297592 Internal ID Balance line Moge ox Except for special automated applications using accurate timing cycles we recommend to Channel tray Location On this computer Door mode Status Baud rate Data hits Parity Stop Bits Handshake control the doors at the balance and to disable the door management function of Calibry as follows Set the Door mode parameter to Disabled In the Options Configuration Balance Other XS XA balances menu you may advise Calibry to inform you when the balance is due f
46. the doors at the balance and to disable the door management function of Calibry Onthis computer Yes o as follows Set the Door mode parameter to Disabled other available settings are sun Be explained in chapter 4 In the Options Configuration Balance XP balances menu you may advise Calibry to inform you when the balance is due for adjustment Balance infa Communication Com port number com Notes on operation Baud rate ae The measured values are transmitted to Calibry when the Print key key with printer ston Bis symbol of the XP balance is pressed a No manual zero setting of the balance is required between subsequent pipetting opera tions Hardware Configuration 103 19 7 Calibry and XP26PC balances This chapter provides information on how to use Calibry in conjunction with the XP26PC microbalance for the calibration of single channel pipettes The XP26PC standard equipment includes a serial RS232C interface optional interfaces are available on request The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and the XP26PC balance are switched off Connection O 6 RS9 RS9 cable 1 1 m f 11101051 Setting up the XP26PC balance set the Host interface to the following values Baud rate 9600 Baud Bit Parity 8 Bit none Stop Bits 1 Handshake XON XOFF End of li
47. the end of the 45 day trial period The license key determines which edition of Calibry is activated Light Single Workstation or Network The option Enter a license key opens the following dialog allowing you to enter the license key You will find the license key in the Calibry packaging Enter the license key into the upper field If you have also purchased an option for Calibry e g RFID enter its license key into the lower field Confirm your entries by clicking Finish Calibry then automatically begins to check the connected balances as described in the next chapter Installing the Software and launching Calibry 12 2 5 Automatic balance check iF Balance Autodetection Status Detection done 1 balanteis found Balances aa 1126300064 MICPIOS MCP COM Detect MCP internal adj 2 6 Activating Calibry Every time the application is launched Calibry automatically checks the balances that are connected to the PC and ready for operation and displays the results in the status area Balances that are readily available to Calibry are shown in the lower part of the window The balance check may be repeated as needed by clicking on Detect lf the results of the check prove to be OK you may click on Close to start working with Calibry Note A gray balance symbol indicates that Calibry cannot verify the respective balance unknown or connected incorre
48. the specifications USP setting The rounding model is chosen at the method definition stage 20 3 Calculating measurement uncertainty in accordance with ISOTR 20461 Through its advanced configuration options Calibry can store all necessary parameters for calculating the expanded measurement uncertainty This chapter describes how to do this using step by step examples 1 To be able to enter the necessary data for the appropriate measuring instruments one of the following methods needs to be selected under Options Configuration Advanced Calibration error mode SE and RE 2 parameters or 2AB 4 parameters The setting Calibration error mode for balances should be selected for balances and if the Calibry Capture Tool is being used also for the measuring instruments used for environmental conditions Calibration error mode for other devices 2 The option Set cubic expansion coefficient may be activated to assign a coefficient of thermal expansion to individual pipette types If a global value needs to be used this should be entered under Default cubic expansion coefficient 3 For all balances used the measurement uncertainty parameters are entered under Balances amp Devices Management Balance and then under Calibrate 3rd party External calibration for the selected balance The following parameters can be used a Guaranteed specifications b Values typical to Mettler sd
49. tolerances are used in Calibry Absolute tolerances are calculated from the relative values depending on the selected volume Manufacturer tolerances This information is taken from the data published by various pipette manufacturers Due to the different methods of displaying the tolerances they are presented as follows Scenario 1 The tolerances SE amp RE are relative values In this case the values were taken exactly as published by the manufacturer Scenario 2 The tolerances SE amp RE are absolute values Based on the number of decimal places of the absolute values their resolution was determined as a relative value which was then applied to the corresponding converted relative specification values so as to determine their decimal places This procedure has ensured that the granularity of the calculated relative tolerances is at least equal to or better than the published absolute values The specifications of those devices which are relevant for the use of Calibry are based on public accessible information and product specifications for each device at the time of the last update of Calibry The database used for Calibry for the devices is based on those public accessible manufacturer information and METTLER TOLEDO conducted utmost care gathering the information This does not however absolve you from personally verifying that the information including but not limited to tolerances are correct and up to date Since the correc
50. used at start of the As Found measurements AFSAirThermA 3rd coefficient for adjustment errors A of the air temperature thermometer used at start of the As Found measurements AFSAirThermB Ath coefficient for adjustment errors B of the air temperature thermometer used at start of the As Found measurements As Found measurements surements ments measurements AFEAirThermErrorMode Error mode for adjustment values of the air temperature thermometer used at the end of the As Found measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB AFEAirThermAloha Ist coefficient for adjustment errors Alpha or SE of the air temperature thermometer used at the end of the As Found measurements AFEAirThermBeta 2nd coefficient for adjustment errors Beta or RE of the air temperature thermometer used at the end of the As Found measurements AFEAirThermA 3rd coefficient for adjustment errors A of the air temperature thermometer used at the end of the As Found measurements AFEAirThermB Ath coefficient for adjustment errors B of the air temperature thermometer used at the end of the As Found measurements the As Found measurements measurements ments measurements Advanced Options 91 ARSAirThermErrorMode Error mode for adjustment values of the air temperature thermometer used at start of the As Returned measurements d
51. with the XP analytical balance by METTLER TOLEDO The XP standard equipment includes a serial RS232C interface optional interfaces are available on request The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and the XP balance are switched off Connection RS9 RS9 cable 1 1 m f 11101051 Setting up the XP balance set the Host interface to the following values Baud rate 9600 Baud Bit Parity 8 Bit none Stop Bits 1 Handshake XON XOFF End of line character lt CR gt lt LF gt and Character set ANSI WINDOWS Except for special applications we recommend to disable the door management function of Calibry see below and to set up the bal ance accordingly In the User Settings you may define the Door function mode automatic or manual Select the manual mode if you leave the doors open permanently e g when using a moisture trap or if want to open and close the doors manually Setting up Calibry Usually Calibry will detect the XP balance automatically otherwise add the XP as a new balance as shown in the example to the left see chapter 4 Balance info Communication oe T N The settings marked with a red dot are mandatory while the other settings may be modi Si a fied to match your local conditions Mode Except for special automated applications using accurate timing cycles we recommend to aay control
52. 000 O00 Pipette History 59 Ifyou select a particular test method as well as a single channel the calibration results for the selected channel will additionally be represented as a graph You can select the required the volume above the graph The dashed lines show the tolerance limits for the selected volume The points and associated values show the result mean value of each calibration on a time axis Note If you select All from the Channel and or Method dropdown menu Calibry quits the graphical view and displays the results as text only Use the Print and Export buttons to print out the history or export it as a text file csv format with no graph whereby only data from the currently selected test method and pipette channel is sent to the printer or file Direct access to functions Quick Access 60 12 Direct access to functions Quick Access You can directly access many of the Calibry functions described in the previous chapters To enable this function select the required pipette in the Pipettes menu and click on the Quick Access button 7 Quick Access Overview Type Contact Status Ki s Assi Model name Description Model name RANTRE Sel ET Manufacturer Senal number ATARE Channel Secondary ID Fange Last service Nest service Next calibration Next quick check won UOC Reset 2nd ID Save 2nd I
53. 000001 Calibration column indicates whether mt Se an adjustment is due for the respective KP56 1234567890 MCP105 1120503103 instru ment MCP105 22334455 MCP 105 1119000033 i CPS 1126300064 Clicking on a particular type of device in the MCP Calibration Stat 78435092 BA 3345 left part of the window reduces the list on Thi Thermometer ai m2 the right displaying only the instruments Barometer BRM 414_1 Barometer ERM 677 belonging to that type e g balances i a Click on the sign to display all instru ments of the respective type Clicking on a particular device displays the adjustment data of that unit in the right part of the window Calibrations Using the menu path File Print Preview or File Print it is possible to format and print records for the entire list of devices or for individual devices see also chapter 3 4 4 1 Defining a new balance To define a new balance highlight the device type Balance or any of the balances in the list in the left part of the window then click on the Add button below the device list A window appears for entering the balance parameters Enter the data for the balance Balance properties Name Designation of the balance Choose a mean Balence info Communication ingful designation e g a model designation of the balance Name MMCPIOS Lat Serial number Serial n
54. 1 19 9199 19 919 ystematic Error ul ystematic Error E 1 0401 0 9600 0 9600f 0 4799 0 0801 0 080 E A A a A A y A andom Error pl 20 0 4804 0 2615 0 0000 0 4130 0 1596 0 159 andom Error T E T E T T E T E ncertainty meas l 1 7524 1 2803 2 0008 1 4830 0 9600 1 3060 0 3994 0 399 tatus wj or cis Oe nT ons ean Ll 99 3600 99 2799 99 5201 99 1999 99 9202 99 920 Systomatc norlM 32 o od od Co os o o o Random Eror 2 o og od oa 0 3 og ogo 02 Urceraniy mees tal f oao 0 6400 0 6400 13333 11204 raoe 15023 _ 0 3006 C S S Od CIN OI ON OY Meant __ 200 000q200 000q 200 eaa 200800 200 2402 100 919 199 9000 190 8401 SstematcEnor fete oo od of o_o ooh od o RaniomErorte fos oof oo oar or ol 04 024 oag Uncertain meas ooo ooon 21179 oeoa toei 00033 10308 07094 sw ooo o y ON ON Ne N N N NN Status 8 Passed Date 18 05 2011 AD Next due date 18 05 2012 Performed by SPI 15 Signed by Not signed Notice 12 Repeated None measurement Generated with Calibry 5 0 17 30468 Printed with Calibry 5 0 17 0 Certificate number 1113800231 0 R1 Page 1 10 Calibration Reports 55 Calibration Report 442 KR A Pipette Serial Number 414K022 D Owner Company Pipette Second ID MERT 262 Owner Department Pipette Type Rainin Pipet Lite 8ch 20 200 ul Owner Name Method ISO type A8x 200ul Method Description 20 pil Systematic Errar 5 16 Ho 0 So 16 Ho se
55. 20 Calibration Settings Tip as found tips ki Add Balance McP os Reference number Environmental parameters Air temperature aia Vater temperature as M Hurmidit y 30 Factor 1 0039 pling Pressure 300 hPa Evaporation 0 pltcy cle Edit Invalidate Pipette Calibrate Cancel After you have started the calibration the window shown at left appears In this window you can specify the following parameters for the current calibration The pipette tips being used The balance which should be used for the calibration An additional reference number for the current calibration this number appears in the title of the report The current environmental conditions Note In the Options Configuration menu chapter 16 you may configure Calibry to acquire the environmental parameters from an external data source automatically NOTE Ifthe current pipette can no longer be calibrated irreparable fault you can click on the Invalidate Pipette button If you answer the subsequent question with Yes no calibration is performed and the pipette is removed from Calibry from the pipette list as well as the Tasks list but without touching previous calibration data Be careful with this option because there is no way of returning the pipette to Calibry after it has been removed except for a new definition G Tips Management Tip Editor m 45 found tips AS Retu
56. 4 ARSBarB Ath coefficient for adjustment errors B of the barometer used at start of the As Returned measurements ARSBarCalCert Number of the adjustment certificate of the barometer used at start of the As Returned mea surements ARSBarCalNote Note on adjustment for the barometer used at start of the As Returned measurements AREBAarSN serial number of the barometer used at the end of the As Returned measurements un AREBarCalDate Last adjustment date of the barometer used at the end of the As Returned measurements O AREBarErrorMode Error mode for adjustment values of the barometer used at the end of the As Returned measure ments disabled none SE and RE Random Error and Systematic Error 2AB 2AB AREBarAlpha Ist coefficient for adjustment errors Alpha or SE of the barometer used at the end of the As Returned measurements AREBarBeta 2nd coefficient for adjustment errors Beta or RE of the barometer used at the end of the As Returned measurements AREBarA 3rd coefficient for adjustment errors A of the barometer used at the end of the As Returned measurements AREBarB Ath coefficient for adjustment errors B of the barometer used at the end of the As Returned measurements AREBarCalCert Number of the adjustment certificate of the barometer used at the end of the As Returned measurements AREBarCalNote Note on adjustment for the barometer use
57. A EA 14 E The menu MING siicisansdasessdiinatadeeienrebasnsennsionetacntenbsndeiiel bora dodbnsdudid nid aijniinndantadnoonisdartenimbaaanta taarianiortnrdinedasainsdaatauiectienans 16 3 4 MALE SM SiSmcrclnl elcome lych s191e 4 at eet he ene tee nr ee ee eT eee 18 30 MS ENT AS a T E tsetse ect EE ne avn gt ate eater acdc E A T 19 l Specifying Managing and Adjusting Balances and Peripheral Devices cssssseeccsssssseeeeesssesseeeeeeseeaeeees 20 4 1 RAE E TAC E E E E A A A EE A E AE A EEE E E 20 4 2 TGC RAC DACE DAO n E A IR E E TE 22 4 3 PREV RONE aiei esc tres nr alacant tt cn dha minnie ped ta Patan ene 22 4 4 Notes about the balance check upon application IAUNCh ssss nnnnssennrrrrresnnrrrrrsrnnnrrrrrnrnrnrrrrnnnnrrrrrennrrrrnnnnnrrrrrennrerrent 22 4 9 A A Wal gles 616 0 el eee nen eee eee S E OE ee ee ee ee 23 4 6 Managing ond adjusting pernpneral devices i isciic ccediaccutesaesnmncevssvetainkalobenatuauleatloccesbedhaubiediiuone ite Moandliecndenestenneseiachdenndveies 24 4 7 PERUNO STMT CLITA DON eeen EE sce E ES E E EEE A A E Zo 5 STUNNING COTS sie ces EE A A A ica de eas tens owes ees E tne snes A E E ANAN 26 5 1 PAE E EE a E e E EE EE S EN EE EAN AE E EE E E 26 92 CIA a COO n AE E A AE E 2 one PESEE ieee ee ee tte ea ee E ee ee ee ee ee 2 6 DOM MING PID ON OS EA A EAA O A AE E N OEN E E A O O A 28 6 1 Bil alle Rem G s a6 Cle cee eee ner E ene A E ee ee eee 28 6 2 EE AURA UNS AE A T E E E tnt A AO eeprom cere A ae po
58. After this a status check is performed As found The status check takes the form of an abbreviated measurement by means of which the accuracy of the pipette is determined before any necessary repair measures are performed After the status has been checked any necessary fault correction measures are performed Finally the calibration itself provides information about the accuracy of the pipette after the fault correction measures have been performed Note In this chapter only those steps are described in detail which are typical for this calibration method Steps which are identical to those of the calibration method already described chapters 9 2 and 9 3 are not described in detail again When the calibration dialog chapter 9 1 is started the Physical inspection window opens to check the pipette for possible faults chapter 9 3 Inspect the pipette and mark in the list any faults you find Click on OK to finish the inspection ir Physical inspection Physical Inspection Unable to obtain 4s found data Description F Corroded piston Electronics broken Note Ifthe inspection reveals that no status check As found can Lint AAE A be performed due to the defects you may check the box Unable Micrometer out of phase es ae to obtain As found data this checkbox appears only if at least Plunger bent one defect has been selected This causes the application to skip Seal leaks
59. D Methods Tasks Reports Task Due Date Status Pipette Seri Schedule Method Wa Pipette 56 Owner Phone P 17 05 2011 a JEOR SKE tl i Custom Beiu MERT 262 E ES 17 05 2011 Fy SRY 414K022 0 Brand New 8 MERT 262 98 765 432 18 05 2012 oh Ri 4i4ko22 p l 150 type AS MERT Z62 98 765 432 Delete Calibrate History Close The top left section of the dialog Overview displays information about the selected pipette detailing the tests and calibrations carried out and still to be carried out Service refers to calibrations with additional status checks see also chapter 7 This data cannot be modified with the exception of the second ID Secondary ID If you modify this ID press Save 2nd ID afterwards to store the ID Reset 2nd ID gives you the option of canceling this change provided that it has not already been saved In the top right section of the dialog you will find information about the type of pipette Type and the contact to which the pipette is assigned Contact You cannot modify this information Note If you are working with the RFID option in the top right section of the dialog you will find additional information which Calibry can read directly from the RFID chip of pipettes fitted with this option You can also modify or re enter data and write this back to the RFID chip on the pipette Further information about working with
60. Error for the As Returned measurement Admissible relative Systematic Error for the As Found measurement MethodVolx_AFReIRE Admissible relative Random Error for the As Found measurement MethodVolX_ARAbsSE Admissible absolute Systematic Error for the As Returned measurement ul MethodVolX_ARAbskE Admissible absolute Random Error for the As Returned measurement ul MethodVoIX_AFAbsSE Admissible absolute Systematic Error for the As Found measurement ul MethodVolxX_AFAbskE Admissible absolute Random Error for the As Found measurement ul Q9 Field name Environmental Condition AFAirlempStart AFWaterlempStart AFHumidityStart AFPressureStart AFZFactor AFEvaporation AFEvaporationError AkAirlempStart AkRWaterlempStart AkeHumidityStart AlkePressureStart AkZFactor AkEvaporation AkEvaporationError AFAirlempEnd AFWaterlempEnd AFHumidityEnd AFPressureEnd AkAirlempEnd ARWaterlempEnd AkeHumidityEnd AkPressureEnd AFBalanceName AFBalanceSN AFBalanceLocation AFBalanceSensibility AFBalanceCalDate AFBalanceCalCert AFBalanceCalNote AFBalanceErrorMode AFBalanceAloha AFBalanceBeta AFBalanceA AFBalanceB ARBalanceName ARBalanceSN ARBalanceLocation AkBalanceSensibility AkRBalanceCa Date AkRBalanceCalCert AkRBalanceCalNote Advanced Options 8 O Description mbient conditions ir temperature at start of the As Found measuremen
61. Found measurements ul X pipette channel Y volume AFAbsSE_ChX_VolY Absolute Systematic Error of As Found measurements ul X pipette channel Y volume AFAbsRE_ChX_VolY Absolute Random Error of As Found measurements ul X pipette channel Y volume AFReISE_ChX_VolY AFReIRE_ChX_VolY AFUncer_ChX_VolY AFStatus_ChX_VolY Relative Systematic Error of As Found measurements X pipette channel Y volume Relative Random Error of As Found measurements X pipette channel Y volume Uncertainty of As Found measurements ul X pipette channel Y volume Result of calibration after As Found measurements X pipette channel Y volume ARMean_ChxX_VolY Mean value of As Returned measurements ul X pipette channel Y volume ARAbsSE_ChX_VolY ARAbsRE_ChX_VolY ARReISE_ChX_VolY ARReIRE_ChX_VolY ARUncer_ChX_VolY ARStatus_ChxX_VolY AF PipetteStatus Absolute Systematic Error of As Returned measurements ul X pipette channel Y volume Absolute Random Error of As Returned measurements ul X pipette channel Y volume Relative Systematic Error of As Returned measurements X pipette channel Y volume R elative Random Error of As Returned measurements X pipette channel Y volume Uncertainty of As Returned measurements ul X pipette channel Y volume esul
62. In Calibry you can set up different users for which different authorizations can be determined When Calibry is installed chapter 2 a user is automatically created with administrator rights Login data is automatically copied from the active Windows user account After the program has started Calibry checks which user is logged onto Windows and whether there is already an entry for this user in Calibry If this is the case the program starts up using the rights for this user If after the program has started Calibry does not find an entry in its user list for the user logged onto Windows then the program start is aborted Users Options He User Levels 7 13 1 Defining a new user Click on Users Management to get access to the user manage ment menu Several users have already been defined in the example shown here in addition to the user who is automatically created by Calibry during installation The list contains information on names login corresponds to the user account in Windows and the level of authorization of each user To define a new user click on the Add button on the bottom left hand side of the User Management main window A screen appears which is used to define the user User properties User properties User name Molander E Login MOL Level Level2 z Add New User level settings will take effect after next login Entering data for the new user User
63. In addition you will have to specify the port to be used for communication between Calibry and the external application The external application needs to monitor the specified port for data requests issued by Calibry and supply the requested data in a specified format The following steps take place in the course of automatic data acquisition The user launches a calibration within Calibry Calibry attempts to communicate with the external application The external application accepts the communication request Calibry asks the external application for the environmental data The external application transmits the requested data to Calibry Calibry terminates communication with the external application SW ODO OH B amp B W N Calibry displays the acquired data in the calibration dialog When a calibration is launched Calibry sends a request for environmental data via the selected port to the appropriate host using the following format lt bal gt m r gt lt dvn gt device number lt dsn gt seria number lt loe gt ocation lt bal gt m r gt Prefix of the request lt dvn gt device number The device number corresponds to the Internal ID of the balance used for the current calibra tion this is a number in the range of 1 to 16 or None see chapter 4 If Calibry runs in demo mode chapter 15 the device number is None lt dsn gt seria number serial number of the balance used for the curr
64. OMotorBurettes 5 ISOHandBurettes ubic expansion coefficient of the pipette 1 C ncertainty of the cubic expansion coefficient 1 C PipetteAlohaC PipetteAlohaCUncert est method data ame of the test method escription of the test method umber of volumes to be measured elected calibration mode umber of pipette channels to be calibrated ipette channels to be calibrated Selected tolerance mode 0 User defined 1 ISOPistonTypeA 2 ISOPistonTypeD1 MethodName MethodDescription MethodVolumeCount MethodCallype MethodChannelCount MethodChannelList MethodToleranceChoice 3 SOPistonlypeD2 4 ISOMotorBurettes 5 SOHandBurettes 10 Manufacturer Systematic Error factor for As Found measurements Systematic Error factor for As Returned measurements MethodAFFactorRE Random Error factor for As Found measurements MethodAFFactorSE MethodARFactorSE MethodARFactorRE Random Error factor for As Returned measurements Volume MethodVolx_MicroLiter MethodVolx_AFReading MethodVolx_ARReading MethodVolX_ARReISE MethodVolX_ARReIRE MethodVolX_AFReISE Measuring parameters per volume X designates the volume 5 Defined volume in microliters Selected number of As Found measurements Selected number of As Returned measurements Admissible relative Systematic Error for the As Returned measurement Admissible relative Random
65. Pipette Calibration Caliory software Tp ar O jenama S Sin ajamaan Ta lt prre ae q Be Version 5 0 Contents 3 Contents 1 SPE G UG TOM EE EEE EE AE E ET E A E TT A E E OE EE T A E 6 1 1 OaS OnO a EE EE E S AA A ee 6 IZ important intormation ABOUT Mese NASTHUIGT ONS vasiceiatiste vexeesnnincrnanineievainaiousnssreicasatgie loca jell aeaaaee aaia 6 2 Installing the Software and launching Calibry ccccccsssssseeeeessessseeeeeesseesseeeesseeaeseeeeeseeaesseessseeeasseeesseneanaees 7 2 1 EE UI Celt lols ae eee eee a he cere ee ee ee ee ene ee E Tr 7 2 2 S lee OO o AEE E A A A E E EA E ee ee 8 2 3 Configuring the database Calibry DB Maintendnce c cect ect etic rete eetireiiesnieetireeiresnesenrssneesneey 9 2 4 Starting the application and selecting the required Calibry CCItION ccccccccccssssceccsssseessseeeeeseesseeesceeseeeessessaeeeseesaass 11 2 5 AOE O CO E a E E E E E E A 12 2 6 PROT OWING AMOI ercstecgunesnets aetrstoas sr cvs uacenseecenrosrenisaucye vocttagivohcuiea euarseunegen cia AEEAE an 12 2 Software Ul TS ONO CS GING a alsce eauearcseqn panel ninen nia nia aaar ET TENANAN EAA TERENA NENEN T ES EEN REA E Eai 13 3 Instructions for Using Calibry ccccccsssssseeeeessessseeeeesseeaseeeeeeseaasseeessseaasseeeesseeassneesseeeassaeeessenaassesessengagaees 14 3 1 WAS OS a nc rss cree a eso aes are A AE T T 14 N SOO r E EE AA teeta A EEE EAA A
66. RFID can be found in chapter 17 In the bottom part of the dialog you will see the Tasks list for the selected pipette You can delete entries from the list Delete or start a calibration Calibrate Further information about the Tasks list can be found in chapter 8 The calibration reports for the selected pipette are found under Reports You can view a report View print it Print save it as a PDF Save as PDF export it as an XML Export as XML or export it as a Microsoft Office file Export to Microsoft Office For further information about the calibration reports refer to chapter 10 Under Methods you will find the list of test methods allocated to the selected pipette With Assign Methods you have the option of assigning additional methods and with New Method you can define new test methods With Set Reminder you can set the calibration date or interval for each test method With Add to Tasks you can insert the calibration and required method into the Tasks list With Calibrate you can immediately calibrate the pipette with the chosen test method Further information about the test methods can be found in chapter 7 At the very bottom left of the dialog you have the option to view the History of the selected pipette Further information about the pipette history can be found in chapter 11 13 User Management User Management 61
67. The following chapters explain how to establish standard settings for calibration for the application and for the appearance of the various lists 16 1 Settings for calibration Options Select the Options Calibration Setup menu Audit ae In the Calibration Setup window you may establish various settings for calibration as Calibration Setup AN e Se Configuration Unscheduled Calibration Methods Editing the list of pipette defects Calibration setup ei In the main window of the Calibration Setup menu click on the Physical Inspection tab When Calibration with physical inspection is used the pipette is checked for a list of possible defects before calibration chapter 9 3 The list installed at the factory contains a selection of the most common defects You can adapt this list to your needs You can delete individual items from the list with the Delete button and with the Add button you can add further items to the list Editing the list of fault correction measures Calibration setup mal In the main window of the Calibration Setup menu click on the Corrective Actions tab If Calibration with physical inspection detected defects in the pipette after the inspec tion a list of possible corrective actions appears chapter 9 3 This list installed at the factory contains a selection of the most common corrective actions You can adapt this list fo your needs
68. You can delete individual items from the list with the Delete button and with the Add button you can add further items to the list Editing the list of reasons for deleting measurement values eS S El n the main window of the Calibration Setup menu click on the Undo Reason tab If during a calibration you want to delete an invalid measurement value Undo measure ment see chapter 9 2 you must select a reason for the deletion from the list The list installed at the factory contains a selection of the most common reasons for deleting measurement values You can adapt this list to your needs You can delete individual items from the list with the Delete button and with the Add button you can add further items to the list Changing the Program Settings 68 Calibration setup Before due After due Calibration setup Calibration setup Physical Inspection Corrective Actions Undo Reason Schedule Notices Sounds Sound effects for calibration T Next volume All done Out of tolerance Undo Error cancel ay Specifying the settings for monitoring pipettes over time In the main window of the Calibration Setup menu click on the Schedule tab In this menu you can define the settings for monitoring pipettes over time in the Tasks list see chapter 8 In the first field Before due you can specify how many days before its n
69. a multi channel pipette Ri EA E eels A E E E EET E E E ET 42 Calibrating a multi channel pipette with inspection and fault correction EJ Ri E ATT E E nate teen 49 Calibrating a multi channel pipette with inspection status check and fault correction uk Fi Riy PEE PTA 50 Calibration ReportS asssnsnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnn nnna 52 The contents of the reports sss nsssssrnrreenrrrrennrrrennrrrttkkr rrt tk tnra knrn n rr rnPAEErrAEEEErEEEEEErEEEEEENEEEEEENEEEEEPEEEEEEPSEEEEEEEEEEE EEEE EE E 93 Pie 101 4 ke 0 16 4 Saar ene eene E ee ee eee 56 BCR IODO ae E E E E E ee 9 Pinen MISIO arenie EEE EE EE 58 Direct access to functions Quick Access ccccsssceeceesseeeeeeeseeeeeeasneesseaaseeeesesaeessaasaeeseoaaseessseaaaeessaasaessoaas 60 User Management sscan a a EAE A 61 DINDO AAT US a E E ua obeanniaies meaeneue E aoeeaneinn 61 Creating editing and deleting levels Of authorization ccccscccccsesseceecseseeeeecessseseeceeeeeeeceeseeeesceseeesscesaeesseensaeeeseesaaes 62 CAOR OT eee eee E ee ee ET E A ETE 63 BE nE RT ie EEE EAEN E N AETA AE A E A es E E E A 63 eL Taol E E E E E A A A A ear EE A E EE EEE 64 DEMO MOUE onp EE E 65 Changing the Program Settings nnennnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnn nnmnnn 67 F TOE CO O a EAE N ine ani aeitacaieseqiasriee en soensamaname
70. alance you wish to adjust The lists contains all balances known to Calibry even those that are not currently connected or have been deleted previously You may launch the adjustment procedure from within Calibry only for those balances that are connected and ready for operation and that have been properly detected by Calibry Connected Deleted balances cannot be adjusted For balances that are available but are not connected to Calibry you will have to launch the adjustment from the balance and then enter the results in Calibry The same applies to balances that are not directly supported by Calibry i e if the adjustment cannot be launched from within Calibry The right part of the window shows a list of all adjustments that have been carried with the selected balance To launch the adjustment procedure click on the Calibrate but ton below the list The Calibrate balance window provides the following options Tool Used Select Calibry if you wish to launch the adjustment from within Calibry assuming the selected balance a Calibrate balance Calibration settings is directly supported by Calibry Select 3rd party if you wish to launch the adjustment from the balance Da e g and then manually enter the result in Calibry or if you e EEEN wish to enter the values of an adjustment certificate aca Sauna g In case Calibry does not directly support a particular balance 3rd party will
71. alibry workstation as shown below Before establishing the connection make sure both the computer and the XP balance are switched off Connection Setting up the XP balance RSI RSY cable 1 1 m f 11101051 Set the Host interface to the following values Baud rate 9600 Baud Bit Parity 8 Bit none Stop Bits 1 Handshake XON XOFF End of line character lt CR gt lt LF gt and Character set ANSI WINDOWS Setting up Calibry ation xp 22 89234988 keee O O OoOo o fi baea e e r 6 Yes C No Disabled Usually Calibry will detect the XP balance automatically otherwise add the XP as a new balance as shown in the example to the left see chapter 4 The settings marked with a red dot are mandatory while the other settings may be modi fied to match your local conditions Set the Door mode parameter to Disabled because these balances do not have automatic doors In the Options Configuration Balance XP balances menu you may advise Calibry to inform you when the balance is due for adjustment Notes on operation The measured values are transmitted to Calibry when the Print key key with printer symbol of the XP balance is pressed No manual zero setting of the balance is required between subsequent pipetting opera tions Hardware Configuration 102 19 6 Calibry and XP analytical balances This chapter provides information on how to use Calibry in conjunction
72. alling Calibry make sure your system meets the displayed requirements Installing the Software and launching Calibry 8 2 2 installing Calibry To install Calibry click the relevant button in the start screen 3 METTLER TOLEDO Bootstrapper es The bootstrapper first verifies whether all necessary Windows components are installed on your PC and up to date If they are not yet installed you can install them the components are contained Welcome to METTLER TOLEDO Boostrapper _ In order to successfully run the application on your system you need to install the following software on the CD ROM After insta lation the system needs to be resta ted The bootstrapper will then reload automatically if not simply Product Hame Detection Status Installation Status Optional re open the file Setup exe from the CD ROM The bootstrapper LY Windows tnstaler 45 Installed Alreadly instaler confirms that the Windows components are installed Lp Meros nET 35 Installed Alresclp installed You can now begin the actual process of installing the Calibry software by clicking the Install button In the first installation window confirm that you agree to the license conditions you can view them if you choose and then click Next Show log Install Calibry 5 0 Beta Setup SES Select the components you wish to install Please Select tite Components to be Installed It is essential that you install the datab
73. ances amp Devices Detect balances menu in the main application window Calibry now recognizes that the balance is no longer connected and can be deleted Ifa deleted balance is reconnected to the PC and switched on it will be recognized and reactivated automatically the next time Calibry is launched 4 4 Notes about the balance check upon application launch Every time the application is launched Calibry automatically checks the connected balances the same check can be done via the Balances amp Devices Detect balances menu If Calibry detects an unknown balance the instrument will be added to the list and all parameters will be configured automatically However if you have connected a balance and it is not recognized automatically this may be a third party product and or a balance that does not support bidirectional data communication Calibry does not recognize such balances automatically but you may add such an instrument to the device list and configure it manually chapter 4 1 Calibry stores the device list in the database If your PC is part of a network where several PCs are accessing the same Calibry database the device list will show all balances including the ones that are not connected directly to your PC For such balances make sure to select the setting On this computer No chapter 4 1 Specifying Managing and Adjusting Balances and Peripheral Devices 23 From the device list select the b
74. arometric pressure hPa ee E E O Temperaturedir_ Airtemperature C D D S R a tureAir used E A measurement DO ned SE for water temperature measurement PP Humidity Hes humidity RH e E E E Advanced Options 85 Group i 1 Subgroup 2 Hi 3 H 4 XML Jt clement o Notes S TestData of data is ae of data E volume pote Ei Measured volume TE pT Reading measurement value is ReadingNo between 1 andthe numberof measure anes specified in the test Sri ce nest a current measurement A e 1 block of data for every pipette channel specified in the method Number of the pipette channel Weight value of the measurement already compensated by the evapora lt D CARE mg ae block of data for every pipette channel eee in the is method Number of the pipette channel ae po SE Absolute Systematic Error u u oo SE Relative Systematic Eror oo RE Absolute Random Eror u o l RE Relative Rando Eror bee aes nR ee a aaa Balance 2 blocks of data for As Found and As Returned used for AS PEUT or AsS Found PID Internal identification of the unit eg pee Name Designation of the balance pt Inter DoF the balance pf location Location of the balance po Sensibility Calculated readability g ef atte Date of last adjustment pp __ _____ Batbanttete __t Nuria of edustent cerifen__ CalNotice Note on Note on
75. art of the As Returned measure ments disabled none SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the hygrometer used at start of the As Returned measurements 2nd coefficient for adjustment errors Beta or RE of the hygrometer used at start of the As Returned measurements 3rd coefficient for adjustment errors A of the hygrometer used at start of the As Returned measurements Ath coefficient for adjustment errors B of the hygrometer used at start of the As Returned measurements Number of the adjustment certificate of the hygrometer used at start of the As Returned measurements Note on adjustment for the hygrometer used at start of the As Returned measurements serial number of the hygrometer used at the end of the As Returned measurements Last adjustment date of the hygrometer used at the end of the As Returned measurements Error mode for adjustment values of the hygrometer used at the end of the As Returned measure ments disabled none SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the hygrometer used at the end of the As Returned measurements 2nd coefficient for adjustment errors Beta or RE of the hygrometer used at the end of the As Returned measurements 3rd coefficient for adjustment err
76. ase utility program Calibry DB Maintenance because it allows existing Calibry databases to Select the Calibry 5 0 Beta components to be installed on this system be converted for use with Calibry 5 0 and secures SQL databases among other functions see chapter 2 3 sai M Install Calibry 6 0 You need to install the Microsoft SQL Server Express database ee program if you do not already use one of the other supported SQL i Install Microsoft SQL Server Express Installation folder C ProgrammeSMETTLER TOLEDO SCalibry 5 Browse server versions see chapter 2 1 Then specify the folder in which you wish to install the software Continue the installation process by clicking Next Back Cancel Calibry 5 0 Beta Setup ME This window only appears if you selected Microsoft SQL Server Ee aa Express for installation in the previous step Enter the instance name under which you wish to install the SQL server If one or more SQL server instances already exist these will be displayed Please setup th SOL Database Server To nstal an SQL Database Server please choose a server instance name and the name of the database Server instance name saexPREss n SS Begin the installation by clicking Install Note If you have chosen to install the SQL server the installation process may take longer Back Cancel Installing the Software and launching Calibry 9 2 3 Configuring the database Calib
77. at communication with Generic balances is only ever unidirectional i e from the balance to Calibry This also means that Calibry does not provide any control functions for the balance METTLERTOLEDO assumes no liability for the connection and operation of Generic balances The corresponding responsibility and risk lie exclusively with the customer Appendix 111 20 Appendix This chapter contains important additional information about Calibry 20 1 Information about time management in Calibry F Calibration Reminder Configuration Establishing calculating the calibration date Calibry offers various options for specifying the next calibration date also see chapter I No date None Direct entry of a fixed date Specific date Period Settings Stat iNextdete 0470520 O Entry of a calibration cycle Period based on Last performed calibration date Mi 14 05 2008 d target date entered ena ater PN Reference date Scheduled calibration date or End by the current calibration date Reference date Performed calibration date Glossary The terms used in Calibry and this description have the following meanings Task Start Date Date on which a task was started Service Date service date corresponds to the calibration modes Calibration with Inspection and Calibration with Inspec tion and As found data Quick Check Date
78. aulty measure ment values Click on the Undo measurement button The window shown at left appears and you have to select the appropriate cause for deleting the values After confirmation the values are deleted and you can perform the respective measurement operation again Notes The admissible number of deletions per calibration can be set in the Options Con figuration menu chapter 16 The list of causes for the deletion of measured values can be edited in the Options Calibration Setup menu chapter 16 Aborting the calibration You can abort the calibration operation at any time and repeat calibration at a later date Note With pipettes using a multi step calibration mode inspection status check fault correction see chapters 9 3 and 9 4 the actual status and the measurement values of the fully completed work steps are saved and you can carry out the steps that were not performed at some later time Once you have confirmed the cancellation of the calibration there will be a second prompt which asks if you would like to repeat the calibration procedure immediately After confirming the message with Yes the window for setting up the calibration parameters will be opened again Calibrating Pipettes 48 3 This pipette didn t conform to the specifications Do you want to delete this pipette From your list Completing the calibration Click on the Finish button to complete the calibrati
79. b see chapter 12 you will see the Pipette RFID tab This will only be displayed for pipettes fitted with an RFID chip The gray fields cannot be edited they are either defined by the manufacturer e g data of manufacture and serial number or automatically defined by Calibry data relating to the last and next calibration There are also nine customized fields Custom field 1 9 which you can use to enter your own information Enter the required information and click on Write data the Reset data button can be used to undo any changes provided that the data has not yet been transfered Calibry will open a dialog containing the data to be written and prompt you to hold the pipette over the reader Once the data transfer has been successfully completed a message will appear to confirm this Note The information entered in the customized fields will only be stored on the RFID chip it will not be stored in the Calibry database Advanced Options 78 18 Advanced Options This chapter provides miscellaneous information on how to customize Calibry for your specific application 18 1 Using the equation editor In the Options Configuration Formulas menu see chapter 16 2 you may define formulas for the calculation of the Z factor and the measurement uncertainty You may select one of the factory settings for the calculation of these values e g according to ISO 8655 or you may set up your own formula Custom
80. be the only option available Mode You may choose whether you wish to perform a simple adjustment with the built in adjustment weight of the SerialNumber Wei balance Internal adjustment or if adjustment is to be followed by a test with an external test weight Internal adjustment with external test Selecting the third option External test and internal adjustment with external test adds an additional external test before the adjustment Vveight Editar Weight Selectthe test weight to be used from the list weight in grams This option is available only for the adjustment Beer modes including a test with an external test weight see above pret Ea If the required test weight is not available from the list you may click on the Add button and then edit the list of test weights In the window shown to the left enter the weight the tolerance and the serial number of the new test weight Click on Save and the new test weight will be readily available from the list a Add weight Weight weight o aoa Tolerance m 7D Serial number eres Specifying Managing and Adjusting Balances and Peripheral Devices 24 tf Calibrate balance P Intormation Calibration done Calibration result bey Serial number 1126300064 Internal ID Mone COM Part COM G Calibrate balance Calibration resul
81. bry Measurement values The weighing values are displayed and saved depending on the readability of the balance used If a Dual Range or DeltaRange balance is used the weighing values are shortened to the higher readability value The weighing values saved in the database are the net weights of the volumes dispensed For calculations e g corrections for evaporation mass volume conversions the results are saved with the maximum possible number of decimal places The volume values calculated from the weighing values are displayed to one more decimal place than the values displayed during the weighing process This results in the following display method Readability g Volume ml Volume ul gt 0 0001 0 00001 0 00001 0 000001 0 001 0 000001 0 0000001 0 0001 lt 0 0000001 0 00000001 0 00001 Volumes of up to and including 1000 ul are measured in ul Above this the volume is shown in ml If data are exported they are not rounded up and may need to be formatted in the application used Environmental conditions determining the Z factor The values for the environmental conditions are saved depending on the method used to acquire the measurements and used for further calculations e Manual entry As many decimal places as have been entered are used e Using the capture tool Iwo decimal places are currently transmitted and used Appendix 118 To determine the Z factor in accordance with ISO 8655 the measurement value
82. ce Increase and intercept of the measurement uncertainty calculation from the balance certificate Thermometer barometer hygrometer Measurement uncertainty from data sheet Other parameters similar to the example in ISO TR 20461 The user must ensure that the formulae used are correct and validate them 20 4 Notes about the audit trail The Calibry audit trail records the following procedures Pipettes poe Methods poe Tasks poe Contact poe User User level poe Balances and peripheral devices poe Pipette methods e g reminder Physical Inspection of a calibration Coreen e foun S s s UP P Pw fucose a Ss sd ww ooo a a O GWP Good Weighing Practice The global weighing guideline GWP reduces risks associated with your weighing processes and helps to e choose the appropriate balance e reduce costs by optimizing testing procedures e comply with the most common regulatory requirements p www mt com GWP www mt com calibry For more information Mettler Toledo AG Laboratory amp Weighing Technologies CH 8606 Greifensee Switzerland Tel 41 0 44 944 22 11 Fax 41 0 44 944 30 60 www mt com subject fo technical changes Mettler Toledo AG 06 201 1 11780791D 2 12 x 11780791
83. ch 20 2 Rainin Midtown Pipette Corporat Montrose Mary req ulremen ts I h ese C h an o es are mqa d e In 9087436 Rainin Pipet Plus R20 Rainin Calibration Co Miller Max v EF222 4 Sorox8ch200u 2m Sorax Calibration Co Miler Max th e O pti on s V lewIn o O pti ons menu an d 45444555 Rainin Pipet Lite Sch 20 2 Rainin Calibration Co Miller Max DTR777444 DT20 200u DT Calibration Co Miller Max are d eta led INC h q pter 5 i 3 XRT444555 Rainin Pipet Lite 8ch 20 2 Rainin Calibration Co Miller Max g MRM878999 Rainin Pipet Lite 8ch 20 2 Rainin Calibration Co Miller Max 9954324 Rainin Pipet Lite 8ch 20 2 Rainin Midtown Pipette Corporat Montrose Mary 65577888844 Rainin EDP PLUS EP 10 33K338 Rainin Midtown Pipette Corporat Montrose Mary 414K022 D Rainin Pipet Lite 8ch 20 2 MERT 262 Rainin _ Sample Corp Cat Fritz View viene Highlight the pipette in the list for which you 1 want to display the history and click on the View button or simply double click on the pipette in the list or select the View option via the context menu The history of the selected pipette appears on the display view history for pipette 76564363 Once the history of a particular pipette has Method been opened the window initially shows the i Pr results of all calibrations done with all test aa in methods for all chan
84. ctions In these operating instructions pipette calibration systems e g a system comprises from 1 up to 5 MCPs are always referred to as balances because this designation is also used in the software itself Key designations are enclosed in double angle brackets e g ESC or Return This symbol indicates safety instructions and hazard warnings Failure to observe such instructions and warnings can cause malfunctioning of the software or of the entire measuring system and in the worst case can even damage system components This symbol indicates additional information and instructions Observing such instructions makes it easier for you to work with the Calibry software and helps to ensure correct and economical use of the software These instructions only describe the Calibry software You must also observe the operating and installation instructions for the balances you want to operate with Calibry Installing the Software and launching Calibry 7 2 installing the Software and launching Calibry This chapter gives you information about the system requirements installation and activation of the Calibry software In addition you will find some information on data backup and the software upgrade procedure Software Installation j g Additional Information gt Manuals gt System requirements METTLER TOLEDO gt Quit 2 1 System requirements System requirements Supported operatin
85. ctly Further information about the balance check on application launch and on balance adjustment is found in chapter 4 You need to activate Calibry 45 days after installation at the latest if you wish to continue working with the program Calibry Licensing 296R6 3CEP2 27633 Y2INJ 258M4 Calibry 5 0 network not For sale Edition key Option key Provide a valid Option key optional Hardware ID SEH3Z XGYHQ 69XMT 5SZ2M HBDGS YOUR SYSTEM IS NOT ACTI ATED AND WILL EXPIRE IN 43 DAY S Activate OK Cancel U ActivationWizard Please Sel et how to Activate Calibry To continue you should have entered all licenses with the License Manager Activation mode Direct Requires an internet connection O Manual vou eae From the menu in Calibry select Help gt License Manager Note Activation requires a valid license key If you have installed a demo version of Calibry you first need to acquire a license from METTLER TOLEDO and enter the license key Edition Key lf you have already entered a valid license key when installing the program you can also start the activation dialog via Help gt Activate Product Click Activate to start the activation dialog You can choose whether to activate Calibry directly or manually Direct activation connects you directly to the METTLER TOLEDO software portal and requires an internet connection You can register for the
86. d at the end of the As Returned measurements AFSHygSN serial number of the hygrometer used at start of the As Found measurements uN n AFSHygCalDate Last adjustment date of the hygrometer used at start of the As Found measurements AFSHygErrorMode Error mode for adjustment values of the hygrometer used at start of the As Found measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB AFSHygAlpha Ist coefficient for adjustment errors Alpha or SE of the hygrometer used at start of the As Found measurements AFSHygBeta 2nd coefficient for adjustment errors Beta or RE of the hygrometer used at start of the As Found measurements AFSHygA 3rd coefficient for adjustment errors A of the hygrometer used at start of the As Found measurements AFSHygB Ath coefficient for adjustment errors B of the hygrometer used at start of the As Found measurements AFSHygCalCert Number of the adjustment certificate of the hygrometer used at start of the As Found mea surements AFSHygCalNote Note on adjustment for the hygrometer used at start of the As Found measurements AFEHygSN serial number of the hygrometer used at the end of the As Found measurements uN au AFEHygCalDate Last adjustment date of the hygrometer used at the end of the As Found measurements AFEHygErrorMode Error mode for adjustment values of the hygrometer used at the e
87. d by the balance The Manual setting is meant for balances equipped with an integrated light barrier that controls the doors e g XP26PC Select Timer to have Calibry control the door movement depending on the working sequence This setting also allows you to configure the opening and waiting times see chapter 16 Status shows the current status of the balance unknown offline or connected Click on the Communication tab and now you can select the RS232C interface of the computer to which the balance is con nected and enter the communication parameter for the selected interface Make sure that the values match those which were set Com port numser eom for the balance otherwise Calibry cannot communicate with the Baud rate e00 balance Data bits Balance properties Balance into Cammunication When all the balance and communication parameters have been entered click on the OK button to save the settings The newly defined balance now appears in the list Parity Stop Bits Handshake es Balances amp Devices lf you wish to test the communication between Calibry and the newly Management set up balance return to the main application window and then select the Balances amp Devices Detect balances menu Calibry Detect balances now checks the communication with all known balances Ifthe newly set up balance does not show up in the
88. d for As Returned measurements Z Advanced Options AkBalanceErrorMode Error mode for adjustment values of the balance used for As Returned measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB ARBalanceAlpha Ist coefficient for adjustment errors Alpha or SE of the balance used for As Returned mea surements ARBalanceBeta 2nd coefficient for adjustment errors Beta or RE of the balance used for As Returned mea surements ARBalanceA 3rd coefficient for adjustment errors A of the balance used for As Returned measurements ARBalanceB Ath coefficient for adjustment errors B of the balance used for As Returned measurements AFSAirThermSN serial number of the air temperature thermometer used at start of the As Found measure ments AFSAirThermCalDate Last adjustment date of the air temperature thermometer used at start of the As Found mea surements AFSAirThermErrorMode Error mode for adjustment values of the air temperature thermometer used at start of the As O Found measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB AFSAirThermAlpha Ist coefficient for adjustment errors Alpha or SE of the air temperature thermometer used at start of the As Found measurements AFSAirThermBeta 2nd coefficient for adjustment errors Beta or RE of the air temperature thermometer
89. e Depending on the selected settings this has the following effects Scenario 1 No calibration date was set None The setting remains None Scenario 2 A specific calibration date Specific date was set The date remains unchanged Scenario 3 A calibration interval Period was set The period start date end date remains unchanged Unscheduled methods In the normal Calibry lists it is not possible to see which methods are unscheduled From the Options Unscheduled Calibration Meth ods menu chapter 7 you can display all pipettes assigned to a method for which no schedules exist This menu also allows new schedules to be assigned Unplanned calibrations Calibry automatically checks whether a calibration has been carried out within the specified time period or whether the calibration is unplanned this may be necessary for example to check the state of a pipette that has fallen on the floor or which may have been damaged in another way lf an unplanned calibration has been carried out Calibry reacts as follows lf the calibration was carried out before the pipette was included in the Tasks list the calibration is considered unplanned and the scheduled date for the next calibration remains unchanged lf the calibration is carried out after the pipette was included in the Tasks list or on the exact date the calibration is considered planned and the next calibration date
90. e mg m Mass of the weighing vessel after pipetting measured by the balance mg Measured volume V m m x Z Measured volume ul Mass of the pipetted water measured by the balance mg Mass lost through evaporation mg Mass to volume conversion factor in accordance with ISO 8655 6 2002 Annex A ul mg S SoS es Average volume n i l V Average volume ul V Measured volume ul n No of measurements Absolute Systematic Error e V y A Absolute Systematic Error ul V Average volume Ul V Selected test volume ul S Appendix 114 Relative Systematic Error e 100x V V V e Relative Systematic Error 7 V Average volume ul V Selected test volume ul Absolute Random Error S S Absolute Random Error ul V Measured volume ul V Average volume ul n No of measurements Relative Random Error CV 100xs V CV Relative Random Error deviation coefficient s Absolute Random Error ul V Average volume ul Uncertainty u le 2s u Uncertainty of the pipetted volume at 95 statistical confidence ul ISO 8655 6 2002 Annex B Absolute Systematic Error ul S Absolute Random Error ul Appendix 115 20 2 2 Formulae in accordance with ISO TR 20461 In accordance with ISO TR 20461 2000 Calibry 5 0 allows the follo
91. e calibration dialog Compensate for evaporation is locked If you activate this setting the Enable evaporation option is not available in the calibra tion dialog Changing the Program Settings 70 Settings for balance doors Balances door configuration These settings apply only to balances that have an automatic door function e g particular METTLER TOLEDO AX and XP models and will only work if you have selected the Timer setting for the Door mode when defining the balance chapter 4 Open door Time This value in seconds determines for how long the door will be open once the calibration has been started Select a duration that allows you to duly complete the pipetting process factory setting is 4 seconds Time delay for reading This value in seconds determines for how long the balance waits before reading the measured value This delay helps the measured value to reach stability before being transmitted to Calibry factory setting is 7 seconds Caution The delay is counted from the start of the calibration process hence the shortest admissible duration is equal to the opening time of the automatic door as selected in the previous setting Display settings Display option Calibration unit type Select the desired measured variable for the calibrations Weight or Volume factory setting Weight Show results unit If you activate this option factory
92. e mandatory while the other settings may be modi Sereinumber pess ooo fied to match your local conditions Internal ID fi 0 Balance line SAG Mode paoros In the Options Configuration Balance SAG balances menu you may advise Calibry to Channel tray ee n inform you when the balance is due for adjustment On this computer Yes Door mode Notes on operation The measured values are transmitted to Calibry when the Transfer key also marked Menu of the SAG balance is pressed No manual zero setting of the balance is required between subsequent pipetting opera tions Hardware Configuration 109 19 13 Calibry and XA balances This chapter provides information on how to use Calibry in conjunction with the XA balances by METTLER TOLEDO The XA standard equipment includes a serial RS232C interface optional interfaces are available on request The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and the balance are Switched off Connection RS9 RS9 cable 1 1 m f 11101051 5 S J f a oe 4 Setting up the XA balance Set the Host interface to the following values Baud rate 9600 Baud Bit Parity 8 Bit none Stop Bits 1 Handshake XON XOFF End of line character lt CR gt lt LF gt and Character set ANSI WINDOWS Setting up Calibry Usually Calibry will detect the XA balance aut
93. e other settings may be modi fied to match your local conditions In the Options Configuration Balance MCP balances menu see chapter 16 set the Process adapter parameter to Off In the same menu you may define further settings for the MCPs as needed you may even advise Calibry to inform you when the instrument is due for adjustment The number of pipette channels to be calibrated is defined when setting up a test method chapter 7 Notes on operation The measured values are transmitted to Calibry when the Start key of the MOP is pressed The entire pipette calibration workflow is controlled by Calibry Hardware Configuration 100 19 4 Calibry and MCP single unit for 1 channel pipettes This chapter provides information on how to use Calibry in conjunction with the MCP Pipette Calibration System by METTLER TOLEDO set up for the calibration of 1 channel pipettes channel kit The MCP is equipped with a serial RS232C interface that is to be connected to the Calibry workstation as shown below Before establishing the connection make sure the computer and the MCP are Switched off Connection USB to RS232 converter cable 11103691 Setting up the MCP First verify the software version of the MCP The version number shows up briefly when switching on the unit The second number should be 1 40 or higher If this is not the case you will have to install the V1 40 or higher program cartridge
94. eleting all items allows or prohibits the unrestricted deletion of data Printing reports determines whether calibration reports can be printed Controlling grants or denies the permission to counter sign calibration reports In the Rights on RFID line you can determine whether or not data may be written to the RFID chip on pipettes This setting is only relevant if you are working with the RFID option Once all rights have been determined click on the Save button to save the level of authorization Deleting a level of authorization To delete an existing level of authorization highlight it in the list and then click on the Delete button Note Authorization levels already allocated to one or more users cannot be deleted In this case you first have to allocate a new Delete User Level A This user level is currently referenced by one or more user and cannot be deleted level of authorization to the corresponding users before deleting the other levels Once an authorization level has been deleted its name cannot be used for future levels 13 3 Changing users 13 4 Deleting users Delete Delete User Bo vou wank bo remove the selected user Delete User k Ji A The current user cannot be deleted User Management 63 In the user list highlight the user for which the data is to be changed and then click on the Edit button You can now edit User name Login
95. ent calibration serscrgnamog If Calibry runs in demo mode chapter 15 the serial number is Test Location of the balance used for the current calibration If no location was specified when defining the balance this item remains empty Note In case of cluster of several MCP units only the data of one unit will be transmitted Example of a request lt bal gt m r gt lt dvn gt 1 lt dsn gt 1120503103 lt loc gt Lab 4 Calibry waits 5 seconds for a response from the external application When this period is exceeded an error message will appear In this case enter the environmental parameters manually Advanced Options 81 The response sent by the external application must be in the following format lt bal gt m r gt lt tea gt air femperature SNetew gt water temperature SNehgr gt relative humidity SNeprs gt barometric pressure SN lt bal gt m r gt Prefix of the response same prefix as used with the request lt tea gt air femperature SN Air temperature in C and serial number of the thermometer that supplied the value lt tew gt water femperature SN Water temperature in C and serial number of the thermometer that supplied the value lt hgr gt elative humiaity SN Relative humidity in and serial number of the hygrometer that supplied the value lt prs gt barometric pressure SN Barometric pressure in kPa and serial number of the barometer that supplied the value With the exception of the p
96. ents to be carried out for each volume If you wish to perform the same number of measurements for all volumes you may enter the respective value in the field at the very end of the line This value will be used for all volumes By default the values 4 and 10 are available for this field these may be modified in the Options Configuration menu see chapter 15 Systematic error in Admissible allowance for the Systematic error in The Systematic error is the difference between the reference value and the arithmetic mean of the actually measured values Random error in Admissible allowance for the Random error in The Random error defines the scatter of the measured values and is related to the standard deviation Defining Test Methods 35 As found These entry fields are displayed only if you have selected the Calibration with inspection and As found data mode For the status check As found you may just select the number of measurements per volume while for the tolerances the same values as for the real calibration As returned are applied automatically If required you may use the Factor fields to change the tolerance values Systematic error and Random Error by an overall factor This may be useful for pipettes that are calibrated to a particular standard but do have tolerance specifications that deviate from the Standard by a fixed factor The Factor
97. erThermB AREWaterThermB Appendix 120 Measuring device Calibration error mode 2AB Equation editor Export to MS Office Air thermometer Alpha dtaAlpha AFSAirThermAlpha AFEAirThermAlpha ARSAirThermAlpha AREAirThermAlpha AFSAirThermBeta AFEAirThermBeta ARSAirThermBeta AREAirThermBeta AFSAirThermA AFEAirThermA ARSAirThermA AREAirThermA AFSAirThermB AFEAirThermB ARSAirThermB AREAirThermB AFSBarAlpha AFEBarAlpha ARSBarAlpha AREBarAlpha AFSBarBeta AFEBarBeta ARSBarBeta AREBarBeta dPA AFSBarA AFEBarA ARSBarA AREBarA dPB AFSBarB AFEBarB ARSBarB AREBarB Beta dtaBeta o i mi mi E mi mi dtaA lt gt N A dtaB Barometer Alpha dPAlpha Beta dPBeta N A N A Appendix 121 Measuring device Calibration error mode SEandRE 2B Equation editor Export to MS Office Hygrometer SE Alpha dHAlpha AFSHygAlpha AFEHygAlpha ARSHygAlpha AREHygAlpha RE Beta dHBeta AFSHygBeta AFEHygBeta ARSHygBeta AREHygBeta N A A dHA AFSHygA AFEHygA ARSHygA AREHygA N A dHB AFSHygB AFEHygB ARSHygB AREHygB Manual entry of environmental conditions The measurement instrument parameters must be defined as individual variables in the equation editor because the values stored in Balances amp Devices Management are only accessed when the measured values are transfered automatically Depending on the measurement instrument parameters the conversion should be taken into account in the
98. ette Contact Method Level3 Create Print Task Pipette Contact Method None To edit an existing level of authorization Level4 Create Edit Delete Print Cont Task Pipette Contact User m Calibration setup Audit manag None highlight it in the list and then click on the Edit button Ey Ee The settings can then be determined or changed Ensure that changes apply to all users who work with this level of authori evel name evel moe Ul m 7 zation Note The Administrator level of Rights on configuration V Device management M Audit management l Calibration setup M User management n BA Rights on tabs V Working in pipettes V working in contacts V working in tasks V Working in methods q uth O ri zq ti O n cd nn ot be m od ified Rights on action V Adding V Editing V Deleting all tems IV Printing reports Controlling Save Cancel J oa ee Permitted actions Rights on RFID Writing In the Rights on configuration row you can determine which system functions are to be accessible using this level of authorization These system functions are found in the menu line of Calibry In the Rights on tabs row you can determine which menus lists are to be accessible In the Rights on action row you can determine which actions are permissible with this level of authorization Adding and Editing activate or deactivate the respective buttons in the menus D
99. ext calibration date a pipette should be automatically added to the Tasks list factory setting 3 days From when they appear in the Tasks list until the scheduled calibration date the pipettes are marked with the symbol shown at left on time In the second field After due you can specify for how many days after the scheduled calibration date a pipette should be given the status delayed if the calibration was not performed During this time the pipette is marked in the Tasks list with the symbol shown at left factory setting 2 days When this time has expired the pipette is marked in the Tasks list with the overdue symbol shown at left Activate the Create tasks automatically option if you want pipettes to be automati cally added to the Tasks list otherwise you will have to manually add the pipettes to the Tasks list as required Defining comments In the main window of the Calibration Setup menu click on the Notices tab You may append a comment to each calibration chapter 9 2 which will appear on the calibration report Instead of entering your own text you may select a preset comment from a list In this menu you can define the comments that you want to be available from the list Note that no comments are preset at the factory Use the Add button to add a new comment to the list With the Delete button you can remove comments fro
100. f the USB converter for details please refer to the information given in the next chapters The figure below provides a basic overview of a multi balance configuration Balance range see chapter MCP 19 2 19 3 19 4 XS incl WX 19 8 USB Hub RS232C to USB AX incl MXYUMX 12 2 1 y lt i AT incl MT UMT 19 10 gt Q 19 1 WN A 1912 Calibry Workstation PC 19 13 Generic 19 14 Q gt Hardware Configuration 98 19 2 Calibry and MCP single unit This chapter provides information on how to use Calibry in conjunction with the MCP Multichannel Pipette Calibration System by METTLER TOLEDO used in single unit configuration The MCP is equipped with a serial RS232C interface that is to be connected to the Calibry workstation as shown below Before establishing the connection make sure the computer and the MCP are switched off Connection USB to RS232 converter cable 11103691 Setting up the MCP 1 First verify the software version of the MCP The version number shows up briefly when switching on the unit The second number should be 1 40 or higher If this is not the case you will have to install the V1 40 or higher program cartridge 11138300 2 If the display of the MCP shows the do Cal message proceed to container calibration as explained in the MCP operating instructions No pipette calibration is possible while the do Cal message is displayed and Calibry will report that
101. ference measurement Calibry checks how much time remains until the balance will request a reference mea surement If this amount of time is less than the value specified here Calibry performs a reference measurement on the balance before the calibration If on the other hand the time until the next reference measurement is longer than the specified value Calibry does not perform a reference measurement before the calibration Factory setting 30 seconds Vibration adapter Setting of the vibration adapter Factory setting Unstable environments Further information on the vibration adapter is found in the Operating Instructions supplied with your MCP balance Process adapter Setting of the process adapter Factory setting Off Further information on the process adapter is found in the Operating Instructions supplied with your MCP balance Repeatability Setting of the repeatability Factory setting Very quick release Further information on the repeatability is found in the Operating Instructions supplied with your MCP balance Recall for internal adjustment day Every MCP balance needs to be adjusted on a regular schedule using the internal adjust ment weight This setting determines the admissible number of days between adjustments As soon as the specified period expires the Required calibration column of the device list menu Balances amp Devices Management will advise you to carry
102. following table provides the complete data structure found in the XML file exported by Calibry together with a brief description of the data Note All documents created and used with programs which are not included in Calibry have to be validated by the user and are not supported by METTLER TOLEDO Group Subgroup 1 Subgroup 2__ Subgroup 3 Subgroup 4 XML element Description __ P Notes o o o o Contact This block of data is present 3 times for Owner Delivery and Invoice ooo ee a ee ee Owner Delivery Invoice po internat identification po Customerinumber S S po ff Company Companryrname S O po baste Farmityngme O po First Firstngme O po Department Deparment S pop ress Ares po Sth Site CE pe Rode po ity ty CE pop tone Phone number O po ro Roemer O ST Mit Emi cdcress S This block of data is present only once as there is just pipette per report ns nl ep ron pop SN Serial number of the pipete po St Second identification o Nome Name of the pipette po Rangetcx Maximum volume of the pipette u1 po Rangetin Minimum volume of the pipette pl po scription Pipettotype S 4 l e e ee e o T o Chae Number of pipette channels ISO class of the pipette 0 Unknown 1 Type A 2 Type D1 3 Type D2 4 Motor driven burette Hand driven burette PipetteAlphaC Cubic cca coefficient of the pipette 1 C eee i a cubic expansion Advanced Opti
103. g systems Windows XP Professional a2 bit with latest serece pack Windows Vista Business and Enterprise a2 bit with latest service pack Windows 7 Business and Enterprise 32 64 bit with latest sarvica pack Software Installation gt Calibry gt Caphure tool Additional information Supported database servers MS SOL Server 2005 with latest semite pack lt M5 SOL Server 2008 With Atest erita pack ME SOL Serwer 2008 A2 With obpst servei piik Shh are IntimnGt Eapontr601 arth atest service pack HET 3 5 Will Bp matiti f nt preeernt Hordware requirements CRU 2 GH Single Core RAM 1 CE Hard Dick 5 GB free space Display resolution 10244708 CD ROM drive for instalation 100 Mbit s Ethernet for Calibry network edmon Freg RS232C serial interface COM Port or U58 Calibry is supplied on a CD ROM Close all running applications on your PC before inserting the CD ROM into the CD drive of your PC Ifthe startup screen does not load automatically after having inserted the CD ROM double click the install exe file on the CD ROM From within the startup screen you may install Calibry and the optional Capture Tool Furthermore you may view the current manual assuming Adobe Acrobat Reader is installed on your PC and you may inquire information about Calibry s system requirements In the startup screen click on the System requirements button Before inst
104. heck Old value New value 24 05 2012 2nd ID Old value avc New value awc Working with the RFID option 77 Save on RFID Once the data transfer is complete Calibry will display the message shown here 1 Data have been saved on the RFID chip 17 3 RFID information Each time that you scan an RFID pipette that has already been defined in Calibry Calibry will automatically open a Quick Access dialog containing additional information about the RFID pipette Note You can also configure Calibry so that the Quick Access dialog does not open automatically Options Configuration RFID menu see chapter 16 a Quick Access Overview Pipette RFID Type Contact Status RFID unique ID 7h ane Custom field Factory date A see Custom field 2 Model name Pipete LTA a Model name ET Custom held 3 Seral number AL FHAN Serial number PHe Custom field 4 Secondary ID BR Secondary ID 212 Custom field 5 Last service ATA SiT Last service Custom field 6 Hest service A a Nest service Custom tield 7 Mest calibration mopa Mest calibration Pa NG ZEN Custom field amp Next quick check Sosan Nest quick check P MT a R Custom field 9 Reset 2nd ID Save 2nd ID Reset data white data Methods Tasks Reports Task Due Date Status Pipette Seri Schedule Method Na Pipette 56 owner Phone Pg 25 0S a MERETE ay RH EE Hiakai Calibrate Alongside the standard information ta
105. hermB Ath coefficient for adjustment errors B of the air temperature thermometer used at the end of the As Returned measurements the As Returned measurements measurements ments AFSWaterThermCalDate Last adjustment date of the water temperature thermometer used at start of the As Found measurements AFSWaterThermErrorMode Error mode for adjustment values of the water temperature thermometer used at start of the As Found measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB AFSWaterThermAlpha Ist coefficient for adjustment errors Alpha or SE of the water temperature thermometer used at start of the As Found measurements AFSWaterThermBeta 2nd coefficient for adjustment errors Beta or RE of the water temperature thermometer used at start of the As Found measurements AFSWaterThermA 3rd coefficient for adjustment errors A of the water temperature thermometer used at start of the As Found measurements AFSWaterThermB Ath coefficient for adjustment errors B of the water temperature thermometer used at start of the As Found measurements AFSWaterThermCalCert Number of the adjustment certificate of the water temperature thermometer used at start of uN uM the As Found measurements Advanced Options 92 measurements surements Last adjustment date of the water temperature thermometer used at the end of the As Found measureme
106. ibration Name of the user who has to counter sign the report assuming the counter signing feature is active see chapter 10 2 Identification number of the report This number is automatically generated by Calibry and is used to clearly identify every single report With calibrations including a status check the report first shows the results of the status check As found while the results of the real calibration appear on the subsequent pages As returned The remaining pages of the report provide separate details of the measurement results for each pipette channel along with a graphical representation For calibrations including a status check there are additional pages holding the results of the Status check for each pipette channel Calibration Reports 54 Q Calibration Report 442 KR A Pipette Serial Number 414K022 D Owner Company Sample Corp Pipette Second ID MERT 262 Owner Department Research Pipette Type Rainin Pipet Lite 8ch 20 200 ul Owner Name Cat Fritz Method ISO type A8x 200ul Method Description 3 Vol 4 Meas 20 100 200 Conditions Balance Water Temperature 25 C Model Demo Humidity 30 Readability 0 000001 g Abs Air Pressure 4 900 hPa Location 5 Z Factor 1 0039 ul mg Tips LTS250 Z Factor Reference ISO 8655 Evaporation 0 ul cycle Inspection Corrective action 6 Calibration test Tpi Tris As returned or ean pl 19 7600 18 7197 18 9599 19 0400 19 0400 19 520
107. ibration Calibry will now acquire the current environmental data from the Capture Tool Note The data export features of Calibry chapters 18 3 and 18 4 include only en vironmental data acquired from an external source e g the Capture Tool Notes on installing the Capture Tool The Calibry CD ROM contains the application and the appropriate source code which lets you customize the application as required The Capture Tool can be installed directly from the startup screen of the Calibry installation CD ROM When working in a network environment the firewall must be configured in a way that all PCs running Calibry can access the Capture Tool After installation first make sure the measuring instrument is properly installed and all sensors are connected Then start the Calibry Capture Tool Further information on the Calibry Capture Tool is found in the help file in PDF format on the Calibry CD ROM Advanced Options 80 Acquiring environmental data from another external source Configure Calibry for automatic data acquisition This can be accomplished in the Options Configuration Environmentals Get environ mental conditions from an external service menu see chapter 16 2 Once you have enabled the automatic acquisition of environmental data you will have to specify the name or IP address of the host computer on which the external application is running this may be the same computer on which Calibry resides
108. if required The user accepts full responsibility for the report layouts Settings for the placement of logos on the reports Logos Up to three logos may be placed on a report Make sure your logos are the appropriate size and resolution Calibry cannot scale the logos and places them in their original size For every logo the following settings are available File name Enter the name of the logo file respect the admissible file types including the file name extension and the path e g D Logo jpg or locate the file using the Browse button Position Set the position of the logo left Distance of the left edge of the logo from the left edge of the paper unit 1 10 mm factory setting 100 setting range 0 max paper width top Distance of the upper edge of the logo from the upper edge of the report content unit 1 10 mm factory setting 100 setting range 0 max paper length Most printers do have a non printing area along the edges Make sure your logo is in the printable area of your printer Make sure the logo does not get in conflict with the contents of the report Positions View on page Select the pages on which the logo will be printed Do not display hides the logo The Page header and Page footer options print the logo at the top or bottom of each page respectively The Calibration footer option prints the logo in the signature area of the
109. ilter click on the symbol 7864767 saerait again and select All Pa 70564363 9087456 7964767 9954324 7 5087436 a0S000894 9954324 AR 444 K as0500089a AR FF764 ARS44 K DIRTI ins eee _ 302062078 gt Sort Ascending Ft Sort Descending Clear Sorting Group By This Colurn of Hide Group By Box Remove This Column Column Chooser EI ml Best Fit Best Fit Call columns T Clear Filter T Filter Editor amp Filter Editor 4nd Pipette Serial Number Begins with lt enter a value Equals Does not equal gt Is greater than Is greater than or equal to Is less than amp Is less than or equal to as Is between 4E Is not between abe Contains ach Does not cantain Elbi Begins with ble Ends with auc Is like Instructions for Using Calibry 15 When you right click on a column header the menu opposite appears containing display options for the column Command expan Group by this Column Groups the entries in the list by the selected column header same function as the Drag a column header here to group by that column area See previous chapter for explanation Hide Group By Box Hides the Drag a column header here to group by that column area at the top of the list Remove this Column Removes the selected column from the list Existing column entries are not deleted this option only affects whether or not they are displayed
110. information than the reports created and displayed by Calibry Before exporting data from Calibry to Excel or Word you will have to create a template to accommodate the data in the respective application dot file for Word or xit file for Excel In Word the exported data is assigned via text form fields while in Excel this is accomplished with cell or range names For detailed information please refer to the documentation that came with Word or Excel The field names to be used are shown in the table below For exporting data right click in the Reports list on the calibration report to be exported and select the option Export to Microsoft Office alternatively you can go to the Quick Access dialog and click on the Export to Microsoft Office bution Then select the appropriate template Word or Excel from the file dialog After confirmation Calibry starts the appropriate application and exports the data to the template Note All documents created and used by applications not being part of the Calibry package must be validated by the user and are not supported by METTLER TOLEDO Field name Description Contact data Client number Owner ompany name Owner amily name Owner irst name Owner epartment Owner ddress Owner OwnerClientNumber OwnerCompany OwnerLastname OwnerFirstname OwnerDepartement OwnerAdaress TI gt OwnerState OwnerZIPCode ZIP code
111. is pipette A new contact can be added by clicking the Add button Previous OK Cancel In the Manufacturer specifications optional area you may enter the calibration specifications set up by the manufacturer for this particular pipette type This data will then be available in the calibration dialog and can be used as the basis of a test method If you do not enter the specifications here you may specify them later when calibrating the pipette You may specify up to 4 volumes to be checked If they are not already active check the boxes labeled Enable Enter the test volumes and the appropriate Systematic error and Random error for explanations of Systematic error and Random error see below Click on Save to save the new pipette type Note If you changed and saved the data of an existing pipette type the respective type might appear twice in the list thereafter however the entries differ in the Specification date date column If you do not want to define any further pipette types click on Close to return to the Pipette Assistant Click on the Next button to call up the next window of the Pipette Assistant Systematic error and Random error The Systematic error is the difference between the reference value and the arithmetic mean of the actually measured values The Random error defines the scatter of the measured values and is re
112. isabled none SE and RE Random Error and Systematic Error 2AB 2AB ARSAirThermAlpha 1st coefficient for adjustment errors Alpha or SE of the air temperature thermometer used at start of the As Returned measurements ARSAirThermBeta 2nd coefficient for adjustment errors Beta or RE of the air temperature thermometer used at start of the As Returned measurements ARSAirThermA 3rd coefficient for adjustment errors A of the air temperature thermometer used at start of the As Returned measurements ARSAirThermB Ath coefficient for adjustment errors B of the air temperature thermometer used at start of the As Returned measurements As Returned measurements measurements surements measurements AREAirThermErrorMode Error mode for adjustment values of the air temperature thermometer used at the end of the As Returned measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB AREAirThermAlpha Ist coefficient for adjustment errors Alpha or SE of the air temperature thermometer used at the end of the As Returned measurements AREAirThermBeta 2nd coefficient for adjustment errors Beta or RE of the air temperature thermometer used at the end of the As Returned measurements AREAirThermA 3rd coefficient for adjustment errors A of the air temperature thermometer used at the end of the As Returned measurements AREAirT
113. l activate None If you want to specify a fixed date for the next calibration activate Specific date and enter the date in the appropriate field or click on the arrow symbol to the right of the entry field to open a calendar where you may simply click on the desired date If the pipette should be calibrated at regular intervals activate Recall period and Day s Week s Month s Quarter s Semester s or Year s and enter the respective number in the appropriate field If you have selected the intervals Period there are other op tions available to you The Start Next date establishes when the first calibration with the set interval should take place The selected interval then applies to all other calibrations Termination establishes how long the interval should be valid For an unrestricted validity choose No end date If the interval should only apply to a certain number of calibrations then choose End after calibrations and enter the desired number of calibrations Using End by you can set a definite expiry date for the interval Using Reference date you can establish the date from which the interval will always be re calculated Scheduled calibration date uses the intended calibration date as a basis for setting the next calibration date Performed calibration date calculates the next calibration interval from the date on which
114. l pipettes See chapter 6 The only difference is thatthe data serial number pipette type manufacturer Serial Number 458 KRST A T TE B number of channels and range is read from the RFID chip Check ab The Serial Number has to be unique and should be written on your pipette t cannot that this data IS correct and make any changes if necessary be changed later The 2nd ID is for your own internal use and can be edited according to your needs Add pipette Step 1 3 Once the pipette assistant is complete the new pipette will be _freviows net cence available in Calibry 17 2 Calibration procedure The calibration procedure itself is the same as for conventional pipettes Once the calibration is complete Calibry will indicate that Status the data is now ready to be written to the pipette s RFID chip The data Calibry is now ready to write the data on the RFID chip of your pipette Please to be transfered will be displayed at the bottom of the dialog put Your pipette on the reader writer Save RFID Data scan the pipette using the reader and wait until the data have been ss transfered Note If your pipette has manual write protection make Old value 19 02 2010 sure that this is deactivated otherwise Calibry will not be able to ec write the data to the RFID chip Old value Values New value 01 01 2000 Next calibration Old value 25 05 2011 New value 25 05 2011 Next quick c
115. laded wetted Methixd Qa Cet Lambo fz Sere ebe fer poia Ge 414600 Perce for postis Gv 44 80 gt a fe 05 201114 00 00 System IN P RUEDI Calibration Pipette SN 414K022 D Added into Tasks list by user Print Close In the menu select Options Audit to open the audit trail Note The audit trail is part of the current database The most recent additions to the audit trail are shown at the top To view earlier records use the scroll bar Each record displays the date user computer and corresponding type and description of the action The audit trail can be very extensive For greater clarity the entries can be filtered by date To enable this select the required time period at the top of the list and click on Apply Filter The list filter options described in chapter 3 are also available to you Note When you open the audit trail Calibry always displays the entries from the last 30 days If you want to display a shorter or longer period you will have to change the filter setting accordingly To view the details of a specific record double click on the respec tive record The buttons below the audit trail list provide the following op tions Opens the print preview where you can format and print the audit trail Closes the audit trail Demo Mode 65 15 Demo Mode The demo mode allows you to simulate measurement values for calibration for example
116. lated to the standard deviation Step 3 Defining a contact In the third and last window of the Pipette Assistant define the contact for the new pipette Click on the arrow by the contact designation to display a list of all available contacts lf the required contact does not exist click on the Add button to define a new contact see chapter 5 Click on the OK button to terminate definition of the new pipette 6 2 Editing pipettes 6 3 Deleting pipettes Delete Pipette i J Are you sure you want to delete the selected pipette s eee Defining Pipettes 31 Once a pipette has been defined the only parameters you can change are the contact that is assigned to the pipette in question as well as the second identification 2nd ID Mark the respective pipette in the list and then click on the Edit button This starts the Pipette Assistant and you may assign a new contact and or a new second identification to the pipette Note If you have assigned a wrong pipette type to a particular pipette you will have to delete the pipette and define it again from scratch However this can be accomplished only after all existing calibration reports of the respective pipette have been deleted chapter 10 To remove a pipette from the list mark the respective pipette in the list and then click on the Delete button A question appears asking whether you really want to delete the pipette If you ans
117. le i i i wai the pipette appears automatically in the Tasks list again C None Specific date f Period gt Period Settings Start Next date Di 17 05 2011 i Last performed calibration date Mi 14 05 2008 Termination i Alo end date C End after i calibrations f End by ii 011 Reference date Scheduled calibration date bj omea 8 3 Starting calibration To start calibration of a pipette from the Tasks list mark the respective pipette in the list and then click on the Calibrate but ton Alternatively you can double click on the respective pipette in the list Instructions on how to carry out the calibration are given in chapter 9 Pai E It IS possible to manage pipettes in Calibry but carry out the calibration outside Calibry In this case click on the Calibrate external button A window appears for the manual entry of the calibration results External Pipette Calibration f lt n i p i The calibration date Certification date will automatically be Pipette Calibration given as the current date but you can change this if necessary Enter the Certificate number Certificate number Certification date Dienstag 17 Mai 20 2 Choose whether the pipette passed the calibration or not Passed Certificate number BR 8088_ERC 0 or Failed Status Passed C Failed If desired you can leave a comment Comment regarding the
118. led Enabled Enabled Piso i Volume in pl f User As found Number Calculation mode Strict Systematic error in Random error in Inverse sampling As returned Number Calculate pipette overall random error Systematic error in Random error in 34 Selecting the calibration mode Mode The calibration mode determines the procedure for the calibration and the steps which must be performed Quick check Simple calibration without additional measures is suited to the daily testing of pipettes You can establish the testing parameters e g number of measurements in such a way that the calibration occurs quickly For Quick Check calibrations a special report is created without graphics and there is no entry in the pipette history Calibration Simple calibration without additional measures Calibration with inspection Calibration with inspection of the pipette for faults and measures for fault correction During a calibration additional windows are opened in which you can enter information regarding inspection and fault correction This information is included in the printed reports Defining Test Methods 34 Calibration with inspection and As found data Calibration with inspection for faults and measures for fault correction see above but with an additional status check As found before the actual calibration The status test takes the form of an inspection on receipt and usual
119. lements Positions Report position top Distance of the report contents from the top edge of the paper unit 1 10 mm factory setting 100 Title position top Position of the report title in relation to the top of the content of the report Report position top setting see above unit 1 10mm factory setting 50 Title horizontal alignment Alignment of the report title center left or right aligned and at the top in the middle or at the bottom of the title field factory setting center aligned in the middle Settings for the fonts Fonts Font name Selects the font for the report All fonts that have been installed under Windows are available Title font size Font size of the title setting range 6 20 points factory setting 16 points Subtitle font size Font size of the subtitle setting range 6 20 points factory setting 10 points Text font size Font size of the report text setting range 6 16 points factory setting 8 points Notice font size Font size of the remarks text for calibrations setting range 6 10 points factory setting 8 points Advanced settings Advanced With the factory settings all advanced settings are deactivated Enable double signing If you activate this option a second user with the necessary authorization rights can countersign reports in print preview Show report at the end of the ca
120. libration If you activate this option the calibration report will be automatically displayed once the measurements are complete Print report at the end of the calibration If you activate this option the print dialog will automatically appear once the measure ments are complete so that you can print the report straight away Do not prompt for filename on export If you activate this option you will not be prompted for a file name when exporting the report data instead the default file name will be used see setting below Default file name Default name for the export file for the report data Shell execute on export Default name for the shell that will automatically open following the export of the report data Shells allow you to automatically process data or input data into other applications it is the customer s responsibility to program shells Changing the Program Settings 73 16 2 5 Settings for the audit trail Audit In this group you define the settings for the audit trail see chapter 14 Audit report title The title of the audit trail printout Audit report subtitle If you wish you can input the text for an additional line of title here 16 2 6 Balance settings Balance General settings General Default balance for single channel calibration Use this setting to determine the standard balance for single channel calibra tions The selected balance wi
121. lick on the View button or simply double click on the desired report in the list The selected report appears in the print preview On the next page you will find a sample report providing the following data 00000 00 0000 Title of the report Reference number if specified upon calibration Information about the company the pipette and the test method that was used Ambient conditions Information about the balance Result of the pipette fault inspection and measures taken to remedy the problems encountered for simple calibrations this information is not available Overview of the calibration results It displays the Mean value the Systematic Error and the Random Error as an absolute and relative value and the Measurement uncertainty according to ISO 8655 6 2002 Annex B for all pipette channels and all volumes that have been tested The detailed values for each channel and volume can be found later on in the report The Status item indicates whether or not the pipette has passed the calibration Causes for deletion of measured values only if measured values have been deleted upon calibration Calibration date Next due date for calibration if available Comment entered during calibration if any Graphical overview of the measurement results Systematic error for each channel and volume The dashed lines show the tolerance limits Name of the user that has carried out the cal
122. list of recognized balances check the communication parameters and cabling between the balance and your computer In addition please check whether the serial number you entered upon balance setup matches the serial number stated on the type plate of the balance Specifying Managing and Adjusting Balances and Peripheral Devices 22 4 2 Changing balance parameters 4 3 Removing a balance Delete Delete balance 2 r Are you sure vou want to delete this balance To change the parameters of a balance which has already been defined mark the respective balance in the list and then click on the Edit button The same window opens as for defining a new balance You may change all parameters except the serial number Note To activate the changes you either need to select the Bal ances amp Devices Detect balances menu fromthe main application window or restart Calibry To remove an existing balance from the list mark the respective balance in the list and then click on the Delete button For safety reasons you are asked whether you really want to delete the balance Selecting Yes does not truly delete the balance from the list but adds the Deleted tag to it Notes Balances currently connected to Calibry carry the Connected tag in the list and cannot be deleted If you need to delete such a balance you will have to switch it off or disconnect it from the PC and then select the Bal
123. ll appear at the top of the balance list in the Before calibration dialog Auto resolution for 4 decimal places pl This setting applies to METTLER TOLEDO high resolution XP and MCP balances only This value determines up to which nominal pipette volume the balance works at a resolution of 0 01 mg above this limit value the display resolution is automatically reduced to 0 1 mg Setting range O 1000 ul 0 automatic resolution switching disabled Factory setting 100 Auto resolution for 5 decimal places pl This setting applies to METTLER TOLEDO highest resolution XP and MCP balances only This value determines up to which nominal pipette volume the balance works at a resolution of 0 001 mg above this limit value the display resolution is automatically reduced to 0 01 mg Setting range 0 1000 ul 0 automatic resolution switching disabled Factory setting 10 Warning limit for Ext Test Permitted tolerance for checking the balance adjustment using an external test weight Enter a percentage of the nominal value for the external test weight Control limit for ext test Limit value for checking the balance adjustment using an external test weight Enter a per centage of the nominal value for the external test weight If this limit value is exceeded the balance may not be used for future calibrations Settings for METTLER TOLEDO MCP balances MCP balances Time limit for re
124. ly consists of a shortened measurement The results of the status check the inspection and the fault correction measures performed are recorded You will find details of the procedures for the individual calibration modes in chapter 9 Selecting the pipette channels to be tested Channel selection At the factory Calibry is pre configured to test all channels of a pipette However you may individually select the channels to be checked Note This setting only applies to conventional balances When using the MCP multi channel calibration system from METTLER TOLEDO all channels are tested Specifications for measurements and tolerances Set Tolerances Completing all fields manually may be a time consuming job Calibry facilitates the task with the three buttons shown at left Use the Manufacturer and ISO radio buttons to quickly insert the values for the volumes and the tolerances into the appropriate fields ISO inserts the values according to the ISO 8655 standard while Manufacturer inserts the volumes and tolerances specified by the pipette manufacturer Important The Manufacturer option is available only if the manufacturer s specifications have been entered when defining the pipette type see chapter 6 Check the User radio button if you wish to set up the volumes to be checked and the tolerances yourself This activates the appropriate entry fields and you may then enter your own values I
125. m the list Activating and deactivating acoustic signals In the main window of the Calibration Setup menu click on the Sounds tab During calibration Calibry emits various acoustic signals when switching to the next volume after having completed all measurements when exceeding a tolerance limit and in case of errors or when deleting erroneous measured values respectively If desired these acoustic signals can be enabled or disabled individually Changing the Program Settings Settings for calibration 69 16 2 General settings Calibry settings SE select the Options Configuration menu The Options Configuration menu holds Sptijngs fox methods a large number of settings that is why etwitorenti Min readings for as found it is divided into various groups that are Default readinas for as found described in the following sections Formulas Mi es a With the OK button you can save changed ie haces pects settings and quit the menu Click on the Report Apply button to save changed settings without exiting the menu Click on the Cancel button to exit the menu without saving any changes Max number of undo s Volumes proceed order Ascending pal l Reference number required Balance V Compensate for evaporation I Compensate for evaporation is locked Balances door configuration Database Open door Time Time delay for reading Advanced v Print
126. measurements for all volumes have been nee completed The values are highlighted with colors HER GRERRTRDARRORE RARER ERR R OTR R ARERR eee _ green The value iS within the tolerance rq nge Status 204i 1001 200p Status 20l 100l 200pl light red the value exceeds the tolerance by 100 200 Systematic Error Random Error Systematic Error Random Error Systematic Error Random Error 16 00 6 00 3 20 1 20 1 60 0 60 dark red the value exceeds the tolerance by 200 or more The completion of all measurements is confirmed in the Instruc tions section of the window Unido measurement Cancel Pipette calibration J Bo you want bo restart this calibration wn Calibrating Pipettes 47 Entering a comment You may append a comment to each calibration This text will appear on the calibration report To add a comment click on the Notice button before terminating the calibra tion procedure with the Finish button Note Instead of entering your own text you may select a preset comment from the list in the lower part of the window in the Options Calibration Setup menu you may define the comments you want to appear in the list see chapter 16 Deleting faulty measurement values If you think you made a mistake in a measurement operation implausible values click on the tab of the respective volume and then mark the column with the f
127. n the Calculation Mode field you can establish the rounding rules for the end results With the USP setting specification the end results are based on the same number of positions as the tolerances and only after this is it decided if the calibration was successful or not With the Strict setting the end results are shown with one more digit after the decimal point than the tolerances and are used for a Pass Fail decision Normally the dispensed volume of a pipette is measured i e you suck water into the pipette dispense it into a measuring vessel on the balance and then the increase in weight will be analyzed by Calibry However for certain pipettes the suction volume needs to be measured In this case you need to active the Inverse sampling option To carry out the measurement there is a full measuring container on the balance Remove liquid from the pipette and the loss in weight will be analyzed by Calibry Using the button Calculate pipette overall random error activate the additional calculation of the Random errors further explanation below for all pipette channels if required This value will also be shown in the calibration report Defining the volumes to be checked the number of measurements and the tolerances Tolerances In the central part of the window you set up the parameters for calibration Volume You may define up to 5 volumes to be checked As returned Number Number of measurem
128. name Freely selectable username Use real names as these will be used in calibration reports and in exported data Name of the relevant user account in Windows Enter the exact name as it is found in Windows When the program starts Calibry checks the active Windows user account and if both designations do not match the program start is aborted Login Select the levels of authorization for the user from the list lf none of the existing levels of authorization are relevant you can define a new one by clicking on the Add button as per the information given in the next section Level As soon as you have entered all of the data click on the Save button to save the new user User Management 62 13 2 Creating editing and deleting levels of authorization The levels of authorization Levels determine which actions a user is allowed to carry out To create edit or delete a level of authoriza tion click on the Add button in the User properties window see above or select levels in the Users User Levels menu asides Creating or editing a level of authoriza tion User levels To create a new level of authorization click Level name Authorized actions Authorized tabs Authorized configuration RFID Rights Administrator Create Edit Delete Print Cont Task Pipette Contact User m Calibration setup Audit manag Wri on the z Add s button Create Edit Delete Print Task Pip
129. nce automatically otherwise add it as a new balance as shown in the example to the left See chapter 4 Balance into Communication The settings marked with a red dot are mandatory while the other settings may be modi Name axta l na Serial number 4908224 S fied tO match your local conditions Balance line amp i Mol Except for special automated applications using accurate timing cycles we recommend to eee control the doors at the balance and to disable the door management function of Calibry Onthis computer Yes No as follows Set the Door mode parameter to Disabled only available for AX Door mode In the Options Configuration Balance AX balances menu you may advise Calibry to inform you when the balance is due for adjustment Notes on operation The measured values are transmitted to Calibry when the Print key key with printer symbol of the AX MX UMX balance is pressed No manual zero setting of the balance is required between subsequent pipetting opera tions Hardware Configuration 106 19 10 Calibry and AT MT UMT balances This chapter provides information on how to use Calibry in conjunction with the AT MT and UMT balances by METTLER TOLEDO The standard equipment of these balances includes a Data I O Port interface The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and
130. nd Secu Error 2 2AB a ee Ist coefficient for adjustment errors Alpho SE ee ee eee aa BAUE po A Bid co ficientfor adjustment errors A TY po CatCertificate Number of adjustment certificate po atNotice Note on adjustment __ Hygrometer 2 blocks of dota for As Found and As Returned Type of measurement the hygro meter was used for As Returned or As Found Internal identification of the unit a o a Serial number of the hygrometer po CaiDate Dote of lost adjustment Error mode for adjustment values ErrorMode 0 none 1 Random Error and Emor 2 8 sn esa are ama cipro iment eros T T e kge Beta RE ey a a ee eee oe asus iesst oe asus iesst po Btn co ficierttor agjustment errors B Oo ee Baaitcte uer of odusment eenean CalNotice Note on adjustment sagan Settings Default cubic expansion coefficient for l Default cubic expansion coefficient for Advanced Options 8 18 4 Exporting data in Microsoft Office format The Calibry calibration reports can be exported to Microsoft Word or Microsoft Excel This way you may design your reports to conform with standards set up by your local accreditation body Exporting data to Word allows for detailed adaptation of the layout while export ing data to Excel is primarily used for further data processing The table below lists all data fields that are exported The exported data is very extensive and provides much more
131. nd of the As Found measure ments disabled none SE and RE Random Error and Systematic Error 2AB 2AB AFEHygAlpha Ist coefficient for adjustment errors Alpha or SE of the hygrometer used at the end of the As Found measurements AFEHygBeta 2nd coefficient for adjustment errors Beta or RE of the hygrometer used at the end of the As Found measurements AFEHygA 3rd coefficient for adjustment errors A of the hygrometer used at the end of the As Found measurements AFEHygB Ath coefficient for adjustment errors B of the hygrometer used at the end of the As Found measurements AFEHygCalCert Number of the adjustment certificate of the hygrometer used at the end of the As Found measurements Field name AFEHygCalNote ARSHygSN ARSHygCalDate ARSHygErrorMode ARSHygAlpha AkSHygBeta ARSHygA ARSHygB ARSHygCalCert ARSHygCalNote AREHygSN AREHygCalDate AREHygErrorMode AREHygAlpha AhkEHygBeta AREHygA AREHygB AREHygCalCert AREHygCalNote ARTip ARTipAloha ARTipAlohaUncert AkDate AkUserName ARUndoCount AkUndo AFTip AF TipAlpha Advanced Options 95 Description Note on adjustment for the hygrometer used at the end of the As Found measurements serial number of the hygrometer used at start of the As Returned measurements Last adjustment date of the hygrometer used at start of the As Returned measurements Error mode for adjustment values of the hygrometer used at st
132. nding on the language enhanced character sets may be required these are usually available in the regional fonts Exporting a report In the report list right click to highlight the report to be exported and select the required export format in the Quick Access view there are corresponding buttons available for the export Export to XML writes the report data into an XML file without graphical representations which can be used with other XML compatible applications Export to Microsoft Office exports the data to either a Microsoft Excel or Microsoft Word template without graphical representations Further information on exporting data in XML or MS Office format is found in chapter 18 Note You can simultaneously select multiple reports from the list and export or print these together in XML format see below For use in Microsoft Office the reports need to be exported one by one Printing out a report To print a report you have two options This button calls up the Windows printer dialog alternatively you can select the Print option from the File menu or context menu Select the required settings and print the report lfyouselect the Print Preview option from the File menu or double click the required report in the list the print preview appears and provides you with further options see chapter 3 Note If counter signing reports is activated you need to print the repo
133. ne character lt CR gt lt LF gt and Character set ANSI WINDOWS In the application specific settings select Smart amp ErgoSens Activate the print function for the ErgoSens to which the photocell is connected Aux 1 or Aux 2 This ensures that the measurement values are automatically transmitted to Calibry via the interface In the user specific settings you can determine whether door opening should be automatic or manual Activate the manual operating mode and setdoor opening to 100 Setting up Calibry Usually Calibry will detect the XP26PC balance automatically otherwise add the XP26PC Baahi commun as a new balance as shown in the example to the left See chapter 4 a a Set the Door mode parameter to Manual Serial number fa28za55 sts C f i f ternal The settings marked with a red dot are mandatory while the other settings may be modi Balance ine fied to match your local conditions Model Channel tray Location z In the Options Configuration Balance XP balances menu you may advise Calibry to On this computer EN inform you when the balance is due for adjustment Status Notes on operation The settings above ensure that Calibry controls the XP26PC automatic door correctly Balance info Communication No manual zero setting of the balance is required between subsequent pipetting opera Com port number feom o tions Baud rate Data kits Parity Stop
134. nels Description If you just wish to see the results of calibra tions done with a particular test method you The history is based only on the results for 4s returned calibrations may select the res pective meth od from the Method drop down menu Measurement Method Date Volume set Channel Actual pl Systematic Passed Random Err Passed Status External atin Pe ESET il OO You may use the Channel dropdown 2 0164 0 170 0 818 2 0059 0 293 2 0078 0 389 2 0094 0 468 2 0068 0 341 2 0023 0 113 2 0074 0 371 10006 A Oe A menu to display the results of a particular channel 0 000 0 170 0 057 0 057 0 170 0 114 OALA RISISISISISIAIS RISISISIAISAIAIS View history for pipette 414K022 D Method Channel Actual volume Method liso type A Multi Sch 200 pl v f Description The history is based only on the results for As returned calibrations Measurement Method Date ISO type A PE Ee I ISO type A 17 05 2011 IsO type A 17 05 2011 volume set Channel Actual yl 98 8800 1 120 199 0400 0 480 16 7998 Volume Systematic error z Jun 2011 30117 000 150485 000 L 150585 000 150485 000 1 150585 000 75192 500 T 16 001 Systematic Passed Random Err Passed Status 102 9600 2 960 CIXIR External A Print Export 200
135. ng up the current database you can locate the database to be imported and begin the import process Do you want to make a backup first Updating an older SQL database for use with Calibry 5 0 The Update option in the database utility program updates the database specified for use with Calibry to version 9 0 Calibry DB Maintenance ea The warning opposite alerts you to the fact that updating the A This operation will delete the existing data in your Calibry database This operation is irreversible without a backup database is an irreve sible operation and that you should therefo re back the data up first Click Yes which will start the backup dialog Nen Abbrechen see below The update is carried out once the current database has been successfully backed up Do you want to make a backup first Backing up restoring or initializing a database You will not need to use the options Backup back database up Restore load a backup copy of a database and Initialize initialize database when you install Calibry for the first time The following section contains a brief explanation of these options Back up database Backup This options allows you to create a backup copy of the current database We recommend that you do this at regular intervals Note The database can be saved under its original name because the date and time are automatically appended to the file name every time it is saved
136. nnetnee 67 EEE TIA o T ET AEE E AA EA E AO at cen A OEE T 69 Calibration settings Calibration Y sisss iadenituereedisntindtehinetonethnetmnspaubichiiiatd niaaa enana AENA N aR EENAA EEEE iRNR 69 Settings for the environmental Conditions Environmentals sssssssrrsesrrsersserrsernsnrrnnnserrsnrnsnnrstenrsnrisnrrssrrsterrsrrrns 70 Seis NOC Ne USE Or TON MIS FOUIS Jenness r E FI E TOF Ale T O ROT aa A T T E E O nen na E 7 senings TOF dle CUCL MON AUO esnea N E yaheieashatnadand E senetathaletiaatereats 73 BINA ILS TN a earraceer rasta E aia chet eto atts eepatusste oleae venues Nab E E cen gan R 73 CTT SOL le IU ODI TAD seawesaiipeca te netted ro eae Laced awe E E E a Renae eenenenei aude 74 TSS SY semings MAINS OF Y sears rater gi effet oop eo nase eae ETENEE 74 OPON TOT CROSS ANO CY n E E E E E seat satan gd saeubamtanabes 74 PARURO I S T gen E ten ene eee E S lie Working with the RFID option isisensiciniisuscenenepacwansncuntwectvewcnteicbtecnislonsucecenvncsiivetunaseanvauaeseudxaiaeniaasinetaveensetenvivests 76 Deining a new DIDS re wihi RFID CHID sesreiisersenturertuninei nn arpoa enanar EAEN OAA A FEET AURET LA EREA 76 CTT WUT HOC CCS an E E E E A A tere A E T N A E E 76 KA O a E A AREA S EAA EAA ig Adv nced OPHONS ics ctescacc ic cceic case aeaucdeneveuaedeanmde dey sbewcaaeuaesbitaausenmeser ees snsuviteeestveuteudsanvaaneeawecesancesdveasuntecrecsiecs 78 USING the equation editor ccisenastex snt seandudsvrivedcdecaciseabdaecebve
137. nt uncertainty of the cubic expansion coefficient Set cubic expansion coefficient for tips You may set up Calibry to display an additional field for the entry of the cubic expansion coefficient when defining a new pipette tip In this case there will also be a second field for the measurement uncertainty of the cubic expansion coefficient Default cubic expansion coefficient for pipettes This setting specifies the standard cubic expansion coefficient for pipettes in the range of O to 1 factory setting 0 Default cubic expansion coefficient for tips This setting specifies the standard cubic expansion coefficient for pipette tips in the range of O to 1 factory setting 0 Calibration error mode for balances You may set up Calibry to display additional fields for the entry of measurement errors when calibrating balances or testing calibration with an external test weight Select SE and RE if you need 2 fields for entering errors e g for Random Error and Systematic Error or select 2AB for a total of 4 measurement error fields Calibration error mode for other devices Same setting as above but for entering the calibration errors of other devices ther mometer hygrometer barometer etc Changing the Program Settings 75 16 2 10 Printing the settings The Print button can be used to print out a detailed report of all settings This report details your own settings and the fac
138. ntal parameters are displayed If these parameters do not correspond with the current environmental conditions click on the Edit button to change the values In the table click on the value which corresponds to the current combination of temperature and atmospheric pressure The values water temperature atmospheric pressure and Z factor are trans ferred to the input fields and you need only to enter the relative humidity Humidity the air temperature and possibly also the evaporation factor Evaporation You can however also enter the values individually the Z factor is calculated automatically Click on OK to transfer the values and close the window Note With the factory settings Calibry assumes the water tem perature and the air temperature are the same i e you can just specify the water temperature However you may configure Calibry in a way that both temperatures can be set up independently The Options Configuration Environmentals menu chapter 16 pro vides many options for the environmental parameters locking of individual values acquisition of environmental data from external sources calculation of the Z factor using a formula etc Calibrating Pipettes 45 Starting the calibration When you have input all the data click on the Calibrate button to start the calibration The window shown below opens a W wks returned Instructions Hext measurement 20pl 1 Pi
139. nts AFEWaterThermErrorMode Error mode for adjustment values of the water temperature thermometer used at the end of the As Found measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the water temperature thermometer used at the end of the As Found measurements 2nd coefficient for adjustment errors Beta or RE of the water temperature thermometer used at the end of the As Found measurements 3rd coefficient for adjustment errors A of the water temperature thermometer used at the end of the As Found measurements Ath coefficient for adjustment errors B of the water temperature thermometer used at the end of the As Found measurements of the As Found measurements measurements surements Last adjustment date of the water temperature thermometer used at start of the As Returned measurements AkSWaterThermErrorMode Error mode for adjustment values of the water temperature thermometer used at start of the As Returned measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the water temperature thermometer used at start of the As Returned measurements 2nd coefficient for adjustment errors Beta or RE of the water temperature thermometer used at start of the As Returned measurement
140. of the Z factor Z Factor ISO 8655 Calculation of the Z factor according to ISO 8655 factory setting ISO TR 20461 Calculation of the Z factor according to ISO TR 20461 Manual The Z factor can be entered directly No calculation is carried out Custom If you select this option you may click on the Open Formula Editor button to launch the equation editor for the Z factor and then define your own formula Chapter 18 provides information on how to use the equation editor Settings for the calculation of the measurement uncertainty Uncertainty ISO 8655 Calculation of the measurement uncertainty according to ISO 8655 factory setting Custom If you select this option you may click on the Open Formula Editor button to launch the equation editor for the measure ment uncertainty and then define your own formula Chapter 18 provides information on how to use the equation editor 16 2 4 Settings for the reports Report In this group you define the settings for the report layouts You can view the effects of the changes immediately by calling up a report in the Reports menu Notes These settings affect all reports including reports that had already been created when the changes were made When designing reports please respect the applicable standards and legal provisions Before making changes please note the current settings thus you can easily revert to the previous values
141. ol indicates that there are at least 3 days remaining between the current date and the calibration date In this case the symbol changes automatically as soon as there are no more than 3 days remaining before calibration must take place see information below The following symbols appear with pipettes for which a calibration date or calibration interval has been set up Usually such pipettes are added to the Tasks list automatically Up to 3 days remain between the current date and the due date for calibration or the due date has been exactly reached The calibration is overdue by not more than 2 days The calibration is overdue by at least 2 days Note In the Options Calibration Setup Schedule menu you can specify how many days before calibration is due the pipette should be automatically added to the Tasks list and the length of time between the individual stages symbols The above entries 2 or 3 days are the factory settings Further information is contained in chapter 16 The Tasks List 41 8 2 Deleting pipettes from the Tasks list Helene To delete a pipette from the Tasks list mark the respective pipette in the list and then click on the Delete button r SSeS ee Faj A window then opens in which you can define a new calibration interval or date for the pipette to be removed from the Tasks list chapter 7 When the interval expires or the specified date is reached Schedu
142. olume for the first measurement operation and start the calibra tion procedure with the Start button of the balance Make sure to pipette the appropriate volume Note The order of volumes in 1126300064 the list can be changed in the Options Configuration Calibration MCP1OS menu chapter 16 However this order does not determine the pipetting sequence Tota progress By clicking on the tab with the current volume in the example at a left for example 20 ul you can observe how the measurement Status 204 1001 20044 values are recorded When the first measurement operation for the oe o TEE commer T first volume is finished pipette the same volume again and then ch 2 0 020560 g 0 020241 g 0 020241 g 0 020241 g start the second measurement on the balance In the example a T re a F at left all measurements for the first volume are already finished T aa n e ToT Perform all the remaining measurements for the first volume When cE sonses concise eeng nees they are all finished a prompt appears in the Instructions section to change the volume Set the second volume on the pipette and then perform all the necessary measurements hou BRE T Tare between readings T Accent ow values Undomessurenert_ Provided thatthere are sufficient values at least 2 measured values per pipette channel you can see the result of the calibration at any time by clicking on the Status tab In the example at left all
143. omatically otherwise add the XA as a new os eee balance as shown in the example to the left see chapter 4 7 _ The settings marked with a red dot are mandatory while the other settings may be modi ks ieee fied to match your local conditions Internal ID Balance line odel X4105DU 5 A 5 In the Options Configuration Balance Other XS XA balances menu you may advise Channel tray 1 Location DOM E Calibry to inform you when the balance is due for adjustment Onthis computer Yes No Door mode Status ttline Notes on operation The measured values are transmitted to Calibry when the Print key key with printer symbol of the XA balance is pressed cee conan No manual zero setting of the balance is required between subsequent pipetting opera tions Com port number loom o Baud rate 9600 Data hits Parity Stop Bits Handshake Xon xOff Hardware Configuration 110 19 14 Calibry and generic balances If a balance is not supported or recognized by Calibry you can try to add it to Calibry as a Generic balance To do this select the Generic setting under Balance line Ensure that the communication settings for Calibry and the balance match After you have added the balance to Calibry select the option Detect balances from the Balances amp Devices menu Calibry will then try to make a connection with the balance Please note th
144. omputer Yes C No Door made Paavel a Notes on operation The measured values are transmitted to Calibry when the Transfer key also marked Menu of the AG balance is pressed Mode z ji In the Options Configuration Balance AG balances menu you may advise Calibry to No manual zero setting of the balance is required between subsequent pipetting opera Balance into Communication tions Com port number loom a Baud rate Data hits Parity Stop Bits Handshake Hardware Configuration 108 19 12 Calibry and SAG balances This chapter provides information on how to use Calibry in conjunction with the SAG balances by METTLER TOLEDO The standard equipment of these balances includes a LocalCAN interface hence connection to the Calibry workstation requires the optional LC RS9 converter cable The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and the balance are switched off Connection LC RS9 Cable 00229065 e P ee Setting up the SAG balance The communication parameters are not set up at the balance but at the converter box of the LC RS9 cable Set the dials as follows Usually Calibry will detect the SAG balance automatically otherwise add it as a new bal ance as shown in the example to the left see chapter 4 Balance into Communication Ae manr aaoo The settings marked with a red dot ar
145. on this button only becomes accessible when the entire calibration process is complete The data is saved the pipette is deleted from the Tasks list the calibration dialog is closed and the Quick Access window appears see chapter 12 lf the calibration was not successful values outside the toler ances you will be asked whether you want to remove the pipette from Calibry lf you answer with No the pipette remains in Calibry and can be calibrated again later lf you answer with Yes the pipette is classified as being no longer capable of calibration status Out of order and is permanently removed from both the pipette list and the Tasks list of Calibry Be careful with this option because there is no way of return ing the pipette to Calibry after it has been removed except for a new definition 9 3 Calibrating Pipettes 49 Calibrating a multi channel pipette with inspection and fault correction lt 2 Fy With this calibration method Calibration with inspection the pipette is inspected for faults before the actual calibration and any necessary measures for fault correction are performed For this purpose while the calibration is being performed additional windows are opened in which you can make inputs for inspection and fault correction These inputs may also be printed on the reports Note In this chapter only those steps are described in detail which are typical for this
146. onal up in this window Notice toptira gt Click on the OK button to confirm your entry This adds the data to the list of adjustments performed with the respective device Calibrate device Result If you wish to remove a particular device select the respective entry from the list and then click on the Delete button 4 7 Printing calibration reports VEe sellneion FAO e To print the calibration report of a balance or another device first select the relevant device in the device list In the Calibrations window all the calibrations carried out for this device will be displayed Select the relevant calibration procedure in the list and click on the button marked View calibration report underneath the list This will open the Print Preview where you can format and print the calibration report chapter 3 4 Defining Contacts 26 5 Defining Contacts For each pipette the corresponding customer data must be available These contacts are part of every pipette definition and must be available before you define a new pipette Click on the Contacts tab to open the menu for defining customer data Calibry File Balances amp Devices Users Options Help Foo In the example at left some contacts have already been defined j Pipettes Methods I AA k P Reports i History Number of contacts displayed 3 Drag a column header here to group by that column Owner Last
147. ons 83 Group Subgroup 1 Subgroup2 Subgroup 3__ Subgroup 4_ XML element Description _ _ O Notes S d S d Metod a a aT po me Name of the test method 4 e o Besteion esenp oe es eho P NBV Number of volumes to be checked selected calibration mode ee 0 Calibration 1 Calibration with SLIT IAL 2 inspection 2 Calibration with inspec tion and As found data Number of pipette channels to be checked Selected tolerance mode 0 Manual 1 ISO Type A 2 ISO Type D1 3 ISO Type D2 Foleranceenolee Nico Wooncnven ourcte 5 ISO Hand driven burette c nee T F T 7 Fe Returned measurements Random Error factor for As Returned a ee el C T T T ee eee measurements ee eT measurement O f all per volume Volume aL for calibration OF f T e peer A Se VolumelD Serre identification Fr Defined volume ul Readin Defined number of As Returned g measurements Defined number of As Found pp Admissible Systematic Error rn Admissible Random Error 7 awm P p ler deni 0 done NoBalance with balance or in demo mode 0 with balance 1 demo mode Indicates whether or notthe As Found AsFoundPossible measurement not possible 0 mea surement possible licerContoler Name of the user who counter signed the report Noe Notice on calibration ee identification measurement was carried out 1 Next calibration date
148. ool Environmental Conditions Capture Fortestopevices 00 ment and display the respective data in the Information 3 Device status nv n at a ee ces mers Device status section of the window to establish the connection i DB fe caede nel er ech aitti ine Eoreecion ski Deen s connected In the same section of the window check 2 Check that the values on the right ars plausible Aut the setings jisti n the plausibility of the environmental data in step 2 as needed ze Capture tine 26200 displayed If a particular value appears to M 1 Configure your device Air temperature in C sa 00tti i SOSOSOCO O C i e a G a e be implausible e g the air temperature COM Pot Cr iT Hui in LT value select a different channel for this e so es papa parameter from the Configure the device s TEE ea dove chai Aea OA channels window ir temperature capture Channel 3 v Setup gt gt Parameter gt gt Calibration gt gt Environmental parameter v Wasttenpectsscatse Gasse CEtle toner Yas Enter the values from the Configure your Humidity capture Cran Atoreadingremotename chi2wehowroom 2 Calibry software section of the window in essure ure Chann S 0 fe f e I 7 i 1 Tyra amei eee ag A E the respective parameter fields in Calibry these are found in the Options Configura Copyright MT CH 2007 Beta 0 3 0 0 Cose tion Environmentals menu Upon every cal
149. or adjustment Notes on operation The measured values are transmitted to Calibry when the Print key key with printer symbol of the AI MT UMT balance is pressed No manual zero setting of the balance is required between subsequent pipetting opera tions Hardware Configuration 107 19 11 Calibry and AG balances This chapter provides information on how to use Calibry in conjunction with the AG balances by METTLERTOLEDO The standard equipment of these balances includes a LocalCAN interface hence connection to the Calibry workstation requires the optional LC RS9 converter cable The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and the balance are switched off Connection i LC RS9 Cable a 00229065 Setting up the AG balance The communication parameters are not set up at the balance but at the converter box of the LC RS9 cable Set the dials as follows Usually Calibry will detect the AG balance automatically otherwise add it as a new bal ance as shown in the example to the left see chapter 4 Balance into Communication Name x6 Pretingua S The settings marked with a red dot are mandatory while the other settings may be modi Sereumber OSES fied to match your local conditions Internal ID Balance line Channel tray s RER or 79 vm inform you when the balance is due for adjustment Onthis c
150. ors A of the hygrometer used at the end of the As Returned measurements Ath coefficient for adjustment errors B of the hygrometer used at the end of the As Returned measurements Number of the adjustment certificate of the hygrometer used at the end of the As Returned measurements Note on adjustment for the hygrometer used at the end of the As Returned measurements Calibration result Pipette tip used for the As Returned measurement Cubic expansion coefficient of the pipette tip used for the As Returned measurement 1 C Uncertainty of the cubic expansion coefficient of the pipette tip used for the As Returned measurement 1 C Date of As Returned measurement Name of the user who carried out the As Returned measurement umber of As Returned measurements cancelled Undo easons for cancelling As Returned measurements plain text ipette tio used for the As Found measurement ubic expansion coefficient of the pipette tip used for the As Found measurement 1 C gt Q lt Q mD O 9D Q O O Z O 5 N Field name Description AFTipAlphaUncert Uncertainty of the cubic expansion coefficient of the pipette tip used for the As Found mea surement 1 C AFDate Date of As Found measurement AFUserName Name of the user who carried out the As Found measurement AFUndoCount Number of As Found measurements cancelled
151. otes on operation The measured values are transmitted to Calibry when the Print key key with printer symbol of the XS WX balance is pressed No manual zero setting of the balance is required between subsequent pipetting opera tions Hardware Configuration 105 19 9 Calibry and AX MX UMX balances This chapter provides information on how to use Calibry in conjunction with the AX MX and UMX balances by METTLER TOLEDO The standard equipment of these balances includes a serial RS232C interface The balance interface is to be connected to the Calibry workstation as shown below Before establishing the connection make sure both the computer and the balance are switched off Connection B RS9 RS9 cable 1 1 m f 11101051 Setting up the AX MX UMX balance set the Host interface to the following values Baud rate 9600 Baud Bii Parity 8 Bit none Handshake XON XOFF End of line char acter lt CR gt lt LF gt and Character set ANSI WINDOWS Except for special applications we recommend to disable the door management function of Calibry as explained below only available for AX and to set up the balance accordingly In the User Settings you may define the Door function mode automatic or manual select the manual mode if you leave the doors open permanently e g when using a moisture trap or if want to open and close the doors manually Setting up Calibry Usually Calibry will detect the AX MX or UMX bala
152. out an adjustment and or test Factory setting O Monitoring of adjustment interval disabled Recall for internal adjustment external test day As above but Calibry also asks you to check the internal adjustment with an external test weight Factory setting O Monitoring of adjustment fest interval disabled Recall for external test internal adjustment external test day As above but Calibry first asks you to check adjustment with an external test weight then adjust the balance with the internal weight and finally recheck the adjustment with the external test weight Factory setting O Monitoring of adjustment fest interval disabled The options for the remaining balances XP AX etc just include the monitoring of the adjustment test interval as explained above Information on how to set up the various balances is found in chapter 19 Changing the Program Settings 74 16 2 7 Settings for the RFID option RFID These settings are only applied when Calibry is operating with the RFID option enabled Filter lists according to pipette serial number If you activate this option all lists will be sorted by pipette serial number Open the quick access dialog automatically If this option is activated factory setting when you import the RFID data for a pipette a Quick Access dialog will automatically open displaying the imported data this dialog can also be used to transfer data to the pipette
153. ow do you want to use Calibry Enter a license key C Calibry Light Demo Calibry Single Workstation Demo C Calibry Network Edition Demo Welcome to Calibry 5 0 You can find the keys on the license sheets e g F2R55 67MHT ABCDE F2345 FDEES Edition key Provide a valid Edition key Option key Provide a valid Option key optional sek C After installation Calibry can be used with its full range of functions for a trial period of 45 days After this period you need to activate Calibry in order to continue using the program To activate the program chapter 2 6 a license key is needed Using Calibry in demo mode If you are using one of the three demo versions of Calibry do you not need to enter a license key but you will not be able to activate and continue to use Calibry after the end of the test period The Calibry Single Workstation edition allows you to use Calibry on a single computer with a local database The Calibry Light edition is identical to the previous edition but does not include support for the METTLER TOLEDO multichannel pipette calibration system MCP The Calibry Network edition allows Calibry to be used on a network up to five Calibry clients can access one SQL Server through the network Entering a license key When you purchase Calibry you automatically receive a license key which allows you to activate Calibry and continue using the program after
154. pette 414K 022 D Rainin Pipet Lite amp ch 20 200 ul 6 channel s Total progress Status 2051 1001 200w Status 201ul 100 200i Random Error 0 60 Random Error 1 20 Random Error 6 00 Systematic Error 16 00 Systematic Error 3 20 Systematic Error 1 60 Method ISO tyge A Mukti ach 200 pl 3 Wol 4 bheas 20 100 200 pl 20i 1 00u 200l 8 channel s Current volume Yolume Measurements Copy m y OT Be oo a Environmental conditions Pressure Humidity Air temp Vater temp Z Factor Evaporation Balance S00 hPa a0 Aa E Aa E 1 0039 pling 0 pltcycle MCP 1 system Tare Notice Jr Balance status 1126300064 MiP TOS Undo measurement Cancel The left part of the window displays information about the pipette the test method the current test volume the environmental conditions and the balance The balance selected for the calibration appears as a colored symbol in the lower part of the window Note If you selected the Demo setting calibration will take place in demo mode and instead of the balance symbol there will be a field for simulating the values see chapter 15 Depending on the color the balance symbol has the following meaning Green The balance is ready for the calibration to be performed 1726200064 17126300064 Red The balance is not yet ready for calibration e g because a reference mea
155. pter 2 3 Remove the old version of Calibry from your computer using the Windows Control Panel Control Panel gt Add or Remove Programs Instructions for Using Calibry 14 3 Instructions for Using Calibry This chapter gives you basic information about the structure of the software and operation of Calibry Note In case you encounter problems with Calibry we recommend to check the application preferences in the first place Options Configuration menu chapter 16 3 1 The tabs i Calibry File Balances Devices Users Options Help 50 4 oy aT Pipettes Methods Tasks B Contacts d Reports shy History Jil i Number of pipettes displayed 14 ja Drag a column header here to group by that column d Pipette Serial Number Pipette Type Description Pipette Second ID Pipette Type Pipette Number of Channels I 414k022 0 Rainin Pipet Lite ach 20 200 ul MERT 262 if Rainin Pipet Lite amp ch 20 200 ul Rainin Pipet Lite amp ch 20 200 ul 655775686844 Rainin EDP PLUSEP 10 3338 Rainin EDP PLUSEP 10 76564363 Rainin Pipet Lite 8ch 2 20 ul i Rainin Pipet Lite 8ch 2 20 ul 7864767 g Rainin Pipet Lite 12ch 20 200 ul Rainin Pipet Lite 12ch 20 200 ul 9087436 Rainin Pipet Plus R20 Rainin Pipet Plus R20 9954324 Rainin Pipet Lite ach 20 200 ul Rainin Pipet Lite 8ch 20 200 ul Add Ecdit Delete Guick Access The menus needed for daily work are available via 6 tabs Pipette Methods
156. r delete pipette types see chapter 6 Management Accesses the menu for the user management of Calibry You can set up different users for which different authorizations can be determined The levels of authorization User Levels determine which actions a user is allowed to carry out In this menu you can create edit or delete levels of authorization Further information on user management and authorization levels is found in chapter 13 Calibry constantly records all work steps which are executed Audit allows you to display the audit trail Further information on the Audit Trail is given in chapter 14 please refer to chapter 16 information is found in chapter 16 Methods User manual Opens the curenusermanuolinAdobeAcrbot o About Dispos information about Calbny S Instructions for Using Calibry 18 3 4 Printing lists settings and reports Calibry allows you to print out lists settings and reports The Report preview function helps you to format the printout The following section contains brief explanations of the report preview options F Report preview Oo Ss Fa E Close Print Quick PDF Fie Scale Margins Orientation Size Previous Nest Last _ Many Pages Zoom Out Zoom Zoom In Print ki age age Page Page k k Document Page Setup Tj Navigation foom Document ciwse osese reponpein O Prim Calls up the Windows printer dialog which lows yout select he printer you wi
157. r shipping and invoicing data are the same as for the owner data Using the Next and Previous buttons or the tabs you may switch between the entry masks at any time When you have entered all the data on the third menu page Invoice click on the OK button to save the data The newly defined contact now appears in the list 5 2 Changing a contact Edit 5 3 Deleting a contact Delete i Delete Contact i 7 Are you sure that you want to delete this contact e Defining Contacts 27 To change an existing contact mark the respective contact in the list and then click on the Edit button The same window appears as for defining a new contact Note Changes affect all pipettes to which the respective contact is assigned Changes made to a contact apply to new calibration reports only existing reports will keep the previous contact data To remove an existing contact from the list mark the respective contact in the list and then click on the Delete button If you answer the question with Yes the contact is deleted from the list If the contact you just deleted was part of a pipette definition see chapter 6 an additional information window appears asking you to delete the respective pipettes or to assign a new contact to them Delete contact a This contact is assigned bo one or more active pipettes Please delete these pipettes or assign them to 4 new contact
158. re test methods have been assigned without a known calibration time Options Audit Calibration Setup Configuration Unscheduled Calibration Methods Calibration Reminder Configuration Schedule Mone Specitic date Period Period Settings Start f Mext date Termination Reference date Monthts Di 17 05 2011 Last performed calibration date Mi 14 05 2008 No end date End after lo calibrations C Enel by Di 17 05 2014 Scheduled calibration date cen Choose the menu path Options Unscheduled Calibration Methods The list contains all pipettes to which one or more test methods have been assigned without a known calibration date or interval Click on the symbol for the desired pipette and Calibry shows you the methods which have been assigned to this pipette but have not yet been finished To set the calibration date or interval select the desired method and click on Set reminder This opens the Calibration Reminder Configuration where you can set a date and or intervals for the calibration with the chosen test method for description see chapter 7 2 The Tasks List 39 8 The Tasks List The Tasks list shows a concise overview of all pipettes to be calibrated Calibration can be started directly from the list Pipettes can be manually added to the Tasks list or automatically based on the calibra
159. re you do the calibration Factory setting option not activated Use ISQ 8655 table only If you activate this option you will not be able to enter any values for the water temperature or air pressure you will only be able to select the Z factor from the table Factory setting option not activated Get environmental conditions from an external service If you activate this option Calibry attempts to read the environmental data from an appropriate external application In this case you will have to set up the next two parameters Remote compute name or address and Remote computer port Factory setting option not activated Further information on how to get environmental data from a remote application is found in chapter 18 Remote computer name or address Host name or IP address of the computer that will supply the environmental data Remote computer port Number of the port to be used for communication with the remote computer that supplies the environ mental data Changing the Program Settings 71 16 2 3 Settings for the use of formulas Formulas In this group you define the formulas for the calculation of the Z factor and the measurement uncertainty shown in the reports Caution These are global settings and the formulas defined will be used by all Calibry workstations accessing this database Changes to the formulas take effect for subsequent calibrations only Settings for the calculation
160. refix lt bal gt m r gt all further components of the response are optional i e they are sent only if the respec tive values are available Example of a response lt bal gt m r gt lt tea gt 21 5 1944878 lt tew gt 21 3 1544881 lt hgr gt 95 2 H622471 lt prs gt 95 1 B224842 Once Calibry has received the environmental data from the external application they will be displayed in the Environmental param eters section of the calibration dialog Note The environmental data acquired automatically from an external application may still be modified manually if required If the data transfer fails the error message Failed to get the environmentals will appear and you will have to define the environmental data manually Advanced Options 82 18 3 Exporting data in XML format The calibration reports created by Calibry can be exported in XML format This data can be further processed by any application that supports the import of XML data The exported data is very extensive and contains much more information than the reports created by Calibry To export Calibry report data in XML format right click in the Reports list on the calibration report to be exported and select the option Export to XML alternatively you can go to the Quick Access dialog and click on the Export as XML button For importing and formatting XML data please consult the documentation that came with the respective application The
161. relevant standard deviation GUM Guaranteed specifications Rectangular distribution Typical values Standard deviation no conversion necessary Measurement uncertainty from a data sheet Rectangular distribution Measurement uncertainty from calibration certificate e g DKD k 2 divided by 2 Example formula used with Calibry Capture Tool U UexpnI 2 UgnI 2 1 2 1000 Expanded measurement uncertainty in accordance with ISO TR 20461 Uexpnl REAbs 1000 Nb 1 2 Experimental standard deviation of the mean calibration value 1000 2 dBAlpha dBBeta Vol 1000 oo EO 0 0000002 1 dtwAlpha 34 1 2 Vol 1 000000 10 12 0 0000000045 dtaAlpha 3 1 2 Vol 1 000000 10 12 Appendix 122 0 000000001 2 dpAlpha 3 1 2 Vol 1 O00000 10 12 Uncertainty of air pressure 0 0000000001 dHAlpha 3 1 2 Vol 1 000000 10 12 Uncertainty of relative humidity k7 1 10 2 3 1 2 Vol td 20 Uncertainty of pipette coefficient of thermal expansion k8 2 3 1 2 0 00000001 Vol 1000000 10 12 Uncertainty of pipette temperature 2 k1 2 k2 2 k3 2 k4 2 k5 2 k6 2 k7 2 k8 2 1 2 Standard measurement uncertainty of gravimetric determination of the volume standardized to 20 C V20 Note If the calculated measurement uncertainty needs to be compared with another value the functions Min x x and Max x X can be used The following parameters were used for the example above Balan
162. report The Report header and Report footer options print the logo at the top or bottom of the first page of the report respectively Selection of data to be reported Layout These settings are used to define the data you want to include in your reports With the factory settings all data are selected with the exception of the calibration time Show calibration time Show mean volume Mean value of the measurements Show relative systematic error Systematic error as a relative value Show absolute systematic error Systematic error as an absolute value Changing the Program Settings 72 Show absolute random error Random error as an absolute value Show relative random error Random error as a relative value Show measurement uncertainty Measurement uncertainty Show notice title Title of the comments for calibrations Show humidity Air humidity value Show inspection results Result of the inspection relevant only for calibrations including a physical inspection for faults Show undo s Aborted calibration and the reasons for aborting Show notice Comments entered upon calibration if any Show graphics Graphical representation of the calibration results Show next due date Next scheduled calibration date Show calibration time Time of the calibration Settings for positioning the report e
163. resents the nominal volume and the two marks at left and right represent the specified tolerances for the Systematic error Every time you click on the scroll bar the value is input that corresponds to the current position of the mouse pointer In the example at left several values have already been input Notice y p When you have input all the values for one volume Calibry changes automatically to the next volume and inputs a value every time you click However the display does not change automatically to the next volume so if you want to see the values you input you must click on the tab for the corresponding volume Just the same as for a real calibration you can view the result of the calibration at any time by clicking on the Status tab provided you already entered enough values Needless to say in demo mode all the other calibration options delete invalid measurement values restart calibration print a report etc can also be used inputting precise values If you want to input precise values e g for testing the procedure described above is not sufficiently accurate In this case you must enter the desired value in the field to the right of the scroll bar and then click on the Send button The value you input is then inserted in the next free position in the table Changing the Program Settings 67 16 Changing the Program Settings Calibry can be adapted to your specific requirements
164. rned tips epTIPS150 LTS250 TEL Certitied tips _ Mame E l Balance Environmental parameters Air temperature 250E Water temperature 25 C Humidity 30 Factor 1 0039 plima Pressure 900 hPa Evaporation O plicycle Edit Invalidate Pipette Calibrate Cancel Calibrating Pipettes 43 Selecting the pipette tips Tip From the list select the type of tips which are mounted on the pipette If the current type is not in the list click on the Add button to add a new type of tip Inthe Tips Management window you can delete tips from the list or add new ones to it To add a new tip click on the Add button enter the name of the tip and then click on Save Note It is possible to configure Calibry in such a way that two additional fields for entering the volume expansion coefficient of the pipette tips and their measurement uncertainty are displayed chapter 16 To delete a tip from the list mark the tip and then click on De lete If you answer the confirmation question with Yes the tip is deleted from the list Then click on OK to return to the previous window Selecting the balance In the Balance part of the window you can select the balance on which the calibration should be performed All balances recognized by Calibry are shown in the list If Calibry did not recognize a balance only the Demo setting will be available This
165. rresnnrrrsenrrrrernrrrrrnnrrrnrerrrrrerrrs 118 NOTES COE TAS CIC HNN e esaaerateueasa ni dudaieeduatcatd 122 Introduction 6 1 Introduction This chapter gives you basic information about the Calibry software Please read through this chapter carefully even if you already have experience with similar applications and pipette calibration systems Important note Please make sure to back up the database before updating the Calibry software see chapter 2 1 1 Short description of Calibry Thank you for choosing the Calibry software from METTLER TOLEDO Calibry is an application for calibrating pipettes and other dispensing systems for liquids in the range from 0 1 ulto 100 mi The applica tion supports a large number of weighing systems from METTLER TOLEDO Provided that enough hardware ports are available multiple weighing systems can be connected to Calibry Calibry is optimized for operation with the MCP multi channel pipette calibration systems and the XP26PC balance from METTLER TOLEDO and supports the special characteristics of these systems Calibry runs under Microsoft Windows see system requirements chapter 2 and provides a convenient user interface for intuitive and efficient working Together with a network licence the application is networkable and up to 5 PCs on which Calibry runs can access a common database 1 2 Important information about these instructions The following conventions apply throughout these operating instru
166. rts via the print preview since this countersigning option is only available there see below Counter signing a report If counter signing reports has been activated in the Options Configuration Report Ad vanced menu chapter 16 a further option appears in the print preview which can be used by a different user with the corresponding authorizations chapter 13 to counter sign the report simply by clicking this button Note The counter signing button is only available for reports that are yet to be counter signed Calibration Reports 57 Sign report If the same user who carried out the calibration tries to counter sign a report the error A amp calibration report cannot be signed by the person who performed the calibration Message shown here IS displayed Report settings The Options Configuration Report menu chapter 16 provides a variety of options for customizing the design of reports contents fonts logos etc The user is responsible for the layout of the report 10 3 Deleting reports Teel Highlight the reports that are to be deleted from the list and click on the Delete button or select the Delete option from the context menu Before the reports are deleted the following prompt appears If you answer yes to the Delete Report prompt the reports are deleted Calibration data will be lost Are vou sure you Want to delete this report Note Deleting reports disables any
167. ry DB Maintenance Before you can work with Calibry you need to configure the database or an error message will appear when Calibry is started startthe database utility program Calibry DB Maintenance from the Windows start menu or by double clicking on CalibryDBMaintenance exe in the METTLER TOLEDO folder in the Windows program directory Calibry DB Maintenance METTLER TOLEDO Current SQL Server SQL server instance SQLEXPRESS_1 Version f 0 50 1600 1 Status Calibry can be installed on this instance of SQLServer Current Calibry Database New_Calibry Version 5 0 17 0 Status 0K Initialize Restore Backup Upda Import Close Database name Database configuration SEL server instance Database name iM y Calibry Databasel Version Calibr can be installed on this instance of SQLServer Database does not exists a The specified database doesn t exist om this SQL Server instance as Do vou wank Calibry bo create it For you wi Using the database utility program you can selectan existing Calibry 5 0 database or create a new database Configure initialize an existing Calibry database i e delete all existing data records Initialize reload a backup copy of a Calibry database Restore create a backup copy of the Calibry database Backup update an older SQL database for use with Calibry 5 0 Update
168. s 3rd coefficient for adjustment errors A of the water temperature thermometer used at start of the As Returned measurements Ath coefficient for adjustment errors B of the water temperature thermometer used at start of the As Returned measurements the As Returned measurements measurements measurements measurements AkEWaterThermErrorMode Error mode for adjustment values of the water temperature thermometer used at the end of the As Returned measurements disabled none SE and RE Random Error and Systematic Error 2AB 2AB Ist coefficient for adjustment errors Alpha or SE of the water temperature thermometer used at the end of the As Returned measurements 2nd coefficient for adjustment errors Beta or RE of the water temperature thermometer used at the end of the As Returned measurements Field name AREWaterThermA AREWaterlThermB AREWaterThermCalCert AREWaterThermCalNote AFSBarSN AFSBarCalDate AFSBarErrorMode AFSBarAlpha AFSBarBeta AFSBarA AFSBarB AFSBarCalCert AFSBarCalNote AFEBarSN AFEBarCalDate AFEBarErrorMode AFEBarAloha AFEBarBeta AFEBarA AFEBarB AFEBarCalCert AFEBarCalNote ARSBarSN ARSBarCalDate ARSBarErrorMode ARSBarAloha ARSBarBeta ARSBarA Advanced Options 9 3rd coefficient for adjustment errors A of the water temperature thermometer used at the end of the As Returned measurements Ath coefficient for adjustment errors
169. s for the environmental conditions are rounded as follows If a measurement value forthe temperature is between 20 0 C and 20 5 C values greater than or equal to 20 25 C are rounded up to 20 5 C Values smaller than 20 25 C are rounded down to 20 0 C The same procedure applies to air pressure values Therefore values of between 900 hPa and 950 hPa are rounded up to 950 hPa from 925 hPa and above while values smaller than 925 hPa are rounded down to 900 hPa A similar procedure is followed for the standard pressure of 1013 hPa Between 1000 and 1013 hPa the mid point is 1006 50 hPa between 1013 and 1050 hPa this point is 1031 50 hPa In addition the following rules apply to the Z factor determined from the environmental conditions SO 8655 Four decimal places are used in accordance with the ISO 8655 6 conversion table ISO 20461 Five decimal places Calibry equation editor five decimal places Manual entry As many decimal places as have been entered are used Rounding of results conformity assessment The determining values for the conformity assessment are the relative measurement or specification values Calibry offers two rounding models The conformity assessment is only carried out after values have been rounded The results are shown to one more place than featured in the relevant specification Strict setting The results are rounded in accordance with USP Section 4 7 to the same number of places as
170. setting causes Calibry to work in demo mode see chapter 15 Note concerning the MCP system from METTLER TOLEDO To calibrate 1 channel pipettes choose the MCP from the list of balances Formulti channel pipettes the checkbox Use MCP x System is displayed under the list of balances instead of x there is the number of recognized MCP systems Activate this option in order to calibrate the pipette with the MCP Entering the reference number You can enter a reference number for the current calibration This appears on the report and makes identification of the specific ca libration easier Note In the Options Configuration menu chapter 16 you may specify whether the reference number is optional or mandatory Calibrating Pipettes Ad r Environmental conditions Environment Temperature in C Vater 22 0 Factor pl f mg CE Air Evaporation ul cycle lo Fressure hFa Humidity o Factor according to ISO 8655 950APa 1000 hPa 19 0 C 1 0026 1 0026 195 C 1 0027 1 0027 20 0 C 1 0026 1 0026 1013 hPa 1050 hPa 1 0027 1 0027 4 00265 1 0026 1 0029 1 0029 205 C 1 0029 1 0029 1 0030 1 0030 21 0 C 1 0030 1 0031 21 5 C 1 0031 1 0032 220 C 1 0032 1 0033 220 1 0033 1 0034 1 0031 1 0031 1 0032 1 0032 1 0034 1 0034 emen Specifying the environmental parameters In the lower part of the window the current settings for the Envi ronme
171. seusieadanlsadcdeep aboptent deed act svidvehidiecdaasndobautseseeusdceeealbadadacddanianens 78 Automatic acquisition of environmental data from an external SOUICE ccccceccceeccsssseeeececcsssseeteceecssssueeeseretsssueteeserrnns 79 0 6 gilarsteo o1 com ate ly e1 086 E ener ae Le tar ere tern as nent er eR ee re ie eee 82 Expornino dota in Microsont OMGES TOU EVI arurae issie ene at uate ge EEEn ETNE 87 19 193 19 2 19 3 19 4 19 9 19 6 19 7 19 8 t29 19 10 19 11 19 12 19 13 19 14 20 20 1 20 2 20 2 1 20 2 2 20 2 3 20 2 4 20 3 20 4 Contents 5 Hardware Configuration ccccsccccsssseeeceseeeeeeeeesaseeeeaeseeeaaseescasaeesasaeeeeaseeeeasaeaeassesseaseseeasaeesaaaeaeeaneseeaseessageess 97 Connecting several balances to a single Calibry workstation ss sssersserrsserrsenrrrserrrsnrrrssrrrsenrrssnrrssnrrrsnerrsrnrrsrerrssnn 97 CAPI TC MOP SOE eige A AEE A E EE A eee 98 Calibry and a cluster of MCP UNITS cccccccccccsssececseccsssseeeecescesssseeeesecesssseeeesecesesseaeeecesseessueeeseeceessaneeseeeestssaateesersesaaaees 99 Calibry and MCP single unit for 1 channel PiPettes sesiis aeaa EERE 100 Galibi ond AP precision DG IONICS S os ic co irises arena E tunes EEEE E 101 COM ond AF CAG TICE DUCOS ak cauae cappogeracuendanne casita EENAA E AA EEEE EAEN ETET 102 caloy CMG AP2OPC DAANGC Sasis naransan EAE EE EEE EE DESE EA EETA EEA DESERTS 103 CDr ONTA A DCO aE AAS T A AATE OAA 104 calibri ond
172. sh ouse Quick print Prints ne document det othe standerd printer denedin Windows Porre creates a PDF fle ofthe document Page Setup You can enlarge or reduce the print output in percentages Adjust to xx normal size or divide the content between a number of pages of your choice Fit to x pages wide The effects of your adjustments are immediately displayed on the screen Sets the margins Paper orientation either portrait or landscape size Paper format Navigation Displays the first page of the document Displays the previous page of the document Displays the next page of the document Displays the last page of the document Cursor Hand Lupe Using the hand symbol you can scroll up and down the current page Using the magnifying glass you can zoom in or out Click on the cursor symbol to return to the normal mouse arrow function Many Pages This option allows you to display several pages at once Select as many pages as you want to display and click with the mouse Note The number of pages that can be displayed at the same time depends on the size of the preview window Reduces the display size of the document select the display size of the document from a list You can set the size as a percentage or resize the document so that one or two whole pages whole Page or two Pages are displayed The document can also be resized in terms of text width or page width Zoomin
173. spective item and then click on Edit This transfers the selected item to the Details window where it can be edited Click on Save to save your definitions The Test button may be used to verify the formula Important The test routine does not verify the plausibility of the formula but simply checks if all used components are properly defined and the formula can thus be evaluated Hint Use the following syntax to enter the radical of n 1 n Example 10 Entry 10 1 2 Advanced Options 79 18 2 Automatic acquisition of environmental data from an external source You may configure Calibry in a way that the environmental data air and water temperature relative humidity and barometric pressure is acquired from an external application Capture Tool supplied with Calibry is such an application however you may use other applica tions as well Please read the information below The Calibry Capture Tool The Capture Tool supplied with Calibry is a sample application that can supply environmental data to Calibry Currently the Calibry Capture Tool supports the Testo 435 635 735 measuring instruments Please proceed as follows if you wish to use the Calibry Capture Tool Install the Capture Tool on your PC see information below Install the Testo measuring instrument Start the Capture Tool The Calibry Capture Tool will automatically recognize the connected measuring instru 74 Calibry capture t
174. t Result Click on the Next button to launch the adjustment Calibry starts the adjustment and asks you to stand by until the procedure is complete The example at left confirms completion of an adjustment with the built in weight of the balance without external test Click on the OK button to terminate the adjustment The adjust ment just completed is added to the list of adjustments Notes f you have selected one of the adjustment modes including an external test Calibry will ask you to put on the external test weight before and or after adjustment and to launch the test from the balance The balance sends the results of the test measurement s to Calibry where they appear in the As Re turned and As Found fields respectively The opposite windows appears if you do not start the adjustment from Calibry but from the balance Tool Used 3rd party Once the adjustment has been completed you may enter the result Pass or Fail manually In addition you may enter the number of the adjustment weight certificate or the number of an external calibration certificate as well as a notice Certificate No Optional Notice Optional 4 6 Managing and adjusting peripheral devices Besides the balances the device list contains auxiliary devices such as barometers hygrometers and thermometers Note When working with the Calibry Capture Tool which automatically transmits
175. t C ater temperature at start of the As Found measurement C umidity at start of the As Found measurement rH Barometric pressure at start of the As Found measurement hPa Z factor for As Found measurement ul mg Evaporation factor for As Found measurement ml cycle Uncertainty of the evaporation factor for As Found measurement ul cycle Air temperature at start of the As Returned measurement C Water temperature at start of the As Returned measurement C Humidity at start of the As Returned measurement rH Barometric pressure at start of the As Returned measurement hPa Z factor for As Returned measurement ul mg Evaporation factor for As Returned measurement ml cycle Uncertainty of the evaporation factor for As Returned measurement ul cycle Air temperature at the end of the As Found measurement C Water temperature at the end of the As Found measurement C Humidity at the end of the As Found measurement rH Barometric pressure at the end of the As Found measurement hPa Air temperature at the end of the As Returned measurement C Water temperature at the end of the As Returned measurement C umidity at the end of the As Returned measurement rH arometric pressure at the end of the As Returned measurement hPa gt m Instrument data Type of balance used
176. t of calibration after As Returned measurements X pipette channel Y volume Overall status of the pipette upon completion of the As Found measurements 1 not required 0 not done 1 failed 2 done passed Overall status of the pipette upon completion of the As Returned measurements 1 not required 0 not done 1 failed 2 done passed AkPipetteStatus Hardware Configuration 9 19 Hardware Configuration The following chapters provide information on the cooperation between Calibry and various METTLER TOLEDO balances You will learn how to connect several balances to a single Calibry workstation and how to set up the application and the instruments Calibry is compatible with the following balance lines AG AT AX MCP SAG XP XS XA Generic 19 1 Connecting several balances to a single Calibry workstation You will need a USB hub for connecting several balances to a single Calibry workstation Connect the hub to the Calibry workstation In addition you will need a RS232C to USB converter for each balance to be connected Connect the USB plug of the converter to the USB hub and the DB9 plug to the RS232C interface of the balance Note This also applies to balances that do not have a RS 232C inter face However in this case you will need additional accessories to connect the balance interface to the DB9 plug o
177. tablishing the connection make sure the computer and all MCP units are switched off Connection Setting up the MCP units 1 First verify the software version of every MCP The version number shows up briefly when switching on the unit The second number should be 1 40 or higher If this is not the case you will have to install the V1 40 or higher program cartridge 11138300 USB hub 11600611 USB to RS232 converter cable 11103691 n c 2 If the display of a particular MCP shows the do Cal message proceed to container calibration as explained in the MCP operating instructions No pipette calibration is possible while the do Cal message is displayed and Calibry will report that the balance is not operational red balance symbol Setting up Calibry Balance into Communication Name Serial number Internal IB Balance line Model Channel tray Location On this computer Door mode Status Mcp Calibration Station 1 1 MCP Menos cc i tstststsi i S j2 tie a e O io Yes Balance info Communication com 9600 Com port number Baud rate Data bits Parity Stop Bits Handshake 8 XonxOff 78435092 Usually Calibry will detect the MCPs automatically otherwise add every MCP as a new balance as shown in the example to the left see chapter 4 The settings marked with a red dot are mandatory while th
178. tailed explanation of the method Calibry suggests a description based on the selected parameters Confirm with OK and the new method is immediately available from the list 7 2 Assign test methods and set calibration time select one or more test methods in the method list which you wish to assign to one or more pipettes and then click the Assign ier a Pipettes button as ot hort exo s O11212 TOAN EEE E T ar Only pipettes which are suitable for calibration with the chosen test methods will be displayed in the list Select the desired pipettes and confirm by clicking OK 1502 Hiten HEREREEE 1502 Ri ones You will then be prompted to establish when selected pipettes Should be calibrated with the selected test methods Defining Test Methods 36 Calibration Reminder Configuration Schedule f None Specific date f Period gt Period Settings Start f Mext date Termination Reference date Di 17 05 2011 7 Last performed calibration date Mi 14 05 2008 No end date 0 End after calibrations C End by Di 5 2011 r Scheduled calibration date ka coca Setting up the date or interval for calibration For calibration with a praticular test method you can define a date and or interval can optionally also be shown on the calibration report for settings see chapter 16 If you do not want to define a calibration date or interva
179. tatoe ie Seis daca E T 3 6 3 OS TIN OCR Si vaca tess E A EEE E EN N A E AA E 3 6 4 Nole OTT OU CR FG ee renererien EEN E AE leanne SAE EEA ARNEE EEEa AAA EEEN aa aan i 3 7 Denning TOST MOU OOS snared T EE OERE ANERE EESAN 32 A DENING ONEWE MEMO eei a ae E E EA E EEE E N oa inl E eyed T A AE 32 7 2 Assign test methods and set calibration tiMe sessnsssssrrrssnnrrrnennrrrenrrrrttkrrrntkkr rr ntk nr nE tEErrEEEEErEEEEEEEEEEEEEEEEEEEEEE EEEren 39 la PAUNO SM NO a en eee E E E A E EE E S E ee eee 3 7 4 THN Te ST US UO epee ices sec ance E E E OE TE 3 La An overview of the methods for which no calibration POINT 1S KNOWN sssssssrrrrsssnnrrrrrssnnnrrrrnsnnrrrrrssrrrriereenrrrrrenerrrrrn 38 Contents 4 8 1 8 2 8 3 9 92 93 9 4 10 10 1 10 2 10 3 11 12 13 13 1 13 2 13 3 13 4 14 15 16 16 1 16 2 16 2 1 16 2 2 16 2 3 16 2 4 16 2 5 16 2 6 16 2 7 16 2 8 16 2 9 16 2 10 17 17 1 17 2 17 3 18 18 1 18 2 18 3 18 4 me SES LIS Esasen E A N ES 39 Monnaiontin me T a E A SAAE 39 Deleting pipettes from ihe TASKS MISH scinertssensenieseiincstciainnetarenaetadpanadaetonndaleio eaan ia Eaa EE NESNA 4 ANd CAAO M cesinta TEE SAE EA 4 Calibrating PIDGIN OS arioiicscsccesecacaccensnnsesacosacunnnscundenascdubannteauseneteanccessdestencuismsiancouiatacsncunseasnncauveruceseassceaseanersceees 42 SANO ME COM OE CN VO sires conten tap ago E eon pte aie eect epee oie gn E ia oer 42 simple calibration of
180. terminate the inspection Note If a fault was found and marked in the list a wrench symbol is displayed in the Correction Status column of the Tasks list to indicate that a repair is necessary chapter 8 If you a fault was detected upon inspection and marked it in the list another window appears where you can mark the measures taken to correct the fault s The list installed at the factory contains a selection of the most common measures Note In the Options Calibration Setup menu you can edit the list of the most common corrective measures or if desired translate them into your own language see chapter 16 Mark the measures taken in the list Click on OK to save the inputs and close the window The next window is identical to the window for a simple calibration chapter 9 2 except that it contains two additional buttons With Physical Inspection and Corrective Action you can if necessary re open the previous windows and edit the list of faults or measures for fault correction The Calibrate button allows you to start the calibration The calibration procedure is identical to that for a simple calibration chapter 9 2 Calibrating Pipettes 50 9 4 Calibrating a multi channel pipette with inspection status check and fault correc tion amp Fy Fy With this calibration method Calibration with inspection and As found data the pipette is first inspected for faults
181. ters a Air temperature 25 C Vater temperature ais le Hurnidity 30 Z Factor 1 0039 lng Pressure S00 hPa Evaporation 0 plicycle Edit Invalidate Pipette Calibrate Cancel Demo Mode 66 y As returned Instructions Hext measurement 200pl Ch 6 4 Status b 2041 100 1 20041 Pipette 414K022 D Rainin Pipet Lite 8ch 20 200 ul 8 channel s Method Custom 8x 2001 3 Vol 4 Meas 20 100 200 20pl 100p 200p1 8 channel s M Current volume Volume Measurements 4 Environmental conditions Pressure 900 hPa 30 Humidity Air temp Evaporation Ba HE Vater temp Paya Z Factor 1 0039 pling 0 plicycle Balance are 8 713168 g Balance status Total progress Channel 1 Ch 2 Ch 3 Ch 4 Ch 5 Ch 6 Ch 7 Ch 8 0 198745 g 0 198745 g 0 198904 g 0 198904 g 0 199064 g 2 01987459 0 198745 g 01987459 0 198904 g 0 199064 g 0 199064 g Tare between readings Accept low values 3 0 198745 g 0 198745 g 0 198745 g 0 198904 g 0 199064 g 0 199064 g 4 0 198745 g 0 198745 g 0 198745 g 0 198904 g 0 199064 g Undo measurement The Demo indication at bottom left in the window tells you that Calibry is running in demo mode and no real measurement values are being determined Now input measurement values by clicking with the mouse on the scroll bar The vertical mark in the middle of the field rep
182. the balance is not operational red balance symbol Setting up Calibry Usually Calibry will detect the MCP automatically otherwise add the MCP as a new bal ance as shown in the example to the left see chapter 4 Balance info Communication oe ro The settings marked with a red dot are mandatory while the other settings may be modi Senanur passe OOOO fied to match your local conditions Internal ID Balance line vo HAN In the Options Configuration Balance MCP balances menu see chapter 16 set the Channel tray f2 Location apn Process adapter parameter to Off In the same menu you may define further settings ae gea a P for the MCP as needed you may even advise Calibry to inform you when the instrument Door mode nasv tsi Satus T is due for adjustment The number of pipette channels to be calibrated is defined when setting up a test method chapter 7 Notes on operation The measured values are transmitted to Calibry when the Start key of the MOP is pressed The entire pipette calibration workflow is controlled by Calibry Xon xOff Hardware Configuration 99 19 3 Calibry and a cluster of MCP units This chapter provides information on how to use Calibry in conjunction with a cluster of MCP Multichannel Pipette Calibration Systems by METTLER TOLEDO All MCPs are equipped with a serial RS232C interface that is to be connected to the Calibry workstation as shown below Before es
183. the calibration actually took place Example You have set the calibration interval as 1 month and the calibration is planned for April 14 You will however only carry it out on April 16 April durch Using Scheduled calibration date the next calibration will be set for the May 14 with the Performed calibration date on May 16 Click on OK to save the date If you have specified a date or an interval the pipette will automatically appear in the Tasks list some time before the next calibration date How long before the calibration date can be specified in the Options Calibration Setup menu see chapter 16 You can find more information on time management with Calibry in chapter 20 Defining Test Methods 37 7 3 Editing a Test Method If required you may edit an existing method Mark the respective method in the list and then click on the Edit button When saving the changed method the prompt shown will ap pear If you answer Yes then the changes will also apply to the Do you want to apply the changes to existing tasks calibrations that have already been defined and which use these a _ i ri Only tasks which haven t been started will be affected by the change methods provided these have not already been started If you Tasks which are already in progress will not be affected choose No then the changes only apply for the calibrations which Nein Abbrechen are defined later Edit Me
184. thod 7 4 Deleting a test method To remove an existing test method from the list mark the method Delete l i F you want to delete in the list and then click on the Delete button Confirm in the prompt that you really want to delete these methods Delete Method lf the method you wish to delete is already assigned to one or more Y This operation will delete aaa At vee method is referenced by a pipette The reference to the pipette will also be deleted pipettes th en the prompt sh own will appear If you an Swer Yes a a then the connection with the relevant pipettes will be broken and q second prompt will appear If you answer the second question with Yes pipettes in the Tasks list that are using the deleted method will immediately be removed from the Tasks list unless at least one stage of the calibration procedure has already been carried out e g the As found status check If however you answer No to the second prompt the pipettes concerned will remain in the Tasks list and the existing calibrations can then be carried out using the parameters of the deleted method 2 Di you sank L Getol lie tks each hann not beer Saind rainn the deleted mathais Tasks viih aro currendly in progress rE net bo doied C Defining Test Methods 38 7 5 An overview of the methods for which no calibration point is known Calibry shows you an overview of all pipettes to which one or mo
185. tion data defined in the test method Please refer to chapter 7 for the respective descriptions 8 1 Information in the Tasks list Calibry Click on the Tasks tab to open the Tasks File Balances oT Options Heli list 4 i RT Most columns of the Tasks list contain pans X om 1 information which you already know test u Gove om method pipette type contact The columns sP Number of tasks displayed 41 es with specific information are explained der here to group by that column Schedule Inspec Pipett Pipette Type Cor Method N eg Ai ve ie Owner Phone be OW 7864767 Rainin Pipet Lite 12ch 20 20 test4 Sam Cat 98765 432 42467892 Rainin Pipet Lite 8ch 20 200 ul test Midt ii Mont ii 000 111 222 9954324 Rainin Pipet Lite Sch 20 200 ul test Midt Mont 000 111 222 T k D D a TEP L TEPIP 8ch 20 200 ul in j Tepip_Calib Mettl Merini 41 44 944 22 11 as u e q e 9954324 Rainin Pipet Lite Sch 20 200 ul Testi Midt Mont 000 111 222 rs DTR777444 DT20 200 ul 150 type A s Calib Miller 01 123 456 Due date for calibration of the pipette 4R444 K Biohit E Pet El 100 5000ul Manufacturer Calib Miler 01 123 456 42467892 Rainin Pipet Lite 8ch 20 200 ul Rainin Pipet R Midt Mont 000 111 222 You specify this date when defining q test 42467892 _ Rainin Pipet Lite Gch 20 200 ul Rainin Pipet R
186. tness of the manufacturer information and the change thereof is beyond METTLER TOLEDO s control METTLER TOLEDO cannot accept any responsibility for the correctness of the information and the correctness of the calibration based on such manufacturer information ISO 8655 specifications The formulae below were used to determine the relative ISO 8655 specifications for the following reasons SO 8655 applies its relative specifications exclusively to the nominal value and standardizes the measured results of the SE amp RE so that the same specification value applies to all selected volumes In Calibry different tolerance sets can be used for calibration manufacturer tolerances or customer specific tolerances The relative SE amp RE results cannot be standardized because different tolerances are possible for every volume selected Appendix 117 In Calibry standardization is carried out in line with ISO 8655 for relative tolerance values Tol absTol 100 2 Vn Vs Zlol relative tolerance value SE or RE absTol absolute tolerance value SE or RE ul or ml Vn Nominal volume ul or ml Vs volume selected ul or ml To obtain the same granularity for the relative specifications as for the absolute specifications the following rules apply Tlol lt gt 2 Decimal places Tol between 1 and 10 gt 1 Decimal place Tol 10 gt 0 Decimal places 20 2 4 Using measurement values and rounding in Cali
187. tory settings for all parameters and also includes a column for individual comments Working with the RFID option 76 17 Working with the RFID option The RFID option allows you to read and write data to RFID chips fitted in pipettes The RFID chip stores data about the pipette the calibrations performed and next calibration dates In order to use RFID the following prerequisites must be fulfilled The RFID option Calibry upgrade must have been purchased from METTLER TOLEDO and the key entered in Calibry under the Help License Manager Option key menu In some instances it may then be necessary to restart Calibry See chapter 2 An RFID reader must be installed and connected to the Calibry workstation Important The reader must be connected and set up before Calibry is started otherwise Calibry will not recognize the device The pipettes must be fitted with an RFID chip whose data structure is compatible with Calibry The Calibry user rights must indicate that the user is authorized to write to pipette RFID chips Users User Levels Rights on RFID menu 17 1 Defining a new pipette with RFID chip scan the pipette using the reader and wait until the data has been read this will usually be indicated by the LEDs on the reader Calibry will detect that it is a new pipette and automatically open the pipette assistant The rest of the process for defining the pipette at aac tus is the same as for conventiona
188. ts sy History Configuration tasks that are required every once in a while are available via various menus located in the menu line above the tabs The menu line offers the following options Opens the print preview where you can format and print the lists displayed Print Ctrl P Calls up the Windows printer dialog in which you can select the printer on which you want current list to be printed Methods Writes the contents of the currently display list into a text file and saves the file in a selectable directory Exit Quits the program Instructions for Using Calibry 17 BALANCES amp DEVICES Management Launches a menu for manually adding or deleting balances and other peripheral instruments ba rometer thermometer and hygrometer to Calibry In addition you may enter adjustment data of these devices It is worthwhile updating the list of executed device adjustments on a regular schedule as this will provide an instant overview of all adjustments performed for a particular device together with the respective date and result Furthermore this menu includes an option to start the internal adjustment of some METTLER TOLEDO balances directly e g MCP series without resorting to the balance s keys or menu For further information please refer to chapter 4 Carries out the same balance check as on application launch see chapter 2 Pipette types Calls up a menu which allows you to add edit o
189. umber of the balance Caution This Serial aR B se53 number must exactly match the serial Internal ID one number stated on the type plate of the Balance line balance Calibry verifies the number the Model Meros serial number must be unique annel tr n i wrn 42 E Internal ID This entry is optional and only relevant if ee laboratory ss ocation Laboratory two or more balances of the same type are connected The Internal ID allows the balances to be uniquely identified Onthis computer Yes E No Door mode Status Specifying Managing and Adjusting Balances and Peripheral Devices 21 Balance line special communication protocols for certain METTLER TOLEDO balances Choose the appropriate balance from the list or select Generic if you are using a balance which is not automatically detected Model Balance type Channel tray Maximum number of pipette channels which is supported by the balance Location Location of the balance On this computer Determines whether the balance is connected locally to the PC on which Calibry is running Yes or to a remote PC No You may work only with balances that are locally connected to your PC also see chapter 4 4 Door mode This setting applies only to balances that have an automatic door function otherwise Not Available will show select Disabled if you do not want Calibry to control the doors in this case the doors will be controlle
190. wer the question with Yes the pipette is deleted along with the associated entries in the Tasks list 6 4 Note on Quick Access GUICK ACCESS Using the Quick Access button in the bottom right of the Pipettes window you are able to gain direct access to many of the functions described in the following chapters In order to open the Quick Access window select the desired pipette in the list and then click on the button alternatively you can just double click on the desired pipette A description of the Quick Access window can be found in chapter 12 Defining Test Methods 32 7 Defining Test Methods A test method determines the calibration procedure for a particular pipette At least one test method must be assigned to a pipette otherwise no calibration can be carried out F Calibry icles Click on the Methods tab to open the File Balances amp Devices Uggugy Options Help menu for defining test methods s a ad 5 0 In the example at left some methods are om Pipettes Methods A Tasks amp Contacts ad Reports zy History alre d dy d efin e d 7 aul Number of methods displayed 1159 1 slumn header here to group by that column Method Name Method Description Range Method Number of Channels b Biozym PreCision 0 5 10 ul SYol Meas OS E f ul 20 pl A test method is made up of the following parameters Biozym PreCision 0 5 10 ul 3Vol 4Meas 105 1 1 pul 10 pl Bio
191. which calibration mode is used for the pipette and which steps were already completed Quick Check Simple Testing of Pipettes Calibration Simple calibration without additional measures Calibration with inspection Calibration with inspection of the pipette for faults and measures for fault correction Calibration with inspection and As found data Calibration with inspection for faults and measures for fault correction see above but with an additional status check As found before the actual calibration The pipette requires repair faults were found during the inspection The colors of the symbols show the status of the procedure Gray step not yet executed Green Step executed and passed Red step executed but not passed Note Information aboutthe selection of the calibration mode is found in chapter 7 Chapter 9 provides information on the running sequence of the individual calibration modes The symbols in the Schedule column show the time related status of a pipette in relation to the due date for calibration The pipette has been added manually to the Tasks list If no calibration date or interval has been specified for this pipette Calibry does no automatic monitoring with regard to calibration In this case the symbol will not change and it is the user s responsibility to monitor the pipette However if either a calibration date or an interval has been specified this symb
192. wing calculations to be performed when configured appropriately see chapter 16 2 Volume of the pipetted water Vo mMxZxY Vie Volume of pipetted water at 20 C m Mass of the pipetted water measured by the balance mg Z Mass to volume conversion factor ul mg 4 Correction factor for thermal expansion of the dispensing apparatus e g pipette Conversion factor Z factor 1 2 ya ged E a P Py B Pa Z Mass to volume conversion factor m kg P Density of the standard weight used to adjust the balance 8000 kg m P Air density kg m p Water density kg m Correction factor for thermal expansion Y 1 q 1 tyq Y Correction factor for thermal expansion of the dispensing apparatus e g pipette CA Expansion coefficient of the dispensing apparatus C i Temperature of the dispensing apparatus C td 20K Water density P Water density kg m t Water temperature C a 999 85308 kg m a 6 32693 10 C kg m a 8 523829 10 C kgm a 6 943248 e 10 C kg m a 3 821216 107 C kg m Appendix 116 Air density p k p kt T ks f a0 P Air density kg m P Air pressure hPa t Air temperature C m 2 3 15 C p Relative humidity k 0 34844 kg m C hPa k 0 00252 kg m k 0 020582 kg m C 20 2 3 Entering or calculating tolerances specifications Only relative
193. zym PreCision 2 20 ul 3Vol 10Meas 20 10 2 2 ul 20l Biozym PreCision 2 20 ul 3Vol 4Meas 20 10 2 9 2pl 20 l Biozym PreCision 5 50 ul 3Vol 10Meas 50 25 5 i ls pl 50 ul Biozym PreCision 5 50 ul 3Vol 4Meas 50 25 5 S pl 50 pl Biozym PreCision 10 100 ul 3Vol 10Meas 1005010 Hi 10yl 100 pl Biozym PreCision 10 100 ul 3Vol 4Meas 100 50 10 10 pl 100 pl Biozym PreCision 20 200 ul 3Vol 10Meas 200 100 20 SR 20 pl 200 pl BiozymPreCision 20 200ul 3 ol 4Meas 200 100 20 l 20 pl 200 pl Biozym PreCision 50 200 ul 3vol 10Meas 200 100 50 RH 50 pl 200 pl Biozym Precision 50 200 ul 3 ol 4Meas 200 100 50 oF 50 pl 200 pl Add Edit Delete Assign Pipettes The calibration mode The volumes to be checked The pipette channels to be checked Thenumberof measurements pervolume The admissible tolerances The calibration data optional peepee ieee ee epee S 7 1 Defining a new test method To define a new test method click on the Add button below the method list Method Editor cay In this window you establish the fundamental characteristics of the new testing method pete Precom Range From the list select the volume range of the pipette s which need to be calibrated using the new testing method Channels 5 ap SQ Class Range 20 jl 200 Range editar If no suitable range is available click on the

Operating Instructions Calibry 5.0 Pipette

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