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YSI MultiLab 4010-1 & 4010P-1 Instruction Manual

1. 49 7 2 6 Calibration data 51 8 Conductivity o Rr LE REA 53 8 1 MESSUNG 5 8 1 1 Measuring the 53 8 1 2 Measuring the temperature 55 8 2 Temperature compensation 55 8 3 Calibration src Ek bene CRETA GRE 56 8 3 1 Why calibrate estate Ae tue se aci RR 56 8 32 1 56 8 3 3 Determining the cell constant calibration in control standard 56 8 3 4 Calibration 57 9 Settings 59 9 1 pH measurement settings 59 9 1 1 Settings for pH 59 9 1 2 Buffer sets for calibration 60 9 1 3 Calibration 62 9 2 measurement 63 4 ba76141e03 03 2014 MultiLab 4010 1 Contents 9 2 1 Settings for ORP measurements 63 9 3 measurement 63 9 3 1 Settings for D O sensors menu for measurement and calibration settings 63 9 3 2 Enter Sensor cap 65 9 3 3
2. ba76141e03 03 2014 Overview MultiLab 4010 1 1 2 MultiLab 4010P 1 meter with integrated printer The integrated printer of the MultiLab 4010P 1 enables to document measure ments according to GLP requirements The information concerning the printer of the MultiLab 4010P 1 is il given in a separate chapter see section 12 PRINTER ONLY MULTILAB 4010P 1 page 83 1 Keypad 2 Display 3 Socket field 4 Printer 5 Control panel of the printer 1 3 Sensors A measuring system ready to measure consists of the MultiLab 4010 1 meter and a suitable sensor Suitable sensors are IDS pH sensors IDS ORP sensors IDS conductivity sensors and IDS D O sensors 1 3 1 IDS sensors IDS sensors support the automatic sensor recognition show only the settings relevant to the specific sensor in the setting menu process signals in the sensor digitally so that precise and interference free measurements are enabled even with long cables facilitate to assign a sensor to a measured parameter with differently colored couplings ba76141e03 03 2014 MultiLab 4010 1 Overview Sensor data from IDS sensors have quick lock couplings with which to fix the sensors to the meter IDS sensors transmit the following sensor data to the meter e SENSOR ID Sensor name Sensor series number e Calibration data Measurement settings The calibration data are updated in the IDS sen
3. EE ERJHYSZES 28 5 1 1 Measuring the pH value 28 5 1 2 Measuring the temperature 29 5 2 pHcalibration 0 02 30 5 21 30 5 2 2 When do you have to calibrate 30 5 2 3 Carrying out automatic calibration AutoCal 30 5 2 4 Carrying out manual calibration ConCal 33 5 25 36 5 2 6 37 5 2 7 Continuous measurement control CMC function 39 5 2 8 QSC function sensor quality control 40 6 ni aU ieu a qa ern 43 5 1 Measuring nasser ln 43 6 1 1 Measuring the ORP 43 6 2 44 7 Dissolved 45 1 1 MBASUNING iuri itch cee i at ele erit ma etn aane dox 45 7 1 1 Measuring ic Ree 45 7 1 2 Measuring the temperature 47 7 2 Calibrationians zoe ua 288 ps 0 pe UC ep ER oy 47 7 2 4 Wig calibrate dot a esrb a ek E RR 47 7 22 When to calibrate 47 7 2 3 Calibration 47 7 24 1 point 48 7 255 2
4. continue Od03h00min 03 04 2013 08 00 1 Adjusted entire data storage duration 2 Max available data storage duration 3 Graphical display of the data storage usage 1 U 180 min 2 1d17h33min 3 Settings You can configure the automatic data storage function with the following set tings Menu item Possible setting Description ID number 1 10000 ID number for the dataset series Interval 15 5 5 105 Storage interval 30 s 1 min 5 min 10 min The lower limit of the storage interval 15 min 30 min can be restricted by the number of free 60 min storage locations The upper limit is restricted by the stor age duration Duration 1 min x min Storage duration Specifies after which time the auto matic data storage should be termi nated The lower limit of the storage duration is restricted by the storage interval The upper limit is restricted by the number of free storage locations 74 ba76141e03 03 2014 MultiLab 4010 1 Data storage Starting the start the automatic data storage function select continue with lt amp gt lt W gt and automatic data confirm with lt MENU ENTER gt The meter switches to the measured value dis storage function play 0d03h00min 03 04 2013 08 00 1 Remaining storage duration 2 Graphical display of the storage duration The active automatic data storage function can be recognized by the progres
5. i 4 00 7 00 10 00 08 00 4 5 4 Example 1 on navigation Setting the language 1 Press the lt On Off gt key The measured value display appears The instrument is in the measuring mode pH i E 14 7 007 25 0 0 2 Using lt MENU ENTER__ gt open the Storage amp config menu The instrument is in the setting mode Storage amp config System Data storage 08 00 3 Select the System submenu with lt A gt lt Y gt The current selection is displayed with a frame 4 Open the System submenu with lt MENU ENTER gt 24 ba76141e03 03 2014 MultiLab 4010 1 Operation System LLL General Interface Clock function Service information Reset 03 04 2013 08 00 Select the General submenu with lt A gt lt Y gt The current selection is displayed with a frame Open the General submenu with lt MENU ENTER gt General L Language English Audio signal Illumination Contrast Shutoff time Temperature unit Stability control 03 04 2013 08 00 Open the setting mode for the Language with lt MENU ENTER gt General LL Language English Audio signal Illumination Contrast Shutoff time Temperature unit Stability control 03 04 2013 08 00 Select the required language with lt A gt lt Y gt Confirm the setting with lt MENU ENTER gt The meter switches to the measurin
6. AutoRead measurement signal The stability has a considerable impact on the reproduc amp HOLD function ibility of measured values The measured parameter flashes on the display as soon as the measured value is outside the stability range when the automatic Stability control is switched off You can start the Stability control manually at any time irrespective of the set ting for automatic Stability control see section 9 5 3 AUTOMATIC STABILITY CON TROL page 69 in the System menu 1 Freeze the measured value with AR The HOLD status indicator is displayed The HOLD function is active ba76141e03 03 2014 43 ORP MultiLab 4010 1 Criteria for a stable measured value You can terminate the Stability control function and the HOLD func il tion with lt AR gt or lt M gt at any time Using MENU ENTER activate the Stability control function manu ally The AR status indicator appears while the measured value is assessed as not stable A progress bar is displayed and the display of the measured parameter flashes The HOLD AR status indicator appears as soon as a stable mea sured value is recognized The progress bar disappears and the display of the measured parameter stops flashing The current measurement data is output to the interface Measurement data meeting the stability control criterion is marked by AR You can prematurely terminate the Stability control function manu il ally with lt
7. Error message Cause Remedy Error Sensor contaminated Clean the sensor Measured temperature value Keep to the temperature range for outside the operating conditions the test sample display of OFL UFL instead of a temperature value Calibrate Change sensor cap Defective sensor Replace sensor 14 3 Conductivity More information and instructions on cleaning and exchange of il sensors are given in the documentation of your sensor Error message The measured value is outside the measuring range OFL UFL Cause Remedy Measured value outside the Use suitable IDS conductivity sensor measuring range Error message Cause Remedy Error Sensor contaminated Clean the sensor and replace it if necessary Calibration solution not suitable Check the calibration solutions 14 4 General information Sensor symbol Cause Remedy flashes Calibration interval expired Recalibrate the measuring system 90 ba76141e03 03 2014 MultiLab 4010 1 What to do if Display Instrument does not react to keystroke You want to know which software version is in the meter or IDS sensor Cause Remedy Batteries almost empty Cause Replace the batteries see section 13 1 MAINTENANCE page 86 Remedy Operating condition undefined or EMC load unallowed Cause Processor reset Press the ENTER and lt On Off gt
8. Buffer solutions too old Use only once Note the shelf life Buffer solutions depleted Change solutions 88 ba76141e03 03 2014 MultiLab 4010 1 What to do if No stable measured value Obviously incorrect measured values Error message OFL UFL Cause Remedy IDS pH sensor pH sensor contaminated Test sample Clean pH sensor pH value not stable Measure with air excluded if neces sary Temperature not stable IDS pH sensor test sample Adjust temperature if necessary Conductivity too low Use suitable IDS pH sensor Temperature too high Use suitable IDS pH sensor Organic liquids Cause Use suitable IDS pH sensor Remedy IDS pH sensor pH sensor unsuitable Use suitable IDS sensor Temperature difference between buffer and test sample too great Adjust temperature of buffer or sam ple solutions Measurement procedure not suitable 14 2 Dissolved oxygen Follow special procedure More information and instructions on cleaning and exchange of il sensors are given in the documentation of your sensor The measured value is outside the measuring range Cause Remedy Measured value outside the measuring range Use a suitable IDS D O sensor ba76141e03 03 2014 89 What to do if MultiLab 4010 1
9. Output to RS232 USB Outputs the calibration data stor age to the interface After the calibration the meter automatically evaluates the current status of the calibration The evaluation appears on the display and in the calibration record Display Calibration record Relative slope S 0 94 1 06 S 0 92 0 94 or i S 1 06 1 08 S 0 90 0 92 or i S 1 08 1 10 Error Error S lt 0 90 or S gt 1 10 Error elimination see section 14 WHAT DO IF page 88 CALIBRATION Ox 03 04 2013 07 43 33 ProOBOD Ser no 12B100016 ProOBOD Cap Relative slope Sensor 0 98 12B100015 52 ba76141e03 03 2014 MultiLab 4010 1 Conductivity Selecting the displayed measured parameter Stability control AutoRead amp HOLD function 8 Conductivity 8 1 Measuring 8 1 4 Measuring the conductivity NOTE When connecting a grounded PC printer measurements cannot be performed in grounded media as the values would be incorrect The USB interface is not galvanically isolated 1 Connect the conductivity sensor to the meter The conductivity measuring window is displayed The measuring cell and cell constant for the connected IDS conductivity sensor are automatically taken over 2 f necessary select the measured parameter x with M 3 Immerse the conductivity sensor in the test sample 25 0 c 1417
10. System Service information Date format Datum Time Settings of time and date For details see section 4 5 5 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 26 Hardware version and software version of the meter are displayed 68 ba76141e03 03 2014 MultiLab 4010 1 Settings Menu item Setting Description System Reset Resets the system settings to the default values For details see section 9 6 2 RESETTING THE SYSTEM SETTINGS page 72 9 5 2 Data storage This menu contains all functions to display edit and erase stored measured values Detailed information on the memory functions of the MultiLab 4010 1 are given in section 10 DATA STORAGE page 73 9 5 3 Automatic Stability control The automatic Stability control AutoRead function continuously checks the stability of the measurement signal The stability has a considerable impact on the reproducibility of measured values You can activate or switch off the automatic Stability control function see section 9 5 SENSOR INDEPENDENT SETTINGS page 68 The measured parameter flashes on the display as soon as the measured value is outside the stability range when the automatic Stability control is switched off 9 5 4 Automatic shutoff function The instrument has an automatic shutoff function in order to save the batteries see section 9 5 1 SYSTEM page 68 The automatic shutoff function swi
11. Tr25 nLF 0 835 1 cm 01 02 2014 08 00 USB output You can switch between the following displays with lt M gt Conductivity uS cm mS cm Resistivity Q cm kQ cm MQ cm e Salinity SaL 2 psu Total dissolved solids TDS mg l g l The multiplier to calculate the total dissolved solids is set to 1 00 in the factory You can adjust this multiplier to meet your requirements in the range 0 40 1 00 The multiplier is set in the menu for the parameter TDS The stability control function AutoRead continually checks the stability of the measurement signal The stability has a considerable impact on the reproduc ibility of measured values The measured parameter flashes on the display as soon as the measured value is outside the stability range when the automatic Stability control is switched off You can start the Stability control manually at any time irrespective of the set ba76141e03 03 2014 53 Conductivity MultiLab 4010 1 Criteria for a stable measured value ting for automatic Stability control see section 9 5 3 AUTOMATIC STABILITY CON TROL page 69 in the System menu 1 Freeze the measured value with AR The HOLD status indicator is displayed The HOLD function is active You can terminate the Stability control function and the HOLD func il tion with lt AR gt or lt M gt at any time 2 Using lt MENUI ENTER3 gt activate the
12. l 92 mg l 760 mmHg 25 1 v 11 1 Comp 03 04 2013 08 00 10 Switch to the measured value display with lt MENU ENTER gt 7 2 6 Calibration data The calibration record is automatically transmitted to the interface after calibrating Displaying the The calibration record of the last calibration is to be found under the menu item calibration record Calibration Calibration record To open it in the measured value display press the lt CAL_ gt key The calibration records of the last 10 calibrations are to be found in the menu Calibration Calibration data storage Display To open the Calibration menu press the MENU ENTER key in the measured value display ba76141e03 03 2014 51 Dissolved oxygen MultiLab 4010 1 Calibration evaluation ProOBOD calibration evaluation Calibration record USB output Menu item Setting function Description Calibration Calibration data stor age Display Displays the calibration records Further options Scroll through the calibration records with lt A gt lt Y gt Output the displayed calibra tion record to the interface with lt F2 gt USB output Output all calibration records to the interface with F2 USB output Quit the display with lt F1 gt Back or lt MENU ENTER gt Switch directly to the mea sured value display with M Calibration Calibration data stor age
13. 01 07 2011 08 00 3 Calibration with the buffers of the QSC Kit is done like a normal three point calibration Follow the user guide Carry out the QSC initial calibration very carefully It determines the reference value for the sensor This reference value cannot be overwritten or reset As soon as the QSC function was enabled it is not possible to return to the sensor evaluation with the sensor symbol 4 Assoonasthe three point calibration has been successfully carried out you can decide whether to accept or discard the calibration as the QSC initial calibration The QSC initial calibration is completed The sensor is calibrated If you want to calibrate with special buffers for your measurements you can subsequently carry out a normal calibration with your buffers The reference values deter mined with the QSC calibration are also used for the evaluation of normal cali brations In the measured value display the QSC scale of the QSC function is always displayed A double arrow on the QSC scale indicates the current sen ba76141e03 03 2014 41 pH value MultiLab 4010 1 Carrying out a QSC control calibration sor evaluation pH 14 7 007 1 25 0 C 01 02 2014 08 00 USB output 1 QSC scale The double arrow on the QSC scale indicates the current sensor evaluation A QSC control calibration can e g be useful if the sensor evaluation noticeably changed after some normal calibra
14. 48 0 5 654 5 408 5 172 4 947 4 730 4 523 49 0 5 565 5 324 5 094 4 872 4 660 4 457 50 0 5 477 5 242 5 016 4 799 4 591 4 392 ba76141e03 03 2014 103 Appendix MultiLab 4010 1 19 2 DO Calibration values Pressure Altitude Calibration value Inches Hg mm Hg kPa mbar Feet Meters Saturation 30 22 767 6 102 3 1023 276 84 101 29 92 760 101 3 1013 0 0 100 29 62 752 4 100 3 1003 278 85 99 29 32 744 8 99 3 993 558 170 98 29 02 737 2 98 3 983 841 256 97 28 72 729 6 97 3 973 1126 343 96 28 43 722 96 3 963 1413 431 95 28 13 714 4 95 2 952 1703 519 94 27 83 706 8 94 2 942 1995 608 93 27 53 699 2 93 2 932 2290 698 92 27 23 691 6 92 2 922 2587 789 91 26 93 684 91 2 912 2887 880 90 26 63 676 4 90 2 902 3190 972 89 26 33 668 8 89 2 892 3496 1066 88 26 03 661 2 88 1 881 3804 1106 87 25 73 653 6 87 2 871 4115 1254 86 25 43 646 86 1 861 4430 1350 85 25 13 638 4 85 1 851 4747 1447 84 24 84 630 8 84 1 841 5067 1544 83 24 54 623 2 83 1 831 5391 1643 82 24 24 615 6 82 1 821 5717 1743 81 23 94 608 0 81 06 811 6047 1843 80 23 64 600 4 80 05 800 6381 1945 79 23 34 592 8 79 03 790 6717 2047 78 23 04 585 2 78 02 780 7058 2151 77 22 74 577 6 77 01 770 7401 2256 76 22 44 570 0 75 99 760 7749 2362 75 22 14 562 4 74 98 749 8100 2469 74 21 84 554 8 73 97 739 8455 2577 73 21 54 547 2 72 95 729 8815 2687 72 21 26 539 6 71 94 720 9178 2797 71 20
15. resolution accuracy 92 15 2 92 16 Firmware update esa RR RR an 94 16 1 Firmware update for the meter MultiLab 4010 1 94 16 2 Firmware Update for IDS Sensors 95 17 Glossary vo ae I BE 96 18 IndBX voces TDi ee 99 19 Appendix nee 102 19 1 Oxygen solubility 102 19 2 DO Calibration values 104 20 1 105 20 1 Ordering amp Technical 105 20 2 Service Information 105 6 ba76141e03 03 2014 MultiLab 4010 1 Overview 1 Overview 1 1 MultiLab 4010 1 meter The compact digital precision meter MultiLab 4010 1 enables you to carry out pH measurements ORP measurements conductivity measurements and dis solved oxygen D O measurements quickly and reliably The MultiLab 4010 1 provides the maximum degree of operating comfort reli ability and measuring certainty for all applications The MultiLab 4010 1 supports you in your work with the following functions Automatic sensor recognition CMC continuous measurement control QSC sensor quality control Electronic access control e e e Data transmission via the USB interface USB B 1 Keypad 2 Display 3 Connectors
16. 011 25 C Merck 1 4 000 7 000 9 000 20 C Merck 2 1 000 6 000 8 000 13 000 20 C Merck 3 4 660 6 880 9 220 20 C Merck 4 2 000 4 000 7 000 10 000 20 C 60 ba76141e03 03 2014 MultiLab 4010 1 Settings No Buffer set pH values at Merck 5 4 010 7 000 10 000 25 C 10 DIN 19267 1 090 4 650 6 790 9 230 25 C 11 Mettler Toledo USA 1 679 4 003 7 002 10 013 25 C 12 Mettler Toledo EU 1 995 4 005 7 002 9 208 25 C 13 Fisher 2 007 4 002 7 004 10 002 25 C 14 Fluka BS 4 006 6 984 8 957 25 C 15 Radiometer 1 678 4 005 7 000 9 180 25 C 16 Baker 4 006 6 991 10 008 25 C 17 Metrohm 3 996 7 003 8 999 25 C 18 Beckman 4 005 7 005 10 013 25 C 19 Hamilton Duracal 4 005 7 002 10 013 25 C 20 21 Precisa Reagecon TEC 3 996 7 003 8 999 2 000 4 010 7 000 10 000 25 25 C C ba76141e03 03 2014 61 Settings MultiLab 4010 1 No Buffer set pH values at 22 Reagecon 20 2 000 20 C 4 000 7 000 10 000 13 000 23 Reagecon 25 2 000 25 C 4 000 7 000 10 000 13 000 24 Riedel de Haen 2 000 20 C 4 000 7 000 10
17. 03 2014 MultiLab 4010 1 Printer only MultiLab 4010P 1 Integrated printer does not print Printer operating paper not being Integrated printer printed prints automatically 12 5 What to do if printer Cause Remedy Printer switched off LED flashing Switch on the printer LED illuminated No power pack connected Connect the power pack USB cable connected Disconnect the USB cable from the meter Function automatic storing at intervals with long intervals is switched on Switch off the function see section 10 2 AUTOMATIC DATA STORAGE AT INTERVALS page 74 No paper available Cause Insert a roll of paper Remedy Paper inserted the wrong way up Cause Turn the roll of paper around and insert it with the other side upwards Remedy The function Automatic storage at intervals or Transmit data automatic at intervals is switched on Switch off the function see section 10 2 AUTOMATIC DATA STORAGE AT INTERVALS page 74 or section 11 4 OPTIONS FOR DATA TRANSMISSION TO A PC page 80 ba76141e03 03 2014 85 Maintenance cleaning disposal MultiLab 4010 1 13 Maintenance cleaning disposal 13 1 Maintenance 13 1 1 General maintenance activities The only maintenance activity required is replacing the batteries See the relevant operating manuals of the IDS sensors for instruc tions on maintenan
18. 3 2 Enter Sensor cap coefficients il 1 Change the digit of the highlighted position with lt A gt lt W gt The values of the coefficients are provided with the sensor cap 2 Goto the next position with lt gt lt gt 3 Confirm with ENTER when a coefficient is completely entered 9 3 3 DO Saturation local Irrespective of the height or air pressure the calibration value is set to 100 DO Saturation local is ideal for EU compliance When DO Saturation local is enabled an L will appear next to D O on the display D O mg L readings are unaffected by the selection of DO Saturation local ba76141e03 03 2014 65 Settings MultiLab 4010 1 Settings Setting menu of 4310 9 4 Cond measurement settings 9 4 1 Settings for IDS conductivity sensors The settings are made in the menu for the measured parameter conductivity To open the settings display the required measured parameter in the mea sured value display and press the MENU ENTER key After completing the settings switch to the measured value display with M The possible settings are individually displayed for each sensor Below the set ting menu is displayed for two IDS sensors 4310 4320 Default settings are printed in bold Menu item Possible Description setting Calibration Cali Displays the calibration record of the bration record last calibration Calibration Cali Displays the last cali
19. 94 532 70 93 709 9545 2909 70 20 64 524 69 92 699 9917 3023 69 20 35 517 68 91 689 10293 3137 68 20 05 509 67 9 679 10673 3371 67 19 75 502 66 89 669 11058 3371 66 104 ba76141e03 03 2014 MultiLab 4010 1 Contact Information 20 Contact Information 20 1 Ordering amp Technical Support Telephone 800 897 4151 937 767 7241 Monday through Friday 8 00 AM to 5 00 PM ET Fax 937 767 1058 Email environmental Q ysi com Mail YSI Incorporated 1725 Brannum Lane Yellow Springs OH 45387 USA Internet www ysi com When placing an order please have the following information available YSI account number if available Name and Phone Number Model number or brief description Billing and shipping address Quantity Purchase Order or Credit Card 20 2 Service Information YSI has authorized service centers throughout the United States and Internationally For the nearest service center information please visit www ysi com and click Support or contact YSI Technical Support directly at 800 897 4151 When returning a product for service include the Product Return form with cleaning certification The form must be completely filled out for an YSI Service Center to accept the instrument for service The Product Return form may be downloaded at www ysi com and clicking on the Support tab ba76141e03 03 2014 105 Contact Information MultiLab 4010 1 106 ba76141e03 03 2
20. International Oceanographic Tables ba76141e03 03 2014 55 Conductivity MultiLab 4010 1 8 3 Calibration 8 3 1 Why calibrate Aging slightly changes the cell constant e g due to coatings As a result an inexact measured value is displayed The original characteristics of the cell can often be restored by cleaning the cell Calibration determines the current value of the cell constant and stores this value in the meter Thus you should calibrate at regular intervals 8 3 2 When to calibrate After connecting a sensor Routinely within the framework of the company quality assurance When the cleaning interval has expired 8 3 3 Determining the cell constant calibration in control standard You can determine the actual cell constant of the IDS conductivity sensor by calibrating with the control standard in the following range 0 450 0 500 cm e g 4310 nominal cell constant 0 475 The cell constant is determined in the control standard 0 01 mol l KCI In the delivery condition the calibrated cell constant of the IDS sensor is set to 0 475 cm conductivity measuring cell 4310 For this calibration procedure the Type setting must be set to cal Proceed as follows to determine the cell constant 1 Connect the conductivity sensor to the meter 2 Inthe measured value display select the conductivity parameter with M 3 Start the calibration with CAL The
21. MENU ENTER at any time If the Stability control func tion is prematurely terminated the current measurement data are output to the interface without the AutoRead info Using lt MENUJ ENTER3 gt start a further measurement with stability con trol or Release the frozen measured value again with lt AR gt or lt M gt The AR status display disappears The display switches back to the previous indication The Stability control function checks whether the measured values are stable within the monitored time interval Measured parame Time interval Stability in the time inter val ORP 15 seconds A Better than 0 3 mV Temperature 15 seconds A Better than 0 5 C The minimum duration until a measured value is assessed as stable is the monitored time interval The actual duration is mostly longer ORP calibration ORP electrodes are not calibrated You can however check ORP electrodes by measuring the ORP of a test solution and comparing the value with the nominal value 44 ba76141e03 03 2014 MultiLab 4010 1 Dissolved oxygen Selecting the measured parameter displayed Salinity correction Air pressure correction DO Saturation local function 7 Dissolved oxygen 7 1 Measuring 7 1 4 Measuring D O 1 Connect the IDS D O sensor to the meter The D O measuring screen is displayed 2 f necessary select the measured parameter with M 3 Check or ca
22. Saturation local 65 9 4 Cond measurement settings 66 9 4 1 Settings for IDS conductivity sensors 66 9 5 Sensor independent 68 9 5 1 DVSIQII 5 attt uud vU A rA bue 68 952 Dalla SIOFBQes RSS ott eu Qus E doses 69 9 5 3 Automatic Stability control 69 9 5 4 A Automatic shutoff function 69 9 5 5 69 9 6 Resale ae Dee aes 70 9 6 1 Resetting the measurement settings 70 9 6 2 Resetting the system 5 72 10 73 10 1 Manual data storage 73 10 2 Automatic data storage at intervals 74 10 3 Measured value data storage 76 10 3 1 Editing the measured value data storage 76 10 3 2 Erasing the measurement data storage 77 10 3 3 Measurement dataset 77 10 3 4 Storage 5 78 11 Transmitting data USB interfaces 79 11 1 Outputting current measurement 79 11 2 Transmitting data 79 11 3 Connecting the PC USB B interface USB Device 79 11 4 O
23. cell constant that was calibrated last is displayed 0 475 3 25 0 c 03 04 2013 08 00 56 ba76141e03 03 2014 MultiLab 4010 1 Conductivity Displaying the calibration record 4 Immerse the conductivity sensor in the control standard solution 0 01 mol l KCI 5 Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes 6 Wait for the end of the measurement with stability control HOLD AR status indicator or take over the calibrated value with lt MENU ENTER gt The calibration record is displayed and output to the interface 7 Switch to the measured value display with lt MENU ENTER gt 8 3 4 Calibration data The calibration record is automatically transmitted to the interface after calibrating The calibration data can be displayed and then output to the interface The calibration record of the last calibration is to be found under the menu item Calibration Calibration record To open itin the measured value display press the lt CAL_ gt key The calibration records of the last 10 calibrations are to be found in the menu Calibration Calibration data storage Display To open the Calibration menu press the MENU ENTER key in the measured value display Menu item Calibration Calibration data storage Display Setting fun
24. current measurement data to the USB B interface with F2 USB output 11 2 Transmitting data to a PC The meter has a USB B interface USB Device e g to connect a PC Via the USB B interface USB Device you can transmit data to a PC or printer and update the meter software 11 3 Connecting the PC USB B interface USB Device Connect the MultiLab 4010 1 to the PC via the USB B interface System requirements of the PC for installation of the USB driver PC with at least one free USB connection and CD ROM drive e Windows 2000 Windows XP Windows Vista or Windows 7 1 Insert the supplied installation CD in the CD drive of your PC 2 Install the driver from the CD Follow the Windows installation instructions as necessary 3 Connect the MultiLab 4010 1 to the PC via the USB B interface The meter is listed as a virtual COM interface among the connections in the Windows instrument manager 4 Setthe same transmission data at the connected instrument PC Baud rate to be selected in the range 1200 19200 e Handshake RTS CTS Set at the PC only Parity none Data bits 8 Stop bits 2 ba76141e03 03 2014 79 Transmitting data USB interfaces MultiLab 4010 1 11 4 Options for data transmission to a PC Via the USB B interface you can transmit data to a PC The following table shows which data are transmitted to the interface in which way Data Control Operation
25. description Current measured val ues of all con nected sensors manual e With lt F2 gt USB output Simultaneously with every manual storage process see section 10 1 MANUAL DATA STORAGE page 73 automatic at intervals e With lt F2__ gt USB output Then you can set the transmission interval e Simultaneously with every auto matic storage process see section 10 2 AUTOMATIC DATA STORAGE AT INTERVALS page 74 Stored mea sured values manual e Displayed dataset with lt F2 gt USB output after calling up from the data storage All datasets with the Output to RS232 USB function see section 10 3 1 EDITING THE MEASURED VALUE DATA STORAGE page 76 Calibration records manual Calibration record with lt F2 gt USB output see section 5 2 6 CALIBRA TION DATA page 37 section 7 2 6 CALIBRATION DATA page 51 section 8 3 4 CALIBRATION DATA page 57 automatic Atthe end of a calibration proce dure il The following rule applies With the exception of the menus shortly pressing the lt F2 gt USB output key generally outputs the display contents to the interface displayed measured values measuring datasets calibration records 11 5 MultiLab Importer With the aid of the MultiLab Importer software you can record and evaluate measuring data with a PC More detailed information can be found in the MultiLab Importer il operat
26. key simultaneously Remedy g a question by the service department Switch on the meter Open the menu ENTER Stor age amp config System Service infor mation The instrument data are displayed or Connect the sensor Press softkey lt F1 gt nfo lt F1 gt More The sensor data are displayed see section 4 1 5 SENSOR INFO page 18 ba76141e03 03 2014 91 Technical data MultiLab 4010 1 15 Technical data 15 1 Measuring ranges resolution accuracy Measuring ranges Parameter Measuring range Accuracy accuracy Air pressure abso 225 825 mm Hg Hg lute Dimensions Weight Mechanical structure Electrical safety Test certificates Ambient conditions Power supply il Available only if aD O sensor is connected Further data are given in the documentation of your sensor 15 2 General data MultiLab 4010 1 Approx 230 x 190 x 80 mm 9 06 x 7 48 x 3 15 inches MultiLab 4010 1 Approx 0 8 kg 1 76 pounds Type of protection IP 43 Protective class cETLus 25 65 C Operation 5 55 C With the power pack connected 5 40 C Admissible relative humidity Yearly mean lt 75 30 days year 95 Other days 85 Batteries 4 x 1 5 V alkali manganese batteries type AA Operational life Approx 150 h Po
27. regarded as correct Often this expression is also used when the measuring system is adjusted at the same time see adjusting ba76141e03 03 2014 97 Glossary MultiLab 4010 1 Measured parameter Measured value Molality Reset Resolution Stability control AutoRead Standard solution Temperature function Test sample The measured parameter is the physical dimension determined by measuring e g pH conductivity or D O concentration The measured value is the special value of a measured parameter to be determined It is given as a combination of the numerical value and unit e g 3 0 5 s 5 2 A 373 15 Molality is the quantity in Mol of a dissolved substance in 1000 g sol vent Restoring the original condition of all settings of a measuring system Smallest difference between two measured values that can be dis played by a meter Function to control the measured value stability The standard solution is a solution where the measured value is known It is used to calibrate a measuring system Name of a mathematical function expressing the temperature behav ior of a test sample a sensor or part of a sensor Designation of the test sample ready to be measured Normally a test sample is made by processing the original sample The test sample and original sample are identical if the test sample was not processed 98 ba76141e03 03 2014 MultiLab 4010 1 Index 18 Ind
28. similar detergents that contain sol vents Remove any splashes immediately 13 3 Packing This meter is sent out in a protective transport packing We recommend Keep the packing material The original packing protects the meter against damage during transport 13 4 Disposal At the end of its operational lifetime the meter must be returned to the disposal or return system statutory in your country If you have any questions please contact your supplier ba76141e03 03 2014 87 What to do if MultiLab 4010 1 14 What to do if 14 1 pH More information and instructions on cleaning and exchange of il sensors are given in the documentation of your sensor Error message Cause OFL UFL Remedy IDS pH sensor Measured value outside the measuring range Use suitable IDS pH sensor Air bubble in front of the junction Remove air bubble Cable broken Exchange IDS pH sensor Gel electrolyte dried out Error message Cause Exchange IDS pH sensor Remedy Error IDS pH sensor The values determined for zero point and slope of the pH sensor are outside the allowed limits Recalibrate pH sensor contaminated Clean IDS pH sensor pH sensor broken Exchange IDS pH sensor Buffer solutions The used buffer solutions do not agree with the set buffer set Set different buffer set or Use different buffer solutions
29. the password Forgotten the password The login is done immediately if no password is required If a il sensor is connected the measured value display appears If a password is required Using lt amp gt lt W gt select the menu item Password and confirm with lt MENU ENTER gt The user specifies the password when he or she first logs in with a user name A valid password consists of 4 digits The user can change the password with the next login Change the digit of the highlighted position with lt gt lt gt Go to the next digit of the password with lt F2 gt P When the password was completely entered confirm with lt MENU ENTER gt The login takes place If a sensor is connected the measured value dis play appears If the administrator has set up the access with password protection Switch the meter on with lt On Off gt The Login dialog appears Using lt A gt lt W gt select the menu item User name and confirm with lt MENU ENTER gt The user name is highlighted Using lt A gt lt V gt select a user name and confirm with lt MENU ENTER gt Using lt A amp gt lt W gt select the menu item Change password and confirm with lt MENU ENTER gt In the Password field enter the old password with lt A gt lt W gt and lt F2 gt gt and confirm it with lt MENU ENTER gt In the New password field enter the new password with lt amp gt lt W gt and lt F2 gt gt
30. update program During the programming process a corresponding message and a progress bar in 96 are displayed The programming process takes up to 15 minutes A terminatory mes sage is displayed after a successful programming process The firm ware update is completed 7 Disconnect the MultiLab 4010 1 from the PC The MultiLab 4010 1 is ready for operation again After switching the meter off and on you can check whether the meter has taken over the new software version see YOU WANT TO KNOW WHICH SOFTWARE VERSION IS IN THE METER OR IDS SENSOR PAGE 91 94 ba76141e03 03 2014 MultiLab 4010 1 Firmware update 16 2 Firmware Update for IDS Sensors With the Firmware Update program and a PC you can update the firmware of an IDS sensor to the newest version You can find available firmware update files for your IDS sensor on the Internet For updating connect the IDS sensor to the MultiLab 4010 1 and the MultiLab 4010 1 to a PC For the update via the USB B interface the following is required a free USB interface virtual COM port on the PC the driver for the USB interface on the enclosed CD ROM the USB cable included in the scope of delivery of the MultiLab 4010 1 1 Install the downloaded firmware update on a PC An update folder is created in the Windows start menu If an update folder already exists for the sensor or sensor type the new data are displayed there 2 Inthe windows start m
31. 000 25 USABlueBook 4 000 25 C 7 000 10 000 Brand names or trade names are trademarks of their respective owners pro tected by law The buffers are selected in the menu pH MENU ENTER Cal ibration Buffer see section 9 1 1 SETTINGS FOR PH MEASURE MENTS page 59 9 1 3 Calibration interval The calibration evaluation is displayed as a sensor symbol After the QSC function has been enabled the sensor symbol is replaced by the QSC scale see section 5 2 8 QSC FUNCTION SENSOR QUALITY CONTROL page 40 After the specified calibration interval has expired the sensor symbol or the QSC scale flashes It is still possible to measure To ensure the high measuring accuracy of the measuring system il calibrate after the calibration interval has expired Setting the calibration interval is set to 7 days in the factory calibration interval You can change the interval 1 999 days 1 Open the menu for measurement settings with lt MENU ENTER gt 2 Inthe Calibration Calibration interval menu set the calibration interval with A W 62 ba76141e03 03 2014 MultiLab 4010 1 Settings 3 Confirm the setting with lt MENU ENTER gt 4 Quit the menu with M 9 2 measurement settings 9 2 1 Settings for ORP measurements The settings are made in the menu for measuring settings of the ORP measure ment To open the settings display the required measured parameter in the measured valu
32. 014 Xylem zilem 1 The tissue in plants that brings water upward from the roots 2 a leading global water technology company We re 12 500 people unified in a common purpose creating innovative solutions to meet our world s water needs Developing new technologies that will improve the way water is used conserved and re used in the future is central to our work We move treat analyze and return water to the environment and we help people use water efficiently in their homes buildings factories and farms In more than 150 countries we have strong long standing relationships with customers who know us for our powerful combination of leading product brands and applications expertise backed by a legacy of innovation For more information on how Xylem can help you go to www xyleminc com porga YSI HHHH 1725 Brannum Lane mmm mm Yellow Springs OH 45387 IEEN Tel 1 937 767 7241 800 765 4974 YS li Fax 1 937 767 1058 Email environmental ysi com Web www ysi com a xylem brand Xylem Inc
33. 049 7 624 7 221 19 0 9 276 8 792 8 333 7 896 7 483 7 090 20 0 9 092 8 621 8 174 7 749 7 346 6 964 21 0 8 915 8 456 8 021 7 607 7 214 6 842 22 0 8 743 8 297 7 873 7 470 7 087 6 723 23 0 8 578 8 143 7 730 7 337 6 963 6 609 24 0 8 418 7 994 7 591 7 208 6 844 6 498 25 0 8 263 7 850 7 457 7 093 6 728 6 390 26 0 8 113 7 711 7 327 6 962 6 615 6 285 27 0 7 968 7 575 7 201 6 845 6 506 6 184 28 0 7 827 7 444 7 079 6 731 6 400 6 085 29 0 7 691 7 317 6 961 6 621 6 297 5 990 30 0 7 559 7 194 6 845 6 513 6 197 5 896 31 0 7 430 7 073 6 733 6 409 6 100 5 806 32 0 7 305 6 957 6 624 6 307 6 005 5 717 102 ba76141e03 03 2014 MultiLab 4010 1 Appendix Temp Chlorinity 0 5 0 ppt 10 0 ppt 15 0 ppt 20 0 ppt 25 0 ppt C Salinity 0 9 0 ppt 18 1 ppt 27 1 ppt 36 1 ppt 45 2 ppt 33 0 7 183 6 843 6 518 6 208 5 912 5 631 34 0 7 065 6 732 6 415 6 111 5 822 5 546 35 0 6 950 6 624 6 314 6 017 5 734 5 464 36 0 6 837 6 519 6 215 5 925 5 648 5 384 37 0 6 727 6 416 6 119 5 835 5 564 5 305 38 0 6 620 6 316 6 025 5 747 5 481 5 228 39 0 6 515 6 217 5 932 5 660 5 400 5 152 40 0 6 412 6 121 5 842 5 576 5 321 5 078 41 0 6 312 6 026 5 753 5 493 5 243 5 005 42 0 6 213 5 934 5 667 5 411 5 167 4 993 43 0 6 116 5 843 5 581 5 331 5 091 4 861 44 0 6 021 5 753 5 497 5 252 5 017 4 793 45 0 5 927 5 665 5 414 5 174 4 944 4 724 46 0 5 835 5 578 5 333 5 097 4 872 4 656 47 0 5 744 5 493 5 252 5 021 4 801 4 589
34. 4 0 9C Voltage 2 3 0 mV 24 0 C Voltage 3 177 0 mV 24 0 Slope 60 2 mV pH Asymmetry 4 0 mV Sensor etc 38 ba76141e03 03 2014 MultiLab 4010 1 pH value 5 2 7 Continuous measurement control CMC function The Continuous Measurement Control CMC function facilitates to evaluate the current measured value instantly and definitely After each successful calibration the scale of the pH measuring range is dis played in the measured value display Here you can very clearly see whether or not the current measured value is in the calibrated part of the measuring range The following information is displayed 1 Currently measured pH value needle 2 Marking lines for all nominal buffer values used with the last valid cali bration 3 Measuring range for which a valid calibration is available Measured values in this range are suitable for documentation 4 Measuring range for which no valid calibration is available shaded Measured values in this range are not suitable for documentation Calibrate the meter with buffers covering this measuring range If the current measured value is outside the calibrated range this area is shaded stronger If a measured value is outside the measuring range pH 0 14 over flow arrows are displayed at the left or right edge of the measuring range The limits of the calibrated range are determined by the buffers used for cali bration Lower l
35. IDS D O sensor into the reference solution When calibrating in water vapor saturated air Cal Put the IDS D O sensor into the calibration vessel with water vapor saturated air As the calibration vessel use a BOD bottle that contains a il small amount of clean water approx 40 ml The sensor must not be immersed in the water Leave the sensor in the calibration bottle long enough 5 to 10 minutes so that the air is water vapor saturated and the sensor can adapt to the ambient temperature 4 Start the calibration with CAL Cal calibration in water vapor saturated air or Comp calibration via Comparison meas according to the Winkler method is displayed The calibration point DO Sat is displayed DO Sat T 92 mg l 760 mmHg 25 1 C Cal 03 04 2013 08 00 5 Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes 48 ba76141e03 03 2014 MultiLab 4010 1 Dissolved oxygen 6 Wait for the AutoRead measurement to be completed audio signal When calibrating in water vapor saturated air Cal The calibration record is displayed and output to the interface When calibrating via comparison measurement Comp Set the concentration value with lt A gt lt W gt and accept it with ENTER The calibration record is displayed and output to the interfac
36. OPERATIONS MANUAL ba76141e03 03 2014 4010P 1 MultiLab 4010 P 1 DIGITAL METER FOR IDS SENSORS PH ORP D O COND a xylem brand MultiLab 4010 1 il For the most recent version of the manual please visit www ysi com Contact YSI 1725 Brannum Lane Yellow Springs OH 45387 USA Tel 41 937 767 7241 800 765 4974 Email environmental Q ysi com Internet www ysi com Copyright 2014 Xylem Inc ba76141e03 03 2014 MultiLab 4010 1 Contents MultiLab 4010 1 Contents 4 OVGIVIEW rue FEES Se ee ee 7 1 1 MultiLab 4010 1 7 1 2 MultiLab 4010P 1 meter with integrated printer 8 1 3 SENSora etos fe cibuste Aunty sth ate Bee Gelade plaka tee eae dus be 8 1 3 1 DS Senso codd ovs ea Bee teur rl 8 1 3 2 Automatic sensor recognition 9 2 ee I PN LL EIE 11 2 1 11 2 1 1 Safety information in the operating manual 11 2 1 2 Safety signs on the 11 2 1 3 Further documents providing safety information 11 22 Safe operation 2 2 llle 12 2 21 12 2 2 2 Requirements for safe operation 12 223 12 3 COMMISSIONING 13 3 4 Scope of deliver
37. Stability control function manu ally The AR status indicator appears while the measured value is assessed as not stable A progress bar is displayed and the display of the measured parameter flashes The HOLD AR status indicator appears as soon as a stable mea sured value is recognized The progress bar disappears and the display of the measured parameter stops flashing The current measurement data is output to the interface Measurement data meeting the stability control criterion is marked by AR You can prematurely terminate the Stability control function manu tion is prematurely terminated the current measurement data are il ally with MENU ENTER at any time If the Stability control func output to the interface without the AutoRead info 3 Using lt MENU ENTER3 gt start a further measurement with stability con trol or Release the frozen measured value again with lt AR gt or lt M gt The AR status display disappears The display switches back to the previous indication The Stability control function checks whether the measured values are stable within the monitored time interval Measured parameter Time interval Stability in the time interval Conductivity x Temperature 10 seconds 15 seconds A x better than 1 0 of measured value A Better than 0 5 C The minimum duration until a measured value is assessed as stable is the mon itored time interval
38. The actual duration is mostly longer 54 ba76141e03 03 2014 MultiLab 4010 1 Conductivity Application tips 8 1 2 Measuring the temperature For reproducible conductivity measurements it is essential to measure the temperature of the test sample IDS sensors measure the temperature with a temperature sensor integrated in the IDS sensor 8 2 Temperature compensation The calculation of the temperature compensation is based on the preset refer ence temperature 20 C or 25 C It appears on the display as 7r20 or Tr25 You can select one of the following temperature compensation methods Nonlinear temperature compensation nLF according to EN 27 888 Linear temperature compensation Lin with adjustable coefficients of 0 000 3 000 K No temperature compensation off The reference temperature and temperature compensation are set in the menu for the parameter conductivity see section 9 4 1 SET TINGS FOR IDS CONDUCTIVITY SENSORS page 66 Select the following temperature compensations given in the table according to the respective test sample Test sample Temperature compensation Display Natural water nLF nLF ground water surface according to EN 27 888 water drinking water Ultrapure water nLF nLF according to EN 27 888 Other aqueous solu Lin Lin tions Set linear temperature coefficient 0 000 10 000 K Salinity seawater Automatic nLF according to IOT Sal nLF
39. and confirm it with lt MENU ENTER gt The password is changed The login takes place If a sensor is connected the measured value dis play appears Contact the administrator ba76141e03 03 2014 21 Operation MultiLab 4010 1 4 5 Navigation 4 5 1 Operating modes Operating mode Description Measuring The measurement data of the connected sensor are shown in the measured value display Calibration The course of a calibration with calibration information functions and settings is displayed Storing in memory The meter stores measuring data automatically or manu ally Transmit ting data The meter transmits measuring data and calibration records to a USB B interface automatically or manually Setting The system menu or a sensor menu with submenus set tings and functions is displayed 4 5 2 Measured value display In the measured value display you can open the menu for calibration and measurement settings with MENU ENTER short keystroke open the Storage amp config system menu with the sensor independent set tings by pressing MENU ENTER long keystroke approx 2 s change the display in the selected measuring screen e g pH gt lt mV by pressing M 4 5 3 Menus and dialogs The menus for settings and dialogs in procedures contain further subelements The selection is made with the lt amp gt lt W gt keys The
40. ayed Thoroughly rinse the sensor with deionized water Immerse the sensor in the next buffer solution Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes Wait for the measurement with stability control to be completed or ter minate the stability control and take over the calibration value with lt MENU ENTER gt The pH value of the buffer solution is displayed Buffer 3 9 958 24 8 C 01 07 2011 08 00 ba76141e03 03 2014 35 pH value MultiLab 4010 1 22 Set the nominal buffer value for the measured temperature with lt A gt lt V gt 23 Accept the calibration value with lt MENU ENTER gt The calibration display for the next buffer appears voltage display 24 f necessary use lt M gt to finish the calibration The calibration record is displayed or Continue calibrating using the next buffer with lt MENU ENTER gt After the fifth buffer has been measured the calibration is automat ically finished Then the calibration record is displayed The calibration line is determined by linear regression 5 2 5 Calibration points Calibration can be performed using one to five buffer solutions in any order single point to five point calibration The meter determines the following values and calculates the calibration line as follows Calibration Determined val
41. ble as long as no initial calibra tion was carried out with the connected IDS sensor QSC Record of first Displays the calibration record of the QSC initial calibration calibration QSC Control calibra Starts the control calibration with QSC buffers tion This menu item is only available if an initial calibration was carried out with the connected IDS sensor Man temperature 25 25 Entry of the manually determined temperature 130 C This menu item is only available if an IDS adapter is con nected ba76141e03 03 2014 59 Settings MultiLab 4010 1 Menu item Possible Description setting PH resolution 0 001 Resolution of the pH display 0 01 0 1 mV resolution 0 1 Resolution of the mV display 1 Reset Resets all sensor settings to the delivery condition see sec tion 9 6 1 RESETTING THE MEASUREMENT SETTINGS page 70 9 1 2 Buffer sets for calibration You can use the buffer sets quoted in the table for an automatic calibration The pH values are valid for the specified temperature values The temperature dependence of the pH values is taken into consideration during the calibration No Buffer set pH values at 1 YSI 4 000 7 000 10 000 25 C ConCal Any Any NIST DIN DIN buffers according to DIN 19266 and NIST Traceable Buffers 1 679 4 006 6 865 9 180 12 454 25 C TEC Technical buffers 2 000 4 010 7 000 10
42. bration of cal points Calibration Cali 1 180 Calibration interval for the IDS D O bration interval 999 d sensor in days The meter reminds you to calibrate regularly by the flashing sensor sym bol in the measuring screen Calibration Com on Enables to adjust the measured value parison meas off with the aid of a comparison measure ment e g Winkler titration For details see section 7 2 CALIBRA TION page 47 Calibration K1 Enter the cap coefficients here after Sensor cap coef be exchanging the sensor cap ficients K5 For details see section 9 3 2 ENTER KC SENSOR CAP COEFFICIENTS page 65 SalinitylSal cor on Manual salt content correction for con rection off centration measurements SalinitylSalinity 0 0 70 0 Salinity or salinity equivalent for the salt content correction This menu item is only available if the manual salt content correction is switched on Resolution 0 1 Set a high or low resolution 1 The setting of the resolution is sepa rately stored for each measured parameter DO Saturation on DO Saturation local is a procedure local off that takes the local air pressure into account for each saturation measure ment For details see section 9 3 3 DO SATURATION LOCAL page 65 Reset Resets all sensor settings to the deliv ery condition see section 9 6 1 RESETTING THE MEASUREMENT SET TINGS page 70 64 ba76141e03 03 2014 MultiLab 4010 1 Settings 9
43. bration records bration data stor max 10 age Display Calibration Outputs the calibration data storage to Calibration data the interface storage Output to RS232 USB Calibration Cali 1 150 Calibration interval for the IDS con bration interval 999 d ductivity sensor in days The meter reminds you to calibrate regularly by the flashing sensor sym bol in the measuring screen Type Measuring cell used cal Measuring cells whose cell constant is determined by calibration in the KCL control standard solution Calibration range 0 450 to 0 500 cm The currently valid cell constant is dis played in the status line man Manually adjustable cell constant in the range 0 450 0 500 cm Cell const man 0 450 Display and setting options for the 0 475 manually adjustable cell constant 0 500 Temp comp TC nLF Procedure for temperature compen Method Lin sation see section 8 2 TEMPERATURE off COMPENSATION page 55 This setting is only available for the measured parameters conductivity x and resistivity p 66 ba76141e03 03 2014 MultiLab 4010 1 Settings Setting menu of 4320 Menu item Possible Description setting Temp 0 000 Coefficient of the linear temperature Linear coeff 2 000 compensation 3 000 K This menu item is only available when the linear temperature comp
44. ccept the calibration value with lt MENU ENTER gt The calibration display for the next buffer appears voltage display If necessary finish the calibration procedure as a single point calibra tion with lt M gt The calibration record is displayed For single point calibration the instrument uses the Nernst slope 59 2 mV pH at 25 C and determines the zero point of the IDS pH sensor Thoroughly rinse the sensor with deionized water Immerse the pH sensor in buffer solution 2 Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes 34 ba76141e03 03 2014 MultiLab 4010 1 pH value Continuing with three to five point calibration 14 15 16 17 18 19 20 21 Wait for the measurement with stability control to be completed or ter minate the stability control and take over the calibration value with lt MENU ENTER gt The pH value of the buffer solution is displayed p H Buffer 2 4 035 24 8 C 01 07 2011 08 00 Set the nominal buffer value for the measured temperature with lt A gt lt V gt Accept the calibration value with lt MENU ENTER gt The calibration display for the next buffer appears voltage display If necessary finish the calibration procedure as a two point calibration with lt M gt The calibration record is displ
45. ce 13 1 2 Replacing the batteries You can operate the meter either with normal batteries or with rechargeable batteries Ni MH In order to charge the batteries an external charging device is required 1 Open the battery compartment 1 on the underside of the meter E o 1 1 Battery compartment CAUTION A Make sure that the poles of the batteries are positioned cor rectly The signs on the batteries must correspond to the signs the battery compartment 2 Place four batteries type Mignon AA in the battery compartment 3 Close the battery compartment 1 4 Set the date and time see section 4 5 5 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 26 86 ba76141e03 03 2014 MultiLab 4010 1 Maintenance cleaning disposal il Dispose of used batteries according to the local regulations of your country End users within the European Union are obligated to return used batteries even ecologically compatible ones to a collection point set up for recycling purposes Batteries are marked with the crossed out waste container symbol Therefore they may not be disposed with the domestic waste 13 2 Cleaning Occasionally wipe the outside of the measuring instrument with a damp lint free cloth Disinfect the housing with isopropanol as required A CAUTION The housing is made of synthetic material ABS Thus avoid contact with acetone or
46. ch data storage process transmits the current dataset to the USB interface 10 1 Manual data storage You can save a measurement dataset to the data storage as follows The data set is at the same time output to the USB interface 1 Press the STO key shortly The menu for manual data storage appears Manual data storage 4 von 500 03 04 2013 07 43 33 pH 7 000 24 8 AR ID number continue 03 04 2013 08 00 2 If necessary change and confirm the ID number 1 10000 with lt A gt lt V gt and lt MENU ENTER gt The dataset is stored The meter switches to the measured value dis play When all data storage locations are occupied it is not possible to continue stor ing Then you can e g transmit the stored data to a PC see section 10 3 1 EDITING THE MEASURED VALUE DATA STORAGE page 76 and subsequently erase the data storage see section 10 3 2 ERASING THE MEASUREMENT DATA STOR AGE page 77 ba76141e03 03 2014 73 Data storage MultiLab 4010 1 10 2 Automatic data storage at intervals The data storage interval Interval determines the time interval between auto matic data storage processes Each data storage process transmits the current dataset to the USB interface Configuring the automatic data storage function 1 Press the STO key The menu for automatic data storage appears Automatic data storage L ID number Interval Duration
47. criterion is marked by AR You can prematurely terminate the Stability control function manu ally with MENU ENTER at any time If the Stability control func tion is prematurely terminated the current measurement data are output to the interface without the AutoRead info 3 Using lt MENU ENTER3 gt start a further measurement with stability con trol or Release the frozen measured value again with lt AR gt or lt M gt The AR status display disappears The display switches back to the previous indication 46 ba76141e03 03 2014 MultiLab 4010 1 Dissolved oxygen Criteria for a stable measured value The Stability control function checks whether the measured values are stable within the monitored time interval Measured parame Time interval Stability in the time interval ter D O concentration 20 seconds A better than 0 03 mg l D O saturation 20 seconds A better than 0 4 Temperature 15 seconds A Better than 0 5 C The minimum duration until a measured value is assessed as stable is the mon itored time interval The actual duration is mostly longer 7 1 2 Measuring the temperature For reproducible D O measurements it is essential to measure the tempera ture of the test sample IDS D O sensors measure the temperature with a temperature sensor inte grated in the IDS sensor 7T 2 Calibration 7 2 1 Why calibrate D O sensors age This changes the zero point a
48. ction Description Displays the calibration records Further options Scroll through the calibration records with lt A gt lt Y gt Output the displayed calibration record to the interface with lt F2 gt USB output Output all calibration records to the interface with F2 USB out put Quit the display with lt F1 gt Back or lt MENU ENTER gt Switch directly to the measured value display with M ba76141e03 03 2014 57 Conductivity MultiLab 4010 1 Menu item Setting Description function Calibration 1 Outputs the calibration data storage Calibration data to the interface storage Output to RS232 USB Calibration After calibration the meter automatically evaluates the current status of the cal evaluation ibration The evaluation appears on the display and the calibration record Calibration record USB output Error elimination see section 14 WHAT TO DO IF page 88 Display Calibration record Cell constant cm Within the range i 0 450 0 500 Error Error Outside the range 0 450 0 500 cm CALIBRATION Cond 03 04 2013 07 43 33 4310 Ser no 09250033 Sensor Cell constant 0 476 1 cm 25 0 C 58 ba76141e03 03 2014 MultiLab 4010 1 Settings Settings 9 Settings 9 1 9 1 1 pH measurement settings Settings for pH measurements The settings are made in t
49. current selection is dis played with a frame Submenus The name of the submenu is displayed at the upper edge of the frame Sub menus are opened by confirming with lt MENU ENTER gt Example 22 ba76141e03 03 2014 MultiLab 4010 1 Operation lSystem L General Interface Clock function Service information Reset 08 00 Settings Settings are indicated by a colon The current setting is displayed on the right hand side The setting mode is opened with lt MENU ENTER gt Subse quently the setting can be changed with A W and lt MENU ENTER gt Example General LLL Language English Audio signal Illumination Contrast Shutoff time Temperature unit Stability control 08 00 Functions Functions are designated by the name of the function They are immediately carried out by confirming with lt MENU ENTER gt Example Display the Cal ibration record function pH L Calibration record Calibration data storage Buffer Single point calibration Calibration interval Unit for slope i 4 00 7 00 10 00 03 04 2013 08 00 Messages Information is marked by the i symbol It cannot be selected Example ba76141e03 03 2014 23 Operation MultiLab 4010 1 L Calibration record Calibration data storage Buffer Single point calibration Calibration interval Unit for slope
50. d confirm the setting with A W and lt MENU ENTER gt The minutes are highlighted 5 Change and confirm the setting with lt amp gt lt W gt and lt MENU ENTER gt The seconds are highlighted 26 ba76141e03 03 2014 MultiLab 4010 1 Operation Change and confirm the setting with lt amp gt lt W gt and lt MENU ENTER gt The time is set If necessary set the Date and Date format The setting is made similarly to that of the time To make further settings switch to the next higher menu level with lt F1 gt Back or Switch to the measured value display with lt M gt The instrument is in the measuring mode ba76141e03 03 2014 27 pH value MultiLab 4010 1 Stability control AutoRead amp HOLD function 5 pH value 5 1 Measuring 5 1 4 Measuring the pH value NOTE When connecting a grounded PC printer measurements cannot be performed in grounded media as the values would be incorrect The USB interface is not galvanically isolated 1 Connect the IDS pH sensor to the meter The pH measuring window is displayed 2 f necessary select the measured parameter with M 3 Adjust the temperature of the solutions and measure the current tem perature if the measurement is made without a temperature sensor 4 fnecessary calibrate or check the IDS pH sensor 5 Immerse the IDS pH sensor in the test sample pH TS 14 7 007 25 0 The stabi
51. e DO Adjust l 92 mg l 760 mmHg 25 1 v 11 1 Comp 03 04 2013 08 00 Switch to the measured value display with lt MENU ENTER gt 7 2 5 2 point calibration Calibration in water vapor saturated air Ca and calibration via Comparison meas according to the Winkler method Comp are described jointly here 1 Connect the IDS D O sensor to the meter 2 Check the selected calibration type and selected number of calibration points in the sensor setting menu and if necessary change them 3 Place the IDS D O sensor in a solution that does not contain any dis solved oxygen A solution not containing any dissolved oxygen can be prepared by dissolving approx 8 to 10 g sodium sulfite Na5SO3 in 500 ml tap water Carefully mix the solution It may take up to 60 minutes until the solution is free of oxygen 4 Startthe calibration with CAL Cal calibration in water vapor saturated air or Comp calibration via Comparison meas according to the Winkler method is displayed The calibration point 1 096 is displayed ba76141e03 03 2014 49 Dissolved oxygen MultiLab 4010 1 Oo 0 09 760 mmHg 25 1 C Cal 03 04 2013 08 00 5 Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes 6 Wait for the AutoRead measurement to b
52. e amp config menu press the MENU ENTER key in the measured value display After completing the settings switch to the measured value display with M Default settings are printed in bold Menu item Setting Description System General Language Deutsch Selects the menu language English more System General Audio signal on Switches on off the beep on keystroke off System General Illumination Auto Switches the display illumination on off on off System General Contrast 0 50 100 Changes the display contrast System General Shutoff time 10 min Ih 24h Adjusts the shutoff time System General Temperature C Temperature unit unit F degrees Celsius or degrees Fahrenheit All temperature values are displayed with the selected unit System General Stability con on Switches on or off the automatic stability trol off control during measurement see sec tion 9 5 3 AUTOMATIC STABILITY CON TROL page 69 System Interface Baud rate 1200 2400 4800 Baud rate of the USB Device interface separator System Interface Output header Comma xx x 9600 19200 System Interface ASCII Output format for data transmission Output format CSV For details see section 11 TRANSMIT TING DATA USB INTERFACES page 79 For Output format CSV e System Interface Decimal Dot xx x Decimal separator Output of a header System Clock function
53. e completed audio signal The display for the second calibration point is displayed DO Sat 0 00 s 760 mmHg 25 1 C Cal 03 04 2013 08 00 7 Putthe IDS D O sensor into the calibration medium When calibrating via comparison measurement Comp Put the IDS D O sensor into the reference solution When calibrating in water vapor saturated air Cal Put the IDS D O sensor into the calibration vessel with water vapor saturated air As the calibration vessel use a BOD bottle that contains a il small amount of clean water approx 40 ml The sensor must not be immersed in the water Leave the sensor in the calibration bottle long enough 5 to 10 minutes so that the air is water vapor saturated and the sensor can adapt to the ambient temperature 8 Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes 50 ba76141e03 03 2014 MultiLab 4010 1 Dissolved oxygen 9 Wait for the AutoRead measurement to be completed audio signal When calibrating in water vapor saturated air Cal The calibration record is displayed and output to the interface When calibrating via comparison measurement Comp Set the concentration value with lt A gt lt W gt and accept it with ENTER The calibration record is displayed and output to the interface DO Adjust
54. e display and press the MENU ENTER key After completing the settings switch to the measured value display with lt M gt Default settings are printed in bold Menu item Possible setting Description mV resolution 0 1 Resolution of the mV display 1 Reset Resets all sensor settings to the delivery condition see section 9 6 1 RESETTING THE MEASURE MENT SETTINGS page 70 9 3 D O measurement settings 9 3 1 Settings for D O sensors menu for measurement and calibration settings Settings The settings are available in the menu for measurement and calibration set tings To open the settings display the required measured parameter in the measured value display and press the lt MENU ENTER gt key After completing the settings switch to the measured value display with lt M gt Default settings are printed in bold Menu item Possible Description setting Calibration Cali Displays the calibration record of the bration record last calibration Calibration Cali Displays the last calibration records bration data stor max 10 age Display Calibration Outputs the calibration data storage to Calibration data the interface storage Output to RS232 USB 76141 03 03 2014 63 Settings MultiLab 4010 1 Menu item Possible Description setting Calibration 1 1 point calibration Calibration data 2 or storage Number 2 point cali
55. e required measured parameter in the measured value display and press the lt MENU ENTER key 70 ba76141e03 03 2014 MultiLab 4010 1 Settings ORP Dissolved oxygen Conductivity The following settings for ORP measurements are reset to the default settings with the Reset function Setting Default settings mV resolution 0 1 Man temperature 25 C The sensor settings are reset under the Reset menu item in the menu for cali bration and measurement settings To open the settings display the required measured parameter in the measured value display and press the MENU ENTER key The following settings for D O measurements are reset to the default settings with the Reset function Setting Default settings Calibration interval 180 d Measured parameter D O concentration mg l Salinity value 0 0 Salinity function off Resolution 0 1 DO Saturation local off The sensor settings are reset under the Reset menu item in the menu for cali bration and measurement settings To open the settings display the required measured parameter in the measured value display and press the MENU ENTER key The following settings for conductivity measurements are reset to the default settings with the Reset function Setting Default settings Calibration interval 150 d Measured parameter x Cell constant c Depending on the connected mea suring ce
56. e the stability control and take over the calibration value with lt MENU ENTER gt The calibration display for the next buffer appears voltage display If necessary finish the calibration procedure as a two point calibration with lt M gt The calibration record is displayed Thoroughly rinse the sensor with deionized water Immerse the sensor in the next buffer solution Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes pH Buffer 4 00 180 0 24 8 AutoCal CHE 01 07 2011 08 00 Wait for the measurement with stability control to be completed or ter minate the stability control and take over the calibration value with lt MENU ENTER gt The calibration display for the next buffer appears voltage display If necessary use M to finish the calibration The calibration record is displayed or Switch to calibration with the next buffer with lt MENU ENTER gt 32 ba76141e03 03 2014 MultiLab 4010 1 pH value Calibration is automatically completed after the last buffer of a buf il fer set has been measured Then the calibration record is dis played The calibration line is determined by linear regression 5 2 4 Carrying out manual calibration ConCal Make sure that in the sensor menu Buffer menu the ConCal buffer s
57. e03 03 2014 MultiLab 4010 1 Index ba76141e03 03 2014 101 Appendix MultiLab 4010 1 19 Appendix 19 1 Oxygen solubility table Solubility of oxygen in mg L in water exposed to water saturated air at 760 mm Hg pressure Salinity Measure of quantity of dissolved salts in water Chlorinity Measure of chloride content by mass of water S 0 00 1 80655 x Chlorinity 0 00 Temp Chlorinity 0 5 0 ppt 10 0 ppt 15 0 ppt 20 0 ppt 25 0 ppt C Salinity 0 9 0 ppt 18 1 ppt 27 1 ppt 36 1 ppt 45 2 ppt 0 0 14 621 13 728 12 888 12 097 11 355 10 657 1 0 14 216 13 356 12 545 11 783 11 066 10 392 2 0 13 829 13 000 12 218 11 483 10 790 10 139 3 0 13 460 12 660 11 906 11 195 10 526 9 897 4 0 13 107 12 335 11 607 10 920 10 273 9 664 5 0 12 770 12 024 11 320 10 656 10 031 9 441 6 0 12 447 11 727 11 046 10 404 9 799 9 228 7 0 12 139 11 442 10 783 10 162 9 576 9 023 8 0 11 843 11 169 10 531 9 930 9 362 8 826 9 0 11 559 10 907 10 290 9 707 9 156 8 636 10 0 11 288 10 656 10 058 9 493 8 959 8 454 11 0 10 027 10 415 9 835 9 287 8 769 8 279 12 0 10 777 10 183 9 621 9 089 8 586 8 111 13 0 10 537 9 961 9 416 8 899 8 411 7 949 14 0 10 306 9 747 9 218 8 716 8 242 7 792 15 0 10 084 9 541 9 027 8 540 8 079 7 642 16 0 9 870 9 344 8 844 8 370 7 922 7 496 17 0 9 665 9 153 8 667 8 207 7 770 7 356 18 0 9 467 8 969 8 497 8
58. enance accessories such as buffer solutions electrolyte solutions etc ba76141e03 03 2014 11 Safety MultiLab 4010 1 2 2 Safe operation 2 2 1 Authorized use The authorized use of the meter consists exclusively of the measurement of the pH ORP conductivity and dissolved oxygen in a laboratory environment Only the operation and running of the meter according to the instructions and technical specifications given in this operating manual is authorized see section 15 TECHNICAL DATA page 92 Any other use is considered unauthorized 2 2 0 Requirements for safe operation Note the following points for safe operation The meter may only be operated according to the authorized use specified above The meter may only be supplied with power by the energy sources mentioned in this operating manual The meter may only be operated under the environmental conditions mentioned in this operating manual The meter may only be opened if this is explicitly described in this operating manual example Inserting the batteries 2 2 3 Unauthorized use The meter must not be put into operation if itis visibly damaged e g after being transported e it was stored under adverse conditions for a lengthy period of time storing conditions see section 15 TECHNICAL DATA page 92 12 ba76141e03 03 2014 MultiLab 4010 1 Commissioning 3 Commissioning 1 Scope of delivery Meter MultiLab 4010 1 Mu
59. ensation is set Temp comp TC 20 C Reference temperature Reference temp 25 C This setting is only available for the measured parameters conductivity x and resistivity p Multiplier for TDS 0 40 Multiplier for TDS value 1 00 Reset Resets all sensor settings to the deliv ery condition see section 9 6 1 RESETTING THE MEASUREMENT SET TINGS page 70 Menu item Possible Description setting Cell constant 0 090 Display and setting options for the 0 100 cell constant 0 110 cm Temp comp TC nLF Procedure for temperature compen Method Lin sation see section 8 2 TEMPERA off TURE COMPENSATION page 55 This setting is only available for the measured parameters conductivity x and resistivity p Temp comp TC 0 000 Coefficient of the linear temperature Linear coeff 2 000 compensation 3 000 K This menu item is only available when the linear temperature com pensation is set Temp comp TC 20 C Reference temperature Reference temp 25 C This setting is only available for the measured parameters conductivity x and resistivity p Multiplier for TDS 0 40 1 00 Multiplier for TDS value Reset Resets all sensor settings to the delivery condition see section 9 6 1 RESETTING THE MEASUREMENT SET TINGS page 70 ba76141e03 03 2014 67 Settings MultiLab 4010 1 9 5 Sensor independent settings 9 5 1 System To open the Storag
60. ent 2 Place four batteries type Mignon AA in the battery compartment 3 Close the battery compartment 1 4 Setthe date and time see section 4 5 5 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 26 14 ba76141e03 03 2014 MultiLab 4010 1 Commissioning 3 3 2 Connecting the power pack CAUTION A The line voltage at the operating site must lie within the input voltage range of the original power pack see section 15 2 GENERAL DATA page 92 CAUTION A Use original power packs only see section 15 2 GENERAL DATA page 92 1 Connect the plug of the power pack to the socket for the power pack on the MultiLab 4010 1 2 Connect the original power pack to an easily accessible power outlet 3 3 3 Mounting the stand The stand base can be mounted at the right side of the meter ba76141e03 03 2014 15 Operation MultiLab 4010 1 o 8e Al C ENTER 4 Operation 4 1 General operating principles 4 1 1 Keypad In this operating manual keys are indicated by brackets lt gt The key symbol e g MENU ENTER generally indicates a short keystroke press and release in this operating manual A long keystroke press and hold for approx 2 sec is indicated by the underscore behind the key symbol e g lt MENU ENTER_ gt F1 Softkeys providing situation dependent functions e g F1 lt F1
61. enu open the update folder and start the firm ware update program for the IDS sensor 3 Connect the IDS sensor to the MultiLab 4010 1 meter 4 Using the USB interface cable connect the MultiLab 4010 1 to a USB interface virtual COM port of the PC 5 Switch on the MultiLab 4010 1 6 In the firmware update program start the update process with OK 7 Follow the instructions of the firmware update program During the programming process a corresponding message and a progress bar in 96 are displayed The programming process takes up to 5 minutes A terminatory mes sage is displayed after a successful programming process The firm ware update is completed 8 Disconnect the MultiLab 4010 1 from the PC Meter and sensor are ready for operation again After switching the meter off and on you can check whether the sensor has taken over the new software version see YOU WANT TO KNOW WHICH SOFTWARE VERSION IS IN THE METER OR IDS SENSOR PAGE 91 ba76141e03 03 2014 95 Glossary MultiLab 4010 1 17 Glossary pH ORP Asymmetry see zero point Electromotive force of an electrode Junction ORP voltage U pH value Potentiometry The electromotive force U of the combination electrode is the measur able electromotive force of an electrode in a solution It equals the sum of all the galvanic voltages of the combination electrode Its dependency on the pH results in the electrode function which is char acteri
62. erference in which case the user will be required to correct the interference at his own expense Changes or modifications not expressly approved by the manufacturer could void the user s authority to operate the equipment ba76141e03 03 2014 93 Firmware update MultiLab 4010 1 16 Firmware update 16 1 Firmware update for the meter MultiLab 4010 1 You can find available firmware update files for your meter on the Internet With the Firmware Update program and a PC you can update the firmware of the MultiLab 4010 1 to the newest version For the update you have to connect the meter to a PC For the update via the USB B interface the following is required a ree USB interface virtual COM port on the PC the driver for the USB interface on the enclosed CD ROM the USB cable included in the scope of delivery of the MultiLab 4010 1 1 Install the downloaded firmware update on a PC An update folder is created in the Windows start menu If an update folder already exists for the meter or meter type the new data are displayed there 2 Inthe windows start menu open the update folder and start the firm ware update program for the meter 3 Using the USB interface cable connect the MultiLab 4010 1 to a USB interface virtual COM port of the PC 4 Switch on the MultiLab 4010 1 5 In the firmware update program start the update process with OK 6 Follow the instructions of the firmware
63. ero point and slope when using QSC buffer solu slope when using commercial buffer tions sets Additional QSC calibration required No additional calibration required with special QSC buffer set The QSC function is enabled by once carrying out an additional three point cali bration with special QSC buffer solutions It covers the measuring range of the sensor pH 2 to pH 11 The QSC initial calibration determines the actual condi tion of the sensor and stores it as a reference in the sensor To meet the high requirements of a QSC initial calibration the QSC initial cali bration should optimally be carried out with the initial commissioning of the sensor 40 ba76141e03 03 2014 MultiLab 4010 1 pH value Carry out the normal calibrations for your special measuring range with your usual standard solutions as previously done As soon as the QSC function was enabled for an IDS sensor it is not possible to return to the sensor evaluation with the sensor symbol for this sensor Carrying out a QSC sae Open the menu for measurement settings with lt MENU ENTER gt initial calibration 2 Inthe QSC menu select First calibration with A W The calibration display appears AutoCal QSC Kit is displayed as the buffer Exclusively use the QSC Kit for the QSC calibration If you use other buffers you will have no valid QSC calibration pH Buffer 180 0 24 8 C AutoCal OSC Kit
64. et is correctly selected see section 9 1 1 SETTINGS FOR PH MEASUREMENTS page Use any one to five buffer solutions in ascending or descending order If single point calibration was set in the menu the calibration proce tion 1 and the calibration record is displayed il dure is automatically finished with the measurement of buffer solu Connect the pH sensor to the meter The pH measuring window is displayed Keep the buffer solutions ready Start the calibration with lt CAL gt The calibration display for the first buffer appears voltage display Buffer 1 0 0 24 8 01 07 2011 08 00 Thoroughly rinse the sensor with deionized water Immerse the pH sensor in buffer solution 1 Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes ba76141e03 03 2014 33 pH value MultiLab 4010 1 10 Continuing with two point calibration 12 13 Buffer 7 000 AR CEA 01 07 2011 08 00 Wait for the measurement with stability control to be completed or ter minate the stability control and take over the calibration value with lt MENU ENTER gt The pH value of the buffer solution is displayed Buffer 1 7 000 24 8 C DH 01 07 2011 08 00 Set the nominal buffer value for the measured temperature with lt A gt lt V gt A
65. ex A K Air calibration beaker 47 KEYS rrr 16 Automatic switch off function 69 AutoR amp ead codices ce Ae nts 46 53 M ORP eee 43 Measured value display 22 pH sese n 28 Measurement accuracy 62 Measurement data storage B NINE ERREGER 76 Battery compartment 14 86 PASC uy eis PLUIE teda 76 Storage locations 78 C Measurement dataset 7T Calibration Measuring Conductivity 56 53 Hat sity e Mg 30 44 2 momo om om mon o 3 3 3 3 c c3 3 5 5 3 5 3 3 1 45 Calibration evaluation ORP moo mon ono om om om m m m s 3 s o o o3 5 3 n n s on on n 43 Conductivity 58 pH see nne 28 sr ACD DNO DEREN 52 Menu for calibration and measurement settings DEI see e n ee NONO P 38 66 Calibration interval O2 momo mom m 63 Conductivity 66 59 64 Menus navigation 22 ee DR dan 62 Messages 23 Calibration points MNT 36 P calibration records 57 pH buffer sets 60 Gell constant 56 Printer only Multi 9310P 83 Comparison measureme
66. g mode The selected language is active ba76141e03 03 2014 25 Operation MultiLab 4010 1 Setting the date time and date format 4 5 5 Example 2 on navigation Setting the date and time The meter has a clock with a date function The date and time are indicated in the status line of the measured value display When storing measured values and calibrating the current date and time are automatically stored as well The correct setting of the date and time and date format is important for the fol lowing functions and displays Current date and time e Calibration date e Identification of stored measured values Therefore check the time at regular intervals After a fall of the supply voltage empty batteries the date and time are reset The date format can be switched from the display of day month year dd mm yy to the display of month day year mm dd yy or mm dd yy 1 In the measured value display Using lt MENU ENTER_ gt open the Storage amp config menu The instrument is in the setting mode 2 Select and confirm the System Clock function menu with lt A gt lt W gt and lt MENU ENTER gt The setting menu for the date and time opens up Clock function Date format dd mm yy Date 03 04 2013 Time 14 53 40 03 04 2013 08 00 3 Select and confirm the Time menu with A W lt MENU ENTER gt The hours are highlighted 4 Change an
67. gt Info View information on a sensor F2 F2 gt lt On Off gt Switches the meter on or off M Selects the measured parameter Quits the settings CAL Calls up the calibration procedure CAL gt Displays the calibration data STO Saves a measured value manually STO gt Opens the menu for the automatic save function lt RCL gt Displays the manually stored measured values RCL gt Displays the automatically stored measured values Menu control navigation lt A gt lt V gt Increments decrements values A gt lt V_ gt Increments decrements values continuously lt MENU ENTER gt Opens the menu for measurement settings confirms lt MENU ENTER_ gt entries Opens the menu for system settings lt AR gt Freezes the measured value HOLD function Switches the AutoRead measurement on or off 16 ba76141e03 03 2014 MultiLab 4010 1 Operation 4 1 2 Display Example pH 3 4 2 5 6 1 7 1 Status information sensor 2 Measured value 3 Measured parameter 4 Continuous measurement control CMC function 5 Sensor symbol calibration evaluation calibration interval 6 Measured temperature with unit 7 Status information meter 8 Softkeys and date time 4 1 3 Status information meter AR Stability control AutoRead is active HOLD Measured value is frozen lt AR gt key Batteries are al
68. he menu for calibration and measurement settings of the pH ORP measurement To open the settings display the required mea sured parameter in the measured value display and press the lt MENU ENTER key After completing the settings switch to the measured value dis play with M Default settings are printed in bold Menu item Possible Description setting Calibration Calibra Displays the calibration record of the last calibration tion record Calibration Calibra Displays the last calibration records max 10 tion data storage Dis play Calibration 1 Outputs the calibration data storage to the interface Calibration data stor age Output to RS232 USB Calibration Buffer YSI Buffer sets to be used for pH calibration ConCal More buffers and details see section 9 1 2 BUFFER SETS FOR NIST DIN CALIBRATION page 60 and section 5 2 PH CALIBRATION page 30 Calibration Single yes Quick calibration with 1 buffer point calibration no Calibration Calibra Toi Calibration interval for the IDS pH sensor in days tion interval 999 d The meter reminds you to calibrate regularly by the flashing sensor symbol in the measuring screen Calibration Unit for mV pH Unit of the slope slope The display refers to the Nernst slope of 59 2 mV pH 100 x determined slope Nernst slope QSC First calibration Starts the initial calibration with QSC buffers This menu item is only availa
69. imit Buffer with lowest pH value 2 pH units Upper limit Buffer with highest pH value 2 pH units ba76141e03 03 2014 39 pH value MultiLab 4010 1 General information on the QSC function Sensor evaluation with without QSC function QSC calibration 5 2 8 QSC function sensor quality control The QSC function Quality Sensor Control is a new sensor evaluation for digital IDS sensors It evaluates the condition of an IDS pH sensor individually and with a very fine grading The QSC scale shows the current sensor evaluation with an indicator on the display pH o8 Su 7 007 25 0 C 01 02 2014 08 00 USB output 1 QSC scale The double arrow on the QSC scale indicates the current sensor evaluation In the USB output the sensor evaluation is given as a percentage 1 100 The finely graded sensor evaluation of the QSC function promptly calls your attention to changes of the sensor Thus you can do what is necessary to restore the optimum measuring quality e g clean calibrate or replace the sensor With QSC function Without QSC function sensor sym bol Very fine grading of the sensor eval Rough grading of the sensor evalua uation 100 grades tion 4 grades The reference value is individually A theoretical reference value is used determined for each sensor during for all sensors the QSC initial calibration Low tolerances for zero point and Greater tolerances for z
70. ing manual ba76141e03 03 2014 MultiLab 4010 1 Transmitting data USB interfaces 11 6 BOD Analyst Pro With the aid of the BOD Analyst Pro software you can administrate BOD measurement on the PC and automatically calculate the measured values More detailed information can be found in the BOD Analyst Pro il operating manual ba76141e03 03 2014 81 Transmitting data USB interfaces MultiLab 4010 1 82 ba76141e03 03 2014 MultiLab 4010 1 Printer only MultiLab 4010P 1 12 Printer only MultiLab 4010P 1 N oO KS lt 1 Operating LED I lluminated Printer is switched on Flashing Printer is switched off 2 Control panel with the keys lt ON FEED gt and lt OFF gt 3 Lever to open the paper compartment 4 Lid of the paper compartment 12 1 Commissioning switching the printer on or off Switching on the 1 Connect the power pack to the MultiLab 4010P 1 printer The LED lights up green The printer is ready for operation or If the printer was switched off LED flashing Switch on the printer with OFF The LED lights up green The printer is ready for operation If there is a USB connection such as to a PC the data are output only to the PC Switching off the 1 Switch off the printer with OFF printer The LED flashes The printer is switched off ba76141e03 03 2014 83 Printer only MultiLab 4010P 1 MultiLab 4010 1 12 2 Ope
71. librate the meter with the sensor 4 Immerse the IDS D O sensor in the test sample O 760 mmHg a 92 25 0 C You can switch between the following displays with lt M gt D O concentration mg l D O saturation 96 When measuring the concentration mg l of solutions with a salt content of more than 1 psu a salinity correction is required For this you have to mea sure and input the salinity of the measured medium first When the salinity correction is switched on the Sal indicator is displayed in the measuring screen You can switch the salinity correction on or off and enter the salinity in the menu for calibration and measurement settings see section 9 3 1 SETTINGS FOR D O SENSORS MENU FOR MEASUREMENT AND CALIBRATION SETTINGS page 63 The integrated air pressure sensor of the MultiLab 4010 1 measures the current air pressure During calibration the air pressure correction function is automatically activated For measurement the air pressure correction is applied if the parameter oxygen saturation 9o is displayed and the DO Saturation local function is enabled The current air pressure is displayed when an IDS D O sensor is connected ba76141e03 03 2014 45 Dissolved oxygen MultiLab 4010 1 Stability control AutoRead amp HOLD function The DO Saturation local function for the parameter oxygen sat uration is switched on or off in the menu f
72. lity control function AutoRead continually checks the stability of the measurement signal The stability has a considerable impact on the reproduc ibility of measured values The measured parameter flashes on the display as soon as the measured value is outside the stability range when the automatic Stability control is switched off You can start the Stability control manually at any time irrespective of the set ting for automatic Stability control see section 9 5 3 AUTOMATIC STABILITY CON TROL page 69 in the System menu 1 Freeze the measured value with AR The HOLD status indicator is displayed The HOLD function is active 28 ba76141e03 03 2014 MultiLab 4010 1 pH value Criteria for a stable measured value You can terminate the Stability control function and the HOLD func il tion with lt AR gt or lt M gt at any time 2 Using lt MENU ENTER3 gt activate the Stability control function manu ally The AR status indicator appears while the measured value is assessed as not stable A progress bar is displayed and the display of the measured parameter flashes The HOLD AR status indicator appears as soon as a stable mea sured value is recognized The progress bar disappears and the display of the measured parameter stops flashing The current measurement data is output to the interface Measurement data meeting the stability control criterion is marked by AR You can pre
73. ll 0 475 cm calibrated 0 475 cm set 0 100 cm Temperature compensation nLF Reference temperature 25 C Temperature coefficient TC of the 2 000 K linear temperature compensation Multiplier for TDS 1 00 ba76141e03 03 2014 71 Settings MultiLab 4010 1 The sensor settings are reset under the Reset menu item in the menu for cali bration and measurement settings To open the settings display the required measured parameter in the measured value display and press the lt MENU ENTER key 9 6 2 Resetting the system settings The following system settings can be reset to the default condition Setting Default settings Language English Audio signal on Baud rate 4800 Baud Output format ASCII Decimal separator Contrast 50 Illumination Auto Shutoff time 1h Temperature unit C Stability control on The system settings are reset in the menu Storage amp config System Reset To open the Storage amp config menu press the MENU ENTER key in the measured value display 72 ba76141e03 03 2014 MultiLab 4010 1 Data storage If the data storage is full 10 Data storage You can save measured values datasets to the data storage e Manual data storage see section 10 1 MANUAL DATA STORAGE page 73 Automatic data storage at intervals see section 10 2 AUTOMATIC DATA STOR AGE AT INTERVALS page 74 Ea
74. ltiLab 4010P 1 4 batteries 1 5 V Mignon type AA Power pack 3 e e e USB cable A plug on mini B plug e Stand e Stand holder Comprehensive operating manual Short instructions CD ROM with USB drivers comprehensive operating manual software MultiLab User software MultiLab Importer 3 2 Power supply The MultiLab 4010 1 is supplied with power in the following ways Mains operation with the supplied power pack Battery operation 4 batteries 1 5 V Mignon type AA USB operation via a connected USB B cable 3 3 Initial commissioning Perform the following activities Insert the supplied batteries For mains operation Connect the power pack If necessary mount the stand Switch on the meter see section 4 2 SWITCHING ON THE METER page 19 Set the date and time see section 4 5 5 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 26 ba76141e03 03 2014 13 Commissioning MultiLab 4010 1 3 3 1 Inserting the batteries You can operate the meter either with normal batteries or with rechargeable batteries Ni MH In order to charge the batteries an external charging device is required 1 Open the battery compartment 1 on the underside of the meter 1 1 Battery compartment CAUTION A Make sure that the poles of the batteries are positioned cor rectly The signs on the batteries must correspond to the signs the battery compartm
75. maturely terminate the Stability control function manu ally with MENU ENTER at any time If the Stability control func tion is prematurely terminated the current measurement data are output to the interface without the AutoRead info 3 Using lt MENU ENTER3 gt start a further measurement with stability con trol Or Release the frozen measured value again with AR or M The AR status display disappears The display switches back to the previous indication The Stability control function checks whether the measured values are stable within the monitored time interval Measured Time interval Stability in the time inter parameter val pH value 15 seconds A Better than 0 01 pH Temperature 15 seconds A Better than 0 5 C The minimum duration until a measured value is assessed as stable is the monitored time interval The actual duration is mostly longer 5 1 2 Measuring the temperature For reproducible pH measurements it is essential to measure the temperature of the test sample IDS sensors measure the temperature with a temperature sensor integrated in the IDS sensor ba76141e03 03 2014 29 pH value MultiLab 4010 1 5 2 pH calibration 5 2 1 Why calibrate pH electrodes age This changes the zero point asymmetry and slope of the pH electrode As a result an inexact measured value is displayed Calibration determines and stores the current values of the zero
76. measure pH 14 7 007 25 0 C ur 08 00 USB output ba76141e03 03 2014 19 Operation MultiLab 4010 1 If the user administration function is activated the Login dialog appears after the meter is switched on see section 4 4 LOGIN WITH A USER NAME page 20 The user administration function is not active in the delivery condi tion 4 3 Switching off the meter 1 Switch the meter off with lt On Off gt 4 4 Login with a user name After activation of the user administration by the administrator software MultiLab User on the enclosed CD ROM measurements are only possible after login with a user name The user name is documented with the measured values and in records All user names entered by the administrator are listed in the User name menu The administrator determines for each user whether or not a password is required for the login to the meter If the Password menu item is grayed out no password is required for the login 1 Switch the meter on with lt On Off gt The Login dialog appears ILogin 3 L User name Admin Password Change password 03 04 2013 08 00 2 Using lt A gt lt W gt select the menu item User name and confirm with lt MENU ENTER gt The user name is highlighted 3 Using lt A gt lt W gt select a user name and confirm with MENU ENTER gt 20 ba76141e03 03 2014 MultiLab 4010 1 Operation Changing
77. most empty gt Data are automatically output to the USB B interface at intervals ba76141e03 03 2014 17 Operation MultiLab 4010 1 4 1 4 Instrument connectors N o A 1 IDS sensors pH ORP conductivity D O 2 USB B device interface 3 Stirrer ProOBOD 4 Service interface 5 Power pack CAUTION A Only connect sensors to the meter that cannot return any volt ages or currents that are not allowed gt SELV and gt current circuit with current limiting YSI IDS sensors and IDS adapters meet these requirements 4 1 5 Sensor info You can display the current sensor data and sensor settings of a connected sensor at any time The sensor data are available in the measured value display with the lt F1 gt nfo softkey pH oS 14 7 007 23 0 01 02 2014 08 00 USB output 1 In the measured value display Display the sensor data sensor name series number with lt F1 gt nfo 18 ba76141e03 03 2014 MultiLab 4010 1 Operation 4 2 pH o8 TE 14 7 007 29 0 4110 03 04 2013 ae B09250001 Display further sensor data settings with lt F1 gt More 4110 B092500013 pH resolution mV resolution Buffer Calibration interval Unit for slope QSC Software Version 03 04 2013 Switching on the meter Switch the meter on with lt On Off gt The meter performs a self test Connect the sensor The meter is ready to
78. mportant information on the safe operation of the meter Read this operating manual thoroughly and make yourself familiar with the meter before putting it into operation or working with it The operating manual must be kept in the vicinity of the meter so you can always find the infor mation you need Important safety instructions are highlighted in this operating manual They are indicated by the warning symbol triangle in the left column The signal word e g Caution indicates the level of danger WARNING A indicates a possibly dangerous situation that can lead to seri ous irreversible injury or death if the safety instruction is not followed CAUTION A indicates a possibly dangerous situation that can lead to slight reversible injury if the safety instruction is not fol lowed NOTE indicates a possibly dangerous situation where goods might be damaged if the actions mentioned are not taken 2 1 2 Safety signs on the meter Note all labels information signs and safety symbols on the meter and in the battery compartment A warning symbol triangle without text refers to safety information in this operating manual 2 1 3 Further documents providing safety information The following documents provide additional information which you should observe for your safety when working with the measuring system Operating manuals of sensors and other accessories Safety datasheets of calibration or maint
79. nd slope of the IDS D O sensor As a result an inexact measured value is displayed Calibration deter mines and stores the current values of the zero point and slope 7 2 2 When to calibrate When the calibration interval has expired When your accuracy requirements are especially high Routinely within the framework of the company quality assurance 7 2 3 Calibration procedures The MultiLab 4010 1 provides 2 calibration procedures Calibration in water vapor saturated air e Calibration via a comparison measurement e g Winkler titration according to DIN EN 25813 or ISO 5813 At the same time the relative slope is adapted to the comparison measurement by a correction factor When the correction factor is active the Factor indicator appears in the measuring screen Calibration can be carried out either as a 1 point calibration or 2 point calibra tion procedure ba76141e03 03 2014 47 Dissolved oxygen MultiLab 4010 1 7 2 4 1 point calibration Calibration in water vapor saturated air Ca and calibration via Comparison meas according to the Winkler method Comp are described jointly here 1 Connect the IDS D O sensor to the meter 2 Check the selected calibration type and selected number of calibration points in the sensor setting menu and if necessary change them 3 Putthe IDS D O sensor into the calibration medium When calibrating via comparison measurement Comp Put the
80. nt D O 47 Connect the power pack 15 R Connecting a 79 Rosalie ed d x dE 70 Connectors 18 D S Scope of 13 av M Russe ed Meus 77 Single point calibration Date 26 DEL Lbs ah ER det Nea et 31 34 Default settings Slope Measured parameter 70 Di meane Acum cr Ears tog 30 System settings 72 Stability control Display 4 24 22 eR Rame Laer 17 automatic 2 69 Manual 28 43 46 F Storage 74 Firmware update 94 Storing in memory 73 Automatic 74 Manual 73 Initial commissioning 13 d Serer 70 T Interval for calibration 62 Temperature compensation 55 76141 03 03 2014 99 Index MultiLab 4010 1 Temperature measurement Conductivity 55 925 DIAL aae on ow E REA 47 DA ss ratae ree RR E 29 Three point calibration DEG re a Feige 32 35 Transmitting data 79 automatic 80 manual 80 Transmitting measured values 79 Two point calibration eR RUE 31 34 Z Zero point of pH electrode 30 100 ba76141
81. ntrol The AR status indicator is displayed The measured parameter flashes DH Burer 10 00 180 0 v 24 8 C AutoCal YSI AR CE 01 07 2011 08 00 Wait for the end of the measurement with stability control or accept the calibration value with lt MENU ENTER gt The calibration display for the next buffer appears voltage display If necessary finish the calibration procedure as a single point calibra tion with lt M gt The calibration record is displayed For single point calibration the instrument uses the Nernst slope il 59 2 mV pH at 25 C and determines the zero point of the IDS Continuing with two point calibration 10 11 12 sensor Thoroughly rinse the sensor with deionized water Immerse the pH sensor in buffer solution 2 When measuring without temperature sensor Measure the temperature of the buffer manually and enter it with lt A gt lt V gt Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flashes ba76141e03 03 2014 31 pH value MultiLab 4010 1 Continuing with three to five point calibration 13 14 16 17 18 19 pH ewe 7 000 0 0 24 8 C AutoCal YSI AR CHEZ 01 07 2011 08 00 Wait for the measurement with stability control to be completed or ter minat
82. or calibration and measurement settings see section 9 3 1 SETTINGS FOR D O SEN SORS MENU FOR MEASUREMENT AND CALIBRATION SETTINGS page 63 The stability control function AutoRead continually checks the stability of the measurement signal The stability has a considerable impact on the reproduc ibility of measured values The measured parameter flashes on the display as soon as the measured value is outside the stability range when the automatic Stability control is switched off Irrespective of the setting for automatic Stability control see section 9 5 3 AUTOMATIC STABILITY CONTROL page 69 in the System menu you can start a measurement with Stability control manually at any time 1 Freeze the measured value with AR The HOLD status indicator is displayed The HOLD function is active You can terminate the Stability control function and the HOLD func tion with lt AR gt or M at any time 2 Using MENU ENTER activate the Stability control function manually The AR status indicator appears while the measured value is assessed as not stable A progress bar is displayed and the display of the mea sured parameter flashes The HOLD AR status indicator appears as soon as a stable measured value is recognized The progress bar disappears and the display of the measured parameter stops flashing The current measurement data is output to the interface Measurement data meeting the stability control
83. point and slope of the electrode Thus you should calibrate at regular intervals 5 2 2 When do you have to calibrate Routinely within the framework of the company quality assurance When the calibration interval has expired 5 2 3 Carrying out automatic calibration AutoCal Make sure that in the sensor menu Buffer menu the buffer set is correctly selected see section 9 1 1 SETTINGS FOR PH MEASUREMENTS page 59 Use one to five buffer solutions of the selected buffer set in any order Below calibration with YSI buffers YSI is described When other buffer sets are used other nominal buffer values are displayed Apart from that the proce dure is identical If single point calibration was set in the menu the calibration proce dure is automatically finished with the measurement of buffer solu tion 1 and the calibration record is displayed 1 Connect the pH sensor to the meter The pH measuring window is displayed 2 Keep the buffer solutions ready 3 Start the calibration with CAL The calibration display for the first buffer appears voltage display pH Buffer 180 0 24 8 C AutoCal YSI 01 07 2011 08 00 4 Thoroughly rinse the sensor with deionized water 30 ba76141e03 03 2014 MultiLab 4010 1 pH value Immerse the sensor in the first buffer solution Start the measurement with lt MENU ENTER gt The measured value is checked for stability stability co
84. procal value of the resistivity Itis a measured value of the ability of a substance to conduct an elec tric current In water analysis the electrical conductivity is a dimension for the ionized substances in a solution Fixed temperature value to compare temperature dependent mea sured values For conductivity measurements the measured value is converted to a conductivity value at a reference temperature of 20 C or 25 C Short name for the electrolytic resistivity It corresponds to the recip rocal value of the electrical conductivity 96 ba76141e03 03 2014 MultiLab 4010 1 Glossary Salinity Salt content Temperature coefficient Temperature compensation The absolute salinity S of seawater corresponds to the relationship of the mass of dissolved salts to the mass of the solution in g kg In practice this dimension cannot be measured directly Therefore the practical salinity according to IOT is used for oceanographic monitor ing It is determined by measuring the electrical conductivity General designation for the quantity of salt dissolved in water Value of the slope a of a linear temperature function 2 1 Y Meas 1 a T Tnar Name of a function that considers the temperature influence on the measurement and converts it accordingly Depending on the mea sured parameter to be determined the temperature compensation functions in different ways For conductimetric measurements
85. ptions for data transmission to a 80 11 5 MultiLab 80 TT b BOBD AhalySEPFO nat MEER an LIRE 81 12 Printer only MultiLab 4010 1 83 12 1 Commissioning switching the printer on or off 83 12 2 Operation printing 84 12 3 Pfinter selings 1 Dir 84 12 4 Maintenance 84 12 4 1 Changing the roll of paper thermal paper 84 12 5 What to do if printer 85 13 Maintenance cleaning disposal 86 13 1 7 Maintenance uie ses UR eS Dg RE oreet b EN be 86 13 1 1 General maintenance activities 86 13 1 2 Replacing the 86 19 2 Cleaning lads o otv ds M as pen ale adopt Er ee 87 19 3 TRACKING Arr tire des is etra denda itp e et eA LAU re Baoan se 87 13 4 Disposal E POS ce VOR A EUR a 87 ba76141e03 03 2014 Contents MultiLab 4010 1 What to dO WE siete seein oe ae ne estas ee ee eet ee 88 TACT aa escort CR A RR AS Uo SOR 88 14 2 Dissolved OxVOG ie au varices see Ras wd ya ene us 89 14 3 GG ODdU CU VID ode eR Sa et X Cut PM te Et S E ERAN 90 14 4 1 90 15 Technical 92 15 1 Measuring ranges
86. ration printing Data are only output to the printer if the following conditions are met e Data are transmitted manually or automatically see section 11 4 OPTIONS FOR DATA TRANSMISSION TO A PC page 80 the printer is switched on LED illuminated there is no USB connection 12 3 Printer settings To open the Storage amp config menu press the F1 Men key in the mea sured value display After completing the settings switch to the measured value display with M Default settings are printed in bold Menu item Possible set Description ting System Printer 12x20 Select the font size for the printer Font size 8x16 7x16 A print sample character set of the printer to view the available font sizes can be printed with OFF gt System Printer The printer prints the meter informa Print test page tion from the System Service infor mation menu The current printer settings are used for the printout 12 4 Maintenance 12 4 1 Changing the roll of paper thermal paper 1 Pull the lever 3 until the lid 4 of the paper compartment opens 2 f necessary remove any remains of the old roll of paper 3 Insert the new roll of paper The start of the paper should poke out of the paper compartment 4 Close the lid 4 of the paper compartment so that it clicks into place 5 f necessary move the printer paper forward with lt ON FEED gt 84 ba76141e03
87. s bar in the status line The progress bar indicates the remaining storage dura tion Ifthe automatic data storage function is activated only the follow ing keys are active lt M gt lt STO__ gt and lt On Off gt The other keys and the automatic switch off function are deactivated Terminating the Proceed as follows to switch off the automatic data storage function before the automatic data adjusted storage duration has expired storage function prematurely Press the STO gt key The following window appears Warning LLL Stop automatic storage 03 04 2013 08 00 2 Using lt amp gt lt W gt select yes and confirm with lt MENU ENTER gt The meter switches to the measured value display The automatic data storage function is terminated ba76141e03 03 2014 75 Data storage MultiLab 4010 1 Editing the data storage Settings 10 3 Measured value data storage 10 3 1 Editing the measured value data storage The contents of the manual or automatic measurement data storage can be shown on the display Each of the measurement data storages has a function to erase the entire contents The data storage is edited in the menu Storage amp config Data storage To open the Storage amp config menu press the lt MENU ENTER__ gt key in the measured value display Open the manual or automatic data storage directly with the lt RCL gt or lt RCL_ gt key The settings are e
88. sor after each calibration proce dure A message is displayed while the data are being updated in the sensor In the measured value display you can display the sensor name and series number of the selected sensor with the Info softkey You can then display further sensor data stored in the sensor with the More softkey see section 4 1 5 SENSOR INFO page 18 1 3 2 Automatic sensor recognition The automatic sensor recognition for IDS sensors allows to operate an IDS sensor with different meters without recalibrating to assign measurement data to an IDS sensor Measurement datasets are always stored and output with the sensor name and sensor series number to assign calibration data to an IDS sensor Calibration data and calibration history are always stored and output with the sensor name and sensor series number to hide menus automatically that do not concern this sensor To be able to use the automatic sensor recognition a meter that supports the automatic sensor recognition e g MultiLab 4010 1 and a digital IDS sensor are required In digital IDS sensors sensor data are stored that clearly identify the sensor The sensor data are automatically taken over by the meter ba76141e03 03 2014 Overview MultiLab 4010 1 10 ba76141e03 03 2014 MultiLab 4010 1 Safety 2 Safety 2 1 Safety information 2 1 4 Safety information in the operating manual This operating manual provides i
89. tasets you have the following options Switch directly to the measured value display with M Quit the display and move to the next higher menu level with lt F1 gt Back 10 3 2 Erasing the measurement data storage Erasing the measurement data storage see section 10 3 1 EDITING THE MEASURED VALUE DATA STORAGE page 76 10 3 3 Measurement dataset A complete dataset includes Date time Meter name series number Sensor name series number ba76141e03 03 2014 77 Data storage MultiLab 4010 1 ID number Measured value of the connected sensor Measured temperature value of the connected sensor AutoRead info AR appears with the measured value if the AutoRead crite rion was met while storing stable measured value Otherwise the AR dis play is missing e Calibration evaluation 4 levels or no evaluation or QSC percentage 10 3 4 Storage locations The MultiLab 4010 1 meter has two measurement data storages The measured values recorded either manually or automatic are stored separately in individual measurement data storages Data storage Maximum number of datasets Manual data storage 500 Automatic data storage 5000 78 ba76141e03 03 2014 MultiLab 4010 1 Transmitting data USB interfaces Installation of the USB driver on the PC 11 Transmitting data USB interfaces 11 1 Outputting current measurement data 1 Output the
90. tches off the meter if no key is pressed for an adjustable period The automatic shutoff function is not active if the power pack is connected if a USB B cable is connected e if the Automatic data storage function is active or with automatic data trans mission 9 5 5 Display illumination The meter automatically switches off the display illumination if no key is pressed for 20 seconds The illumination is switched on with the next keystroke again ba76141e03 03 2014 69 Settings MultiLab 4010 1 pH You can also generally switch on the display illumination See section 9 5 1 SYSTEM page 68 9 6 Reset You can reset initialize all sensor settings and sensor independent settings separately from each other 9 6 1 Resetting the measurement settings The calibration data are reset to the default settings together with the measuring parameters Recalibrate after performing a reset The following settings for pH measurements are reset to the default settings with the Reset function Setting Default settings Buffer YSI Calibration interval 7d Unit for slope mV pH Measured parameter pH Unit for slope 0 001 mV resolution 0 1 Asymmetry 0 mV Slope 59 2 mV Man temperature 25 C Single point calibration off The sensor settings are reset under the Reset menu item in the menu for cali bration and measurement settings To open the settings display th
91. the measured value is converted to a defined reference temperature For potentiometric measurements the slope value is adjusted to the tem perature of the test sample but the measured value is not converted Dissolved oxygen D O saturation Salinity Salt content Short name for the relative D O saturation Relation of the D O partial pressure in the test sample to the D O par tial pressure of air at the current air pressure Example 100 means that the test sample and the ambient air have the same D O partial pressure air and test sample are balanced The absolute salinity S4 of seawater corresponds to the relationship of the mass of dissolved salts to the mass of the solution in g kg In practice this dimension cannot be measured directly Therefore the practical salinity according to IOT is used for oceanographic monitor ing It is determined by measuring the electrical conductivity General designation for the quantity of salt dissolved in water General information Adjusting AutoRange Calibration To manipulate a measuring system so that the relevant value e g the displayed value differs as little as possible from the correct value or a value that is regarded as correct or that the difference remains within the tolerance Name of the automatic selection of the measuring range Comparing the value from a measuring system e g the displayed value to the correct value or a value that is
92. tions You can carry out QSC control calibrations at greater intervals than normal cali brations 1 Open the menu for measurement settings with lt MENU ENTER gt 2 Inthe QSC menu select Control calibration with A W The calibration display appears AutoCal QSC Kit is displayed as the buffer Exclusively use the QSC Kit for the QSC calibration If you use other buffers you will have no valid QSC control calibration 3 Follow the user guide The calibration is carried out like a normal three point calibration As soon as the three point calibration has been successfully carried out you can decide whether to accept or discard the calibration as the QSC control calibration 42 ba76141e03 03 2014 MultiLab 4010 1 ORP Stability control 6 6 1 Measuring 6 1 1 Measuring the ORP NOTE When connecting a grounded PC printer measurements cannot be performed in grounded media as the values would be incorrect The USB interface is not galvanically isolated IDS ORP sensors are not calibrated However you can check IDS ORP sensors using a test solution 1 Connect the ORP sensor to the meter The ORP measuring window is displayed 2 Adjust the temperature of the solutions and measure the current tem perature 3 Check the meter with the ORP sensor 4 Immerse the ORP sensor in the test sample 157 0 m The stability control function AutoRead continually checks the stability of the
93. ues Displayed calibration data 1 point Asy Zero point Asy Slope Nernst slope 59 2 mV pH at 25 C 2 point Asy Zero point Asy Sip Slope Sip 3 point to 5 Asy Zero point Asy point Sip Slope Sip The calibration line is calculated by linear regression You can display the slope in the units mV pH or see section il 9 1 1 SETTINGS FOR PH MEASUREMENTS page 59 36 ba76141e03 03 2014 MultiLab 4010 1 pH value 5 2 6 Calibration data The calibration record is automatically transmitted to the interface after calibrating Displaying the calibration record of the last calibration is to be found under the menu item calibration data Calibration Calibration record To open it in the measured value display press the CAL gt key The calibration records of the last 10 calibrations are to be found in the menu Calibration Calibration data storage Display To open the Calibration menu press the lt MENU ENTER gt key in the measured value display Menu item Setting func Description tion Calibration Displays the calibration records Calibration data stor age Display Further options Scroll through the calibration records with lt A gt lt Y gt Outputthe displayed calibration record to the interface with lt F2 gt USB output Output all calibration records to the interface with lt F2__ gt USB output Q
94. uit the display with lt F1 gt Back or lt MENU ENTER gt Switch directly to the measured value display with lt M gt Calibration Outputs the calibration data stor Calibration data stor age to the interface age Output to RS232 USB ba76141e03 03 2014 37 pH value MultiLab 4010 1 Calibration evaluation Calibration record USB output After calibrating the meter automatically evaluates the calibration The zero point and slope are evaluated separately The worse evaluation of both is taken into account The evaluation appears on the display and in the calibration record Display Calibration Zero point Slope mV pH record mV i TUE 15 15 60 5 58 0 20 lt 15 2 58 0 57 0 or 215 20 25 lt 20 61 0 lt 60 5 or or gt 20 25 2 57 0 56 0 30 lt 25 62 0 61 0 or or gt 25 30 gt 56 0 50 0 Clean the IDS sensor according to the sensor operating manual Error Error lt 30 lt 62 0 or or gt 30 gt 50 0 Error elimination see section 14 WHAT TO DO IF page 88 For pH IDS sensors you can optionally enable a more finely graded calibration evaluation QSC see section 5 2 8 QSC FUNCTION SENSOR QUALITY CONTROL page 40 CALIBRATION pH 03 04 2013 07 43 33 4110 Ser no B092500013 YSI Buffer 1 4 00 Buffer 2 7 00 Buffer 3 10 00 Voltage 1 184 0 mV 2
95. wer pack Kuantech Co Ltd KSAC 0900110W1UV 1 Input 100 240 V 50 60 Hz 270 mA Output 9V 1 1A Connection max overvoltage category II Primary plugs contained in the scope of delivery Euro US UK and Australian The operational life is shorter fs the display illumination is switched on permanently 92 ba76141e03 03 2014 MultiLab 4010 1 Technical data USB interface device Applicable directives and standards Type USB 1 1 USB B Device PC Baud rate Adjustable 1200 2400 4800 9600 19200 Baud Data bits 8 Stop bits 2 Parity None Handshake RTS CTS Cable length Max 3m EMC EC directive 2004 108 EC EN 61326 1 EN 61000 3 2 EN 61000 3 3 FCC Class A Meter safety EC directive 2006 95 EC EN 61010 1 UL 61010 1 CAN CSA C22 2 61010 1 IP protection class EN 60529 FCC Class A Equipment Statement Note This equipment has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 ofthe FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment This equipment generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instruction manual may cause harmful interference to radio communications Operation of this equipment in a residential area is likely to cause harmful int
96. xplained here using the manual data storage as an example The same settings and functions are available for the automatic data storage Menu item Setting Description function Data storage Displays all measurement datasets Manual data storage page by page Display Further options Scroll through the datasets with lt A gt lt V gt Output the displayed dataset to the interface with F22 USB output Quit the display with lt F1 gt Back Data storage Outputs all stored measurement Manual data storage data to the interface Output to RS232 USB Data storage Erases the entire manual measure Manual data storage ment data storage Erase Note All calibration data remain stored when this action is performed 76 ba76141e03 03 2014 MultiLab 4010 1 Data storage Display representation of a dataset Representation of a dataset USB output Quitting the display Manual data storage 3 of 64 03 04 2013 07 43 33 ID number 1 4110 B20234008565 pH 7 000 24 8 AR Sensor 03 04 2013 USB output 53 00 03 04 2013 07 43 33 MultiLab 4010 1 Ser no 09250023 ID number 2 4110 Ser no B092500013 pH 6 012 24 8 C AR S 03 04 2013 07 43 53 MultiLab 4010 1 Ser no 09250013 ID number 2 4110 Ser no B092500013 pH 6 012 24 8 C AR S CEC To quit the display of stored measurement da
97. y cues end yee He xd EIER E IR 13 3 2 13 3 3 Initial 5 13 3 3 1 Inserting the batteries 14 3 8 2 Connecting the 15 3 9 8 Mounting the 5 15 4 16 4 1 General operating 16 4 1 1 Keypad ee Ae UE EAT DRE 16 412 DISpldy ierant ee 17 4 1 3 Status information 17 4 14 Instrument 18 41 5 Sensor iNO scs oan zc nn 18 4 2 Switching on the 19 43 Switching off the 20 4 4 Login with 20 4 9 Navigation acres raring ea e bie a ber aedi 22 4 5 1 22 4 5 2 Measured value 22 4 5 3 5 22 4 5 4 Example 1 on navigation Setting the language 24 ba76141e03 03 2014 3 Contents MultiLab 4010 1 4 5 5 Example 2 on navigation Setting the date and time 26 9 PH ValUE oues Sa y Ea RE 28 31 Measuring cesare
98. zed by the parameters slope and zero point The junction is a porous body in the housing wall of reference elec trodes or electrolyte bridges It arranges the electrical contact between two solutions and makes the electrolyte exchange more dif ficult The expression junction is also used for ground or junction less transitions The ORP is caused by oxidizing or reducing substances dissolved in water if these substances become effective on an electrode surface e g a gold or platinum surface The pH value is a measure of the acidic or basic effect of an aqueous solution It corresponds to the negative decadic logarithm of the molal hydrogen ions activity divided by the unit of the molality The practical pH value is the value of a pH measurement Name of a measuring technique The signal depending on the mea sured parameter of the electrode is the electrical potential The elec trical current remains constant Slope The slope of a linear calibration function Zero point The zero point of a pH combination electrode is the pH value at which the electromotive force of the pH combination electrode at a specified temperature is zero Normally this is at 25 C Conductivity Cell constant C Conductivity x Reference temperature Resistivity p Characteristic quantity of a conductivity measuring cell depending on the geometry Short form of the expression specific electrical conductivity It corresponds to the reci

YSI MultiLab 4010-1 & 4010P-1 Instruction Manual

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YSI MultiLab 4010-1 &amp; 4010P-1 Instruction Manual

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YSI MultiLab 4010-1 & 4010P-1 Instruction Manual