User`s Manual
Contents
1. button and the current minutes set point will flash Press the increase or decrease button until the desired run minutes 00 to 59 is displayed Press the SET button and save will flash on the display The new program is now entered the display will show the current chamber temperature Setting the run time to 00 00 will turn off the program timer With the timer off the unit will operate at the set point temperature until manually turned off The temperature set point range is 35 C to 65 C 14 Product Service 1 800 522 7658 Chapter 4 Using Your CentriVap micro IR The time set point range 1s 00 00 on to 99 59 99 hrs 59 min Preheat To preheat the chamber program the desired temperature and time Make sure the chamber door is closed Select the desired heat mode IR HEAT is recommended for preheating Turn the Run Mode Selector to Standby The heaters will raise the chamber temperature to the programmed set point The actual chamber temperature will be displayed The chamber will continue to preheat until either the START STOP button is pressed or the mode selector is turned to the off position Opening the lid will also turn the heater off Operating the CentriVap micro IR CAUTION To avoid personnel injury Do not operate the CentriVap micro IR if the lid is scratched or nicked or shows signs of damage A damaged lid could fail under vacuum 4 amp CAUTION Moving rotor can cut hands Do not lift the lid2. Do not operate 1n environment with relative humidity exceeding 80 for temperatures up to 88 F 31 C decreasing linearly to 50 relative humidity at 104 F 40 C Doing so could cause electric leakage or corrosion Do not expose unit to direct sun light or high temperatures The recommended indoor operating temperature is 20 C 30 C Do not use flammable substances near the product Doing so could create a fire hazard Provide a minimum space of 7 8 inches 20cm behind the unit for clearance of the power cord Install unit on solid level surface Failure to do so can result in excessive vibration Do not lay the unit down on its sides or top Doing so can result in damage to the unit Secure lid and any other moveable parts when moving the unit Failure to do so can result in injury or damage to the unit When moving the unit always lift do not slide Failure to do so may result in damage to the unit Warning Precautions for use Do not disassemble or attempt to repair the unit without proper training or personal injury or damage to the unit could occur Do not use the product for anything other than what it was intended for or personal injury or damage to the unit could occur Product Service 1 800 522 7658 3 Chapter 1 Introduction 9 Do not use flammable sprays near the product Doing so could cause fire Prohibition Q Protect the control panel from spills by wiping off any water or solvent with a clea
3. Labconco Corporation 8811 Prospect Avenue Kansas City MO 64132 USA Ph 816 333 8811 Fax 816 363 0130 labconco labconco com is in conformity with the standards listed below LVD EN 61010 1 2001 EN 61070 2 010 2003 IEC 61010 2 051 2003 EMC EN 61326 1997 A1 A2 A3 2003 EN 6100 3 2 2000 EN 61000 3 3 1995 A1 2001 following the provisions of the following directives 89 336 EEC 92 31 EC 2006 95 EC 2002 95 EC RoHS when installed and operated in accordance with the manufacturers installation and operating instructions o Passas Cry USA 2 8 2otl fo Mark Schmitz Place and date of issue x Vice President Research and Engineering Labconco Corporation Labconco P N 3696077 Rev Product Service 1 800 522 7658
4. CentriVap can cause skin eye respiratory and digestive system disorders Locate the CentriVap inside a fume hood Space Requirements Refer to Appendix C CentriVap micro IR Specifications for dimensional drawings of the CentriVap micro IR No person or any hazardous material should be within 12 inches of the CentriVap Concentrator while it 1s operating 6 Product Service 1 800 522 7658 Chapter 3 Getting Started Now that the site for your CentriVap micro IR 1s properly prepared you are ready to unpack inspect install and test the unit Read this chapter to learn how to e Unpack and move your CentriVap micro IR e Setup your CentriVap micro IR e Connect the electrical supply source to your CentriVap micro IR e Properly exhaust your CentriVap micro IR e Safely use solvents with your CentriVap micro IR Unpacking Your CentriVap micro IR Carefully unpack your CentriVap micro IR and inspect it for damage that may have occurred in transit If your CentriVap is damaged notify the delivery carrier immediately and retain the entire shipment intact for inspection by the carrier The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen 15 days of delivery NOTE Do not return goods without the prior authorization of Labconco Unauthorized returns will not be accepted If your CentriVap micro IR was damaged in transit you must file a claim directly wit
5. hazardous solvents the CentriVap micro IR should be operated inside a fume hood If a sample is spilled in the chamber it must immediately be cleaned up Hazardous materials such as strong acids or bases radioactive substances and volatile organics must be handled carefully and promptly cleaned up if spilled Do not store flammable or hazardous solvents within 12 inches 300 mm of the CentriVap micro IR IMPORTANT The disposal of substances used in connection with this equipment may be governed by various Federal State or local regulations All users of this equipment are urged to become familiar with any regulations that apply in the user s area concerning the dumping of waste materials in or upon water land or air and to comply with such regulations Product Service 1 800 522 7658 11 Chapter 4 Using Your CentriVap micro IR After your CentriVap micro IR has been installed as detailed in Chapter 3 Getting Started you are ready to begin using your CentriVap Read this chapter to learn how to e Set operating parameters e Operate the controls e Properly select and position glassware inside your CentriVap micro IR e Understand the display e Interrupt a cycle after it has begun NOTE Do not store or stack supplies or equipment on top of the CentriVap micro IR Planning Thoroughly understand procedures and the equipment operation prior to beginning work The unique performance of the CentriVap micro IR is depend
6. not connected to electrical power Circuit breaker blown Lid open Sample vials not located symmetrically in rotor Vent hose exhausting into lab area Heater inoperable Vacuum pump failure Liquid in vacuum line CAUTION Electrical shock hazard See appendix C CentriVap specifications for electrical operating parameters CORRECTIVE ACTION Connect unit to proper electrical receptacle Correct electrical problem and reset circuit breaker Close lid Reposition sample vials Redirect hose to fume hood Contact Labconco Check pump Clear vacuum line Product Service 1 800 522 7658 Chapter 7 Troubleshooting PROBLEM CORRECTIVE ACTION Evaporation rate is Obstruction in hose Remove obstruction or replace hose reduced continued Lack of adequate vacuum See below Temp set point too low Increase temperature set point No vacuum poor vacuum Liquid in glass trap Empty trap Leaks in lines or Locate and repair connectors or gasket Foreign material on lid Clean gasket and lid gasket Product Service 1 800 522 7658 21 Appendix A CentriVap micro IR Components The following pages list components that are available for your CentriVap micro IR The parts shown are the most common replacement parts If other parts are required contact Product Service l 7549200 Control Board IR Pus o o l 7549300 SSRelaySetmicroIR o o l 7549400 Display board microIR
7. o tr pt 7549500 Vacuum PumpmicrolR l 7549600 Transformer LOOVA o o pt 7549700 Transformer SOVA _ _ SS pt 7549800 FanMotormicroIR _ o o pt 7549900 Selector Switch SSS 1 Lid Gasket p pd pb pad pa 22 Product Service 1 800 522 7658 Appendix B CentriVap micro IR Dimensions Product Service 1 800 522 7658 23 Appendix C CentriVap micro IR Specifications This Appendix contains technical information about the CentriVap including specifications environmental operating conditions wiring diagrams and evaporation rates Electrical Specifications Nominal amperage for 115V CentriVap model 7701020 including vacuum pump 5A Nominal amperage for 230V CentriVap models 7701030 35 37 including vacuum pump 3A Frequency all models 50 60 Hz Phase Single Heater power 300 watts Rotor Speed Up to 1 700 RPM The vacuum pump 1s capable of achieving an ultimate vacuum pressure of 160 MBAR Environmental Conditions 24 Indoor use only Maximum altitude 6562 feet 2000 meters Ambient temperature range 41 to 104 F 5 to 40 C Maximum relative humidity 80 for temperatures up to 88 F 31 C decreasing linearly to 50 relative humidity at 104 F 40 C Main supply voltage fluctuations not to exceed 10 of the nominal voltage Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary vo
8. show signs of hardening permanent set or deterioration 2 Using a soft cloth sponge or chamois and a mild non abrasive soap or detergent clean the glass lid 3 Using a soft cloth sponge or chamois and a mild non abrasive soap or detergent clean the exterior surfaces of the unit Liquid spray cleaners and polishes may be used on the exterior surfaces Do not use solvents to remove stains from the exterior surfaces as they may damage the finish 18 Product Service 1 800 522 7658 Chapter 6 Accessories for Your CentriVap micro IR The following accessories are available for the CentriVap micro IR Concentrator PART amp DESCRIPTION 7548400 Rotor 5 ml x 24 Holds 24 0 5 ml microcentrifuge tubes 7548500 Rotor 1 5 ml x 24 Holds 24 1 5 ml microcentrifuge tubes 7548600 Rotor 10 ml x 16 Holds 16 10ml 18mm x 65mm vials 7548700 Rotor 15 ml x 12 Holds 12 15ml 20mm x 70mm vials 7548800 Rotor 30 ml x 8 Holds 8 30ml 30mm x 73vials 7548300 Secondary Glass Trap Assembly Product Service 1 800 522 7658 19 Chapter 7 Troubleshooting Refer to the following if your CentriVap micro IR fails to operate properly If the suggested corrective actions do not solve your problem contact Labconco for additional assistance CAUTION Disconnect power before corrective action is taken PROBLEM Unit will not operate Excessive vibration Sample odor in lab Evaporation rate 1s reduced 20 Unit
9. that claims be filed with the delivery carrier within fifteen 15 days of delivery Limitation of Liability The disposal and or emission of substances used in connection with this equipment may be governed by various federal state or local regulations All users of this equipment are required to become familiar with any regulations that apply in the user s area concerning the dumping of waste materials in or upon water land or air and to comply with such regulations Labconco Corporation is held harmless with respect to user s compliance with such regulations Contacting Labconco Corporation If you have questions that are not addressed in this manual or 1f you need technical assistance contact Labconco s Customer Service Department or Labconco s Product Service Department at 1 800 821 5525 or 1 816 333 8811 between the hours of 7 00 a m and 6 00 p m Central Standard Time Part 7539801 Rev ECO F897 TABLE OF CONTENTS CHAPTER 1 INTRODUCTION Safety Symbols CHAPTER 2 PREREQUISITES Electrical Requirements Location and Exhaust Requirements Space Requirements CHAPTER 3 GETTING STARTED Unpacking Your CentriVap micro IR CentriVap micro IR Components Setting Up Your CentriVap micro IR Emergency Access Into the Chamber Electrical Connection Rotor Installation Installing a CentriZap IR Strobe Light Chemical Resistance of CentriVap micro IR Components Solvent Safety Precautions CHAPTER 4 USING YOUR CENTRIVAP MI
10. An additional heater 1s provided for applications were samples maybe sensitive to radiant heat A PTFE coated diaphragm vacuum pump is included which requires no maintainance The vacuum pump pulls vapor out through the center of the chamber to minimize cross contamination A glass trap is also provided to condense and collect solvent exiting the chamber The CentriVap micro IR Concentrator has a standby function to preheat or maintain the chamber temperature A safety switch prevents the concentrator from starting when the lid is in the open position and a latch prevents the lid from being opened while the rotor 1s turning The compact low profile design allows the concentrator to be placed on a bench top or other laboratory work surface The CentriVap micro IR Concentrator also comes standard with a CentriZap IR LED strobe light for viewing the samples during the run The microprocessor controls the operation of the heaters from 35 C to 65 C The rotor speed of 1700 RPM and vacuum down to 120 mbar provides excellent regulation and reproducibility of protocols Product Service 1 800 522 7658 1 Chapter 1 Introduction Safety Symbols Your CentriVap micro IR Concentrator was designed with safety in mind however conditions may exist that could be hazardous h WARNING Read and understand operator s manual before using this machine Failure to follow operating instructions could result in death or serious injury Throughout
11. CRO IR Planning Sample Vial Selection Loading Glassware Into the CentriVap micro IR Temperature Setting Guidelmes Time Setting Guidelines CentriVap micro IR Controls Operating the CentriVap micro IR Controls Operating the CentriVap micro IR Operational Notes Interrupting a Cycle After it Has Begun Safety Precautions CHAPTER 5 MAINTAINING YOUR CENTRIVAP MICRO IR NO m NN nn OOO WW WH N N ph CO CHAPTER 6 ACCESSORIES FOR YOUR CENTRIVAP MICRO IR CHAPTER 7 TROUBLESHOOTING APPENDIX A CENTRIVAP MICRO IR COMPONENTS APPENDIX B CENTRIVAP MICRO IR DIMENSIONS APPENDIX C CENTRIVAP MICRO IR SPECIFICATIONS Electrical Specifications Environmental Conditions Evaporation Rates DECLARATION OF CONFORMITY 20 22 23 24 24 25 26 Chapter 1 Introduction Congratulations on your purchase of a Labconco CentriVap micro IR Vacuum Concentrator The CentriVap micro IR Concentrator uses centrifugal force with heat and vacuum to rapidly evaporate and condense solvents from biological and analytical samples Centrifugation eliminates bumping and foaming as vacuum is applied and also concentrates the solute in the bottom of the vial This allows recovery of solutes from sample volumes as small as a few microliters The concentrator 1s equipped with two separate heaters to speed evaporation by warming the chamber during processing The clear lid heater uses radiant heat to efficiently heat samples under vacuum conditions
12. User s Manual CentriVap micro IR Vacuum Centrifugal Concentrators Models 77010 Series To receive important product updates complete your product registration card online at register labconco com Protecting vour AF Va jaboratory environment Labconco Corporation 8811 Prospect Avenue Kansas City MO 64132 2696 800 821 5525 816 333 8811 FAX 816 363 0130 E MAIL labconco labconco com HOME PAGE www labconco com Please read the User s Manual before operating equipment Copyright O 2011 Labconco Corporation All rights reserved The information contained in this manual and the accompanying products are copyrighted and all rights reserved by Labconco Corporation Labconco Corporation reserves the right to make periodic design changes without obligation to notify any person or entity of such change Warranty Labconco provides a warranty on all parts and factory workmanship The warranty includes areas of defective material and workmanship provided such defect results from normal and proper use of the equipment The warranty for all Labconco products will expire one year from date of installation or two years from date of shipment from Labconco whichever is sooner except the following e Purifier Logic Biological Safety Cabinets and PuriCare Lab Animal Research Stations carry a three year warranty from date of installation or four years from date of shipment from Labconco whichever is sooner S
13. ctual times must be determined by the user CentriVap micro IR Controls The control panel for the CentriVap micro IR is shown below with a description of its functions Product Service 1 800 522 7658 13 Chapter 4 Using Your CentriVap micro IR E mM AMS s el 1 Display Shows set point parameters and actual measured conditions 2 Start Stop Button Used to start or stop a run and reset the timer 3 Time Button Used to display time remaining 4 Set Button Use to program temperature and time 5 Increase Button Use to increase temperature and time in set up mode 6 Decrease Button Use to decrease temperature and time in set up mode 7 Standby Light Indicates that the selected heater 1s on and cycling 8 Power Light Indicates the unit is in Standby or Run mode 9 Heat Mode Selector Use to select IR IR Heat or Heat only modes 10 Run Mode Selector Use to select Off Standby Preheat or Run modes Operating the CentriVap micro IR Controls Change Temperature and Run Time Set Point To change the temperature set point press the SET button The current temperature set point will flash on the display Press the increase or decrease button until the desired temperature set point is displayed Press SET button and the current hour set point will flash Press the increase or decrease button until the desired run hours 00 to 99 is displayed Press SET
14. e hot Operational Notes Turn the mode switch to OFF before turning the power switch off When the CentriVap micro IR power is turned on the program returns to the same mode that 1t was in when the power was turned off The timer will reset Pressing the START STOP during a run will turn the system off and reset the timer Pressing it again will restart the program from the beginning To display the time remaining press the TIME button Interrupting a Cycle After it has Begun To interrupt the cycle during a run select STANDBY This shuts off the rotor vacuum pump releases vacuum and unlatches the lid After the rotor stops the lid may be opened If it 1s necessary to re start the CentriVap micro IR close the lid and select RUN The cycle resumes operation at the same set point parameters and the timer continues to count down from the time at which the cycle was stopped Safety Precautions Special precautions must be observed if the materials used in the CentriVap micro IR Concentrator are known to be hazardous toxic radioactive or contaminated with pathogenic micro organisms These actions should include but are not limited to the following e Refer to the World Health Organization Laboratory Biosafety Manual paying special attention to information about centrifuges and the handling of hazardous materials e Operate or vent the CentriVap micro IR Concentrator inside a suitable fume hood or venti
15. ent upon the proper balance of heat vacuum and centrifugal force If the proper balance 1s not established it 1s possible to damage or lose a portion of the sample Therefore 1f you are unfamiliar with the CentriVap micro IR or are attempting a new protocol it may be helpful to make a trial run using a representative sample Sample Vial Selection Normally sample vials should be filled no more than approximately half full Select the size of the sample vial so it is compatible with the rotor and the desired sample size Vials should not be loose in the rotor Rotors are available with holes for various size vials Refer to Chapter 6 Accessories for your CentriVap micro IR Concentrator for available rotor sizes Loading Glassware into the CentriVap micro IR Smooth operation of the CentriVap micro IR 1s dependent upon proper balance of the machine Therefore if less than a full load of samples is run it is important to load samples in a fairly symmetrical manner distributing the weight of the samples evenly in the rotor 12 Product Service 1 800 522 7658 Chapter 4 Using Your CentriVap micro IR Temperature Setting Guidelines The evaporation rate achieved by the CentriVap micro IR 1s dependent upon a variety of factors These include the nature of the solvent the temperature set point the temperature mode and the pressure in the vacuum system The Centrivap micro IR was designed to quickly evaporate small samples at elevated tem
16. h the freight carrier Labconco Corporation and its dealers are not responsible for shipping damage Do not discard the carton or packing material for your CentriVap micro IR until you have checked all of the components and installed and tested the unit Product Service 1 800 522 7658 T Chapter 3 Getting Started CentriVap micro IR Components As previously mentioned the CentriVap micro IR System is available in 115V or 230V Locate the model of CentriVap you received in the following table Verify that the components listed are present and undamaged Catalog Product Description 7701020 CentriVap micro IR Concentrator 115V USA 1334500 Power Cord with NEMA 5 15P Plug 7548500 Rotor 1 5ml x 24 7539801 User s Manual 7548900 Wrench Rotor 7549000 CentriZap micro IR LED Strobe Light 7701030 CentriVap micro IR Concentrator 230V EU 1336100 Power Cord with CEE 7 7 Plug 7548500 Rotor 1 5ml x 24 7539801 User s Manual 7548900 Wrench Rotor 7549000 CentriZap micro IR LED Strobe Light 7701035 CentriVap micro IR Concentrator 230V UK 1332600 Power Cord with BS 1363 Plug 7548500 Rotor 1 5ml x 24 7539801 User s Manual 7548900 Wrench Rotor 7549000 CentriZap micro IR LED Strobe Light 7701037 CentriVap micro IR Concentrator 230V CHINA 1332700 Power Cord with CHI 10P Plug 7548500 Rotor 1 5ml x 24 7539801 User s Manual 7548900 Wrench Rotor 7549000 CentriZap micro IR LED Strobe Light If you do not rece
17. ions If the plug supplied with the CentriVap Does not match the available receptacle remove this plug and replace it with an approved plug of the suitable style It is recommended that an emergency switch for disconnecting the power in the case of a malfunction be located remote from the CentriVap micro IR preferably outside the room in which the unit is housed or adjacent to the exit from that room Product Service 1 800 522 7658 5 Chapter 2 Prerequisites Location and Exhaust Requirements The CentriVap micro IR Concentrator should be located on a surface that is stable flat and level WARNING The CentriVap Concentrator should be located within a fume hood if hazardous or flammable solvents are used Heating of materials could lead to the liberation of hazardous gases In all cases regardless of the solvent used it is strongly recommended that the vacuum pump is vented in a fume hood A glass trap is included with the unit to minimize the exhausting of solvents into the atmosphere but if flammable solvent are used a secondary trap is recommended See Chapter 6 for available accessories The use of the glass traps does not negate the need to exhaust the vacuum pump into a fume hood Failure to properly vent the CentriVap will expose personnel to potentially harmful chemicals The CentriVap has not been evaluated by an approval agency for the use of biological radio toxins or flammable liquids or materials Solvents used in the
18. ive one or more of the components listed for your CentriVap micro IR or if any of the components are damaged contact Labconco Corporation immediately for further instructions Setting Up Your CentriVap micro IR After you verify receipt of the proper components move your CentriVap micro IR to the level and sturdy location where you want to install it There is no need to secure the CentriVap micro IR Concentrator to the work surface Then follow the steps listed below Emergency Access Into the Chamber The CentriVap micro IR is designed to prevent access to the chamber in the event of a power disruption If it is necessary to open the lid when there 1s no electrical power connected to the unit you can unlock the latch by pulling on cable release located in the top left hand rear corner of the back panel Pulling the cable out will unlock the lid latch mechanism While holding the latch open raise the lid with the other hand 8 Product Service 1 800 522 7658 Chapter 3 Getting Started CAUTION Never attempt to defeat the latch or open the lid while the CentriVap micro IR is running Personal injury can result from moving parts and chemicals CAUTION Moving rotor can cut hands Do not lift the lid while it is turning Do not disable the lid latch Do not reach into the chamber if rotor is turning Electrical Connection Plug the power cord into the receptacle on the back of the CentriVap micro IR Concentrator and pl
19. lation device Load rotors in a ventilation device e Periodically inspect all parts of the CentriVap micro IR Concentrator including the lid gasket chamber plumbing components and rotors 16 Product Service 1 800 522 7658 Chapter 5 Maintaining Your CentriVap micro IR Under normal operation the CentriVap micro IR requires little maintenance The following maintenance schedule 1s recommended Before servicing disconnect electrical power Special precautions must be observed if materials used in the CentriVap micro IR Concentrator are known to be hazardous toxic radioactive or contaminated with pathogenic micro organisms Before servicing the CentriVap micro IR Concentrator must be suitably decontaminated Wear appropriate eyewear gloves and other safety apparel As needed Before using any cleaning or decontamination method except those recommended by the manufacturer users should check with the manufacturer that the proposed method will not damage equipment 1 Clean up all spills remove liquids from the chamber Clean or decontaminate all surfaces using agents suitable for the substance spilled 2 Clean lid and gasket using soft cloth sponge or chamois and a mild non abrasive soap or detergent 3 At the end of the run liquid collected in the glass traps should be removed To empty the trap remove the glass from the mounting bracket remove the silicone stopper Dispose of the liquid in accordance with all codes Rein
20. ltage spikes on the AC input line that may be as high as 1500V for 115V models and 2500V for 230V models are allowed Used in an environment of Pollution degrees 2 1 e where normally only non conductive atmospheres are present Occasionally however a temporary conductivity caused by condensation must be expected in accordance with IEC 664 Product Service 1 800 522 7658 Appendix C CentriVap micro IR Specifications Evaporation Rates ml Samples Size ml C Dry min Mode is ht j3s fo Rca ts o 55D eat HS 36 Ha HT Ed 24 E eee eee eee O eee eee 1 5 24 es 24 Doo Ti 24 60 225 Heat Is Et IR Heat Is 4 129 IR IR R 180 9 IR Heat 34 IR Heat 30 31 180 Ee E O O O e M 40 R C o o 49 a 30 E 31 IR Heat Es IR Heat IR Heat Product Service 1 800 522 7658 25 26 Protecting your LF _ laboratory environment aF l LABCONCO CORPORATION 816 333 8811 800 821 5525 8811 Prospect Avenue FAX 816 363 0130 Kansas Cily MO 64132 2696 www labeonce com CE Declaration of Conformity We Labconco Corporation 8811 Prospect Avenue Kansas City MO 64132 USA Ph 816 333 8811 Fax 816 363 0130 labconco labconco com being the representative party in the EU solely responsible for this certification hereby declare that the following product Equipment Laboratory Equipment CentriVap micro IR Concentrators Type Model CentriVap micro IR System 770103X Series Manufacturer
21. n dry cloth Failure to do so could cause an unsafe condition or create a fire Compliance hazard Q Do not clean the product with excessive quantities of water thinner benzene or petroleum based products Failure to do so could cause an unsafe Compliance Condition or create a fire hazard 4 Product Service 1 800 522 7658 Chapter 2 Prerequisites Before you install your CentriVap micro IR you need to prepare your site for installation Carefully examine the location where you intend to install your CentriVap You must be certain that the area is level and of solid construction In addition an exhaust means must be provided An electrical source must also be located near the installation site Carefully read this chapter to learn e The electrical supply requirements e The exhaust requirements e Space requirements Refer to Appendix C CentriVap micro IR Specifications for complete CentriVap electrical and environmental conditions specifications and requirements Electrical Requirements The CentriVap micro IR Concentrator requires a grounded electrical outlet This outlet requires a 15 Amp circuit breaker or fuse for models rated at 115V 60 Hz An 8 Amp circuit breaker or fuse 1s required for models rated at 230V 50 60 Hz Various models are available for use in different locations throughout the world Each has a unique plug suitable for the specific location See CentriVap Components in Chapter 3 for detail plug specificat
22. peratures The temperature can be set from 35 C to 65 C Asa general guideline to speed the evaporation process the CentriVap temperature should be set as high as possible as long as the temperature will not damage the sample or cause the sample to bump Typically the fastest evaporation rates will be obtained using the IR heat mode IR Heat second then Heat At lower temperatures depending on the mode of heat and the type of samples vapor can sometimes condense inside the chamber slowing the evaporation process For instance at temperatures below 50 C aqueous samples can begin to condense inside of the chamber becoming worse at lower set points When evaporating at lower temperatures we recommend running in the IR Heat mode This mode distributes the heat more evenly around the chamber reducing the potential for condensation As always when attempting a new protocol it is recommended that a trial run be made Time Setting Guidelines The CentriVap micro IR Concentrator has a timer that can be set from 00 00 to 99 hours and 59 minutes The run time setting 1s used to turn the concentrator off after a set period of time This stops the rotation turns off the heater vacuum pump and bleeds vacuum from the system The 00 00 setting allows the unit to run at the set point temperature until manually turned off The tables in Appendix C CentriVap micro IR Specifications indicate approximate times required to evaporate various common solvents A
23. pump Chapter 3 Getting Started Chemical Resistance of CentriVap micro IR Components Your CentriVap micro IR Vacuum Concentrator is designed to be chemical resistant to compounds that are commonly used in the concentration processes However by necessity the CentriVap is comprised of a number of different materials some of which may be attacked and degraded by certain chemicals The degree of degradation is obviously dependent on the concentration and duration of exposure Some major components of the CentriVap that are susceptible to degradation are as follows Dimethyl Sulfoxide DMSO NI Chrome plate PTFE coated Aluminum PTFE coated Aluminum gt gt 5 ese t f eniom oo Sulfuric Acid 10 _ Acids Bases Solvents se O N ES LD z E o O D D O O x x oom TOROGUN Stainless Steel Soest tte AJAJAJA Stainless Steel etetetopota H ta taataa AJA C 5 D AJA A A AJA A A AJA A A Acceptable C Moderate Degradation Questionable use D Severe Degradation Infrequent use recommended immediate thorough cleaning required o O lt O O m gt gt gt DO DL gt Prd KIO gt D LO gt gt gt ugr When using compounds in the Centri Vap micro IR that are hostile to the materials of construction it is imperative that the equipment is appropriately maintained e After each run clean up all residues spills and materials that might have splashed in the chamber using agents sui
24. stall the silicone stopper and replace the glass trap to its mounting bracket 4 To prolong the life of the vacuum pump and to optimize its performance it 1s important to purge all liquid from within it Once the concentration process 1s completed and the glass trap has been emptied open the CentriVap micro IR lid and turn the Mode selector switch to ON The pump will operate and will draw air through the system The rotor will not turn with the lid open The length of the liquid purge time is dependent on the volatility of the solvents used Once all of the liquid is purged from the vacuum lines turn the mode selector switch to OFF 5 Check rotors for loose or missing parts Tighten or replace as required Do not use defective rotors 6 Inspect the chamber to insure that there are no cracks or structural damage Call Labconco if defects exist Product Service 1 800 522 7658 17 Chapter 5 Maintaining Your CentriVap micro IR 7 Check the continuity of the protective earth ground between the ground terminal on the power inlet and a bare metal housing panel Contact Labconco 1f there is no continuity 8 Repair any defects to the surface where the unit is installed Monthly 1 The rubber and silicone components on the CentriVap may eventually deteriorate and require replacement The effective life of those parts depends upon both their usage and the surrounding environment Check all hoses and gaskets and replace any that
25. table for the substance involved e Remove the contents and clean the glass trap after each use 10 Product Service 1 800 522 7658 Chapter 3 Getting Started Solvent Safety Precautions CAUTION The CentriVap micro IR is not classified as explosion proof It has been designed with safety as a primary consideration and should be used in a prudent manner using good laboratory practices It has been designed for use with compounds as described in the United States National Electrical Code Class I Group D The heater may be programmed to run as hot as 65 C however the heater elements may be hotter An over temperature protection device limits the heater to a maximum temperature of 80 C It is important that the solvents used are compatible with these temperatures Do not evaporate solvents that have an autoignition temperature below 180 C Do not evaporate solvents that are classified as Group A B or C by the National Electrical Code Evaporate only non flammable or Group D solvents with autoignition temperatures 180 C or above Use of other compounds could cause an explosion Solvents may be flammable Evaporate only non flammable or group D solvents with autoignition temperature 180 C or higher Keep sources of ignition away from solvents CAUTION Solvents used in the CentriVap micro IR may be flammable or hazardous Use extreme caution and keep sources of ignition away from the solvents When using flammable or
26. teamScrubber amp FlaskScrubber Glassware Washers carry a two year warranty from date of installation or three years from date of shipment from Labconco whichever is sooner Blood Drawing Chairs carry a ten year warranty Carts carry a lifetime warranty Glassware is not warranted from breakage when dropped or mishandled This limited warranty covers parts and labor but not transportation and insurance charges In the event of a warranty claim contact Labconco Corporation or the dealer who sold you the product If the cause is determined to be a manufacturing fault the dealer or Labconco Corporation will repair or replace all defective parts to restore the unit to operation Under no circumstances shall Labconco Corporation be liable for indirect consequential or special damages of any kind This statement may be altered by a specific published amendment No individual has authorization to alter the provisions of this warranty policy or its amendments Lamps and filters are not covered by this warranty Damage due to corrosion or accidental breakage is not covered Returned or Damaged Goods Do not return goods without the prior authorization from Labconco Unauthorized returns will not be accepted If your shipment was damaged in transit you must file a claim directly with the freight carrier Labconco Corporation and its dealers are not responsible for shipping damages The United States Interstate Commerce Commission rules require
27. this manual potentially hazardous conditions are identified using the following words and symbols This is the safety alert symbol It is used to alert you to potential personal injury hazards Obey all safety messages that follow this symbol to avoid possible injury or death DANGER indicates an imminently DANGE R hazardous situation which if not avoided will result in death or serious injury WARNING indicates a potentially A WARNING hazardous situation which if not avoided could result in death or serious injury CAUTION indicates a potentially A E AUTION hazardous situation which if not avoided may result in minor or moderate injury CAUTION used without the safety alert C AUT O N symbol indicates a potentially hazardous situation which if not avoided may result in property damage It is important that you understand the warnings listed throughout this manual before you operate the CentriVap micro IR Concentrator 2 Product Service 1 800 522 7658 Compliance 9 Prohibition 9 Prohibition 9 Prohibition Compliance 2 Compliance Compliance Compliance 9 Prohibition D No disassemble Prohibition Chapter 1 Introduction Warning Precautions for installation Connect to proper supply voltage Verify that the supply voltage matches the voltage and hertz written on serial tag Failure to do so could damage the unit or affect performance
28. ug the other end into a suitable power receptacle Rotor Installation The CentriVap micro IR Concentrator comes with a 1 5ml rotor installed If a different rotor is required you may remove the standard rotor and replace it with one of the other available rotors To remove the rotor loosen the left handed 19mm hex nut using the rotor wrench The rotor nut is left handed so turn the nut clockwise to remove Once the nut is removed the rotor can be lifted off of the drive hub Place the alternate rotor on the drive hub making sure the drive pins are properly engaged with the drive holes in the rotor Replace the 19mm hex nut by turning counter clockwise secure the nut using the rotor wrench Do not over tighten the hex nut IMPORTANT Do not leave the rotor wrench in the chamber Do not use a rotor if it shows any signs of damage Installing a CentriZap micro IR Strobe Light An LED strobe light comes standard with each CentriVap micro IR Concentrator This light will enable you to see the samples as they are rotating in the chamber Attach the connector on the strobe light harness into the receptacle on the back of the CentriVap micro IR marked STROBE To use the strobe light while the unit is operating press the pushbutton on the light and shine the light on the samples in the rotor Product Service 1 800 522 7658 9 COMPONENT MATERIAL Chamber Hub nut Chamber Rotor Lid Gasket Tubing Motor shaft Bearings Vacuum
29. while it is turning Do not disable the lid latch Do not reach into the chamber if rotor is turning While the CentriVap micro IR Concentrator is operating do not lean on the lid and do not place hazardous materials within 12 inches 305mm 1 Turn ON the CentriVap micro IR power switch located on the right side of the back panel Turn the run mode switch to STANDBY 2 Program the desired temperature set point and run time 3 Preheat the chamber if desired 4 Place samples in vials Normally the vials should be no more than half full Place vials in the rotor Use caution as the lid and rotor could be hot 5 Close the lid 6 Turn the Run mode selector switch to RUN The rotor and vacuum pump will start The display will show the actual chamber temperature 7 Set point parameters can be altered at any time during a run If the run time set point is used at the end of the set time the display will show END Product Service 1 800 522 7658 15 Chapter 4 Using Your CentriVap micro IR 9 Select OFF or STANDBY to terminate operation if the CentriVap micro IR rotor and to release the vacuum Selecting OFF will turn the system off and reset the timer Selecting STANDBY will turn the vacuum pump and rotor off and pause the timer 10 When the evaporation is complete allow the rotor to stop moving lift the lid and remove the samples Use caution as the lid and rotor could b
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