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0210 Split/Splitless Inlet

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1. 1 From inside the oven remove the column and column fitting from the bottom of the inlet 2 Remove the left side cover from the GC 3 From the top of the 6890 GC remove the blue inlet carrier cover or the tray bracket if installed 4 Unclip the heater sensor leads from the connector to the left of the inlet carrier 5 Unscrew the top insert assembly large inlet nut and flow lines on the top of the inlet that has the carrier gas and septum purge lines plumbed to it 6 Raise this assembly up and away from the inlet Purge Top insert assembly Carrier in Figure 210 5 Removing the inlet 8 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Replacement procedures Remove the 1 8 inch Swagelok nut using a 7 16 inch open end wrench Use a Torx T 20 screwdriver to loosen the three captive screws that attach the inlet weldment plate to the top of the inlet carrier Pull the inlet up out of the inlet carrier If necessary you can also slide the insulation sleeve off of the bottom of the inlet Top insert assembly replacement 1 The top insert assembly is replaced as one assembly if required For EPC inlets a Disconnect the pneumatics block from the front of the EPC module one Torx T 10 screw Be careful not to lose the three O rings from the pneumatics module b Follow the split vent flow line back from the pneumatics block and disconnect
2. flow sensor FS V is an on off valve which is turned on to allow flow out of the split vent PV2 is a back pressure regulator controlling the inlet pressure as measured by the pressure sensor PS SPR is a calibrated regulator frit which is used to control the septum purge flow Flow Total flow Septum purge control loop Septum holder Pressure regulator sensor not adjustable Septum purge 3 mL min He Ny AR CH limiting Ey 6 mL min H3 PVI Flow Column head pressure A control loop Proportional sensor valvel Inlet vent flow split 100 mL min Valve open Proportional valve 2 To Detector Figure 210 1 EPC control split mode flow diagram 100 1 split ratio Pulsed split mode For EPC inlets in this configuration the split flow and the column pressure flow are programmed up to a higher value prior to sample injection The 2 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 EPC inlet split ratio remains constant due to electronic control The actual flow rate through the inlet is much higher during the injection period transferring the analytes quickly onto the column which minimizes sample losses that can occur in glass inlet liners After the pulsed time expires the split flow and column flow are returned to the lower flows selected for best chromatography Splitless mode For an EPC inlet during splitless injections PV1 is u
3. 0960 contains a longer ribbon cable to allow you to lay the EPC module on the benchtop for testing Caution Be sure to wear an ESD strap grounded to the 6890 GC chassis while performing this procedure 1 Turn off the main power switch 2 Remove the top plastic pneumatics cover and the detector cover 3 Remove the top rear cover on the GC 4 Disconnect the ribbon cable for the module from the main EPC board You may have to remove the adjacent ribbon cable also 5 Usea Torx T 20 screwdriver to remove the screw from the top of the module and slide the module out of the back of the GC Jun 2001 Inlets 27 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Leak testing the EPC module only 6 Connect one end of the leak test ribbon cable G1530 61370 to the ribbon cable connector on the EPC module and connect the other end to the appropriate connector on the EPC board Reconnect the gas supply and turn on the main power switch Set the pressure to 25 psi and the flow to 60 mL min 7 Lay the EPC module on the lab bench and use an electronic leak detector to locate the leaky component on the module Ribbon cable from leak test kit i To gas supply IS Figure 210 16 Leak testing the EPC module on the lab bench 8 Ifthe leaky component is serviceable such as a vent inlet fitting see diagram of serviceable parts Figure 210 17 replace it Otherwise replace the EPC module 28
4. 210 Split Splitless Inlet The theory and procedures described in this section apply to both the standard 10 to 30 psig split splitless inlet and the high pressure 0 to 100 psig split splitless inlet Theory of operation The split mode of operation is used when small quantities of sample need to be introduced into a capillary column The injected sample is vaporized and then split between the column and an inlet vent Typical split ratios used are 20 1 up to 500 1 where the majority of sample is vented out the inlet split vent The splitless mode of operation is generally used for trace analysis In trace analysis sample splitting would further dilute the amount of analyte entering the column and is not desired In splitless mode nearly all the analyte and solvent enter the column To avoid solvent interferences an initial column temperature of 25 to 30 C below the solvent boiling point is recommended and an inlet purge time of 0 5 to 1 0 minute time be used This splitless mode of operation is best for compounds with a retention index greater than 600 Jun 2001 Inlets 1 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet EPC inlet EPC inlet Safety shutdown mode Proportional valvel closed Proportional valve 2 open On off valve open Split mode operation For an EPC inlet in split mode the proportional valve PV1 is a mass flow controller for the total inlet flow as measured by the
5. artridge 1 2 3 Turn off the inlet and the oven and allow to cool Set all GC flows to zero Remove the pneumatics cover Lift the filter trap assembly form the mounting bracket and unscrew the filter trap assembly Remove the old filter cartridge and O rings and replace them Jun 2001 Inlets 15 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Replacement procedures 6 Reassemble the trap 16 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Replacement procedures Replacing the inlet EPC flow manifold WARNING Before proceeding cool the heated zones then turn offthe main power switch Set pressure flow to 0 0 Follow ESD precautions All EPC inlets and the ECD detector in the 6890 GC use Type 1 flow manifolds 1 Shut off the main gas supply to the manifold and remove the 1 8 inch Swagelok fitting for the gas supply 2 Remove the plastic detector cover and the plastic pneumatics cover 3 Remove the metal RFI shield and the rear top cover on the back of the GC 4 Disconnect the ribbon cable for the module from the main EPC board The adjacent ribbon cable may have to be disconnected as well Figure 210 11 Removing the Type 1 EPC flow manifold Jun 2001 inlets 17 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Replacement procedures 5 Remove the plumbing block from the fr
6. ation of septum liner O ring and lower inlet seal 4 Cap the septum purge vent and the inlet s column fitting Use solid no hole Vespel type ferrules 1 8 inch part no 0100 1372 and 1 16 inch part no 5181 7458 with a 1 8 inch Swagelok nut part no 5180 4103 and a capillary column nut Note As alternate capping devices a 1 8 inch Swagelok cap can be used for the septum purge vent A capillary column nut with a solid piece of wire the size of a paper clip and a 0 5 mm ID graphite ferrule may be used for the inlet column fitting Jun 2001 inlets 19 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Leak testing EPC and manual inlets Manual Septum purge vent EPC Split vent Figure 210 14 Capping the bottom of the inlet and septum purge vent Note Make sure that the carrier gas source pressure is at least 35 psi Carrier source pressure should always be at least 10 psi greater than the desired inlet pressure 20 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Leak testing EPC and manual inlets Performing the leak test EPC inlets Note Be sure to complete all of the preparation steps on pages 20 and 21 before continuing 1 Set the inlet to Split Mode IP Wen es ens ee ee an ts Presss Se a ee ee AT FRONT INLET S SL Mode Type Mode Sp
7. e Be sure to complete all of the preparation steps on pages 18 and 19 before continuing 1 Turn the Total Flow controller counter clockwise to obtain approximately 60 mL min flow at the split vent Use a flow meter to verify this flow rate 2 Turn the column head pressure controller clockwise until the column head pressure reaches 25 psi Column head pressure controller TOTAL FLOW SEPTUM PURGE Flow controller SPLIT SPLITLESS SEPTUM PURGE Oe INLET VENT FWE Septum purge vent Figure 210 15 Manual flow panel 3 Wait approximately 15 seconds for equilibration If pressure cannot be achieved either a very large leak is present in the system or the supply pressure is not high enough 4 Shut off the flow controller by turning it fully clockwise Do not overtighten Use a flow meter to verify that the split flow is off 24 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Leak testing EPC and manual inlets Turn the column head pressure controller an additional half turn clockwise to assure that it will be closed and monitor the column head pressure gauge for 10 minutes e If there is less than 0 5 psi pressure loss approximately 0 05 psi min consider the system leak tight e Ifpressure loss is much greater than 0 5 psi there is a leak that must be found and corrected See Correcting leaks later in this section When the system is considered leak t
8. ent 6890 Gas Chromatograph Service Manual Jun 2001
9. ight the caps may be removed the column reinstalled and the split flow and column pressure may be set Jun 2001 Inlets 25 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Leak testing the EPC module only Leak testing the EPC module only Occasionally to locate small leaks you will need to isolate the EPC module from the inlet weldment and leak test the EPC module separately 1 On the keyboard turn off pressure to the inlet being tested Press Front Inlet or Back Inlet scroll to the Pressure field and press Off Use a Torx T 10 screwdriver to remove the screw in the plumbing block on the front of the module Remove the plumbing block from the EPC module being careful not to lose the O rings between the block and the module Replace the inlet s plumbing block with the leak test block part no G1530 20660 from the leak test kit part no G1530 60960 Make sure you install O rings if needed between the block and the EPC module to create a seal The leak test block is a special fitting that plumbs the carrier gas coming out of the module directly back into the septum purge and split vent flow paths on the module It allows the carrier gas septum purge and split vent line to function normally as if an inlet were present Perform the normal leak test for the EPC inlet as described previously in this section With the inlet removed the internal volume is quite small and a
10. l inlet flow The Purge Control Valve PCV is a three way solenoid valve that switches prior to injection to divert the higher part of the flow across the top of the liner through the PCV and out the inlet split vent At a user specified time after injection the valve switches back to split mode see Split mode to purge remaining sample vapor out of the inlet split vent V2 is a manually controlled back pressure regulator in the split vent path controlling the inlet pressure and thus flow through the column SPR is a manually controlled septum purge regulator used to control the septum purge flow 6 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Manually controlled inlet Total Flow Septum purge Control Septum holder regulator Septum purge 3 mL min Inlet pressure control Inlet Vent Flow split 100 mL min Purge Control Valve PCV To Detector 1 mL min Column Flow Figure 210 4 Manual control splitless mode flow diagram pre run to purge time Jun 2001 Inlets 7 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Replacement procedures Replacement procedures Removing the inlet WARNING Turn off the oven and turn off the heater of the inlet you are replacing and let them cool down Turn off all detector flows Turn off the carrier gas supply pressure then turn off the main power switch and unplug the power cord
11. let nut weldment Top insert assembly Note Locking tab on front of top insert assembly weldment should be inserted into the slot next to the split vent flow line on the inlet plate before tightening the nut ma ON Da Split vent flow line Sy bo So Oblong slot Figure 210 7 Reinstalling the inlet 5 Reinstall the top insert assembly with septum and carrier lines attached Make it finger tight plus a quarter turn with the inlet wrench provided in the ship kit part number 19251 00100 Note Make sure the locking tab fits into the oblong slot on the left side of the inlet weldment plate 6 Tuck the service loop of the septum purge and carrier gas lines under the tabs on the left side of the GC 7 Seat the heater sensor leads into the channel on the inlet carrier 8 Reconnect the heater sensor assembly into the provided connector front or back on the left side of the GC 9 Reinstall the insulated thermal cup and insulation in the GC oven 12 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Replacement procedures 10 Reinstall the blue inlet plastic cover or tray bracket to the top of the inlet area Figure 210 8 Reinstalling the inlet cover or tray bracket Replacing the split vent trap For GCs manufactured before May 1997 the split vent trap part no G1544 80550 or EPC units can be replaced by the Replacement Split Ve
12. lit Split Temp 75 75K Splitless Pressure 25 0 off l Pulsed splitless _ _ Split ratio 100 Split flow 76 6 Tot flow 60 60 Gas saver 2 Configure the column as 0 length Press Config Column lJor Config Column 2 and enter 0 in the first column of the Dim field Se ee ees CONFIG COLUMN 1 OR 2 Length m 0 0 Diameter u 320 LFilm Thickness ___0 00 Inlet Front Detector Front Vacuum Correct off Pres correct Jun 2001 Inlets 21 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Leak testing EPC and manual inlets 3 Set the inlet s Total Flow to 60 mL min Press Front Inlet or Back Inlet and enter 60 in the Tot flow field FRONT INLET S SL Node Split temp 25 off 4 Set the pressure to 25 psi Scroll to Pressure and enter 25 in the Pressure field 5 Wait 10 minutes for pressure equilibration If pressure cannot be achieved either a very large leak is present in the system or the supply pressure is not high enough 6 After 10 minutes turn the inlet pressure Off Press Front Inlet or Back Inlet scroll to the Pressure field and press Off Both the flow controller and the back pressure valves will close Note When the inlet pressure or flow is turned off the safety shutdown feature including the audible alarm is not functional The inlet will not automatically shut down This will pr
13. mode of operation for conservation of split and inlet purge flows when not in use or in between runs A gas saver flow rate and start time can be set independently of normal flow rates being used 4 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Manually controlled inlet Manually controlled inlet Split mode For a manual inlet in split mode V1 is a manually regulated mass flow controller that controls total inlet flow PCV is a three way purge control valve that remains in the normally open position to allow flow out of the split vent V2 is a manually controlled back pressure regulator in the split vent path controlling the inlet pressure and thus flow through the column SPR is a manually controlled septum purge regulator used to control the septum purge flow This flow is set to approximately 3 0 mL minute for operation Total Flow Control Septum purge Septum holder regulator Septum purge Figure 210 3 3 mL min Inlet pressure control Inlet Vent Flow split Zz 100 mL min Purge Control Valve To Detector 1 mL min Column Flow Manual control split mode flow diagram 100 1 split ratio Jun 2001 Inlets 5 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Manually controlled inlet Splitless mode For a manual inlet in splitless mode V1 is a manually regulated mass flow controller that controls tota
14. nsor assembly replacement 1 Follow the Removing the inlet procedure described previously in this section 2 Remove both the bottom reducing nut 1 2 inch and the larger thermal nut 3 4 inch from the bottom of the inlet Be careful not to lose the lower inlet seal and thrust washer inside the reducing nut Note You may want to use a vise to hold the heat sink when removing the thermal nut 3 Slide the aluminum heat sink off of the inlet weldment 4 Remove the Torx T 20 screw and washer from the top of the heat sink and slide the heater sensor elements out of the heat sink 5 Replace the heater sensor assembly being careful not to damage the sensor Replace the washer T 20 screw and reassemble the rest of the inlet Reinstalling the inlet 1 Make sure the heater sensor assembly is installed and the inlet insulation sleeve is in place 2 Installa column nut and blank ferrule on the bottom of the inlet to prevent insulation contamination and place the inlet into the inlet carrier Note Make sure the insulation is properly seated around the inlet and that the heater sensor wiring harness insulation sleeve is tucked under the top inlet plate 3 Retighten the three screws Torx T 20 to secure the top inlet weldment plate to the inlet carrier 4 Reconnect the split vent flow line Jun 2001 Inlets 11 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Replacement procedures Side view of in
15. nt Trap kit part no G1544 60610 The new split vent trap uses a replaceable filter cartridge which is sold in a package of 2 each part no G1544 80530 To replace the filter cartridge in the trap see Replacing the split vent trap filter cartridge below Jun 2001 inlets 13 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Replacement procedures Pe Split vent back weldment Replacement filter kit We NO Filter cartridge ILIZ O rings 2 SZ MA Sy Z Figure 210 9 Replacement split vent filter trap kit part no G1544 60610 Split vent front weldment f WARNING Turn off the oven and turn off the heater of the inlet you are replacing and let them cool down Turn off all detector flows Turn off the carrier gas supply pressure then turn off the main power switch and unplug the power cord 1 Disconnect the spit vent trap line from the inlet assembly 14 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Replacement procedures EPC pneumatics block HPM8 fitting Old trap assembly 1 8 inch OD fitting Figure 210 10 EPC manifold configuration For EPC inlets follow the split vent line from the trap to the HPM8 connector from the pneumatics block on the EPC manifold Disconnect the plastic fitting and remove the old trap assembly and connected plumbing Replacing the split vent trap filter c
16. of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Leak testing the EPC module only CAUTION Aluminum bracket removed for clarity DO NOT completely remove the bracket during valve replacement Aluminum bracket Cen l O rings gt gt N 7 we H 9 Supply fitting O ring Inlet split vent fitting Septum purge fitting Figure 210 17 EPC module serviceable parts Correcting leaks 1 Useanelectronic leak detector to checkall areas of the inlet and plumbing that are potential sources of a leak 2 Tighten loose connections to correct leaks if necessary You may need to repeat the leak test 3 Ifthe pressure drop is now 1 0 or less you can consider the inlet system leak free If the pressure drops faster than the acceptable rate continue to search for leaks and repeat the pressure test Jun 2001 inlets 29 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Leak testing the EPC module only Potential leak points Check the following areas when checking an inlet system for leaks In the oven Make sure the bottom of the inlet is correctly capped On the inlet e Septum e O ring in top of inlet e Lower inlet seal at bottom of inlet At EPC module e Three O rings behind block where the inlet s pneumatic lines enter module e Two O rings for each valve e Septum purge cap 30 of 30 Inlets Agil
17. ont of the manifold one captured Torx T 10 screw Replace the three rubber O rings behind the block if they are worn or damaged 6 Remove the long screw Torx T 20 from the top of the manifold and slide the manifold out of the back of the GC 7 Reinstallation is the reverse of removal Replacing the supply fitting on a Type 1 flow manifold Carrier gas enters an inlet EPC flow manifold through a fritted stainless steel fitting If the frit in this fitting clogs and cannot be cleaned replace the assembly as a whole Remove the two screws attaching the fitting to the manifold replace the O ring behind the fitting and install a new fitting To clean the supply fitting frit use solvents and or an ultrasonic bath then dry the supply fitting with an No or air stream Figure 210 12 Replacing the supply fitting 18 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Leak testing EPC and manual inlets Leak testing EPC and manual inlets Preparation 1 Cool the column to ambient and cool inlets to below 75 C to avoid damage to deactivated glass liners 2 Remove the column from the inlet fitting on the inside of the oven 3 Ifthe quality of the septum the O ring on the glass liner and the lower inlet seal are unknown replace them now Inlet liner Septum O ring 2 3 mm from top Lower inlet seal SO t Washer Reducing nut Figure 210 13 Loc
18. ovide you with unlimited time to locate leaks 22 of 30 Agilent 6890 Gas Chromatograph Service Manual Pressure 25 0 25 0 Total Flow 60 0 60 0 Caen a ae ee he Split Splitless Inlet 210 Leak testing EPC and manual inlets Note the Actual reading on the display and monitor the pressure for 10 minutes You can use the stopwatch feature of the 6890 GC to monitor the time Press Time and then Enter to start timing then toggle between the time and the pressure reading with the Time and the Front Inlet Back Inlet keys e If there is less than 0 5 psi pressure loss approximately 0 05 psi min consider the system leak tight e Ifpressure loss is much greater than 0 5 psi there is a leak that must be found and corrected Note however that you may want to slightly decrease the leak test time based on the internal inlet volume which changes with the liner type used smaller volumes shorter acceptable leak test times See Correcting leaks later in this section e Ifthere is arise in pressure see Forward pressure valve leaks below When the system is considered leak tight the caps may be removed the column reinstalled its dimensions configured at keyboard and the desired pressure and flow rate set Jun 2001 Inlets 23 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Leak testing EPC and manual inlets Performing the leak test manual inlets Not
19. pressure loss of 1 0 psi or less in 10 minutes time is considered to be leak free If there is a leak you will probably need to remove the flow manifold to try to isolate the leak as described in the following Locating leaks on the flow manifold procedure If there is an increase in pressure see the following Forward pressure valve leaks procedure 26 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Leak testing the EPC module only Forward pressure valve leaks Occasionally an increase in pressure rather than a decrease may be observed This is usually due to slight leakage into the module across the forward pressure control proportional valve Although slight leaks of this nature do not create chromatographic problems they may obscure other small leaks that do cause problems by allowing air into the system The valves can leak at about 0 2 mL min and be within specification To check for internal valve leakage when leak testing the EPC module only 1 Remove the supply pressure at the carrier inlet fitting and quickly cap the fitting with a solid 1 8 inch Vespel plug and a Swagelok nut 2 Check the actual pressure on the display and monitor it for 5 minutes Pressure loss should not be greater than 0 5 psi Locating leaks on the flow manifold If the EPC module appears to have a leak you can remove it to locate the leaky component The leak test kit part no G1530 6
20. sed to control the inlet pressure as measured by PS V is an on off valve which is turned off so there is no flow out of the split vent PV2 is turned on at a nominal value so that there is no back pressure on V FS will still be measuring flow but it is no longer used to control PV1 In this configuration the total flow into the inlet is the column flow septum purge flow At the user specified purge time the inlet control is returned to split mode see Figure 210 1 to allow the inlet to be purged Jun 2001 Inlets 3 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet EPC inlet Flow Septum purge limiting Flow Septum holder regulator not frit sensor adjustable Septum purge 3 mL min Pressure sensor PV1 Proportional valve 1 Inlet vent split Valve PV2 closed Proportional valve 2 Safety shutdown mode Proportional valve 1 closed Proportional valve 2 open On off valve open Figure 210 2 EPC control splitless mode flow diagram pre run to purge time Pulsed splitless mode For EPC inlets set to pulsed splitless mode the column head pressure is increased to some selected value and selected time period prior to sample introduction Like the split mode the increased flow through the column during the injection period minimizes sample losses in glass liners Gas saver mode For EPC inlets Gas Saver mode may be used in splitless or split
21. the line from the split vent trap c Remove the carrier and septum purge lines from the left side of the GC For non EPC inlets a Unscrew the top insert assembly large inlet nut and flow lines on the top of the inlet that has the carrier gas and septum purge lines plumbed to it Raise this assembly up and away from the inlet b Follow the split vent flow line back from the pneumatics block attached to the top insert assembly and disconnect the line from the split vent trap c Remove the carrier and septum purge lines from under the plastic tabs on the left side of the GC Use a 7 16 inch wrench to unscrew the split vent flow line nut from the Swagelok fitting at the top of the inlet Use a Torx T 20 screwdriver to loosen the three captive screws that attach the inlet weldment plate to the top of the inlet carrier Jun 2001 Inlets 9 of 30 Agilent 6890 Gas Chromatograph Service Manual 210 Split Splitless Inlet Replacement procedures 4 Pull the inlet up out of the inlet carrier If necessary you can also slide the insulation sleeve off of the bottom of the inlet Captured Torx T 20 screw Upper insulation Torx T 20 A O E Heat sink Thermal nut Lower seal Thrust washer Reducing nut Figure 210 6 Removing the heater sensor assembly 10 of 30 Inlets Jun 2001 Agilent 6890 Gas Chromatograph Service Manual Split Splitless Inlet 210 Replacement procedures Heater se

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