簡易操作マニュアル
Contents
1. 4 2 97 6 6 1 Service Tube Replacement Helium Tank Replacement C gt Helium Tank Replacement OK2. OK Please wait 1 minute 1 Finished purging Water trap Press OK OK Tighten the top nut on the Water trap Increase pressure to normal Press OK 0 12MPa OK Done OK Tube Replacement for CHN Analysis
3. 1000 80 150 C 30 7 6 99 995
4. 4 CE 440 CE 440
5. Benzoic Acid cond cond blank blank STD1 STD1 BC BH BN BN BC BH
6. Re tighten hand purge valve or replace entrance plug Press OK OK Please wait 30 minutes 80 Finished purging the Reduction Tube Press OK OK Replace the END CONNECTER or U tube IMMEDIATELY Press OK
7. 53 7 3 Tube Replacements Combustion and Reduction Tube Replacement 2 Replace Combustion and Heduction Tubes 54 7 4 CO Tube Packing Information CO2 Trap CHN Carbon Dioxide Trap 200 70804
8. Continue SSI 1 1 23 SSI Run Data Entry 1 Cancel 24 3 4 1
9. Sample ID blank for al1 ID Date blank for all Day Month Year Begin Counter no blank for all End Counter no
10. Sample to run xx 15 O 4
11. 2 OK Done OK Tube Replacement for CHN Analysis 300 400
12. 0 12MPa OK 5 Helium Tank Replacement Done OK 40 6 2 Service Tube Replacement Oxygen Tank Replacement C OK Oxygen Tank Replacement CE 440
13. 20 3 3 Run Carbon Hydrogen Nitrogen Enter Data Message text for run series SSI Enter Data 1 ID SSI Run Data Entry 8Start Run SSI plug Carbon Hydrogen Nitrogen Run 21 SSI plug
14. CE 440 450mV ON
15. 59
16. FT 30 40 FT 30 FT 40 2 10 1 2 2 4 2mg 20 4mm 2 9mm no 5mm 2 9mm
17. 0 12MPa OK Done OK Tube Replacement for CHN Analysis CO2 500 80 150C 30 7 5 Tub
18. OK Tube Replacement for CHN Analysis Tube Replacements Combustion Tube Replacement Heplace ombustion Tube OK OK Relieve pressure via entrance plug or hand purge valve Press OK OK
19. 3 STD1 17 P N 6703 0418 6x2 9mm 2
20. 12 OK 3 16 Standby Parameters Leaktest _ He Scrub _ Scrub 02 Scrub E Trap H Trap Comb Tube _Red Tube _ Tube _ Oxygen _ 138 138 138 138 138 138 ON Elapsed Time Comb Temp Red Temp Oven Temp Pressure 00 00 CC CC Cc 22 mmHg Cancel cond blank cond STD1 STD1 10 STD1 10
21. 14 11 Run 6 ID Sealed No Start Run Garbon Hydrogen Nitrogen Run 1 Upen hand purge yalye 2 Hemoye spent capsules from capsule receiver Cancel 3 Upen iniector box cover 4 Install sample wheel mark touching tooth Close coyer and tiqhten 5 Tighten hand purqe yalye 7 Eheck paper in printer He 2
22. Relieve pressure via entrance plug or hand purge valve Press OK OK Remove the END CONNECTOR Comb Red tubesl Press OK 2 OK
23. 50 7 2 Tube Packing Information Combustion Tube CHN Combustion Tube 6703 0514 0240 1225 0240 1118 0240 1147B 0240 1344C 0240 0113 0240 1117C 0240 0092B mm
24. Replace the END CONNECTER or U tubel IMMEDIATELY Press OK 2 OK Done OK Tube Replacement for CHN Analysis 800 1000
25. 15mm 0240 0092B OK Tube Replacement for CHN Analysis 1 48 Tube Replacements Reduction Tube Replacement Heplace Heduction Tube Hemoye he END CONNECTOR Comb Red tubes Press DOK Cancel Heplace Heduction Tube Piess UK Re tighten hand purqe yalye or replace entrance pluq Press UK Please wait 30 minutes Finished purqing the Reduction Tube Press UK Replace the END CONNECTOR or U tubel IMMEDIATELY_ Press UK Done OK OK
26. STANDBY READY CHECK Servicee Bridges C H N eroes Temperatures and Pressures 2 7 Customize Set Automation Type HA 64 Sample Automation SST OK HA 64 Sample Automation SST OK Set Automation Type Manual No Drive Mechanism SAl Single Sample Automaltion SSI Si Using HA Single Sample Using HA PR 2 8
27. 1 5 2 OFF DEDECTOR RESET 3 Customize Set Parameters Oxygen Valve ON during run Combustion Time 0 Purge Time 60 32 Set Parameters 4 a FETE BEFOR ED Run Carbon Hydrogen Nitrogen Sample to run 3 Carbon Hydrogen Nitrogen Run Counter we 126 ho 1129 I130 1133 134 135 _ I136 137 139 140 SW Start Run
28. OK 41 5psig 0 084MPa OK 200psig 1 4MPa 5 OK 42 Oxygen Tank Replacement 0 14MPa OK Done OK Oxygen Tank Replac
29. 1800 COs HzO Ns Reduction Tube Ns Mixing Volume 80C 2 Sample Volume 3 6 TCD Detector HzO TRAP COs TRAP Ns 2 CE 440
30. 30 3 Customize Set Parameters Oxygen Valve ON during run Combustion Time 0 Purge Time 60 44 Set Parameters 4 a FETE BEFOR ED Run Carbon Hydrogen Nitrogen Sample to run 3 Carbon Hydrogen Nitrogen Run I126 EE I129 I130 133 134 135 I136 137 eggmen EE I140 he Start Run OK 3 3 45 Garbon Hydrogen Nitrogen Run 11 Open hand purge valve 2 Remove spent capsules from capsule receiver Cancel 3 Upen injector box coyer 4 Install
31. OK OK Lower the Helium pressure to 10 psig Loosen trap nuts Press OK 0 07MPa OK 58 Replace the Water Trap Tighten 1ower nut only Press OK O O O O O O
32. Print Print nr Iransmit Data Select Output Mode lt Dutput to Printer Transmit Dala Cancel Sand allrecards Select Output Mode Output to Printer Options Send this record only Continue Options Send all records Select Output Mode Transmit Data 31 5 1 RM OFF 0 1 FUNCTION SYSTEM ON
33. O O O O Re tighten hand purge valve or replace entrance plug Press OK OK Please wait 80 minutes 80 Finished purging the Reduction Tube Press OK OK
34. ON 450mV SYSTEM FUNCTION SYSTEM DRDECTOR RESET DEDECTOR RESET 5 1 OFF DEDECTOR RESET
35. ON OFF 2 1 OPEN 2MPa 2MPa 6 0 12 0 01MPa 2 2 OPEN 2MPa 2MPa 6 0 14 0 01MPa
36. OFF 32 5 2 OFF 32 5 3 0M 0 6 CN CS ea 34 5 4 ON 093NR80S2R2NNSSC2REH0S 8037482RE208S 33 35 5 OFF tii 37 6 No 38 920 38 KN MSBMNMRLS08R00203GRNG2M2080228029220500246 41 3 ER 44 7 CHN ki 47 2 Oakeai2Ked325RE2SRAB2223CS 0 RSS 48 EO EN NN RN NR a 51 NN 54 0 NSRNNSSR 55 209 ER 57 936 SS a 59 1 1 1 CE 440
37. CHN CHN 113 0021 2 29 24 9F TEL 03 3946 4993 FAX 03 3946 4983 523 0893 294 YP1 4F TEL 0748 31 3942 FAX 0748 31 3943 info systems eng coJD Web http www systems eng coJD 1 2
38. 3 1 Customize Set Automation Type SSI Single Sample Using HA OK Set Automatipn Type Manual No Drive Mechanism SAl Single Sample Automation Cancel HA 54 Sample Automation SSI 3 2 Customize Set Parameters OK Set Parameters Printer Expanded Heading DK fx30 tmes sianall Laser Printer Cancel Laser Printer LE rH Runs per page 5 Lines per page 56 Communications Balance Combustion Time len 0 120 secl Theory Calculation per Run Purge Time so Expanded Reporting EH 0 90 secl Stop Run at any WARNING Profile Scale 5 Imysl SNB 130 Use Hegression
39. Customize Set Parameters OK Set Parameters Printer Expanded Heading fx30 times sianall Hk Laser Printer Cancel Laser Printer LE Runs per page 5 H CN Lines per page 56 ro Communications None Balance iDxygen Valve ON during runi Theory Calculation per Run Combustion Time 0 120 secl 50 Purge Time ED Expanded Heporting EE EEE I0 90 secl Stop Hun at any WARNING Profile Scal mW SNB 30 Use Regression Er 2 9 Run Carbon Hydrogen Nitrogen Is this a new run Yes Carbon Hydrogen Nitrogen Run
40. BN K ID STD2 18 2 11 Run Overnight Standby Start Overnight Standby Mode Pr ol Start Overnight Standby Mode I 2 12 CE 440 CE 490 PC 19 3 SSI Single Sample Using HA 64 HA Horizontal Automation 1
41. 2 4cm mm 3 5cm mm 4 5cm mm 1cm O O 51
42. SSI 26 4 CSV PC CE 440 Calculate Recalculate data and Statistics CE 440 Elemental analyser DEMONSTRATION RUN File Run EE Service Customize Help Recalculate data and Statistics BTU b Dry Dry Ash Free HG N G C H C N Ratios CC H H N N 0 0 S S Ratigs Empirical Formula CE 440 Elemental Ana lvzer Exeter Analytical Inc Recalculate Data Statistics Search Parameters Ok Sample ID flankforal Cancel Date fblank for am Day Month Begin counter no blank for al End counter no lt Fresh Data Hecalculated Data 27
43. SS 1 Next 8s 1 SSTI 1 ID 3 3 SSI 25 SSI SSI SSI SSI SSI
44. Helium Tank Replacement 38 CE 440 OK Helium Tank Replacement 5psig 0 084MPa OK Helium Tank Replacement 200psig 1 4MPa 5 OK 39 Helium Tank Replacement
45. OK 3 8 33 Carbon Hydrogen Nitrogen Run 1 Open hand purge valve 2 Remove spent capsules from capsule receiver Cancel 3 Open injector box coyer 4 Install sample wheel mark touchinn tooth 5 Close coyer and tighten 5 Tighten hand purge yalve 7 Eheck paper in printer DEDECTOR RESET 1 5 3 OFF 0 12 0 01MPa HH C I 30
46. SS1 plug 22 SST plug Continue Carbon Hydrogen Nitrogen Run 2 Load sample and install plug SSI plug SSI plug
47. Weight 1 E ID 4 5 STD1 STD1 Sealed No ID STD1 CE 440 5 DD Carbon Hydrogen Nitrogen Oxygen Sulfur STD1 Fe 71 09 6 71 10 36 11 84 Acetanilide STD2 9 68 85 4 95 26 20 Benzoic acid s STD3 47 40 5 47 13 82 15 82 s Benzylthiuronium chloride STD4 Ail 29 99 5 03 11 66 26 63 26 68 es STD5 75 99 12 79 11 22 Stearic acid ID
48. Exit Sample ID Blanks K factors Weight Chart Statistics Regression 6 4 1 CSV Export Export Data Type 29 Alternative Exports Export as CSV e g for Excel Option Current Record Contimue CSV
49. 2 3 DETECTOR RESET 2 4 PC CE 440 Run Stop Overnight Standby H C 1 1 ON 2 5 2 GE 440 ElEmErntal nalyser DEMONSTRgTIION RUN Stop Overtight Standby CE 440 Elemental Analyzer Exeter Analytical Inc COMBUSTTON 980 C REDUCTION 620 C 2
50. Service Tube Replacement CHN Analysis End Tube Replacement for CHN Analy E Tube Replacements Helium Scrubber Replacement Oxygen Scrubber Replacement CO2 Trap Replacement Water Trap Replacement Combustion Tube Replacement Reduction Tube Replacement Combustion and Reduction Tube Replacement Tube Packing Information Combustion Tube Reduction Tube CO2 Trap Water Trap Helium and Oxygen Scrubber 47 7 1
51. 12 4 Run Carbon Hydrogen Nitrogen Is this a new run Yes 5 Carbon Hydrogen Nitrogen Run Enter Data Message text for run seriesl Carbon Hydrogen Nitrogen Run Enter the Ks and blanks automatically Cancel Messaqe text for run series Delay Start of Hun 2 6 ISample to run xx 1 ll Garbon Hydroeen Nitrogen Run Start Run Samples to run 10 Start Aun Cancel Eounterlwreight ID Sealed 129 2000 0 cond No Insert Row 130 0 0 blank No 131 2000 0 cond No 132 20120 STD1 No Delete How 133 1997 0 STD1 No 134 2023 0 sample1 No 135 2017 0 sample2 No 136 2009 0 sample3 No 137 1994 0 sample4 No 138 m No 139 140 141 142 143 144 145 146 147 148 EE oon nn ewlm n 10 l oon nn ewl
52. OK Garbon Hydrogen Nitrogen Run SSI 3 Garbon Hydrogen Nitrogen Run 11 BC BH BN BC 200 BH 1000 BN 200 3
53. Analysis CHN CNS O Data Fresh Data Recalculated Data OK Recalculate Data amp Statistics There are 7 runs that meet the following criteria Thursday September 18 2008 to Thursday September 18 2008 Results From nn e Cancel Analysis Earbon Hydrogen Nitrogen 7 Search Results Cancel 28 Recalculate Data amp Statistics gt gt lt lt
54. 52 Remove the END CONNECTOR Comb Red tubesl Press OK 2 OK Replace Combustion Tube Press OK O OK
55. 1 3 CE 440 1 3mg 500mg gt 1 A G IT Pressure Sonple Wolune Tronsducer Conbustion Feduction gt Mixin yolume cc LJ 1 Ce Ce 9 9 He He SUPPLY SUPPLY LE 440 FLHw_ SCHEMATIC Combustion Tube
56. 1 2 5mm 2 2mg 20 1 59 64 3
57. Replace Reduction Tube Press OK O OK 49 O O O O
58. Tube Packing Information Reduction Tube CHN Heduction Tube Silyer Gauze Huartz Wool Copper Cuprin 0240 1573 0240 1118 15mm 0240 1362 8cm
59. OK mExport as CSV File File will be exported as CSV file Please enter file narme withnut file extension Export fle name CE 440 X 440W95 Exportdata Alternative Rxports Export as CSV e g for Exce Option All Records Continue CSV Alternative Exports Export as Displayed on Screen Option Current Record Contimue Alternative Exports Export as Displayed on Screen Option All Records Continue 30 4 2
60. O O CO2 CO2 OK Please wait 1 minute CO2 1 Finished purging Carbon Dioxide trap Press OK OK 56 Tighten the top nut on the Carbon Dioxide trap Increase pressure to normal Press OK CO2
61. 1 6 3 4mm 6 10mesh 50g 3 200 200 91804 0 7 1 7mm 10 24mesh 50g 3 800 0240 1217 0240 1118 1cm 5mm 12cm mm 5cm 5mm 1cm CO2 OK Tube Replacement for CHN Analysis 55 Tube Replacements CO2 Trap Replacement Heplace arbon Dioxide Trap Lower the Helium newe te10 psig Loosen ap nts Press OK 5 Replace the arbon Dioxide Trap Tiqhten lower n
62. 3 Customize Set Parameters Oxygen Valve ON during run Combustion Time 0 Purge Time 60 Set Parameters Printer Expanded Heading fx30 tmes siqnall Laser Printer CE Runs per page 5 CN Lines per page 56 Communications None Balance Daen Valye ON during run 0 120 secl Theory Calculation per Run Combustion Time Purge Time Expanded Reporting 0 90 secl Stop Hun at any WARNING SNB Use Hegression Profile Scale sl Run Carbon Hydrogen Nitrogen Sample to run 3 34 Carbon Hydrogen Nitrogen Run Start Hun Samples to run 3 Eounterlwreight IID H23 ml Insert Row Delete Row Start Run OK 3 3 Carbon Hydrogen
63. Enter Data Carbon Hydrogen Nitrogen Run Enter the Ks and blanks automatically2 Messaqe text for run series Cancel Delay Start of Run Weight Enter Tab 0 0 ID blank Sealed No 2 3 Start Run 5 Carbon Hydrogen Nitrogen Run Samples to run 3 Cancel Counter Weight 124 125 127 128 129 130 131 132 ooNnN nn wm Dn 133 134 135 136 137 138 139 140 141 142 Start Run 123 0 0 Insert Row A 126 Delete Row
64. sample wheel mark touching tooth 5 Close coyer and tighten 6 Tighten hand purge yalve 7 Eheck paper in printer DEDECTOR RESET 1 4 CE 440 10 FT 46 7 CHN CHN
65. EA CE 440F CHN O S Elemental Analyzer 5 minutes leads to hi throughput Low consumables cost Wide range of applicat Organic amp inorganic mVolatiles IE 1 Ceanography Systems Engineering NO SN 38888 000 282 4 NR ER NC Ns 4 2 EESCTD EE LE Ek kL SE EE 4 ISANSRNSRRSSO RS 5 2 GE 440 NN a 7 NUKI 7 2 NE NSRNISIRSNNSSSRIREANIRURRNRINSSNMSSS SRSAeDS 7 7 NARI IA ER DE NN NN 7 5 SS 8 8 LR 8 SSR RRBRRRSRSSRERSRSRNERRRUESR 9 2 8 2 RR RNR 9 LTC TOME SR SE 9 OE NN A NS 12 RTD Nn Ia CN Oo Otro ee 19 212 SS SE lt 19 3 SSI Single Sample Using HA uu 20 EE 20 S32 OE 20 SE 21 3 4 i 25 4 2 00 NO 27 2 Ch 29 A RE SS CN GNA RN ES 2 31 NE 32 5 1
66. Nitrogen Run 1 Open hand purge yalye 2 Hemoye spent capsules from capsule receiver Cancel 3 Upen injector box coyer 4 Install sample wheel mark touching tooth Close coyer and tighten 6 Tighten hand purge yalve 7 Eheck paper in printer DEDECTOR RESET 1 5 4 OFF 0 12 0 01MPa HH C 1I 2 3 Customize Set Parameters Oxygen Valve 35 ON during ru
67. e Packing Information Water Trap 57 200 91804 0 7 1 7mm 10 24mesh 50g 8 800 0240 1217 0240 1118 1cm 5mm 17cm 5mm 1cm OK Tube Replacement for CHN Analysis Tube Replacements Water Trap Replacement Heplace Water Trap
68. ement 43 6 3 1 2 OFF SYSTEM FUNCTION SYSTREM ON SYSTEM FUNCTION SYSTEM DEDECTOR RESET 0 12 0 01MPa H C I
69. mn J 7 Run 1 Weight 2000 0 r g ID cond conditioner Sealed 8 Run 92 No 0 0 Weight Enter ID Tab blank Sealed No 9 Run 3 Run 1 10 Run 4 5
70. n Combustion Time 0 Purge Time 60 Set Parameters ET ET EO DT Run Carbon Hydrogen Nitrogen Sample to run 8 Garbon Hydrogen Nitrogen Run 123 90 124 126 127 130 1 136 ho Start Run OK 3 8 36 Garbon Hydrogen Nitrogen Run 1 Upen hand purqe yalye 2 Remove spent capsules from capsule receiver Cancel 3 Upen iniector box cover 4 Install sample wheel mark touching tooth 5 Close coyer and tighten 6 Tighten hand purqe yalye 7 Eheck paper in printer DEDECTOR RESET 1 5 5 OFF
71. ut only Press UK Please wait 1 minute Finished purqing arbon Dioxide trap Press UK Tiqhten the top nut on the arbon Dioxide trap Increase pressure to normal Press DOK Done OK OK Lower the Helium pressure to 10 psig Loosen trap nuts Press OK 0 07MPa OK Replace the Carbon Dioxide Trap Tighten 1ower nut only Press OK CO2 O CO2 O O O
Download Pdf Manuals
Related Search