CHIRALPAK IB-3 カラム取扱説明書
Contents
1. gt e 1 0 ml min 30 2 s 48 es n 2 90 10 v v 1 0 ml min 60 4 6 mm2. MTBE MTBE 2 1 lt 5 lt 20 2 1 70 30 50 50 70 30 100 0 100 0 v v V 95 5 80 20 85 15 80 20 100 0 v v V 0 100 0 100 0 1
3. MITBE THF 1 l 42 TBES CH CL 80 20 80 20 0 98 2 50 50 v v v 99 1 99 1 90 10 0 0 100 0 85 15 v v v 50 50 50 50 0 60 40 0 60 40 0 100 n iso n
4. 90 10 0 100 pH gt 9 0 pH7 0 25 0 5um HPLC 0 5ml min 2
5. 0 EDA TFA EDA EHMA DEA I 2 BI 0 0 1 0 5 0 5
6. 4 6mm 60 40 vV y CHIRALCEL CHIRALPAK CROWNPAK CPI 108 8230 2 18 1 TEL 03 6711 8222 FAX 03 6711 8228 530 0001 3 4 5 TEL 06 6342 6161 FAX 06 6342 6168 _4
7. 1 n 2 90 10 v v A DEA pH 9 0 _ 60 40 DEA NHHC0 CH CN MeO0H EtOH TPA THF 73002 0 7 50 lt 100mM 100mM KPF NaPF CHIRALPAK IB 3 p
8. nie HPLC pH 7 0 25C gt 0120 780 104 gt 73002 0 7
9. gt CHIRALPAK IB 3 HPLC MTBE CHIRALPAK IB 3 THF 2 A 1 2
10. 00 0 100 0 100 2 THF 2 THF UV RI ELSD UV B EDA EtNA DEA 0 1 73002 0 7 EDA EtNA DEA
11. Al CE Te PestSolutlon oF YOU CHIRALPAK IB 3 Cellulose tris 3 5 dimethy lpheny lcarbamate 9 Um 5 oo R O n 2 90 10 v v mmS OR 3 silica gel x 4 6 x 50 mm 2 1 x 150 mm 4 6 x 100 mm 2 1 x 250 mm 4 6 x 150 mm 4 6 x 250 mm I AER CBC Ns Co 908 Ket ia EANEI TD RRNA UE 0 40C 5 40C pH 7 5 25C pH 7
12. H 2 0 100mM KPF NaPF THIFT 2 0 5Hm 60 40 v v
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