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2-11-13J

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2. ppm 5 5 4 TSKprecolumn IC Conc A 3 6 6 1 6 1 1 TSKgel IC Anion PW TSKgel IC Anion PWx TSKgel IC Anion PWxr PEEK TSKgel IC Cation TSKguardcolumn IC A TSKguardcolumn IC AS TSKguardcolumn IC C TSKgel IC Anion SW TSKgel IC Cation SW
3. TSKgelIC Anion SW TSKgelIC Cation SW TSKgel IC Cation 1 I HR TSKegel IC Anion PWxr TSKgel IC Anion PW TSKguardcolumn IC Cation I I HR TSKguardcolumn IC AS TSKguardcolumn IC A TSKgel IC Anion SW TSKgel IC Cation SW TSKgel IC Cation 1 Il HR TSKgeuardcolumn IC Cation 1 I1 HR a 12 3 0 5 pH 8 5 TSKgel IC Anion PWxr 4
4. 15 TSKegel IC Anion SW TSKgel IC Cation SW
5. TSKgel IC Cation HR 1 2 ij TSKguardcolumn IC A TSKgel IC Anion PW TSKgel IC Anion SW TSKguardcolumn IC AS TSKgel IC Anion PW TSKgel IC Anion SW TSKguardcolumn IC C TSKgel IC Cation TSKgel IC Cation SW TSKguardcolumn IC Cation I I HR TSKgel IC Cation 1 HR 4 TSKgel IC Anion PWx SUS 5 E TSKgel IC Cation I I HR gt O mm a TSKgel IC Anion PWx PEEK 4 6 mml D X 3 5 cm FLOWL TSKqgel IC Anion PWx PEEK 4
6. TSKgel IC Anion PWxr TSKgel IC Anion PWxr PEEK TSKgel IC Anion PW TSKgel IC Anion SW TSKguardcolumn IC AS TSKguardcolumn IC A TSKgel IC Cation TSKgel IC Cation SW TSKgelIC Cation 1 Il HR TSKgelIC Cation TSKgel IC Anion PWxr TSKgel IC Anion PWxL PEEK TSKgel IC Anion PW TSKguardcolumn IC Cation I Il HR TSKguardcolumn IC AS TSKguardcolumn IC A TSKguardcolumn IC C TSKgel IC Anion SW TSKeel IC Caton SW 1 1 2 ooo 1 3 FPPPPPPPPTTPPCTPLCPPLLPPPPPLPTITP 2 4 PPPPPPPPPPPPPPPFTTPPPPPPPPPPYTYTPPPPPTTPFPCPPPLTTYYYYPP 4 5 5 6 PPPPPPPPPPPPPPTPFPTPPPPPPPPPPYYYPPPPPPTTPFPPPPFTLTPTYYYYPP 7 7 PODCPLCLPCPCPLPPLPLPLPEPLCPUCPPPCPCCCLLCLCLECCCCCLLLLLLEL 8 8 FPPPPPPPPPTPPTPTPPCPPPPPPPPPPPPPPPPPPPTCPPLPPLPPPPYYPPLPYPPYT 9 9 PPPPFPPPFPPPPTTPPFTYPPYPPPPPPPPPPPPTPPFPPLLPPC
7. 0 7 2 pH pH TSKgel IC Anion PW TSKgel IC Anion PWx TSKgel IC Anion PWx PEEK TSKgel IC Cation TSKguardcolumn IC A TSKguardcolumn IC AS TSKguardcolumn 1C C PT PF pH 2 0 12 0 TSKgel IC Cation I HR TSKguardcolumn IC Cation 1 HR esseseeeeeese pH 2 0 10 0 TSKgel IC Anion SW TSKgel IC Cation SW eee pH 2 0 7 5 pH TSKgel IC Anion SW TSKgel IC Caton SW pH 7 5 TSKgel IC Anion PWx TSKgel IC Caion 1 II HR
8. 7 0 MPa 9 TSKgel IC Anion PW TSKgel IC Anion PWxr TSKgel IC Anion PWxr PEEK TSKgel IC Cation TSKguardcolumn IC A TSKguardcolumn IC AS TSKeuardcolumn Or OE 60 TSKgel 1IC Anion SW TSKgel 1IC Cation SW PPPPCLCCCCCPLLLPPKTEPPPPPPYYEPPLPPP 45 C TSKgel IC Cation 1 Il HR TSKguardcolumn IC Cation 11 HR iASS RN tts ei 40 10 10 1 1 0 mL min TSKgel IC Anion PW TSKgel IC Anion PWx TSKgel IC Anion PWx PEEK TSKgel IC Anion SW
9. a b 1 0 mL min c d Nit oe 5 4 3 1 3 2 NPR 0014594 0 45 m lt a a b TSKqguardcolumn IC A TSKguardcolumn IC AS TSKguardcolumn IC Cation I I HR 3 1 TSKgel IC Cation I I HR OO
10. 4 B e e e e e e e e
11. 1 TSKgel IC Cation 1 II HR TSKguardcolumn IC Cation 1 II HR 1 100 0 8 mL min 40 5 6 1 2 15 30 7 7 1 1
12. 47 2 rw1 Datn 6 05 32 1 dd 97X9 JHq4d 9eX9 SHHdd Ad UOIHV OI IS8ySL 0T08T00 6008T00 SnS 6X9 AdFUOIHV OI INASL e9100 1 2 rw1 Daun 6 05 AAFEN AULLENE Z lt GX9 Md UOUV OI INSL Z889000 O7 22 m3 X TOUU 7 2 7 6 2 TsKgel IC Anion PW TsKgel IC Anion PWxr TSKgel IC Anion PWxr PEEK F CI NOs Br PO SOZ TSKgel IC Anion SW SCN S2032 BrOs TSKgel IC Cation TSKgel IC Cation SW RAN RaN R
13. TSKgel IC Cation TSKgel IC Cation SW gt TSKguardcolumn IC C 3 2 5 5 5 5 1 0 45 m 5 5 2 ODS TSK Separation Report No 21 5 5 3 1 100 ppm
14. pH 2 0 7 3 TSKgel IC Anion SW TSKgel IC Cation SW ee 0vol 100 vol TSKgel IC Anion PW TSKgel IC Anion PWx TSKgel IC Anion PWx PEEK TSKguardcolumn IC A TSKguardcolumn IC AS ee 20vol TSKeel IC Cation I I HR TSKguardcolumn IC Cation I HR SRE EE RE EE SRE EERIE TSKgelIC Cation TSKeuardcolumn IC C ieee 10vol TSKgel IC Anion SW TSKgel IC Cation SW 7 4 1
15. 2 0 5 zm 3 4 pH pH 5 pH pH pH 9 0 8 8 1 8 2
16. 3 0 5 pH 8 5 TSKgel IC Anion PW TSKguardcolumn IC AS TSKguardcolumn IC A 2 mmol L TSKgel IC Cation TSKguardcolumn IC C 15
17. 5 1 10h As b a As 12 12 1 0 5 mol L 5 3 13 13 1 4 TSKgel
18. pH 8 5 IC Anion PW 360 mg 360 mg TSKgel 500 mg 575 mg IC Anion PWxr 5 0g 5 0g TSKgel 300 mg 350 mg IC Anion PWxr PEEK 120 mL 40 mL 30 mL 30 mL 1000 mL TSKgelIC Anion PWxr TSKgel IC Anion PWxr PEEK TSKgel pH 3 2 IC Anion SW 2 0 mmol L 1mol LKOH pH 3 2 TSKgel IC Cation TSKgel IC Cation SW TSKgel IC Cation I Il HR 2 mmol L HNOs 20 mmol L HNOs CHsCN 7 3 v v 2 mmol L HNOs 5 TSKgel IC Anion PW TSKgel IC Anion PWxr SO4 TSKgel IC Anion PWxr PEEK TSKgel IC Anion SW CT TSKgel IC Cation Nar TSKgel IC Cation SW C4Hs 4N TSKgel IC CationI I HR Ir 13 2 2008E 12mL min TSKgel IC Cation I I HR 0 8mL min 100zL 35 TSKgelIC Cation 1 II HR 40 6 mmLD J X cm TP column 0006837 TSKgel IC Anion PW 4 6X5 1100 0 9 1 5 0014463 TSKgelIC Anion PWxr 4 6X3 5 1000 0 8 1 5 0018009 TSKgel IC Anion PWxr PEEK 4 6X3 5 1000 0 8 1 5 0018010 TSKgel IC Anion PWxr PEEK 4 6X7 5 2000 0 8 1 5 0006839 TSKgelIC Anion SW 4
19. 1 4 ox9T T OHeO OI 09pIENIYSL 0 6 EA DeIOVN TT IOW GO T g8498T00 1T IOCm K ts T b9 2 0 0 2 4 SX9T DDI 09pIENIYSL 6 TZ000 7 2 rw 1 Datn g 08 452 1 Xn TX0 SV OI 0ODTenSYSL 8069I00 4 rw 1 Dar e 06 4 52 1 SX9T VOI Tnn OODTenSYSL STZ000 47 rwT be 0T lt 1 UA ELA EC NE SS 0TX9 AH II T noe OI ISYSL 2298I00 ja 7 K Il98AI 8 bauu GT 0 G 0 2 lt 9X9 AS uOHg OI ISSYSL SGO8000 1 IOt i T bau 2 FgT TY 4 lt 9X9 uoneO OI ISYSL IT000 sa 17 zx 38ArT 8 Daur T0 0 URUK NL GAELEL XIT MS UOUY II PIASL 6689000
20. 6X5 1400 0 5 1 1 0007171 TSKgelIC Cation 4 6X5 1400 1 0 1 8 0008055 TSKgelIC Cation SW 4 6X5 2000 1 2 2 0 0018677 TSKgel IC Cation1 l HR 4 6X10 4000 0 9 1 4 13 4 2 2 14 HLC TSK GEL TSKgel TSKgel SuperMultipore BioAssist Enantio PStQuick
21. Enviropak TOYOPEARL ToyoScreen TOYOPEARL GigaCap TOYOPEARL MegaCap TOYOPEARLPAK TOYOPAK TOSOH 03 5427 5180 105 8623 3 8 2 G 06 6209 1948 541 0043 4 4 9 G 052 211 5730 460 0003 1 17 13 0120 17 1200 252 1123 2743 1 Printed in Japan T1008 500
22. TSKguardcolumn IC A TSKguardcolumn IC AS 100 mmol L 50 mL TSKgel IC Cation TSKgel IC Cation SW TSKguardcolumn IC C YT ET 100 mmol L 50 mL TSKgel IC Cation Il HR TSKguardcolumn IC Cation I Il HR TTT 10 mmol L 50 mL 10 2 6 3 11 INSPECTION DATA 11 1 Injection 4 N 5 54 Ve Wrz Ve min Wiz mmn h N 11 2 Ve Injection
23. 6 mml D X 7 5 cm FLOWL TSKgel IC Anion PW TSKgel IC Anion SW TSKgel IC Cation TSKqgel IC Cation SW LFLow 2 5 5 1 TSKgel IC Anion PWs TSKgel IC Cation 1 1 HR 1 16 TSKgel IC Anion PWx PEEK 1 16 1 4 28UNF 5 2 2 FLOW 5 3
24. Rev CO030000 TSKgel IC Anion PWx TSKgel IC Anion PW TSKgel IC Anion SW TSKgel IC Cation I I HR TSKgel IC Cation TSKgel IC Cation SW TOSOH
25. YPPPYPPYYYYYT TP 10 10 PPPPPPPPPTPPPTPPPYPLPPPPPPPPPPPYTTP 10 11 eseeeeeeeeeeseeeeeeeees eseeee 11 12 POUPPPCPPPPPTTTPCLPLLPPLPLPLLLLLTPTIYT 12 13 wisenenioss sess erika ovinas soces esis 12 14 14 1 2010 7 2004 4 TSK GEL IC E ta 2 1 oe 1 INSPECTION DATA 1 4 rwT Da 0T lt gt gt 47 T IOWU ET 6 0

2-11-13J

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