User Manual - Dorset Environmental Science Centre
Contents
1. DORSET ENVIRONMENTAL SCIENCE CENTRE User Guide For the Collection and Submission of Water Samples Ministry of Environment Chemistry Laboratory Dorset Ontario Peter Sutey 1 Don Evans 1 Ron Xu 1 Jim Rusak 1 Vicki Jackson 2 Christiane Masters 2 Cathy Thomson 2 1 Ontario Ministry of Environment 1026 Bellwood Acres Road Dorset Ontario POA 1E0 2 District of Muskoka 21 Pine Street Bracebridge Ontario P1L 1N3 February 2011 Version 2011 1 1 www desc ca Table of Contents Introduction A Basic instructions for obtaining water samples for chemical analysis B Detailed Instructions for Completing the Sample Submission and Field Data Forms Lake Samples Stream Samples Precipitation Samples Laboratory Samples pour 5 Field Data Explanations and Codes 6 Submission Check List 7 Parameter perishability limits 8 Minimum Volumes required for analysis 9 Partial List of Special Study IDs February 2010 10 List of valid LIMS Program Codes 11 List of LIMS Products and Parent Products 12 Collection Bottles 13 Glossary of Terms 14 Contacts 15 Revision History 16 Notes Introduction This guide is intended for use mainly by scientists supervisors and field sampling crews submitting samples to the Dorset Chemistry laboratory All groups intending to send samples to the Dorset Chemistry lab should obtain a test load the number of samples and type of sample allowed and a2. 49 9 62 25 Sep 2009 21 00 Sample has sat for extended period o 49 9 62 26 Sep 2009 22 00 Sample has sat for extended period 49 9 62 29 Sep 2009 01 00 Sample has sat for extended period 49 9 62 30 Sep 2009 02 00 Sample has sat for extended period 49 9 62 01 Oct 2009 03 00 Sample has sat for extended period of time use with caution 49 9 62 02 Oct 2009 04 00 Sample has sat for extended period o 49 9 62 03 Oct 2009 05 00 Sample has sat for extended period o 4 Laboratory Samples Date Submitted 21 Oct 2009 Sampled by C T Form Type LAB Submitted by DORSET LAB Sub Description DORSET LAB Client ID 4 3 7 6 2 WHMIS Program Code of of of 3 of 3 o 1 HEALTH 0 FLAMMABILITY 0 Client Contact REACTIVITY 0 Name Johnny Su PROTECTION 0 Phone LAB SAMPLE NUMBER 705 766 1291 Address DESC Bellwood Acres Rd Dorset POA 1E0 DATE dd mmm yyyy TIME STATION hh mm POTENTIAL HAZARD HEALTH FIELD SAMPLE IDS All LDESC loom _ or bonos 21 Oct 2009 14 55 01 1 3147 MMNO3374 DORCSI3422 somme looms monsur 21 Oct 2009 14 55 C 01A 2 ANION3147 MMNO3374 DORCSI3422 zone looms _ 21 Oct 2009 14 55 C 01A 3 ANION3147 MMNO3374 DORCSI3422 looms nns mese bonos 21 Oct 2009 14 55 C 01A 4 ANION3147 MMNO3374 DORCSI3422 PARENT PRODUCT PRODUCT 5
3. Field Data Explanations and Codes SPECIAL STUDY_ID SAMPLE TYPE SDESC SDEPTH BGDEPTH WDEPTH WLAYER TEMP NUMERIC integer Project ID assigned by Database Manager NUMERIC integer Sample Type collection method Method Origin of Water 10 profile lakes 11 grab sample single depth lakes streams 12 depth composite lakes 13 time proportional composite streams 14 flow proportional composite streams 61 wet only collector precip 62 bulk collector precip 63 on ground snow precip 71 groundwater sample groundwater CHARACTER sample description Information about the sample that may help people reviewing the data interpret the results e g pollen in sample Indicate if a sample comes to the lab fixed here Maximum 256 characters to be entered including spaces All on one line NUMERIC integer sample depth in m or top of composite for depth composite SAMPLE TYPE 12 samples bottom depth in m of composite samples SAMPLE TYPE 12 NUMERIC integer or decimal depth in m of water at sample location NUMERIC integer identifier for Lake Layer sampled 1 whole lake composite spring and fall turnover epilimnion metalimnion hypolimnion euphotic zone surface to 2 x Secchi grab Kemmerer etc use with type 11 general layer 0 5 m composite etc Wh NUMERIC integer decimal water temperature in degrees Celsius SAMPLE GEAR TYPE SECCHI
4. pHalk3042 pH PH pH Gran Alkalinity ALKTI mg L Total Alkalinity ALKT mg L 3025 True Colour COLTR TCU Cond3024 Conductivity at 25 C COND25 ms em Ammno3374 Ammonia Ammonium NNHTUR ug L Nitrate Nitrite NNOTUR ug L Dorcsi3422 Dissolved Organic Carbon DOC mg L Silicates SIO3UR mg L Tp3036 Total Phosphorous PPUTI PPUT2 ug L Carb3028 Dissolved Inorganic DIC mg L Carbon also known as Total Inorganic Carbon Anion3147 Chloride CLIDUR mg L Sulphate SSO4UR mg L Cat3249 Calcium CAUT mg L Magnesium MGUT mg L Sodium NAUT mg L Potassium KKUT mg L Dtkn3424 Total Kjeldahl Nitrogen TKN ug L Ammonia is by far the largest fraction of the two components of NNHTUR in shield lakes Rexdale Product Common Name Oracle Name Units Code Dchl3169 Chlorophyll A CHLRAC mg L Corrected CHLRAT mg L Chlorophyll A Total Met3386 Aluminum ALUT ug L Barium BAUT ug L Beryllium BEUT ug L Calcium CAUT mg L Cadmium CDUT ug L Cobalt COUT ug L Chromium CRUT ug L Copper CUUT ug L Iron FEUT ug L Magnesium MGUT mg L Manganese MNUT ug L Molybdenum MOUT ug L Nickel NIUT ug L Lead PBUT ug L Strontium SRUT ug L Titanium TIUT ug L Vanadium VVUT ug L Zinc ZNUT ug L Hardness HARDT mg L Products Matrix Description Products Included DRCCHLO WS Dorset Chlorophyll Dchl3169 DRCLKA WS Dorset A Lakes Phalk3042 3025 Cond3024 Ammno3374 Dorcsi3422 Tp3036 Carb3028 Anion3147 Cat3249 D
5. Bill Keller 76 Lake of the Woods Tributary Andrew Paterson Ron Ingram 77 University of Guelph mobile bulk depositions Jenny Winter Bahram 79 Dorset Temporal Streams Benthos Chris Jones Jim Rusak 80 Sudbury Temporal Streams Benthos Chris Jones Chantal Sarrazin Delay 81 Far North Sampling New 2009 Chris Jones Andrew Paterson 10 List of valid LIMS Program Study codes 0170701 Dorset Lakes Dr Andrew Paterson Ron Ingram 0170702 Dorset Streams Dr Huaxia Yao Chris Mcconnell 0170703 Dorset Precipitation Dr Huaxia Yao Chris Mcconnell 017070401 Spatial Reference lakes CAISN Study 017070402 York Flames Lab Studies Dr Norm Yan 017070403 Queen s University Studies 017070404 University of Toronto Studies 017070405 OBBN Reference sites Chris Jones 0170705 Dorset Internal Laboratory testing Chemistry Lab 0170201 Lake Simcoe LSEMS Study Dr Jennifer Winter 017020201 Lake Simcoe Tributary Study Dr Jennifer Winter 0170204 Lake Simcoe Precipitation Study Dr Jennifer Winter 0170601 Trent University Studies 010120701 Lake Partners Anna DeSellas 010120710 Sudbury Laurention University Jocelyne Heneberry 11 List of LIMS Products and Parent Products Dorset Product code Common Test Name Oracle Name Units pH3042 pH PH pH
6. NUMERIC integer or decimal Gear Identifier 1 hand sample bottle filled by hand all media 2 peristaltic pump lake groundwater 3 Van Dorn or Kemmerer Bottle lake 4 tube composite lake 5 composite bottle lake 6 Sangamo collector precip 7 Aerochemmetric collector precip 8 MIC collector precip 9 bulk collector summer funnel precip 10 bulk collector winter funnel precip 11 hand held manual pump groundwater 13 lysimeter zero tension groundwater 14 auto sampler Stream Secchi depth in meters must be present when WLAYER 5 6 Submission Check List Have you contacted the lab to find out what they require from you Do you have all the bottles for sampling the parameters that are of importance How will you deliver the samples to the lab During work hours or after hours Will your samples arrive at the lab within the described perishability limits Are any of your samples preserved Have they been identified either a note on the bottle or a note on the submission form as being preserved The only samples to be preserved are Metals 0 25ml conc Trace metal grade HNO3 80ml sample and Chlorophyll 0 5 ml MgCO3 500ml sample This is normally done by the lab However this can be done in the field if the sample is taken at a distant source Do you have a Ministry of Environment contact person Do you have an allocated test load approved by the Lab Supervisor Any exceedances mu
7. mmm yyyy 19 Nov 2009 11 05 CNW SUBNUM DORNUM LOGIN ID PARENT LDESC PRODUCT PRODUCT DRCLKA MET 3386 222227 0002 222227 0003 19 2009 11 05 CNW 5 0 0 7 7 5 1 1 1 0 0 7 7 5 1 1 1 19 Nov 2009 11 05 CN EUPH DRCCHLO TP 3036 The Field data part of the submission sheet will look something like this SPECIAL SAMPLE SAMPLE STUDY ID GEAR TYPE TYPE WLAYER SDEPTH BGDEPTH WDEPTH SECCHI 47 2 12 1 0 20 2 5 47 2 12 1 0 19 20 2 5 47 2 12 5 0 5 20 2 5 SDESC Light rain Light rain Light rain The highlighted fields in light green generally need to be completed SDESC can remain blank Form Completion Instructions Ensure that every sample container is labelled with either a Field Sample ID or a Sample location description Text that is in the LDESC field e g CN W Accurately fill out the following fields at the top of the form a Date Submitted submission date in dd mmm yyyy format b Sampled by and Submitted by sampler name Accurately fill out the following cells in the form table c Sample Set numeric Beginning at 1 VERY IMPORTANT the sample set identifier is intended to provide a way of retrieving replicate samples that have been taken at the same time and location If samples are identical but are taken for different parameters then they may require a different sample set number e g a lake composite sa
8. samples should be kept cool If sampling in more rugged terrain keep the glass sample containers in their foam wraps and make sure samples remain upright with the help of suitable packing material Ice can be used if placed on the cooler bottom and samples are isolated from it but contamination can occur if sample containers come into direct contact with meltwater 2 Use non powdered vinyl gloves To avoid washing any of your personal chemistry into the sample bottle samplers must obtain their sample with gloves on their hands Please change gloves when you change waterbodies 3 Make sure you will have a valid StationID If you re sampling a new station that hasn t been sampled before make sure you collect latitude and longitude NAD83 UTM Zone17N with a GPS or find out the lat long of where you were once back in the lab with GoogleEarth or FlashEarth 4 Filter Most samples need to be filtered through an 80um mesh prior to collection in the sample container irrespective of whether they originate from lake stream precipitation or groundwater sampling The only samples for which this is not the case are DIC TIC TOC and pH alkalinity see appendix 12 for photos Because carbon is dissolved in water as introducing oxygen to the sample via filtration is not advisable pH is also affected by exchange of when the water sample is not in equilibrium with the atmosphere 5 Rinse sample containers three times Including samp
9. NO more than 1 0 cm above PP cap the etched line PET 3025 30 ml Polyethylene terephthalate Cond3024 30 ml Ammno3374 30 ml Dorcsi3422 30 ml Anion3147 30 ml Cat3249 30 ml Dtkn3424 60 ml Chlorophyll DCHL3169 500 ml Amber wide mouth HDPE 500 or 1000ml Metals Met3386 25 ml 60 ml clear PP specimen jar with blue cap Total Organic Carbon TOC Carb3028 Must be filled to top with septum in and or Total Inorganic Carbon place No visible air bubble TIC 40 ml glass vial with septum New Multi Parameter pHalk3042 Must be filled to top with septum in Analyzer PET with septum 3025 place No visible bubble Cond3024 9 Example List of Special Study ID Codes February 2010 STUDY ID STUDY DESCRIPTION PERSONNEL 65 Crayfish Survey 2007 Brie Edwards Keith Somers Don Jackson 66 Mercury Greg Mierle Murray Richardson 67 Martha Celis Flames Lab Martha Celis Norm Yan 68 Dallas Flames Chemistry Dallas Norn Yan 69 2008 MNR Broad scale Monitoring Andrew Paterson 70 A Cairns MSC Ca Project Allegra Cairns Norm Yan 71 Great Lakes John Thibeau 72 York University Natalie Kim Norm Yan 73 Trent University Watershed P project Andrew Paterson Huaxia Yao 74 McGill University Special Project Erin Gertzen Brian Leung NOBM Northern Ontario Benthic Monitoring 75 Sudbury Sept 2008 Jocelyne Heneberry Chantal
10. and where the sample has been taken In some cases the perishability limits can be exceeded with out much change taking place within the sample For example DIC pH Alkalinity taken from deep soft water lakes are very sensitive to perishability limits whereas a surface sample less sensitive Samples with high conductivity and high pH can sit for more than 5 but less than 10 days with no change If in doubt please contact the lab Leave a note on the submission form indicating samples that can exceed holding time if you are aware of the nature of the water sample Products that have Holding Times of 14 days or less Parameter s Holding Time days pH 5 pH Alkalinity 5 TIC 5 Conductivity 7 Total Phosphorous 10 Ammonia Nitrate 14 TKN 14 DOC 14 Cations Ca Mg K Na 14 Chlorophyll 2 Chlorophyll samples that cannot meet the perishability limit should be fixed in the field with 0 5 ml of 1 MgCO3 500ml sample 8 Minimum Volumes required for analysis Note If volume 18 not an issue then all containers are to be filled to the top Total phosphorus tubes are the only exception Bottle Type Parameter Minimum sample volume pH Alkalinity phalk3042 Must be filled to the top and capped Amber narrow mouth HDPE with gas cap No air bubble 125 or 250ml TP tube TP3036 Must be filled to above the etched 50 ml glass boro silicate with line but
11. ection 5 below for explanations The Excel file is to be saved with a descriptive name followed with the date in MMDDYY format E g Crosson_01_19_10 xls The file should also be in the Office 2003 format xls Sample Submission to Chemistry Laboratory Samples are to be left on the counter in the sample reception trailer Building 18 during the day and refrigerated if after 4 00 pm Samples will normally be accepted only Monday to Thursday However if samples could not be submitted in time on Thursday or are collected early Friday morning they can be accepted until noon on Friday If leaving samples in the refrigerator after hours be sure to submit your completed submission form before going to the field on the next day Samples should be placed in order on the counter as they appear on the submission sheet from left to right If there were any bottles that did not get filled or the bottle was misplaced in the field then place a note with the submission on the counter or in the cooler The lab will decide to pour or re pour the missing bottles for analysis Completed submission forms should be available for the sample submission clerk to review on the Dorset file server in G General SampleSubmission XCOMPLETED_FORMS Your Project current submissions just before the samples arrive at the lab The clerk through LIMS will assign a submission number C number catalogue the samples and queue the analysis For those
12. groups who are submitting samples in coolers shipped by Purolator please send your completed submission forms to the submission clerk by email cathy thomson2 gmail com 2 Stream Samples Sampled by Christoper McConnell Submitted by Christiane Guay Sub Description A Streams SUBNUM DORNUM Client ID Program Code Date Submitted 12 Jan 2010 0 Form Type STREAMS Laf 3 7 6 2 Lol 7 of v of 2 1 Client Contact Name Johnny Su Address DESC Bellwood Acres Rd Dorset POA 1E0 Phone 705 766 1291 Cont DATE Sent STATION dd mmm yyyy LAB SAMPLE Sample 5 8 11 Jan 2010 1 8 11 Jan 2010 NUMBER 11 Jan 2010 14 30 CB1 DRCSTRMB LOGIN ID TIME hh mm PARENT PRODUCT PRODUCT 0001 1 11 15 CBOL DRCSTRMB Met3386 C 0002 11 15 CBOL TP3036 0003 2 Met3386 n 0004 2 mM 11 Jan 2010 14 30 CB1 TP3036 0005 5 8 11 Jan 2010 10 30 CB2 DRCSTRMB Met3386 222227 0006 10 30 CB2 TP3036 SPECIAL STUDY_ID 46 46 46 46 46 46 SAMPLE GEAR_TYPE 1 1 1 SAMPLE TYPE STREAM TEMP 0 0 SDESC Clear and 5C partially frozen Clear and 5C partially frozen Clear and 5C complete ice and snow cover Clear and 5C complete ice and snow cover Clear and 5C deep snow and ice cover beaver dam in place Clear a
13. le container caps Additionally the filter apparatus also needs to be rinsed three times prior to the acquisition of the first water from a particular sample 6 No air in DIC TIC TOC and pH alkalinity samples For the reasons stated above these samples should have no air bubbles in the container Invert to check in transparent containers 7 Fill phosphorus tubes correctly Water height should above the etched line but no more than 1 cm above 8 Do not fix water samples in the field This is particularly true for samples to be analyzed for metals high grade nitric acid needs to be used for these samples and this grade is not readily available There may be occasions where chlorophyll samples need to be fixed to avoid perishability limits but please see the lab if you think this might be a problem 9 Sample with care Do not disturb the water column sample from the surface to the bottom or stream substrate discard rinse water downstream unnecessarily when sampling Ensure unfiltered samples are free from debris 10 Ensure samples are properly labeled the description on the bottle should match the description on the sample submission sheet 11 Submit samples properly to the Chemistry Laboratory Smile Gifts of chocolate are always welcome If after hours please properly refrigerate samples until they can be submitted the following morning also see detailed instructions below B Detailed Instructions for Comple
14. mple for Total Phosphorous is one sample set number and a lake composite sample for chlorophyll will be another sample set number but generally when the samples are taken from the same water sample or pumped from the same depth the Sample Set is not incremented d Cont Sent numeric number of containers submitted for that sample e STATION Alphanumeric Identifier See database manager currently Johnny Su johnny su ontario ca for the creation of unique station ID codes for your project f DATE and TIME time of sampling Date format as above time in 24 hour clock g LDESC Location Description A short or abbreviated description of where the sample originated E g PC Epi or PC W Please ensure that this identifier is entered in the same manner from now on 1 if PC W is entered with no spaces and a dash DO NOT insert spaces or remove the dash h PARENT PRODUCT and PRODUCT Alphanumeric Identifier Unique Code to identify the tests that you require See Section 10 below i SPECIAL STUDY_ID Numeric Identifier Mandatory field See database manager or sample submission clerk for a new SSID if you do not already have one Please email a thorough written description of your project to the database manager johnny su ontario ca when obtaining a new Special Study ID j Field Data Columns U AB Fill in whenever possible projects are strongly encouraged to submit these data along with their chemistry data See s
15. nd 5C deep snow and ice cover beaver dam in place 3 Precipitation Samples Date Submitted 04 Nov 2009 Form Type PRECIPITATION Client ID Program Code Sampled by Chris McConnell Submitted by Chris McConnell Sub Description Dorset Precip WHMIS HEALTH FLAMMABILITY Client Contact Name Johhny Su Phone 705 766 1291 Address DESC Bellwood Acres Rd Dorset POA 1E0 REACTIVITY PROTECTION FIELD SAMPLE IDS 0 POTENTIAL HAZARD HEALTH All SUBNUM DORNUM LOGIN ID LAB SAMPLE NUMBER DATE dd mmm yyyy STATION 3 08 Oct 2009 PCP2 BULK COLLECT PARENT PRODUCT PRODUCT DRCPRECIP Met3386 2 08 Oct 2009 02 Nov 2009 PCP2 BULK COLLECT 3 s 438518 wm cocoa TP3036 Met3386 TP3036 Met3386 TP3036 Met3386 TP3036 COND3024 time use with caution time use with caution time use with caution time use with caution time use with caution time use with caution time use with caution time use with caution SUBNUM DORNUM LOGIN ID SPECIAL SAMPLE SAMPLE INITIAL INITIAL STUDY_ID GEAR_TYPE TYPE DATE TIME SDESC 49 9 62 21 Sep 2009 17 00 Sample has sat for extended period o 49 9 62 22 Sep 2009 18 00 Sample has sat for extended period o
16. pproval from the current lab supervisor presently jim rusak ontario ca before field sampling begins for the year Sampling staff are encouraged to visit email or phone the Dorset submission entry clerk presently Cathy Thomson to be provided with a customized submission form The lab is currently configured to process primarily surface water samples from central Ontario lakes Please enquire if you plan on submitting other types of samples A list of all available chemical analyses that can be performed by the Water Chemistry Laboratory can be found in Section 11 The first step in ensuring quality results is the process of taking the sample correctly Make sure that the proper technique is understood before you sample For a complete discussion of sampling methodologies used in Dorset Environmental Science Centre DESC long term monitoring programs please consult the following manuals Lake Sample Collection Methods Final edits doc for lake sampling techniques G Programs Inland Lakes Lake Documents contact Ron Ingram or Hydrometeorology Sampling Methods doc for stream and precipitation sampling G Programs Inland Lakes Lake Documents contact Chris McConnell For a general overview please refer to the section Basic Instructions for obtaining water samples for chemical analyses Chemistry results are archived in our Dorset Oracle Database Dorset Data Store The evolution of the sample submission form has transformed it into
17. st be approved Have you provided the sample reception clerk your cell phone number or email address so that we may contact you in case there is a problem Remember to report your Field Data if at all possible Make arrangements with the database manager to send you the final results What file format will the results be in How quickly do you need your results Is the date submitted correct Is the sample date correct If the date is not correct the sample may be discarded if the perishability limit has been exceeded Are all samples listed on the submission form Count the containers and then count the number listed Correct any discrepancies Delete rows that are not used Is the sample time correct and in 24 hour format Does the description on the bottle match the description on the sheet Are your containers leak free If a total phosphorous tube leaks it and its companion should be repoured in new tubes Total Phosphorous tubes should be transported upright in the cooler in a rack or wrapped in foam protectors The protectors are just foam pipe wrap cut the same length as the tube Ask the lab if you need any use of freezer packs rather than ice is recommended to keep samples cool to avoid sample contamination If ice has to be used make sure samples are isolated from melt water Ask if you re not sure The Chem Lab phone number is 705 766 0632 7 Parameter perishability limits Many parameters are no
18. t stable over extended periods of time even stored at 5 4 and the methods for analyzing those parameters specify l mits known as Holding Times see table below beyond which samples must be discarded or flagged Holding Time is defined as the time between the collection of the sample and the start of analysis It is the responsibility of the sampler to ensure that the sample arrives at the lab within an appropriate period of time For parameters with short perishability limits 5 days the sample should arrive within 24 and not more than 48 hours after time of sampling The sampler also needs to take into account weekends especially long weekends If shipping by Purolator consider not shipping on Friday if the samples will sit in their warm warehouse for the weekend The lab needs to have perishable samples available for a 2 3 day period not including weekends during which it can schedule an analytical run If a sample for pH alkalinity or DIC is taken on Wednesday but doesn t reach the lab until Friday the earliest that it could be analyzed is Monday The lab will attempt to analyze the samples within the perishable time limit however if a run of required method is not scheduled for that day its perishability limit would be exceeded Samples for chemistry products may be analyzed after the holding time and be qualified with the remark UAL Unreliable Sample Age Exceeds Normal Limit It is also important to consider the chemistry
19. the best method to load sample information to our Oracle database It can not be stressed enough how important it is to create digitally correct submission forms These forms are to be populated in Excel Mobile handheld devices such as Palm Pilots or Tablet computers can be also be used to fill in the forms The form used will depend on whether or not you are sampling a lake stream or collecting precipitation samples There is also a special form for samples originating in a Laboratory E g FLAMES lab or Waterloo lab Please refer to the section Detailed Instructions for Completing the Sample Submission and Field Data Forms for specific instructions on completing forms for the various types of sampling The latest version of this guide can be found at G General Sample submission Basic Instructions for obtaining water samples for chemical analyses The intent of this section of the guide is to highlight the practical aspects of obtaining a water sample that will yield the best water chemistry results irrespective of whether the sample comes from a lake stream precipitation collector or underground aquifer As such users should also seek instruction from the lead scientist on the project being sampled for details on the sampling procedure for their particular system of interest 1 Ensure you can store samples properly once you collect them A cooler with freezer packs and a test tube rack is the preferred method of transport as the
20. ting the Sample Submission and Field Data Forms Every sample submitted to the lab for analysis must be accompanied by a properly completed sample submission form containing the appropriate data describing that sample it will not be processed Those data are initially illustrated with reference to a lake sample submission but the fields that require completion are the same for all other types of samples and examples of those forms follow this initial illustration 1 Lake Samples Below is an example of what a typical lake submission sheet would look like with the fields that need modification highlighted in light green No new columns are to be added or deleted but more rows are acceptable Cyan shaded sections are filled in by the lab Project Submission forms Excel 2003 format will be emailed to you at the start of the sampling season or if access to the Dorset File Server is possible can be found here G General SampleSubmission COMPLETED_FORMS Date Submitted 19 Nov 2009 Form Type LAKES Client ID 4 3 7 e 2 Program Code Lol 17017011 1 Client Contact Name Johnny Su Address DESC Bellwood Acres Rd Dorset POA 1E0 Phone 705 766 1291 LAB SAMPLE Sample Cont Set Sent NUMBER STATION 222227 0001 Sampled by Ron Ingram Submitted by Ron Ingram Sub Description A Lakes HEALTH 0 FLAMMABILITY 0 REACTIVITY 0 PROTECTION 0 POTENTIAL HAZARD HEALTH FIELD SAMPLEIDS TIME hh mm DATE dd
21. tkn3424 DRCLKB WS Dorset B Lakes Phalk3042 Ammno3374 Tp3036 Anion3147 Cat3249 Dtkn3424 DRCYORKBYL WS York University Phalk3042 Co13025 Cond3024 Dorcsi3422 Tp3036 Cat3249 DRCPRECIP WP Dorset Precipitation Phalk3042 Cond3024 Ammno3374 Dorcsi3422 Tp3036 Anion3147 Cat3249 Dtkn3424 DRCSIMPRI WP Simcoe Precipitation Phalk3042 Cond3024 Ammno3374 Tp3036 Anion3147 Cat3249 Dtkn3424 DRCSTRMB WS Dorset Streams Phalk3042 3025 Cond3024 Ammno3374 Dorcsi3422 Tp3036 Carb3028 Anion3147 Cat3249 Dtkn3424 DRCSEVNS WS Severn Sound Ph3042 Cond3024 Ammno3374 Tp3036 Dtkn3424 SUDLKGEN WS Sudbury Lakes General Phalk3042 Co13025 Cond3024 Dorcsi3422 Carb3028 Anion3147 Cat3249 SUDLKALL WS Sudbury Lakes All Phalk3042 3025 Cond3024 Ammno3374 Dorcsi3422 Tp3036 Carb3028 Anion3147 Cat3249 Dtkn3424 SUDLKNUT WS Sudbury Lakes Nutrients Ammno3374 Dtkn3424 Tp3036 DRCKEN WS Kenora Lakes Phalk3042 3025 Cond3024 Ammno3374 Dorcsi3422 Tp3036 Anion3147 Cat3249 Dtkn3424 DRCUSGS WS Chemistry Lab PT Testing Ph3042 Cond3024 Ammno3374 Anion3147 Cat3249 12 Collection bottles TOC TIC Tubes Total Phosphorus tubes m MPA PET with Septum pH Alkalinity bottles Fa Metal jars 13 Glossary of Terms Term E
22. xplanation LIMS Laboratory Information Management System Software used by the lab to enter information and results about the sample for archiving Product LIMS code for a type of analysis Can have one or more tests Parent A LIMS code for a group of products Product 14 Contacts Peter Sutey 105 766 0632 Peter Sutey Cathy Thomson 705 766 0632 Cathy Thomson2 0 gmail com Don Evans 705 766 0632 Don Evans ontario ca Jim Rusak 705 766 0659 Jim Rusak ontario ca Ron Ingram 705 766 2499 Ron Ingram ontario ca Chris Mcconnell 705 766 1293 Chistopher Mcconnell ontario ca Johnny Su 705 766 1291 Johnny Su Ron Xu 705 766 0632 Ron Xu ontario ca 15 Revision History 15 1 January 2010 First draft 15 2 May 2010 Final version 1 10 15 3 February 2011 revised 2010 manual 16 Notes
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