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GC-2014 Service Manual

1. en es 87 SS FTD 20140 89 5 0 mE 91 CHAPTER 6 MAINTENANCE PARTS LISTS 95 lt GC 2014 MAIN UNIT gt cce tenete ta erdt 95 lt FID 2014 SNOEN 96 OISEAU 96 lt FTD 2014 CAPILLARY se 97 lt FTD 2014 PACKED ae 97 EDNA 97 TD 98 ED SG 98 LE EE lated ots odie cea 98 SOR feet 98 GC 2014 Service Manual Table of Contents CHAPTER 7 5 99 7 1 Gas and Pressure Flow Rate Settings 99 7 1 1 Precautions for Flow Rate Control Settings CAR 99 7 1 1 1 When the control mode is SPLIT or SPLITLESS 99 7 1 1 2 When the control mode is TOTAL FLOW and the injection mode is DIRECT eos RT 102 7 1 1 3 When the control mode is PRESS or LINEAR VELOCITY and the injection mode is DIRECT 102 7 1 1 4 Precautions for Flow Rate Control Settings DetAPC 104 7 2 Temperature u ua In en tener ERE Po ne 888 105 F D 0 0 ROE 105 u a Oa Na 105 LaL PPD benene s 106 106 7 4 Chromatogram and 106 55
2. pics 107 CHAPTER 8 SERVICE 109 CAR ZL u kyu 110 8 2 Flow Adjust DetAP aa 111 8 3 Flow Adjust 111 8 4 Temp Sensor Use Time 112 112 8 6 Serial Number 113 8 6 1 Main Body Serial Number renee ener kn enne 113 8 6 2 Unit Serial Numbers uu Uu a a 114 8 7 Maintenance 00 0 4 12 20 2 2 1 1 1 114 8 8 Fan amp LCD Use Time de su Dea ugs 115 8 9 Init for Shipment sects traten ind eo ter deed enr gae rear 115 CHAPTER 9 APPENDIX 117 GC 2014 Service Manual Chapter 1 Installation Chapter 1 Installation 1 1 Installation Space DANGER Hot Air Hot air is discharged from the opening Do not expose flammable objects directly to the hot air V 400 mm min V V r 2 5 SOOO 5 V EE NE f E Width 400 mm 50 mm min 100 mm min 1 1 1 Rear Space Hot air is blown out of the exhaust holes at the
3. 221 42511 92 RESISTANCE TUBE ASSY H2 FID2010 APC FTD Assembly Configuration Chart 221 47740 95 221 48981 91 APC 2014 FTD FLOW BOARD ASSY APC 2 221 41116 91 221 45153 91 BASE 55 55 221 46812 92 PIPING 55 221 48813 91 55 221 48468 91 55 221 18713 95 FTD 9 RESISTANCE TUBE ASSY 2 221 18713 96 FTD 9 RESISTANCE TUBE ASSY AIR GC 2014 Service Manual 69 Chapter3 Gas Flow Controller 3 1 3 2 2ch APC APC_FPD Assembly Configuration Chart 221 47742 92 221 48981 91 DET APC FPD FLOW BOARD 55 2 221 48581 91 221 45153 92 BASE 55 FPD 55 2 221 48581 91 55 221 48813 91 VALVE 55 221 48585 91 55 FPD OUT 2014 Service Manual 70 Chapter 3 Gas Flow Controller 3 1 3 3 1ch APC APC_ECD Assembly Configuration Chart 221 47743 92 221 48981 91 DET APC MAKE UP ECD FLOW BOARD 55 2 221 48586 91 221 45153 93 BASE 55 UP 55 1 221 48713 91 55 ECD OUT 221 48813 91 VALVE 55 221 48687 91 PIPING 55 2014 Service Manual 71 Chapter3 Gas Flow Controller 3 2 Flow Line Diagram for Gas Flow Controller 1 Flow Line for Packed Dual Injection The flow line shown applies for use in combination with a
4. Detector control units PCB AUX TEMP 221 45163 91 POWER UNIT 221 48460 92 100 115 V 221 48460 39 220 240 V LCD ASSY 221 48721 91 4 PCB KEY ASSY GC 2014 PCB DET GC 2014 CPU UNIT GC 2014 221 70254 91 221 47632 92 221 70250 91 VS100B 24 FLAT CABLE 34P 074 80654 77 100 115 V 221 47663 01 LEA100F 24 074 80427 61 220 240 V FLOW GC 2010 221 45145 91 SLOT SLOT SLOT SLOT SLOT SLOT Note One AFC be mounted to one odd numbered slot and one even numbered slot AFCs are recognized as CAR1 and CAR2 in order of increasing slot number Fig 2 3 1 Block Diagram GC 2014 Service Manual 27 Chapter2 Configuration of GC 2014 2 3 2 CPU Unit 08 Sr v6003S 15 S e e 8 I gt u lt 1 Fig 2 3 2 Assembly Diagram for CPU Unit GC 2014 Service Manual 28 WRHH D WARG WA Wn SWAT POT WATO ws FPGA PAOG 33 109 PYM n58 2 2K PAIS TIOCOA 2 1 pa 14 2 EEE lt 5 eR ee COR 29 2 i K GA DON D LGA DONE 4 7 0 Ez Chapter 2 Configuration of GC 2014 07 TiocaA 138 Ga 06 06 sy EE pcan bereg il 2 Tocas 2 SI
5. resistance tube 26 Insert wi h rubber plug for port 27 49 N GC 2014 Service Manual 66 x 2 H gt 3m HII AA Air resistance tube 32 Insert with rubber plug for port 27 Chapter 3 Gas Flow Controller 3 1 2 4 AUX 221 70049 94 11 221 18150 93 FLOW CONTROLLER AUX 1PC N BELLOW VALVE 2K 8KIN 16 670 18558 11 2PC PRESSURE GAUGE 200 KPA 17 018 21330 TAPE STICKER 0 1 x 13 x 5 25 221 31745 1PC HOUSING 26 221 19502 08 1PC RESISTANCE TUBE HYDROGEN GC 8A 27 201 47435 1PC RUBBER PLUG PORT SILICON 28 221 09864 18 1PC PIPE 17 2 x 180 29 221 41408 94 1PC PIPE PG MF MF ASSY 37 201 48557 25 1PC PIPE MN2W MM2W GC 2014 Service Manual 67 Chapter3 Gas Flow Controller AUX N S 3 180 250mm resistance tube 26 Insert with rubber plug for port 27 GC 2014 Service Manual 68 Chapter 3 Gas Flow Controller 3 1 3 APC Optional Different APCs are used for each detector 3ch APC FID FTD 2ch APC FPD 1ch APC TCD ECD 3 1 3 1 3ch APC FID Assembly Configuration Chart 221 47740 94 221 48981 91 APC 2014 DET 3CH FLOW BOARD ASSY 2 221 41116 91 221 45153 91 BASE 55 55 3CH 221 46812 92 55 221 48813 91 VALVE 55 221 48468 91 55
6. cs C 1u 1014 1 21 1 21 cio 104 68 016 1014 AGNDref 2 577 AGND Vs PYR Vout 2 I5 1 GND AGND Al A2 A3 5 AT AR AS m B2 B3 BS BS B BS B9 VREF AUXA l tee C AW IIIIb 0OG OF NF2 6 5 4 AUKE 415 4 3 Unk AUXSS AUXSS lt gt AUXAS AUX4S 45 5 w cea AUX4S ht 5 7 ALIXS S 6 m ALIXSS w 5 unt 4 JS 1 l Fe 12 0074 3 J6 Satellite Oven 100K JU HA Urit AGNDe NF4 Pt Ri 270 NF4 M4 C20 JUEL ILT 821 140 28 8 1 74 Don t mount NF4 M4 C20 J9 x Mount 0 ohm register insted of 100K as R2 Fig 2 3 32 Circuit Diagram for PCB AUX TEMP GC 2014 Service Manual 58 Chapter 3 Gas Flow Controller Chapter3 Gas Flow Controller 3 1 Configuration Diagrams for Gas Flow Controller 3 1 1 AFC There are four types of AFC for packed dual injection split splitless injection WBI direct and packed single injection AFC SPL Assembly Configuration Chart 221 47735 93 221 48740 91 AFC 2014 D PURGE SPL FLOW BOARD ASSY AFC2 221 47775 91 221 45749 91 AFC BASE ASSY PCB AFC ASSY GCX 221 46812 91 PIPING ASSY 221 47779 91 VALVE ASSY 221 48187 91 PRESSURE SENSOR ASSY AFC WBI
7. 8 ER Ds AIS 42 Do 0 04 or O 2 07 s oto 1045 14 52 gt NA 0012 046 35 03 k en Dear D4 A is 48 D Dr SNE A D 22 03 1 ce T 1048 0846 1022 Ce En or pr De FB 15 018 4 Kom pi 7 57 2 055306 102 5 RE E 51 19 a LCDCO 17053 1587 1107 s TEDE vn 6 OCS 1 057 5 LED er HWA 1058 HE 9 4 WA LP VOSS FAE 5 VOEO MPUSEL 000 5 DSS308 102 UD UD Tur C WATS gt 0 WAIT UDE rosae 1 05808 4 T ste md 02452 052 OSCI UO63 0502 055305102 um una 3823323233537 WALD 9 1086 S 025 SIO RS 926 DGND gt SC Fo SVR toon r gt RAN TE J er 512000 0 ter 4 RM3 y KEY ST A R2 3U51 DUT L U U U 8151 0000 lt 2 CATE DATA Arsene lt 854 DATA PRG DATA FG CK OPTAN1 N OPTN2 2a OP TINS 94 A54 510 STARTI cem Barr 55 ar we 8 C18 C20 014 0 10 DGND DGND DGND OGND SBC SIO LCDC Fig 2 3 4 Circuit Diagram for CPU Unit 2 4 GC 2014 Service Manual 30 Chapter 2 Configuration of GC 2014 Mia 12V 8050 00 BR R13 Has Ek BUS CKO 9 150 _ 3 252 VENTSENC AJ 92 45 EV
8. JG THEM vb GUARD ASST AD CONTRO LER H FIDLPELSHEATFR FVT CELL BASE ASST 11 Chapter 5 Detector Unit H ZEIT IPC SHELD i IPC BB EXURCE HEATING TRANSFORMER 555 2014 11 IPC CERAMIC TPC RELAY BLOCK TEFLON idm PC HELLA TDM SUPPORT H IH IPC FFDHORTER TIE mA IPC HUT 50521 4 LESE O RING C PH Hn JPC WASHER SUS SPRING 2 IPC SCREW SUS SEMIS FI 1 5 s ABC SET SE REM 6 d 12000317 IPC SCREW HEAD 2 18 PG MASKER SUG PLAN 1 221 70458 91 34 1PC HEATER PT ASSY 100V 230V DET 12 221 70121 1PC DET SINGLE UPPER COVER 13 221 70129 1PC RETAINER PLATE DET SINGLE 14 221 70138 1PC LOCK RING DET SINGLE 16 221 70134 1PC DET SINGLE BLOCK UPPER 17 221 70135 1PC DET SINGLE BLOCK LOWER 31 020 46534 4PC SCREW SUS SEMS P3 M3x6 34 020 46640 2PC SCREW SUS SEMS P4 M3x25 35 020 46542 2PC SCREW SUS SEMS P3 M3x30 GC 2014 Service Manual Chapter 5 Detector Unit blank page GC 2014 Service Manual 94 Chapter 6 Maintenance Parts Lists Chapter6 Maintenance Parts Lists lt GC 2014 MAIN UNIT gt P N Part name Remarks 072 01665 36 FUSE 15 100
9. 221 70623 91 ECD 2014 HEATER ASSY 100 FID 100 V 221 70623 34 ECD 2014 HEATER ASSY 230 FID 230 V 221 48455 92 ECD 2014 CONTROLLER 221 33193 91 CAPILLARY ADAPTER DET SIDE 221 34121 94 MS FILTER Aged 221 19502 08 RESISTANCE TUBE ASSY H2 Resistance tube only for make up gas 221 31745 HOUSING RESISTANCE TUBE 97 GC 2014 Service Manual Chapter6 Maintenance Parts Lists lt TCD 2014 gt P N Part name Remarks 221 70041 91 TCD 2014 CONTROLLER 221 70086 91 DET HEATER ASSY FT 100 221 70086 34 DET HEATER ASSY FT 230 221 70043 91 TCD POWER SUPPLY lt D FID gt P N Part name Remarks 221 70040 91 FID 2014 CONTROLLER DUAL 221 70085 91 DET ASSY F 100 V 221 70085 34 DET HEATER ASSY F 230 V lt D INJ gt P N Part name Remarks 221 70075 91 DUAL AFC ASSY 221 70479 91 HEATER PT ASSY P INJ 100 221 70479 34 HEATER PT ASSY P INJ 230 221 70466 FIN 2014 221 22206 SPACER INJ lt OTHER gt P N Part name Remarks 221 47735 94 AFC 2014 WBI For WBI 221 44496 91 POWER SUPPLY 201 221 44548 94 20 ATTACHMENT PARTS GC 2014 221 48545 92 20 ATTACHMENT KIT GC 2014 For external power supply GC 2014 Service Manu
10. 6 The pressure is higher than the setting in split mode Check whether or not the setting is within the range of settable pressures flow rates for AFCs A graph is given the section on AFCs in the GC 2014 instruction manual Check that a blind has not been erroneously attached to a split bent Check that I time 1 P term 100 and I term 150 If the values are different from the above values input these values and press the pf4 key to write them in the ROM Check the offset and gain values The offset value is normally in the range 32 000 to 33 500 and the gain value is normally in the range 3 000 to 6 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain the correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC Set the inlet pressure to 0 kPa and the total flow rate to 400 mL min At this time pressure is generated due to the flow line resistance of the split line The specified value for this pressure is 50 kPa or less Normally 30 kPa If it is greater than 50 kPa identify the place where resistance exists using the following procedure Remove the AFC s piping line joint with the s mark band one piece at a time If the pressure decreases when the joint
11. Do 07 BPR apy SDIO scu H DSYNC asv MODE 15 ponp Fig 2 3 17 Circuit Diagram for Single FID Controller 2 2 GC 2014 Service Manual 43 Chapter2 Configuration of GC 2014 DSV NFM21CC223 FI DGND 24V DSV M1 SN75C1168 RESET DGND Dd Dd ___________ Reanimar pu E 7 Dur O O i Ck Cc 5 jJ O O Ck 24V 5V BAO BA UM C22 15 BusDu 47u35V gt DGND 15V 11 PGND i d gt DGND PGND DGND ED EEE EY PORT Je 45V DSV DEND gt DEND seg m Ms TMS RESET R1 RESET 100F C20 100p DGND M15 MS 4 240 TATBLOSF 424V 12 15V TA79LOSF ASV 12V 2 a C48 ci c2 9 0 33450 0 1u 0 33u50V o 0 14 0 33u50V o N vel AGND AGND GC 2014 Service Manual C17 XC8536 Fig 2 3 18 PGND AGND DGND Circuit Diagram for Dual FID Controller 1 3 44 2 MAT 01AH 21 223 ca Ca ASV 0 1u film 0 74 u film coe DGND o 2 1 a AGND E DEND 485396 z R26 R3 1K ca lt VREF gt D p Lue 3 10kF o ra AGND MSA 20 10 N FE R14 5102 5V _ AGND me 3 V 11 MITA AGND 3 MAT D1AH BONS m DGND lt 18 BR C29 O Olu film P 1M i C51 17 tu 8 al INPUT R24 330KF BE
12. Chapter3 Gas Flow Controller FTD 2 9 9 8 er NOS N _ N Hin pal 4 he 300mm 250mm resistance tube 250mm Inlet Side with red mark OO AG aa 8 8 N ju BMA A 300mm 250mm bal 8 S Air resistance tube Air resistance tube 32 Insert with rubber plug for port 27 GC 2014 Service Manual 64 3 1 2 3 FPD 221 70049 93 FLOW CONTROLLER H2 AIR FPD Chapter 3 Gas Flow Controller 11 221 18150 91 2PC N BELLOW VALVE 2K 670 18558 11 2PC PRESSURE GAUGE 200 KPA 018 21330 TAPE STICKER 0 1 x 13 x 5 221 42080 92 1PC BRANCHED PIPE AIR FPD V2 221 70483 91 1PC SOLENOID VALVE ASSY 035 60395 43 2PC GASKET 221 31745 2PC HOUSING 221 19502 08 1PC RESISTANCE TUBE HYDROGEN GC 8A 201 47435 4PC RUBBER PLUG PORT SILICON 221 09864 18 2PC PIPE MF MM17 2 x 180 221 41408 94 1PC PIPE PG MF MF ASSY 221 19503 08 2PC RESISTANCE TUBE AIR GC 8AF 221 41410 91 2PC PIPE M5 MF ASSY 221 41527 92 1PC PIPE PG MF MF MMASS 221 70720 02 1PC FPD RESISTANCE TUBE 201 48557 25 2PC PIPE MN2W MM2W 072 83071 08 1PC MARK BAND H 072 83071 01 1PC MARK BAND A GC 2014 Service Manual 65 Chapter3 Gas Flow Controller FPD 4 WE p xu 18 2K 300mm 250mm T NS 250mm
13. gt Primary circuits DIS Fig 2 3 8 Circuit Diagram for Power Unit 1 3 GC 2014 Service Manual 34 Chapter 2 Configuration of GC 2014 SN7SC 158 2 AUXA _ o Ae S AUXAH AS Aundliary Temperature Control Board JN es ZN edges 2 RELAYKI KKS RELAY RE x OVERHEAT Sr E Thermo coupie RN1221 tt DGNO ema C SYSTEM gt H ECK Fig 2 3 9 Circuit Diagram for Power Unit 2 3 GC 2014 Service Manual 35 Chapter2 Configuration of GC 2014 45V 45V 1M Hz 2 8Vref Cs 1u35V NFS v 2 5Vref L SE Ta 3 8 AGND ARS 121K 1 3 CM CC Sppmideg iK cs 2 3 CA Ck D 16 spour 7 COLS 1 00 4 1 15 2 oe 01 C34 2 C m 1 T AS apa IK UNT gt AGNOrg H DSYNC RB AAA UNE 18 MODE c11 jca c gt 4 10 Xn Qiu 1016 0179 0 19 Otu 0 10 21 AGND REF 24 ME ADS1211 2 5Vref 25Vref 2 5Vref 2 5 4 RRA RAT 2121K 2121K 25ppm ceg ARS 121K 17 IK INJ S 16 15 18 10 11 cig C21 C14 6 21 20 REF In REF out 019 1010 1010 AGND AD51211 INJDET Kannect AGND and AGNOref near AD780 Fig 2 3 10 Circuit Diagram for Power Unit
14. 221 47659 92 FID2014 COLLECTOR ASSY FID 600MM 221 41847 93 FILAMENT ASSY 180MM 221 70671 91 ASSY D FID 100 115 221 70671 92 230 221 70761 34 221 18150 91 N BELLOW VALVE 2K 221 41511 91 221 41510 N BELLOW VALVE 2K METAL CAP REPROCESSED WITH RESISTANCE WITH RESISTANCE 221 18150 91 670 18558 11 N BELLOW VALVE 2K PRESSURE GAUGE 200KPA 221 70483 91 SOLENOID VALVE ASSY 042 40043 02 SPEED CONTROLLER ASN M5 221 31745 HOUSING 221 19502 08 RESISTANCE TUBE HYDROGEN GC 8A 201 47435 RUBBER PLUG INJECTION PORT SILICON 221 19503 08 RESISTANCE TUBE AIR GC 8AF GC 2014 Service Manual 17 Chapter2 Configuration of GC 2014 221 70035 91 221 70082 91 221 47221 91 spL 2014ASSY 100 SPL 2014UNIT 100 120 INJECTION PORT A AASY 115V 221 70035 91 1150 0221 70082 91 230 221 70035 34 230 221 70082 98 221 70166 91 BASE VAPORIZING CHAMBER A ASSY 221 70602 91 221 70599 91 HEATER PT ASSY SPL100 HEATER 120 150W ASSY 115V 221 70602 91 115V 221 70599 91 230 221 70602 34 230 221 70599 34 221 70596 91 HEAT SENSITIVE MATERIAL INJ 050 73001 49 R RN AXIAL 1 2W 1001 221 47735 93 AFC 2014 D PURGE SPL 221 48440 93 221 42559 92 PIPING ASSY AFC SPL ASSY WITH BLIND ADDITION 221 48441 91 BUFFER ASSY 221 34121 94 MS FILTER CONDITIONING 221 48619 93 ACCESSORY ASSY SPL 2014 221 70091 91 221 70090 91 9 FID 2014 100 120V 2014 CELL ASSY P 115V 221 70091 91 23
15. Actual 40 2 Offset Gain A GC 2014 Service Manual 100 0 32775 7200 pf4 ROM wrt pf5 Offset pf6 Prim Ofs 110 Resets all displayed parameters to their default values Not written to ROM Press this key to write the values set in this window such as the offset and gain values to ROM The values are not set in ROM unless this key is pressed Performs offset calibration of the pressure sensor flow rate sensor and purge flow rate sensor Be sure to press this key to enable the calculated offset value Performs offset calibration of the primary pressure sensor pressure of supply to GC 2014 When performing offset calibration be sure to remove the GC 2014 s carrier gas supply piping from the GC 2014 Normally the value should be in the range 32 000 to 33 000 8 2 Flow Adjust DetAPC Flow Adjust Det APC 1 DET1 Flow Press 1111111111 2211111111111 Adual 40 2 100 0 Valve Voltage 14 0 Offset Gain 4210 I time P term I term Air Actual 40 2 100 0 Valve Voltage 14 0 Offset 4 8 3 Flow Adjust AUX APC Flow Adjust AUX APC 1 Flow Actual 40 2 Valve Voltage Offset Gain I time P term I term 32855 Chapter 8 Service Window Options only As an example the window on the left shows the items displayed for The items are the same however for the APCs of air and make up gas The displayed contents may vary however depending on the type of Det
16. DSS30 amp 102 C36 vo s 100p 8 DGND EXO 3C 20MMz Chapter 2 Configuration of GC 2014 AGNO DGND Fig 2 3 25 Circuit Diagram for FPD Controller 1 3 GC 2014 Service Manual 51 Chapter2 Configuration of GC 2014 SHIELD INPUT C17 0 1u ne Lt 1 3 1 AGND GC 2014 Service Manual 15953 R10 O28 MAT 03 AGND MOMT NM05 1E AGNO vor VOLIT iG V TH SA We RM3B 1 4 VA NAN VVU AMID RMIB 1Kx4 2 1Kx4 IAN ANN RM20 79 of cS ND AGND CH by ai AGND 1 ky 014 AGND AGND 100p C50 100p 3 Fig 2 3 26 Circuit Diagram for FPD Controller 2 3 Xin REF in REF out ADS1211 b SOOUT SDIC 7 16 15 14 11 AGND R51 1K gt AGND REF in ELS s REF out 20 Vbias 1 51211 C53 0 0lu I AGND 52 24V to 5V CONVERTER 05 88140 42 THERMAL SWITCH kaoi 4 8 2 a BATT 1 PGND lt FAN gt IGNITER 45 iGNITER 24 254377 2 104 C29 100u18V FE gt 816 2K n MISA PGND Q12 25C2458Y 244 PGND PGND Fas 10 HV GENERATOR Chapter 2 Configuration of GC 2014 R18 2 4 A
17. Fig 2 3 20 Circuit Diagram for Dual FID Controller 3 3 GC 2014 Service Manual 46 Chapter 2 Configuration of GC 2014 2 3 6 ECD Controller DE ce 34 Oi Fig 2 3 21 Assembly Diagram for Controller GC 2014 Service Manual 47 Chapter2 Configuration of GC 2014 cas Qu 29 J2 010 dl 4 M OG Du Du or 28 1 A9 424V 5 B1 BAD 82 83 DGND B4 85 B6 87 88 15 PGND Bid CONZOAB p ADEOY ADDY 827 1K n an 53 DACS p DACS 5 gt i DALDA D DALOA lt DADA T BAT DALDB JTAG PORT Jt OADD 5V 1 54 DGND 2 gt DGND TCK TMS 6 CONS CHRESET gt RES AN 100 le 10MHz I M amp 2 Connect near M3 x COND GRESET 1 1 8 ST 1 DSS306 221 Ris 100 2 AGND DGND iV 255306 102 cs voo T Iw Cao B hE DGND 4 GND c DGND DGND DGND 20MHz Fig 2 3 22 Circuit Diagram for ECD Controller 1 2 GC 2014 Service Manual Chapter 2 Configuration of GC 2014 C22 0 10 10x 3 C VOUT gt 5 412 C9 ow alli 3 e INPUT EA gt l ADADY 24V AD S AN CAN An ws 1K 359 N SOK RE 25037
18. 230 Insert the heat sensitive material in the heater block until it hits the bottom depth approx 18 mm Insert the heater in the heater block with the orientation shown below until it hits the bottom To prevent short circuiting of the lead wires bend them at points 1 to 2 mm from the bottom while pressing them so as not to apply stress to the heater insulator GC 2014 Service Manual 78 Chapter 4 Sample Injection Unit 4 4 Packed Dual Injector D CD CH 62 Parts List for Packed Dual INJ 221 70080 34 230V 81 100V 82 115V Number P N Part name Quantity 230V 100V 115V 11 221 70189 91 INJECTION UNIT ASSY 122 2 2 2 12 221 70479 34 HEATER PT ASSY P INJ230 1 12 221 70479 91 HEATER PT ASSY P INJ100 1 12 221 70479 92 HEATER PT ASSY P INJ115 1 13 221 70188 HEATER BLOCK DUAL INJ 1 1 1 14 221 70192 COVER PACKED DUAL INJ 1 1 1 15 221 70193 HOLDING PLATE HEATER 1 1 1 16 221 70196 LOCK RING 1 1 1 17 1221 70480 HEAT SENSITIVE MATERIAL 1 1 1 1 18 221 70481 HEAT SENSITIVE MATERIAL PACKED 2 1 1 1 19 221 70482 HEAT SENSITIVE MATERIAL PACKED 3 1 1 1 20 221 44584 NEEDLE GUIDE AOC 2 2 2 21 221 70466 FIN 2014 2 2 2 24 201 47435 RUBBER PLUG INJ PORT SILICON 2 2 2 25 221 22206 SPACER INJ 2 2 2 GC 2014 Service Manual 79 Chapter4 Sample Injection Unit blank page GC 2014 Serv
19. Check that the source pressure i e the primary pressure has attained a sufficient level e Check that time 10 P term 50 and I term 20 If the values are different from the above values input these values and press the pf4 key to write them in the ROM e Check the offset and gain values for the pressure The offset value is normally in the range 32 000 to 33 500 and the gain value is normally in the range 3 000 to 10 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain the correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC Check the settings to confirm that for example APC is not off and that the ignition operation has not been forgotten If 0 is displayed as the valve voltage this indicates that there is no voltage being supplied from the control system to the valve that is attempting to supply gas 3 The pressure or the linear velocity is higher than the setting e Check that I time 1 P term 50 and I term 20 If the values are different from the above values input these values and press the pf4 key to write them in the ROM e Check the offset and gain values for the pressure The offset value is normally in the range 32 000 to 33 500 and the ga
20. GC 2014 Service Manual 105 Chapter7 Troubleshooting 7 3 2 FPD 1 Ignition is not possible Cause Countermeasure The igniter filament has burnt out Replace the igniter 2 There is a lot or a high level of noise Cause Countermeasure There is a fault in the photomultiplier Replace the photomultiplier The H gt flow rate is fluctuating Replace the APC 7 3 3 FTD 1 The background current does not reach the set value in current mode and the count for the adjustment time does not start Cause Countermeasure There is insulation failure in the FTD electrode Check the background level in the ZERO cleared state with the monitor main screen If it remains greater than the product of the set current value and 20 000 pV 60 000 uV for a current setting of 3 pA and shows no sign of falling measure the insulation between the center pin of the FTD signal cable assembly s BNC connector B in the FTD configuration diagram and earth If the insulation resistance is less than 10 inspect or replace the FTD unit assembly Check whether or not there is a problem with the insulators Reference No 32 in the FTD configuration diagram inside the FTD unit assembly 2 There is a lot or a high level of noise Cause Countermeasure The metal plate on the collector cover is left open after checking the red hot state of the alkali
21. SILICON 221 09864 18 2PC PIPE MF MM17 2 x 180 221 41408 94 1PC PIPE PG MF MF ASSY 221 19503 08 2PC RESISTANCE TUBE AIR GC 8AF 221 41410 91 1PC PIPE M5 MF ASSY 221 41527 92 1PC 55 201 48557 25 2 PIPE MN2W MM2W 072 83071 08 1PC MARK BAND H 072 83071 01 1PC MARK BAND A GC 2014 Service Manual 61 Chapter3 Gas Flow Controller FID 9 03 98 29 2 25 92 88 N 2 3 P 3 180mm 300mm 250mm 250mm AA resistance tube 26 Insert with rubber plug for port 27 12 180mm 250mm TAA Air resistance tube 32 Insert with rubber plug for port 27 250mm 250mm GC 2014 Service Manual 62 3 1 2 2 FTD 221 70049 92 FLOW CONTROLLER H2 AIR FTD Chapter 3 Gas Flow Controller 11 221 18150 91 1PC N BELLOW VALVE 2K 221 41511 91 1PC N BELLOW VALVE 2K WITH RESISTANCE 670 18558 11 2PC PRESSURE GAUGE 200 KPA 018 21330 TAPE STICKER 0 1 x 13 x 5 221 18713 95 1PC FTD 9 RESISTANCE TUBE ASSY H2 221 18713 96 1PC FTD 9 RESISTANCE TUBE ASSY AIR 201 30219 4PC SOCKET 201 47435 1PC RUBBER PLUG PORT SILICON 221 09864 18 2PC PIPE MF MM17 2 x 180 221 41408 94 2 PIPE PG MF MF ASSY 221 19503 08 2PC RESISTANCE TUBE AIR GC 8AF 201 48557 25 2PC PIPE MN2W MM2W 072 83071 08 1PC MARK BAND H 072 83071 01 1PC MARK BAND A GC 2014 Service Manual 63
22. ma uA HORTLE FHH LIS LE AL HATTEHE ALKALL LINH TI FI AP BATTERE BOT FPD APT BATTERE EA TE 11 28205 FOM BELTER L Arc P GELS TREE FIT TER d TII RAT IPL sen p iden AD REST POTE F FH 1 TEC 06 DUET SpDE FI dk aker IPE APR CAP Bod 8 EL DT TED APT PLATE DE POSITION AD A IPE S K PI Du TI M SUR TIAS ALLEE ELA DET 5 TPE TAL FPD ELE SIE IPE AREE TAN HO TAC APP 2 Las 2L TPE ITE 11 Phaedri EEE HEATEB FE ay IH GC 2014 Service Manual 88 Chapter 5 Detector Unit 5 5 FTD 2014C E 29 UPPER SIDE 4 EA T3 3 BET THIS 13 THE VALUE TO BE GIVEN WHEN THE COLLECTOR REACHES THE LOWERMOST POSITION GC 2014 Service Manual 89 Chapter5 Detector Unit Configuration Diagram for FTD 2014C 7H MEHA 2914 vail FTE MH4 CAPR 1 FFE 14 72504 _ HO itii Mr vr
23. source Close the metal plate on the collector cover The Hz flow rate is fluctuating Replace the APC 7 4 Chromatogram and Data 1 Peaks are not output or are extremely small general detector used Cause Countermeasure The channel for detector signal output and the signal cable connection ANALOG OUT do not agree in the case of analog output Set the channel for detector signal output correctly Refer to 2 2 Outputting Aualog Signals to Chromatopac in Instruction Manal Details Offset calibration of the detector signal has not been performed correctly in the case of analog output Perform offset calibration of the detector signal correctly Refer to 2 2 Outputting Aualog Signals to Chromatopac in Instruction Manal Details The data format setting for the detector signal is incorrect In the signal settings in Configuration settings set Datafile data format to Chromatopac in the case of the C R8A and to PC in the case of GCsolution The analog signal type setting is incorrect in the case of analog output Set in accordance with the Chromatopac used Refer to 2 2 Outputting Aualog Signals to Chromatopac in Instruction Manal Details GC 2014 Service Manual 106 Chapter 7 Troubleshooting 2 Peaks are not output or are extremely small FID used as detector Cause Countermeasure The hydrogen flame is out If th
24. 11 2 1 5 GC 20 14AT 5 boe eee 12 2 1 6 GC 2014ATF iier in rete HR OO rer RAD Ted ES 13 21 7 GC 2014AATFSDL geek 14 2 2 Structure f u 2 u prose PERSE FPES SEES 20 2 2 1 External Appearance 20 2 2 2 cc tt Ure t n UE Pe tte nte btt 21 2 2 3 Structure Diagram 2 ed ERR PERPE eR 22 2 2 4 Structure Diagram onere aset e cea ike seede ted 23 2 2 5 PT Sensor and Thermocouple sss 23 2 2 6 Heater and 24 2 2 f Fan Motor iota testet date one 24 PAPA ORAM P TE 25 2 2 9 Structure of Oven Cooling Unit u u 26 2 3 CIRCUITS MP 27 2 35 BOCK i mem tecla mei ds 27 2 9 24 6 PB DIE es trinam iniret int 28 2 3 3 ts 33 2 34 TCD Gonttoller Mete yaa 37 GC 2014 Service Manual Table of Contents 2 3 5 FID Controller nete heredes 40 2 3 0 ECD e RED ER l edu 47 2 3 7 e Sal 50 2 3 8 FTD Power 54 2 9 9 PCB AUX e ERRAT ae evel 57 CHAPTER 3 GAS FLOW CONTROLLER 59 3 1 Configuration Diagrams for
25. 2014ASSY 100V 115V 221 70051 92 230V 221 70051 34 221 70080 91 PACKED DUAL INJ 100V 115V 221 70080 92 230V 221 70080 34 221 70075 91 DUAL AFC ASSY 221 70090 91 FID 2014 CELL ASSY P 221 70040 91 FID 2014 CONTROLLER DUAL 221 70085 91 DET HEATER ASSY F 100V 115V 221 70085 92 230V 221 70085 34 221 70049 91 FLOW CONTROLLER H2 AIR AD 221 70063 91 ACCESSORY GC 2014 115V 221 70063 91 230V 221 70063 96 10 2 1 3 GC 2014AFsc 221 70020 91 GC 2014AFSC 100 115V 221 70020 92 230V 221 70020 34 2 1 4 GC 2014AFSPL 221 70028 91 GC 2014AFSPL 100 115V 221 70028 92 230V 221 70028 34 Chapter 2 Configuration of GC 2014 221 70051 91 GC 2014ASSY 100V 115V 221 70051 92 230V 221 70051 34 221 70035 91 SPL 2014ASSY 100 115V 221 70035 91 230V 221 70035 34 221 70091 91 FID 2014 100 120V 115V 221 70091 91 230V 221 70091 98 221 70049 91 FLOW CONTROLLER H2 AIR AD 221 70049 94 FLOW CONTROLLER AUX 221 70064 91 ACCESSORY SPL 2014 SINGLE 221 70025 91 GC 2014AF 100V 115 221 70025 92 230 221 70025 34 amp 221 70035 91 SPL 2014ASSY 100 115V 221 70035 91 230V 221 70035 34 221 70952 91 DETECTOR ADAPTER ASSY GC 2014 Service Manual 11 Chapter2 Configuration of GC 2014 2 1 5 GC 2014AT 221 70027 91 221 70051 91 GC 2014 AT100V GC 2014ASSY 100V 115V 221 70027 92 115V 221 70051 92 230V 221 70027 34 230V 221 70051 34 221 70080 91 PACKED DUAL INJ 100V 115V 221 70080 92 230V 221
26. 92 FPD 2014 115V 221 70031 34 FPD 2014 230V reply orang ti jH 13811 i kih b r Pihi 4 54 Ed EPC PPT LIT ANE EET NEN IPE FEE KRATER AUTE HEAT LIE 725 MEAT Tj __ BASE 4 Pi hi 18858505 1 mer MEEARIATEHL ED wFACLH F TEL 21 FG rn Huan ASSP SIE MT TET TELE BOT TEA FL arrenar YP AST T PPD err SP PLATI FRE TED Sr bit Sari STAS FR MOSE FHI TRE _ ETT PRA Anc FPD FAT KRG 1511 Fr DE TRES FI ACOEREOITS PFD a EON ELLE FFO SFTS SI WZ PLOS PES SCR FI Ae ENE TES EJ iP MATER PP Trina IPE 1 mata MET TOTI TRE br WPL SETT hira Bp 4x Pr be LEE TAP Peo F md Boe i SERES SOLSET FED FH 386554 ehh TEL Be ARET HPU TP C He EC FIRE Thin FET IPF FREE 21 28308
27. APC Default value same for air Hj and make up gas Default value same for air H2 and make up gas Default value same for air Hj and make up gas pf4 ROM wrt pf5 BASE INJECTION UNIT AASSY There is no display for AUX APCs that have not been installed Default value Default value Default value pf4 ROM wrt pf5 Offset GC 2014 Service Manual 111 Chapter8 Service Window 8 4 Temp Sensor Use Time Temp Sensor Use Time Used time over 450 C Acceptable value h 26280 0 11111111 Column HH I Used time over 300 C h 57 5 INJ SPLI 1111111 Used time over 300 C h 25 3 INJ WBI2 EET 111 Used time over 300 C h 25 4 11111111 DETFIDT 111111111 Used time over 300 C h 32 0 DET 211111111 Used time over 300 C h 32 4 8 5 Mode Mode Service mode INSW Demo mode ECD Max Temp C GC 2014 Service Manual This window is used to check or reset the temperature sensor usage time for each unit Note The display items vary with the unit With the GC 2014 the time for which the temperature sensor has been used at a temperature of 300 or higher is calculated As a rough guide a warning is issued after approx 26 280 hours 3 years Press pf2 after replacing the temperature sensor to reset the usage time pf2 Pressing Reset clears the counter at the cursor position Service mode INSW Be sure to set to 0 in normal use In the following cases
28. DAFC and a manual flow controller W CARRIER L Back of unit top i i Sample Detector CARRIER IN injection unit R 1 Flow rate Back of unit bottom Sensor MERE VE PN u Be lt gt l Packed column Manual flow controller H air W s cim bora a ki a pcd k w Su k su ka w ik wak i I i Bellow valve 2k 1 I we DJ H resistance tube Pressure gauge 200 kPa 1 Bellow valve 2k I i I Air resistance Air resistance tube tube Speed controller Solenoid valve assembly GC 2014 Service Manual 72 Chapter 3 Gas Flow Controller 2 Flow Line for SPL and a The flow line shown applies for use in combination with AFC 2014 D Purge SPL manual flow controller 5 ASSV veps ASSV dari 06 0946 122 dari 3A3IS YVINOATION E8 LZLPE LZZ I 00 114 ASSY HALTS an 0 f 4019919 1HOd L6 6098F L ZZ 26 69967 122 seb dn yewL 1 aqn 5 I kiq ENUEIN aqny iy x e N T o 3 o 2 o o uds 91419913 251 bind uinid s Josues nss id l lui uunjoo 405195 55 oouejsi
29. FM MESS BUT AD Wc SCOR Tim PIRE M PL DOHTRDLLIR PTD ETE IPC SEREW SUS SEM ME DE IFL TPE COLLECTOR 1 TH MEEA 34 142728 2380 PE PibETO Hec 188124 L SEIS MEE 11 173 91433901 125 PL FID USIT F TD 20 4 TPC IMSIRLATCR I R iW SORT ROLLER FTD APC P LB 71 55 SPACER E5U 138 FLOW PL ECRPA HE FR I IPC SOREW SUS SEMIS P3 15 12 221 ABIEI 4 inam PC COVER ASSY FTD 2 COMER TH HB TFC TOP PLATE ffi iod WPW PT Hum IC KHOE L GC 2014 Service Manual 90 5 6 FTD 2014 Chapter5 Detector Unit T KEJ TATE KR GC 2014 Service Manual 92 Configuration Diagram for FTD 2014 dmn Hamid FTD 2 4 PACKED 1004 mne 2004 PACKED 115M PACHED 2184 IPC 2814 PACKED AEST FIBA FACKED 15 2814 TH TIEH 8 IPC H STDAG PACKED FLOW CONTREOL LER Ale FIT FID COLLECTOR ASSY ELECTROOE 2014 AR MILET TRAP ASSY inan BRAHUSED FIFE CAPILLARY ADAPTER DET RIM
30. Thermocouple Silicon glass tube Top side of element PT sensor 221 43695 91 4 Ensure that the top side of MAX 2mm the element is in front Element Thermocouple 221 43696 91 18 1mn WM3 P2 M3X10 One One CROSS PAN WASHER SCREW N3X10 The burring side goes here GC 2014 Service Manual 23 Chapter2 Configuration of GC 2014 2 2 6 Heater and PT Sensor Thermocouple HEATER ASSY Tubular insulators The end of the tube must Heater cable Part number name Heater resistance value ON COLUMN O HEATER ASSY 100 V 1 3 kW 710790 odd COLUMN OVEN HEATER ASSY 230 V 2 1 kW 24 6 to 25 8 Q Rear Side Inside wall of oven Heat insulating material Insulator Insulator 100 mm silicon glass tube 2 Motor die protrude a little from the insulator 2 2 7 Fan Motor 221 28242 01 020 46547 SCREW SUS SEMS P3 M4x8 MOTOR E0521 342 230 V 221 70358 4791 342 100 V 221 70489 MOTOR E4848 342 115 V 221 49649 MOTOR HOLDER GC 2014 Service Manual rR SI 020 46549 SCREW SUS SEMS P3 4 12 24 Chapter 2 Configuration of GC 2014 2 2 8 Fan When the fan P N 221 28247 is mounted onto the motor shaft and pushed to the positio
31. on the lower stream of the filter is removed resistance exists in the split line inside the AFC Next remove the joint on the upper stream of the filter If the pressure decreases the filter is clogged Prepare a new filter Next remove the joint on the upper stream of the buffer If the pressure decreases the buffer is clogged If the pressure does not decrease the cause originates in the INJ Check the glass insert and the split line inside the INJ If a glass insert for WBI is used set the column insertion length normally 34 mm to approx 15 mm 7 The purge flow rate does not agree with the setting Check that the column inlet pressure is sufficiently high A column inlet pressure of approx 4 kPa is required for a purge flow rate of 1 mL min This means that in analysis with inlet pressure of 8 kPa the purge flow rate cannot be set higher than 2 mL min GC 2014 Service Manual 101 Chapter7 Troubleshooting Check that I time 10 P term 50 and I term 100 If the values are different from the above values input these values and press the pf4 key to write them in the ROM Check the offset and gain values The offset value is normally in the range 32 000 to 33 500 and the gain value is normally in the range 7 000 to 12 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain t
32. parameters as shown below Baud rate 115200 Data bits 8 Parity None Stop bits 1 Flow control None Note After completing the settings click OK and leave Hyper Terminal running 3 Start the GC while pressing the SET and HELP keys and select 9 Enter sub menu from the menu that appears Simply press the 9 key on the numeric it is not necessary to press the ENTER key 4 Select 4 Set baud rate and then select 7 115200 The display returns to the Boot Sub menu Note At this point the same contents are displayed in the GC and Hyper Terminal windows Ifthe GC window is not displayed in Hyper Terminal press the PC s ENTER key 5 From Hyper Terminal select 7 Update Flash ROM select Transfer from the menu and then select Send File from the pull down menu 6 Specify the name of the ROM file for updating as the filename extension ROM select Ymodem G as the protocol and then click Send Note The ROM file is sent and the GC s ROM is automatically upgraded If the file s send status or the ROM s upgrade status is not displayed or the display returns to the Boot Sub menu before clicking Send go back to step 4 and repeat the subsequent procedure 7 Select 910 return to the Boot Menu and select 0 The GC runs in normal mode Close Hyper Terminal 8 Press the FUNC key and then press the key Version Check that the Version and Build No displayed correspond to those for the new version If the dis
33. 035 91 230V 221 70035 34 221 70952 91 DETECTOR ADAPTER ASSY 14 221 70051 91 GC 2014ASSY 100V Chapter 2 Configuration of GC 2014 221 70050 90 COMMON ASSY 221 70052 91 221 49613 91 OVEN HEATER ASSY 100V COLUMN OVEN HEATER ASSY 100V 115V 221 70052 92 115 221 49613 92 230 221 70052 34 230 221 49613 34 221 43695 91 PT SENSOR ASSY 17A PLUS 221 43696 91 THERMOCOUPLE 221 70072 91 WITH CONTACTS 17A MOTOR ASSY 100V 115V 221 70072 92 230 221 70072 34 221 48460 92 POWER UNIT 2014 100V 115V 221 48460 92 230V 221 48460 39 221 70706 91 221 46228 91 FILTER 55 100 AC CORD GC2010 100V 115V 221 70706 91 115 221 46228 91 230 221 70706 34 230 221 46228 98 221 70726 91 PS CABLE ASSY 100V 115V 221 70726 91 230V 221 70726 34 075 00072 04 ALTER ZAG2230 11S 100V 115V 075 00069 04 FALTER MBS 1220 22 230V 072 61022 05 CORD STOPPER JPG 16B 100V 115V 072 61012 04 BUSHING FLEX LTF13 5 230V 221 46229 93 PS CABLE STD GC2014 221 46230 91 PS CABLE DC STD 074 80654 77 POWER SUPPLY VS100B 24 100V 115V 074 80427 61 POWER SUPPLY LEA100F 24 201 31219 01 BLOCKING RUBBER TUBE 221 28247 FAN 221 12949 COOLING FAN 6125CCW GC 2014 Service Manual 15 Chapter2 Configuration of GC 2014 221 70050 90 A COMMON ASSY GC 2014 Service Manual 221 70055 91 221 70056 91 OVEN ASSY OVEN UNIT ASSY 221 70057 91 221 49480 AIR SUPPLY EXHAUST ADDITIONAL PROCES
34. 0621 91 1PC ACCESSORY ECD 2014 221 40578 40579 EN 1PC INSTRUCTION MANUAL ECD 2010J 221 40580 40581 EN 1PC INSTALLATION ECD 2010J 221 48455 92 1PC CONTROLLER ECD 2014 221 70049 94 1PC FLOW CONTROLLER AUX 201 42870 221 07755 EN 2PC RI 221 07682 29747 EN 1PC NAMEPLATE ECD VENT 221 41639 1PC LABEL ECD CAUTION 86 020 46147 3PC SCREW SUS SEMS P2 M4x8 023 66140 01 3PC WASHER SUS PLAIN M4 020 46534 1PC SCREW SUS SEMS P3 3 6 020 46547 2PC SCREW SUS SEMS P3 M4x8 221 09688 91 1PC PIPE AIR INLET 221 10115 ECD HEAT RETAINING BLOCK 1 221 10883 1PC MOUNTING PLATE DET SINGLE CENTER 221 00816 04 1PC SIGNAL CABLE AS ECD 2014 221 16036 91 1PC ECD ACCESSORY GC 7A 221 70647 1PC HEAT INSULATING MATERIAL DET S BUILT IN 221 70383 1PC NUT M10 CELL FIXING 221 32705 1PC CAP NUT 5 0 5 SLOTTED 221 33193 91 1PC CAPILLARY ADAPTER DET SIDE 221 41532 99 1PC GRAPHITE JIG ECD 2014 202 58258 02 1PC JOINT GL GN 2X0 5MT 201 48560 05 1PC PIPE MF GF 50 201 32069 1PC WASHER 201 48464 1 NUT M8 221 48602 91 1PC MOLECULAR FILTER WITH PLUG 221 14115 13 1PC ADHESIVE NAMEPLATE MAKE UP 072 60320 02 2PC WIRING BAND T30R 5 4 FPD oe UR Je Chapter 5 Detector Unit GC 2014 Service Manual 87 Chapter5 Detector Unit Configuration Diagram for FPD 221 70031 91 FPD 2014 100V 221 70031
35. 0V 221 70091 98 221 70610 91 221 70087 91 221 70458 91 FID 2014 HETER 55 100 DET HEATER ASSY PT 55 100 DET 115V 221 70610 91 SINGLE 100V 230V 221 70610 34 115V 221 70087 91 230 221 70087 34 050 73001 81 R RN AXIAL 1 2W 2202F 221 46520 92 FID 2014 CONTROLLER 221 70049 94 221 18150 93 FLOW CONTROLLER AUX N BELLOW VALVE 2K 8KIN 670 18558 11 PRESSURE GAUGE 200KPA 221 31745 HOUSING 221 19502 08 RESISTANCE TUBE HYDROGEN GC 8A 201 47435 RUBBER PLUG INJ ECTION PORT SILICON GC 2014 Service Manual 18 Chapter 2 Configuration of GC 2014 221 70086 91 221 70671 91 DET HEATER ASSY FT 100V HEATER PT ASSY D AD 100 115V 221 70086 92 115V 221 70671 92 230 221 70086 34 230 221 70761 34 221 70098 91 221 70743 91 221 70741 91 221 70742 91 TCD 2014 CELL ASSY 100V HOT PLATE ASSY 2014 100V HEATER PT ASSY TCD 100 HEATER ASSY 100V 200W 115V 221 70098 91 115V 221 70743 91 115V 221 70741 91 115V 221 70742 92 230V 221 70098 34 230 221 70743 34 230 221 70741 34 230 221 70742 34 221 32577 91 221 70740 91 ASSY COL TCD1 HEAT SENSITIVE MATERIAL TCD 221 32577 92 PIPE ASSY COL TCD2 050 73001 85 R RN AXIAL 1 2W 3302F 221 70744 91 TCD 100 OHMS 2014 221 13964 91 PIPE BENT 221 70043 91 074 80383 82 TCD POWER SUPPLY ASSY POWER SUPPLY ZWS30 48 J 221 46229 94 PS CABLE AC AUX 2014 221 70669 91 PS CABLE TCD DC 221 70952 91 221 34012 91 DETECTOR ADAPTER
36. 1 47653 91 POWER SWITCH ASSY 221 70082 81 SPL 2014 STOCKED 100 120 SPL 100 V tested for gas leaks and aged 221 70082 38 SPL 2014 STOCKED 220 240 SPL 200 V tested for gas leaks and aged 221 47735 93 AFC 2014 ASSY For SPL 221 48335 01 GLASS INSERT SPLITLESS WBI 221 48398 91 HIGH TEMPERATURE SEPTUM 20 per set 221 48460 92 POWER UNIT 100 V 221 48460 39 POWER UNIT CE 200 V 221 48600 SILICA WOOL 2 G Deactivated 221 47251 91 31 CHROMATOPAC SIGNAL CABLE WIDE For wide range output 31 model is CE compatible 221 47251 92 32 SIGNAL CABLE LINEAR CE For linear output 32 model is CE compatible GC 2014 Service Manua 95 Chapter6 Maintenance Parts Lists lt FID 2014 SINGLE gt P N Part name Remarks 221 70610 91 FID 2014 HEATER ASSY 100 FID 100 V 221 70610 34 FID 2014 HEATER ASSY 230 FID 200 V 221 70630 91 FID 2014 CELL BASE ASSY 221 47659 91 COLLECTOR ASSY FID 221 46520 92 FID 2014 CONTROLLER 221 21910 INSULATOR CERAMIC For FID collector 221 19503 08 RESISTANCE TUBE AIR Resistance tube only for air 221 19502 08 RESISTANCE TUBE H2 Resistance tube only for make up gas 221 31745 HOUSING RESISTANCE TUBE 221 70091 91 FID 2014 ASSY 100 120 V FID 100 V 221 70091 98 FID 2014 ASSY 220 240 V FID 200 V 201 48386 3 WAY SPLIT TUBING M TYPE 221 7016
37. 14 Service Manual 109 Chapter8 Service Window 8 1 Flow Adjust CAR Flow Adjust CAR1 Flow 111111 Carrier AFC Actual 40 2 Valve Voltage 40 2 Offset 32728 4210 I time 1 P term 15 I term 40 P mode I time P mode P term P mode I term 11111111 Purge Pressure v Press 111111 100 0 14 0 This window can be used to set the control parameters for the carrier gas flow controller DAFC for DINJ AFC for SPL 2014 or AFC for WBI 2014 If the set value and the actual measurement value of the flow rate or pressure differ adjustment can be made by changing the Offset or Gain value 32811 Sensor offset for carrier gas 4550 Sensor gain for carrier gas 5 MEN Default value ol Default value 100 1 ____ Default value 10 Default value 30 pf4 wrt pf5 Offset pf6 Prim Ofs Default value of AFC for SPL Default value of AFC for WBI is 12 100 Default value of AFC for SPL Default value of AFC for WBI is 10 Explanation of pf Keys Default pf3 ROM wrt pf4 Offset pf5 Continuation of Above Window Flow Adjust CAR1 INJ1 Flow 11111111 Purge Pressure Actual 40 2 Valve Voltage Offset PrimOfs pf6 Press 111111 100 0 14 0 33012 Gain I time P term 9620 10 1 Default value pl o o Default value I term 1 ____ Default value Primary Pressure 1111
38. 17 100 DGND PS7212 1A parry R54 02 100 15953 CEAT PGND 758140 085306 102 Ras 10K NFS DSS306 102 4 29 C m NFB FAN 5 D55306 102 FAN an os Lu COOLER 2302468 014 T bsssoe 102 C FAN I gt R25 012 88140 FARS i PGND Fig 2 3 27 Circuit Diagram for FPD Controller 3 3 GC 2014 Service Manual 53 Chapter2 Configuration of GC 2014 2 3 8 FTD Power Controller 53717081403 83106 013 16 6 9 122 ASSY se 0069 122 meng Fig 2 3 28 Assembly Diagram for Power Controller GC 2014 Service Manual 54 Chapter 2 Configuration of GC 2014 8 gt THIEF ET c16 5 SI slam 87 LIG DGND 20MH4z Fig 2 3 29 Circuit Diagram for Power Controller 1 2 GC 2014 Service Manual 55 Chapter2 Configuration of GC 2014 GC 2014 Service Manual HIN UN A5 10K D ND Fig 2 3 30 Circuit Diagram for FTD Power Controller 2 2 56 Chapter 2 Configuration of GC 2014 2 3 9 PCB AUX P o i Fig 2 3 31 Assembly Diagram for PCB AUX TEMP GC 2014 Service Manual 57 Chapter2 Configuration of GC 2014 J2 2 ACL 1 to Power 5 NFS AVdd 5 5 86 z ADS1211 22 23 B AGND 25opm deg m te
39. 2 92 NOZZLE ASSY PACKED 221 41532 98 GRAPHITE POSITIONING JIG FID 2014 221 41847 93 FILAMENT ASSY FID 221 70049 91 FLOW CONTROLLER H2 AIR FID 221 70298 91 BASE MAIN ASSY FID 221 47146 92 HIGH VOLTAGE ELECTRODE FID2014 lt FPD 2014 gt P N Part name Remarks 221 70562 FPD PACKING 036 11022 O RING 4C P22 201 48386 3 WAY SPLIT TUBING M TYPE 221 19502 08 RESISTANCE TUBE H2 Resistance tube only for 221 31745 HOUSING RESISTANCE TUBE 221 33193 91 CAPILLARY ADAPTER DET SIDE 221 46552 SILICA TUBE LARGE 221 46310 01 S FILTER FPD GC 2010 221 46310 02 G FILTER FPD GC 2010 221 46310 03 Sn FILTER FPD GC 2010 221 48456 92 FPD 2010 CONTROLLER 221 45647 91 IGNITER ASSY FPD 221 70617 91 FPD 2014 HEATER UNIT 100 FPD 100 V 221 70617 34 FPD 2014 HEATER UNIT 230 FPD 200 V 221 70778 91 FAN ASSY FPD For filter cooling 221 70049 93 FLOW CONTROLLER H2 AIR FPD 221 48578 PHOTOMULTIPLIER R5983 GC 2014 Service Manual 96 lt FTD 2014 CAPILLARY gt Chapter 6 Maintenance Parts Lists P N Part name Remarks 201 48386 3 WAY SPLIT TUBING M TYPE 221 18713 95 RESISTANCE TUBE ASSY H2 For FTD 221 18713 96 RESISTANCE TUBE ASSY AIR FTD 9 For FTD 221 21910 INSULATOR CERAMIC 221 19502 08 RESISTANCE TUBE H2 Res
40. 221 30116 GC 2014 Service Manual Analytical amp Measuring Instruments Division Product Guarantee Thank you for purchasing this product Shimadzu guarantees this product in the way described below 1 Guarantee Period This product is guaranteed for a period of one year from the date of installation This only applies in Japan 2 Scope of Guarantee If a fault that can be attributed to Shimadzu occurs during the guarantee period we will perform repair or part replacement as appropriate without charge 3 ltems Beyond the Scope of This Guarantee Faults that occur in any of the following cases are beyond the scope of this guarantee even if they occur within the guarantee period 1 A fault occurs as a result of incorrect handling 2 fault occurs as a result of repairs or modifications performed by parties other than Shimadzu or companies designated by Shimadzu 3 fault occurs due to factors unrelated to the equipment itself 4 The equipment has been used in a severe environment for example subject to high temperatures high humidity levels corrosive gases or vibrations 5 A fault occurs as a result of a fire or a natural disaster such as an earthquake 6 The equipment has been moved or transported since initial installation 7 fault occurs in a consumable item or a part dependant on a consumable item Note Program tape is a consumable item Disclaimer 1 The copyright of this document is the property of Shimadzu Corp
41. 3 3 GC 2014 Service Manual 36 Chapter 2 Configuration of GC 2014 2 3 4 TCD Controller AL OL n Fig 2 3 11 Assembly Diagram for TCD Controller GC 2014 Service Manual 37 Chapter2 Configuration of GC 2014 DGND 24V DSV ME SN75C1 168 RESET RESE DGND Dd Dd 5 Du Du Ck Ck 24 5V por pole TY 8 gt DGND PGND 5 12 p DGND PGND DGND Rae 5 1K 148 2302081 D2 155190 484 TAF8LOSF 3 PGND AGND CELLPOWER Fig 2 3 12 Circuit Diagram for TCD Controller 1 2 GC 2014 Service Manual 38 RADIATOR SKAW Yi GND2 PC1 DGND TLP 181 GB 200mA max REGISTER SPECIFICATION 1 10W 1 50 unless specified Chapter 2 Configuration of GC 2014 ADuM1300BRW 2 DAC8512F DSV 1 5K lt RANGE gt 1 57212 1 Ras 15KD 9 150 C4 0 1uffilm GND Mi ADS1210U AAA 2p 4 100K 100K 5 AAA 496 abs 0 1 rel IKEK R3 510 25ppm abs 5ppm rel OPA2277 1 abs 0 1 rel C ADS gt ND AGND 25ppm abs 5ppm rel gt Ri 510 gt R2 610 ASV gt AGND 1 8 xi DSV 2 7 S C38 R39 100 a 3 6 3 our cs F2 4 5 ment NFM21CC223 V cas C24 2 AGND EN 023 OPA2277 Y 5 y 50 AGND DGND DGN
42. 3 Configuration of Injection Unit j 221 47721 91 PORT AASSY shaded region 221 44584 NEEDLE GUIDE AOC 1 1 1 221 47435 RUBBER PLUG INJ PORT SILICON SPLIT LINE 221 70166 91 BASE INJECTION UNIT A ASSY Fi shaded region 026 11023 02 PARALLEL PIN SUS A1 6 x 4 221 70598 01 INSULATOR SPL 221 70421 HEATER BLOCK SPL 7 22 201 46833 NUT M10 221 42998 NIPPLE FOR GASKET M 201 30051 WASHER WM 201 30008 NUT MF GC 2014 Service Manual 77 Chapter4 Sample Injection Unit 4 3 1 Heater Resistance Values for HEATER PT ASSY SPL 100 and HEATER PT ASSY SPL 230 Model name Heater resistance values HEATER PT ASSY SPL 100 90 0 to 99 3 Q HEATER PT ASSY SPL 230 429 8 to 48400 4 3 2 Recognized Resistance Values for HEATER PT ASSY SPL 100 and HEATER PT ASSY SPL 230 As shown in the configuration diagrams and flow line diagrams for SPL 2014 and WBI 2014 the sample injection unit for SPL 2014 and WBI 2014 both use the SPL 2014 unit for 100 120 V or 220 240 V which has a recognized resistance value of 1 regardless of the voltage type For this reason it is requested that the temperature control port name is set by the user when installing the WBI 2014 so that SPL and WBI can be distinguished on the monitor screen 4 3 3 Precautions for Replacing HEATER PT ASSY SPL 100 and HEATER PT ASSY SPL
43. 33 1K 2K 1 gt AGND e DION CONE VREF gt _ lt gt P 36414 AGND Ma 51211 Fig 2 3 23 Circuit Diagram for ECD Controller 2 2 GC 2014 Service Manual 49 Chapter2 Configuration of GC 2014 2 3 7 FPD Controller Fig 2 3 24 Assembly Diagram for FPD Controller GC 2014 Service Manua 15 PGND J1 gt gt g SEESUTOR NF3 45V DSS300 102 PLOSV C35 01u l D cao pano _ 147 Dd gt gt gt 556 BusDd 20 mou aa DU bus 19 PROMO 2 I PROM Q 44 BusCk VE TEEN prom 622 Pos js KE 5 ORG 4 BusEn BusEn RA Rao M3 93048 15 BusOu a 10K 10K gt DAND 2 gt gt DGNO 1 ADO ADO PGND DGND AD1 ADS D Ais Ris ll gt 51K 5 1K 41 ADM ADIT Ne AT pent HAT BAI JIMA FORT 4 io Yi 0003 4 5V 1 s ROY2 ROY DGND 2 P0GND 11 TCK 3 x 5 34 HVOVER TDI 4 55 TD HV OVER CHVOVER gt 5 e i 100 TMS 6 TMS L IGNITE IGNITE R14 CERT Astin BATTCK 28 BATTCK BATTER 1 ge IT C m 299202222922 XG9596 TESS xi NF DGND RESET aar 5 ST F 1 085306 221 813100 NF2 p QOMHz un 5
44. 70080 34 221 70075 91 DUAL AFC ASSY 221 70086 91 u DET HEATER ASSY FT 100V 115V 221 70086 92 230V 221 70086 34 221 70063 91 ACCESSORY GC 2014 115V 221 70063 91 230V 221 70063 96 221 70098 91 TCD 2014 CELL ASSY 100V 115V 221 70098 91 230V 221 70098 34 221 70041 91 TCD 2014 CONTROLLER 221 70043 91 TCD POWER SUPPLY ASSY 221 11386 91 TCD ACCESSORY SET GC 2014 Service Manual 12 2 1 6 GC 2014ATF 221 70026 91 GC 2014ATF 100V 115V 221 70026 92 230V 221 70026 34 Chapter 2 Configuration of GC 2014 221 70051 91 GC 2014ASSY 100V 115V 221 70051 92 230V 221 70051 34 221 70080 91 PACKED DUAL INJ 100V 115V 221 70080 92 230V 221 70080 34 221 70075 91 DULA AFC ASSY 221 70090 91 FID 2014 CELL ASSY P 221 70040 91 FID 2014 CONTROLLER DUAL 221 70086 91 DET HEATER ASSY FT 100V 115V 221 70086 92 230V 221 70086 34 221 70049 91 FLOW CONTROLLER H2 AIR AD 221 70063 91 ACCESSORY GC 2014 221 70098 91 TCD 2014 CELL ASSY 100V 115V 221 70098 92 230 221 70098 34 221 70041 91 TCD 2014 CONTROLLER 221 70043 91 TCD POWER SUPPLY ASSY 221 11386 91 TCD ACCESSORY SET GC 2014 Service Manual 13 Chapter2 Configuration of GC 2014 2 1 7 GC 2014ATFSPL 221 70029 91 GC 2014ATFSPL 100 115 221 70029 92 230 221 70029 34 GC 2014 Service Manual 221 70026 91 GC 2014ATF 100V 115 221 70026 92 230 221 70026 34 221 70035 91 SPL 2014ASSY 100 115V 221 70
45. 91 HEAT SENSITIVE MATERIAL 221 41135 94 AFC 2014 D PURGE WBI 221 48440 94 221 42559 92 PIPING ASSY FILTER ASSY WITH BLIND AFC WBI ADDITION 221 34121 94 MS FILTER CONDITIONING 221 48609 91 3 PORT PIPE 221 48619 94 ACCESSORY ASSY WBI 2014 GC 2014 Service Manual 75 Chapter4 Sample Injection Unit 4 2 Piping for Sample Injection Unit Piping for SPL 2014 4 7 AFC2014 D PURGE SPL CARRIER IN Total Flow Controller MOLECULAR SIEVE FILTER Back of unit i Pressure sensor 1 TFC 224 34121 03 Flow rate sensor z 221 42559 92 d FILTER ASSY 221 42550 02 ssure FILTER ASSY Purge Controller 221 48441 01 LL BUFFER ASSY SPL Detector UNIT Column oven 4 Valve Sensor Control valve b so that the value for sensor becomes constant Piping for WBI 2014 221 48609 91 221 34121 93 3 PORT PIPE pr MOLECULAR FILTE Total Flow Controller CARRIER IN I Back of unit Flow rate sensor Pressure sensor 1 9 SE ERR PURGE VENT 221 42559 92 Control mode FILTER ASSY Pressure Flow sensor Rate Li Septum Purge Controller Velocity Pressure I GC 2014 Service Manual 76 Chapter 4 Sample Injection Unit 221 41286 SEPTUM 4
46. ASSY WBC DET ADAPTER WITH PURGE 221 15561 92 JOINT SET DET ADAPTER 221 15563 91 GRAPHITE FERRULE FOUR GC 2014 Service Manual 19 Chapter2 Configuration of GC 2014 2 2 Structure of GC 2014 2 2 1 External Appearance FLOW CONTROLLER UPPER COVER 221 70515 UPPER COVER 221 70378 DOOR ASSEMBLY 221 70065 91 GC 2014 Service Manual gt MEN Pa 20 KEY COVER 221 70368 Chapter 2 Configuration of GC 2014 2 2 2 Structure Diagram 1 KEY RUBBER 1 KEY RUBBER 2 221 4647 1 TAPE WIRE 221 70465 GC 2014 Service Manual 21 Chapter2 Configuration of GC 2014 2 2 3 Structure Diagram 2 POWER UNIT 2014 100 V 100 V system 221 48460 92 POWER UNIT 2014 230 V 200 V system 221 48460 39 FILTER ZAG2230 11S 100 V system 075 00075 04 FILTER MBS 1220 22 200 V system 075 00069 04 PCB DET I F GC2014 221 70254 91 POWER SUPPLY 5100 24 100 system 074 80654 77 POWER SUPPLY ZWS100PF 24 J 200 V system PCB CPU ASSY GC2010 074 80383 56 221 45737 91 GC 2014 Service Manual 22 Chapter 2 Configuration of GC 2014 2 2 4 Structure Diagram 3 MOTORASSY 221 70072 91 MOTOR ASSY 115 221 70072 92 MOTOR ASSY 230 221 70072 34 2 2 5 PT Sensor and
47. Assembly Configuration Chart 221 47735 94 221 48740 91 AFC 2014 D PURGE WBI FLOW BOARD ASSY AFC2 221 47775 91 221 45749 91 AFC BASE ASSY PCB AFC ASSY GCX 221 48625 91 PIPING ASSY WBI 221 47779 91 VALVE ASSY 221 48187 91 PRESSURE SENSOR ASSY DAFC Assembly Configuration Chart 221 70075 91 221 70721 91 FLOW BOARD ASSY DUAL 221 70732 91 221 70258 91 AFC BASE ASSY PCB ASSY D AFC 2014 221 48585 91 PIPING ASSY 221 48813 91 VALVE ASSY 221 48187 91 DIFFERENTIAL PRESSURE SENSOR ASSY 221 48187 92 DIFFERENTIALPRESSURE SENSOR ASSY LONG GC 2014 Service Manual 59 Chapter3 Gas Flow Controller AUX AMC ASSY 221 70721 91 221 701091 91 FLOW BOARD ASSY DUAL 221 70732 92 AMC BASE ASSY 221 48585 91 PIPING ASSY 221 48813 91 VALVE 55 221 48181 91 DIFFERENTIAL PRESSURE SENSOR 55 221 48187 92 DIFFERENTIAL PRESSURE SENSOR ASSY LONG GC 2014 Service Manual 60 Chapter 3 Gas Flow Controller 3 1 2 Manual Flow Controller 3 1 2 1 FID 221 70049 91 FLOW CONTROLLER H2 AIR HD 11 221 18150 91 1PC N BELLOW VALVE 2K 221 41511 91 1PC N BELLOW VALVE 2K WITH RESISTANCE 670 18558 11 2PC PRESSURE GAUGE 200 KPA 018 21330 TAPE STICKER 0 1 x 13 x 5 221 70483 91 1PC SOLENOID VALVE ASSY 042 40043 02 1PC SPEED CONTROLLER ASN2 M5 035 60395 43 2PC GASKET 221 31745 2PC HOUSING 221 19502 08 1PC RESISTANCE TUBE HYDROGEN GC 8A 201 47435 3PC RUBBER PLUG PORT
48. D JXO 5 10MHz AGND AGND 5 V AGND OPA2277 Fig 2 3 13 Circuit Diagram for TCD Controller 2 2 GC 2014 Service Manual 39 Chapter2 Configuration of GC 2014 2 3 5 FID Controller SILK PARTS 1 AFSC FTD or Additional FID Eg NER p 0 BOARD 221 45510C ASSY 22 Birds Vi ud Fig 2 3 14 Assembly Diagram for Single FID Controller GC 2014 Service Manual 40 Chapter 2 Configuration of GC 2014 2 AF ATF AF SPL or ATF SPL 800060008 0 Ri 208 CE gf r ACHE Top Over lay Fig 2 3 15 Assembly Diagram of Dual FID Controller GC 2014 Service Manual 41 Chapter2 Configuration of GC 2014 T DET Interface GC 2014 Service Manual ASV SHIELD 2 5V sj nr pes LET sl 3 ca 1 pGND DGND GND 4 TCK 11 i mo 9 9 Z Z X wm 33 BS gt E 25 1 IGNITE gt 2 PROM AD CONVERTER NC C gt Fig 2 3 16 Diagram for Single FID Controller 1 2 42 Chapter 2 Configuration of GC 2014 I i MAT DLAH 3 AGND SHELD1 gs 29 GEO i 15 AUN AGND 3 10KF v C16 C17 C15 C19 AGND is L NER EAD SHIELD 2 I i CA
49. Detector Unit Number P N Part name Quantity 11 221 70630 91 FID 2014 CELL BASE ASSY 11 1 221 70298 91 BASE MAIN ASSY FID 11 2 221 70162 92 NOZZLE ASSY PACKED 11 3 221 47146 92 HIGH VOLTAGE ELECTRODE FID2014 33 221 47659 92 COLLECTOR ASSY FID 600MM 36 221 41847 93 FILAMENT ASSY 180MM a 83 GC 2014 Service Manual Chapter 5 Detector Unit 5 2 1 DET HEATER ASSY F Vest ORI Parts List for DET HEATER ASSY F 221 70085 34 230V 91 100V 92 115V Number P N Part name 230V 100V 115V 11 221 70671 34 PT ASSY D FID 230 1 11 221 70671 91 HEATER PT ASSY D FID 100 1 11 221 70671 92 HEATER PT ASSY D FID 115 12 221 70124 DET DUAL UPPER COVER FID 13 221 70127 DET DUAL BLOCK PLATEA 14 221 70139 LOCK RING DET DUAL 16 221 70136 DET DUAL BLOCK UPPER a a a a a a 17 221 70137 DET DUAL BLOCK LOWER GC 2014 Service Manual 84 Chapter 5 Detector Unit 5 3 ECD ECD CELL GC 2014 Service Manual 85 Chapter5 Detector Unit Configuration Diagram for ECD 221 25055 91 ECD 9 221 10032 34 ECD 2014 CONTROLLER 230 221 10032 91 ECD 2014 CONTROLLER 100 221 41133 92 ECD 2014 CONTROLLER 115 GC 2014 Service Manual 221 7
50. ENTS1 COM EVENTSTNG 1 EVENIST NO EVEN 92 020M R53 10K START INI STARTAN C34 1 0 14 START IN 1 DGND READY NO2 9902 12 i ALY COM 3 E m 4 ls Ex Bus 1 STANTOUT COM 2 stanou Starl Ready Fig 2 3 5 Circuit Diagram for CPU Unit 3 4 GC 2014 Service Manual 31 Chapter2 Configuration of GC 2014 MC1413 701 16 9 HALO vm FLAP AQ Lid TAI HAPB gt Hi Verte S 10 VARI 2 VAR GC 2014 Service Manual SIGNALI POWER MONITOR SIGNAL 412V Mu CREF 2 5 gt TRIP o NF16 UMP R34 DSS306 102 E gt 9 wes av READY I2 S al ds No AGND Signal out CH1 TC74VHCO4F R38 AGND gt 750 25pprr TLP521 2 GB R43 R44 CREF 2 5 100K 17 TCTVHCOAF po RasaKQSpem 85306102 MwesD 9 je 5 d 039 m 45 sv 1 READY22 Nam 1 7060 6 am SAK AGND F 5 Signal out CH2 AGND AKT V AGND 837 DGND TLPS21 2 GB AGND 750 25 15 7 AN7812F 12 v IN OUT PGND DGNDIEM22 D pi nSttat TIER 2 LM2576T 5 5V Fig 2 3 6 Circuit Diagram for CPU Unit 4 4 32 Chapter 2 Configuration of GC 2014 2 3 3 Power Unit Note Insert PT1 DT5 into PCB untill arr
51. GNAL pS ba uv PRX 1301 me Jl 01 21 NI tar 000 PL sk scko 31 EXTO EN PAS gt DGND 114 CONTRAST Ps WEE EXT AK S poga 10K 28C2458 T8 SEX TX EXTI CK es 07 82 EVENTS VECONTRASD 5 EXTEN aa 5022 4 EVENTOS SEVENTY RE 2023 PD25 STARTO VENTD 1 i AMA e READY 17 tu 7 8 01 PD27 lt READY gt Poze e ep 8810 32 V RAM P020 SPL2 gt KARM 2 mo 1 3 18 Otu GNO 54 Eri MIA pee 1 COLH FAT gt EA pag 51 COL H ra gt Fa Rem MEM ec Hie nac TT TT 1 gt 4580 gt DC WONT TT Td MIC LED2 SE PEIS BIN S eg AK 3 dank CPU ROM RAM FRETEEET pow gt gt gt gt gt gt gt gt gt gt gt gt gt gt s L 6 OGND 33335310 5V mm EI V PMG DGND 3 2 23 m 2 2 z 2 DGND 6 8 8 8 8 5 8 578 Fig 2 3 3 Circuit Diagram for CPU Unit 1 4 GC 2014 Service Manual 29 Chapter2 Configuration of GC 2014 EEE GS Gu iy 01 Olu 019 Olu M19 5V o DGNOT DGNDT C15 C16 014 n 1u O1u D15 A13 014 i D13 p D12 d 2 s lt NA 2 gt 3 2 010
52. Gas Flow Controller 59 SANE ICI Er 59 3 1 2 inh E ure f 69 Nn EHE 69 Le REE EEE uM EE ee 70 21 29 EE ha 71 3 2 Flow Line Diagram for Gas Flow Controller 72 CHAPTER 4 SAMPLE INJECTION UNIT 75 4 1 Configuration Diagrams for Sample Injection 75 4 2 Piping for Sample Injection Unit 76 4 3 Configuration of Injection Unit 77 4 3 1 Heater Resistance Values for HEATER PT ASSY SPL 100 and HEATER PTASSY CSPE 290 S a m isa m em mita 78 4 3 2 Recognized Resistance Values for HEATER PT ASSY SPL 100 and HEATER ASSY SPL 230 2 4 2 78 4 3 3 Precautions for Replacing HEATER ASSY 100 and HEATER PTASSY SPL230 5 7 Etat 78 44 Packed Dual Injector 79 CHAPTER 5 DETECTOR UNIT 81 SEE TED u oaa pcc cc 81 5 1 1 DET HEATER ASSY ET u S R A Na A Aaa 82 n iiec pite dini sapa awama hu ma cmd fase cmd Losa ss 83 5 2 DET AEATERASSY Tu uum edes 84 So ELD eee 85 d ene
53. Hz 2 90 to 110 VAC 104 to 126 VAC 207 to 253 VAC 50 60 2 50 60 2 50 60 2 voltage 1 3 2 Power Supply Capacity Calculate the power supply capacity by totaling the power consumption for each of the following parts Connect the instrument to a terminal with a sufficient capacity Unit Power consumption Standard model equipped with TCD FID 1 850 VA 100 V model 2 650 230 V model Additional temperature control block e g INJ 150 VA or 200 VA dual for FID and TCD only NOTE instrument will not attain its performance specifications if the power supply voltage is unstable or if the power supply capacity is insufficient GC 2014 Service Manual Chapter 1 1 4 Gas 1 4 1 Purity Installation In order to maintain performance specifications prepare the following gases Use air that has been compressed in an oil less compressor and then dehumidified 1 4 2 Supply Pressure Carrier gas Make up gas Hydrogen Air 1 psi NOTE 6 89 kPa 300 to 980 kPa 300 to 980 kPa 300 to 500 kPa 300 to 500 kPa Use the following formulas for approximate conversion between kPa and kgf cm 1 kPa 1 02 107 cm 1 kgf cm 98 1 kPa Use the following formulas for approximate conversion between kPa and psi 1 kPa 1 45 x 10 psi Carrier gas Detector gas Detector He 2 usable Oth
54. ND M128 ADS1210 MAT 01AH 5 Tou T ra p 125 a e sa 21 223 2 4 01 220p HR C46 ui 155190 asy O 4u film 1 11 ADS49KH b di AGND AGND AGND AGND D88 155396 R5 1K 2 T x o HV MON Mian 75 188306 lt HYNON gt 100p 2 16 gt TG MON SR V CENON 10 AGND DEND lt DEND lt R27 VREF VREF 24KF 40kF ren M10B u 100p AGND AD706UR 51211 DEND AGND 3 M13A MAT 01 AH C30 0 01uffilm IHR 1M R25 330KF INPUT2 428 CH M13B M14B 010 MAT 01AH gt x Va TM2 02 V 25 AGND 185190 AD549KH C10 V V 0 tu AGND AGND V AGND M10A AD7OSJR Chapter 2 Configuration of GC 2014 ADRDY1 ADEST lt R13 540F R39 1002 50 100p ADRDY 52 ADI xi DSV DC 1 3 F4 QUT 21 223 GND 2 V DGND DEND JXO 5 10MHz Fig 2 3 19 Circuit Diagram for Dual FID Controller 2 3 GC 2014 Service Manual 45 Chapter2 Configuration of GC 2014 R34 1MF R9 RIO 424V 0 33450 C35 D5 O 01u630V DIFL4AO R32 IMF R41 IMF R42 1MF Q5 171 10 ELN02C SE D10 HV 7A IC N 128180 R3 10 80 PGND PGND 5 d Qa FOND Co da Spore 2SA1201 PGND C36 Li 24V 47u35V 28 97 104 476 5 476854 12 Q10 2802712GA BLM21PG600 BLM21PG600
55. SING PIPE ASSY GEAR MOTOR 221 47652 FLAP MOTOR 221 70060 91 221 70254 91 RIGHT PLATE PCB DET I F GC 2014 GC 2014 221 47632 92 221 45737 91 CPU UNIT GC 2014 PCB CPU ASSY GC2010 221 70065 91 221 70066 91 DOOR ASSY HEAT INSULATING MATERIAL DOOR ASSY 221 70353 DOOR 221 49609 HOOK DOOR 221 49611 SHAFT DOOR 221 70250 91 PCB KEY ASSY GC 2014 221 70368 KEY COVER 221 48721 91 LCD ASSY 221 70244 LCD FILTER 221 70369 UNDER COVER 221 70725 TAPE WIRE 221 70070 91 221 45745 97 AFC UNIT PCB FLOW I F GC2010 221 47663 01 FLAT CABLE 34P 221 47653 91 POWER SWITCH ASSY 221 70515 FLOW CONTROLLER COVER 037 02820 57 KNOB KNURLED 1 4 8 WHITE 16 221 70080 91 PACKED DUAL INJ 100V 115 221 70080 92 230 221 70080 34 221 70090 91 FID 2014 CELL ASSY P 221 70085 91 DET HEATER ASSY F 100V 115 221 70085 92 230 221 70085 34 221 70049 91 FLOW CONTROLLER H2 AIR AD Chapter 2 Configuration of GC 2014 221 70189 91 INJECTION UNIT ASSY 122 221 70479 91 221 70484 91 HETER PT ASSY P INJ100 HEATER 100V 150W ASSY 115V 221 70479 92 115V 221 70484 92 230 221 70479 34 230 221 70484 34 221 44584 221 70596 91 GUIDE FOR NEEDLE FIN HEAT SENSITIVE MATERIAL INJ 221 70466 050 73001 79 FIN 2014 R RN AXIAL 1 2W 1802F 221 22206 SPACER INJ 221 70630 91 221 70298 91 2014 CELL BASE ASSY BASE MAIN ASSY 221 70162 92 NOZZLE ASSY PACKED 221 47146 92 HIGH VOLTAGE ELECTRODE
56. V 072 02004 23 FUSE 218 15 100 V 072 01665 34 FUSE 10A 200 V 072 02004 21 FUSE 218 3 15 200 V 074 73307 01 LITHIUM BATTERY CR2032 074 80427 61 POWER SUPPLY LEA100F 24 200 V 074 80654 77 POWER SUPPLY VS100B 24 100 V 221 48721 91 LCD ASSY GC 2010 Equipped with gasket 201 35584 RUBBER SEPTUM INJ PORT 20 per set 221 12949 FAN 100 V 200 V 221 32126 05 GRAPHITE FERRULE G 0 5 10 per set 221 32126 08 GRAPHITE FERRULE G 0 8 10 per set 036 11203 84 O RING 4D P5 For INJ 5 per set 221 32705 CAP 5 0 5 SLOTTED 221 16325 NUT NOT SLOTTED 221 34121 94 BUFFER TUBE ASSY Aged 221 41286 SEPTUM NUT 221 41444 GLASS INSERT SPL17 221 43597 COVER RADIATING FIN 221 49613 91 HEATER ASSY COLUMN OVEN 100 V 221 49613 92 HEATER ASSY COLUMN OVEN 115 V 221 49613 34 HEATER ASSY COLUMN OVEN 230 V 221 43695 91 PT SENSER ASSY COLUMN OVEN 221 43696 91 THERMOCOUPLE ASSY COLUMN OVEN 221 43710 HOLDER PT SENSOR 221 44584 NEEDLE GUIDE AOC 221 70254 91 DET I F GC2014 221 45745 91 PCB FLOW I F GC 2010 221 70250 91 PCB KEY ASSY GC 2014 221 46470 01 KEY RUBBER 1 KEY PANEL 221 46471 01 KEY RUBBER 2 KEY PANEL 221 70602 91 HEATER PT ASSY SPL100 221 70602 34 HEATER PT ASSY SPL230 221 47632 92 CPU UNIT GC 2014 221 70072 91 FAN MOTOR ASSY 100 V 221 70072 92 FAN MOTOR ASSY 120 V 221 70072 34 FAN MOTOR ASSY 230 V 221 47652 FLAP MOTOR 22
57. ace the FTD collector 7 5 Other Problems 1 The display is dark or goes out Cause Countermeasure Backlight ON OFF or contrast has been adjusted inappropriately Readjust backlight ON OFF and contrast The value set for automatic OFF operation of the backlight in Other configuration settings is inappropriate Change the value set for automatic OFF operation of the backlight 2 Chromatopac is not started by GCSTART when the Chromatopac signal cable is used Cause Countermeasure The channel started by the link device code in Configuration settings is not ON Set the channel started to ON 107 GC 2014 Service Manual Chapter7 Troubleshooting 3 The sample injection unit and the detector are not recognized Cause Countermeasure There is contact failure or caulking failure in the recognized resistance for the sample injection unit or the detector Check the contact state and the caulking state of the recognized resistance The recognized resistance values measured between pins 1 and 2 on the connector are as follows SPL WBI both recognized SPL 1 FID FTD both recognized as FID 221 TCD 33 47 FPD 39 FTD 2014 22 FTD 2014C 22 FID DUAL 27 temperature control port for the detector control unit to be used is not set Make the correct setting fo
58. al 98 Chapter 7 Chapter 7 Troubleshooting Troubleshooting When performing troubleshooting first refer to the chapter on troubleshooting in the instruction manual This chapter mainly describes possible causes and countermeasures not covered by the instruction manual Refer to the item applicable to the symptoms displayed by your instrument 7 1 Gas and Pressure Flow Rate Settings 7 1 1 Precautions for Flow Rate Control Settings CAR 7 1 1 1 When the control mode is SPLIT or SPLITLESS 1 The total flow rate fluctuates unstable Check that I time 1 P term 15 and I term 40 If the values are different from the above values input these values and press the pf4 key to write them in the ROM Check for fluctuations in the cylinder s source pressure If the source pressure is shared e g the helium carrier gas is used for the detector s make up gas and carrier gas check for pressure fluctuations in the other line 2 The total flow rate is lower than the setting Check whether or not the source pressure i e the primary pressure has been attained The source pressure can be ascertained by viewing the Actual value for the primary pressure in the Flow Adjust window It is not necessary to remove any piping Check whether or not the setting is within the range of settable pressures flow rates for AFCs A graph is given in the section on AFCs in the GC 2014 instruction manual Check that a blind
59. aves and Power Supply Noise Do not use this instrument in locations subject to strong electromagnetic waves or use with power supplies that generate high noise levels Doing so may result in malfunction and it may not be possible to obtain data that conforms to specifications 1 2 5 Other Precautionary Items In order to maintain performance specifications give due consideration to the following points 1 Changes in the ambient temperature during operation must be kept to a minimum 2 The instrument must not be directly exposed to the airstream emanating from heating or cooling equipment 3 The instrument must not be exposed to direct sunlight 4 Vibrations must be kept to a minimum GC 2014 Service Manual 1 3 Power Supply DANGER Chapter 1 Installation High Voltage Before connecting the power cable directly to the terminal block in the switchboard be sure to turn OFF the switchboard switch Be sure to supply power from a power supply incorporating a circuit breaker Do not place heavy objects on the power cable Check the following points before connecting the power supply 1 3 1 Power Supply Voltage In order to maintain performance specifications use a power supply that falls within the following specified power supply voltage ranges 100 VAC specifications 115 VAC specifications 230 VAC specifications LIS 95 to 105 VAC 110 to 120 VAC 219 to 241 VAC volte 50 60 Hz 50 60 Hz 50 60
60. back of the instrument when the column oven is cooled Observe the following points when installing the instrument Do not place flammable objects directly behind the instrument Leave a space of at least 40 cm between the back cover and the wall In addition to the space mentioned above give consideration to the space required for maintenance and inspection 1 1 2 Side Space Leave a space of at least 5 cm on the left of the instrument Leave a space of at least 10 cm on the right of the instrument to enable opening and closing of the oven door 1 2 Installation Environment In order to ensure safe correct use of the instrument observe the following points when selecting an installation site 1 2 1 Ambient Temperature and Humidity In order to maintain performance specifications use the instrument within the specified temperature and humidity ranges given below Specified temperature range 18 C to 28 C Specified humidity range 50 to 60 Operating temperature range 5 C to 40 C Operating humidity range 5 to 90 without condensation GC 2014 Service Manual Chapter 1 Installation 1 2 2 Installation Surface Install the instrument on a steady stable flat surface 1 2 3 Corrosive Gas and Dust In order to attain the specified service life and maintain performance specifications do not install the instrument in locations subject to large amounts of corrosive gas or dust 1 2 4 Influence of Electromagnetic W
61. e P term 50 and P mode I term 100 If the values are different from the above values input these values and press the pf4 key to write them in the ROM If the AFC for WBI is used the above values are as follows P mode I time 10 P mode P term 12 and P mode I term 10 Check the offset and gain values The offset value is normally in the range 32 000 to 33 500 and the gain value is normally in the range 3 000 to 6 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain the correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC GC 2014 Service Manual 103 Chapter7 Troubleshooting 7 1 1 4 Precautions for Flow Rate Control Settings DetAPC 1 The pressure or flow rate fluctuates Check that I time 10 P term 50 and I term 20 If the values are different from the above values input these values and press the pf4 key to write them in the ROM Check that the source pressure is not fluctuating If the source pressure is shared e g the helium carrier gas is used for the detector s make up gas and carrier gas check for pressure fluctuations in the other line 2 The pressure or flow rate is lower than the setting e Check for leaks in the line
62. e igniter filament is red hot even though the ignition operation is not being executed this means that the hydrogen flame is out Ignite the hydrogen flame The nozzle is clogged Clean using for example CLEANING WIRE 201 79229 01 or replace the nozzle Refer to 4 11 2 Maintenance Inspection in the instruction manual for details on mounting and removing the nozzle A high voltage is not output Set the detector to ON and check the voltage between the end of the nozzle and earth Ifa DC voltage of approx 160 V when measured using a tester with impedance of 10 is not output it means that there is a fault in the high voltage circuit or contact failure or disconnection in the high voltage electrode assembly Replace the FID control board or repair or replace the high voltage electrode assembly 3 Peaks are not output or are extremely small FPD used as detector Cause Countermeasure The flow rate for hydrogen or air is inappropriate Check the actual measurement value of the flow rate for hydrogen or air and also check the piping to the detector 4 Peaks are not output or are extremely small FTD used as detector Cause Countermeasure Hydrogen is not flowing into the detector Check the actual measurement value of the flow rate for hydrogen or air and also check the piping to the detector The FTD collector has reached the end of its service life Repl
63. e injection port or the detector is not set to line configuration Temperature control is not possible for units not set to line configuration Set the corresponding unit to line configuration 7 3 Detector 7 3 1 FID 1 Ignition is not possible Cause Countermeasure The igniter filament has burnt out Replace the igniter Refer to 4 11 2 Maintenance Inspection in the instruction manual There is a fault in the igniter circuit Check the voltage at both ends of the connector between 1 and 2 of CN2 at ignition with the igniter filament connected If a DC voltage of approx 2 V is not output approx 10 s after Ignition started or Ignition is retried then there is a fault in the ignition circuit Replace the FID control board The nozzle is clogged with the sample or the graphite ferrule residue Clean using for example CLEANING WIRE 201 79229 01 or replace the nozzle Refer to 4 11 2 Maintenance Inspection in the instruction manual for details on mounting and removing the nozzle There is a lot or a high level of noise Cause Countermeasure The collector is dirty After removing the igniter clean the metal portion of the collector in a liquid such hexane Refer to 4 11 2 Maintenance Inspection in the instruction manual for details on mounting and removing the collector The H flow rate is fluctuating Replace the APC
64. er H2 Air Make up recommended FID 99 995 min 99 995 min 99 99596 min RD Mp 99 999 min 99 999 min 99 999 min Cylinder air Mena in in i sensitivity Y 99 999 min Ar etc TCD 99 995 min 99 995 min 99 995 peser 198 99 995 min min Ar etc TCD high Ar etc 99 999 min 99 999 99 9999 sensitivity 99 999 min min ECD 99 99996 min 99 990 min N2 99 999 min high 99 9999 99 9999 sensitivity min 99 9999 min FPD 99 999 min 99 999 min 99 999 min Cylinder air He FTD 99 999 min 99 999 min Cylinder air 99 999 min e For precautions on handling high pressure gas cylinders and using hydrogen gas refer to the instruction manual for the GC 2014 main unit GC 2014 Service Manual Chapter 2 Configuration of GC 2014 Chapter2 Configuration of GC 2014 2 1 Configuration Diagrams for GC 2014 Series 2 1 1 GC 2014A 221 70019 91 GC 2014AD NONE DUAL 100 221 70051 91 GC 2014ASSY 100V 221 70080 91 PACKED DUAL INJ 100V 115 221 70080 92 230 221 70080 34 221 70075 91 DUAL AFC 55 221 70063 91 ACCESSORY GC 2014 115V 221 70063 91 230V 221 70063 96 GC 2014 Service Manual Chapter2 Configuration of GC 2014 2 1 2 GC 2014AF 221 70025 91 GC 2014AF 100V 115V 221 70052 92 230V 221 70052 34 GC 2014 Service Manual 221 70051 91 GC
65. for GC 2014 CPU Board s ROM Software The procedure for upgrading the GC 2014 CPU board s ROM software via RS 232C from a PC is explained below Items Required 1 PC with Windows installed 2 RC 232C cross cable for connecting GC and PC cross cable type 9 pin female to 9 pin female e g P N 228 35397 92 3 ROM file for updating Checking Unit Settings Before performing the version upgrade make a note of the settings for the parameters listed below Note These parameters can be checked by pressing the FUNC key and selecting the 7 Service Maintenance menu 1 1 Installation Position in the Service Maintenance menu 2 2 Installation Piping in the Service Maintenance menu Also record the contents of the analysis file created by the customer for units not controlled by GCsolution Note The contents of the analysis file do not have to be recorded when making a new installation even if GCsolution is not connected Upgrade Procedure 1 Turn OFF the power to the GC If GCsolution is running close GCsolution before turning OFF the power to the GC 2 Connect the GC and the PC using the RS 232C cross cable and start Hyper Terminal on Windows Under Connection Description in Hyper Terminal input an appropriate name and select an appropriate icon In Connect using select direct connection e g Direct to 1 to the port to which the RS 232C cable is connected e g 1 COM2 and under Port Settings set the
66. has not been erroneously attached to a split bent and that there is no clogging Check that I time 1 P term 15 and I term 40 If the values are different from the above values input these values and press the pf4 key to write them in the ROM Check the offset and gain values for the flow rate The offset value is normally in the range 32 000 to 33 500 and the gain value is normally in the range 3 000 to 6 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain the correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC Check that the status is not Flow off or System off If 0 is displayed as the valve voltage this indicates that there is no voltage being supplied from the control system to the valve TFC Total Flow Controller that is attempting to supply carrier gas to INJ GC 2014 Service Manual 99 Chapter7 Troubleshooting 3 The total flow rate is higher than the setting Check that I time 1 P term 15 and I term 40 If the values are different from the above values input these values and press the pf4 key to write them in the ROM Check the offset and gain values for the flow rate The offset value is normally in the range 32 000 to 33 500 and t
67. he correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC 7 1 1 2 When the control mode is TOTAL FLOW and the injection mode is DIRECT 1 The total flow rate fluctuates 2 The total flow rate is lower than the setting 3 1 3 total flow rate is higher than the setting Refer to items 1 to 3 under 7 1 1 1 7 1 1 3 When the control mode is PRESS or LINEAR VELOCITY and the injection mode is DIRECT 1 The pressure or the linear velocity fluctuates Check that P mode time 10 P mode P term 50 and P mode I term 100 If the values are different from the above values input these values and press the pf4 key to write them in the ROM If the AFC for WBI is used the above values as follows P mode I time 10 P mode P term 12 and P mode I term 10 Check that there is no clogging in the purge line flow line The inlet pressure sensor in the AFC is inside the purge line If there is resistance in the purge line the pressure may fluctuate 2 The pressure or the linear velocity is lower than the setting GC 2014 Service Manual Check for leaks in the line Check that the source pressure i e the primary pressure has attained a sufficient level The source pressure can be ascertained by viewing the Actual value for the primary pressure in the Flow Adjust windo
68. he gain value is normally in the range 3 000 to 6 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain the correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC e Ifthe gas is still flowing into the carrier line even when the power is turned OFF replace the AFC 4 The inlet pressure fluctuates unstable Check that time 1 P term 100 and I term 150 If the values different from the above values input these values and press the pf4 key to write them in the ROM glass insert for WBI is used set the column insertion length normally 34 mm to approx 15 mm Set the inlet pressure to 0 kPa and the total flow rate to 400 ml min At this time pressure is generated due to the flow line resistance of the split line The specified value for this pressure is 50 kPa or less The effective value is 30 kPa or less If it is greater than 50 kPa identify the place where resistance exists using the following procedure Remove the AFC s piping line joint with the s mark band one piece at a time If the pressure decreases when the joint on the lower stream of the filter is removed resistance exists in the split line inside the AFC Next remove the joint on
69. however temporarily set the corresponding value To increase the number of digits after the decimal point in the actual measurement value 2 To stop the error confirmation window being displayed 4 To increase the number of digits and stop the error confirmation window being displayed 6 Demo mode Be sure to set to 0 in normal use To make all the actual measurement values equal to the set values 1 Note This is to allow demonstrations in situations where there is no gas piping such as exhibitions Max Temp C Default value is 350 In Japan allowing the ECD temperature to exceed 350 C is prohibited by law This law does not apply overseas however and a temperature of up to 400 C can be set To be on the safe side 350 C was selected as the default value 112 Chapter 8 Service Window 8 6 Serial Number Serial Number 1 Main Body Serial 2 Listof Serial No 8 6 1 Main Body Serial Number Serial Number Up to 20 characters can be input The unit serial number is input before shipment This Serial No for this GC information is shown on self diagnostic reports If for some reason the serial number does not appear it can be input C11323800000 from this window 1 ABC 2 DEF 3 GHI 4 JKL 5 MNO6 7 STU 8 VWX 9 YZ 009 Symbol The type of character can be changed using the pf2 and pf3 Alphat keys The pf2 key is used to switch between alphabetical Upper Chr and numerica
70. ice Manual 80 Chapter 5 Detector Unit Chapter5 Detector Unit 5 1 TCD Parts List for TCD 2014 CELL ASSY 221 70098 38 230V 81 100V 82 115V Number P N Part name 230 100 115V 1 221 70743 34 PLATE ASSY 2014 220 1 1 221 70743 91 PLATE ASSY 2014 100 1 1 221 70743 92 PLATE ASSY 2014 115 1 2 Left 221 32577 91 PIPE ASSY COL TCD 1 145mm 1 1 1 R 221 32577 92 PIPE ASSY COL TCD 2 210mm 1 1 1 3 221 70744 91 TCD 100 OHMS 2014 1 1 1 4 221 14018 BLOCK DETECTOR COVER 1 1 1 GC 2014 Service Manual 81 Chapter5 Detector Unit 5 1 1 DET HEATER ASSY FT OO Cn lt G3 FO Parts List for DET HEATER ASSY FT 221 70086 34 230V 91 100V 92 115V Quantity Number P N Part name 230V 100V 115V 11 221 70671 34 HEATER PT ASSY D FID 230 1 11 221 70671 91 HEATER PT ASSY D FID 100 1 11 221 70671 92 HEATER PT ASSY D FID 115 1 12 221 70125 DET DUAL UPPER COVER TCD 1 1 1 13 1221 70127 DET DUAL BLOCK PLATE 1 1 1 14 221 70139 LOCK RING DET DUAL 1 1 1 15 1221 70141 TCD BLOCK 1 1 1 16 1221 70136 DET DUAL BLOCK UPPER 1 1 1 17 221 70137 DET DUAL BLOCK LOWER 1 1 1 GC 2014 Service Manual 82 5 2 FID Parts List for FID 2014 CELL ASSY 221 70090 91 Chapter 5
71. in value is normally in the range 3 000 to 10 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain the correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC GC 2014 Service Manual 104 Chapter 7 Troubleshooting Also it may be possible to stop fluctuation by changing the P term or the I term to a value several times or a fraction of the original value Use this method to stop fluctuation in urgent cases 7 2 Temperature Control The temperature does not rise or does not agree with the setting Cause Countermeasure generated Overheating was detected and an error was Check for burnout in and check the EMF of the oven thermocouple If either of these is the cause of the error replace the oven thermocouple The EMF at both ends of the thermocouple connector is equal to 40 uV multiplied by the difference measured in C between the local temperature and the ambient temperature The column s set temperature is higher than the detector s set temperature The software automatically ensures that the column temperature does not exceed the detector temperature Set the detector s set temperature higher than the column s set temperature The sampl
72. istance tube only for make up gas 221 31745 HOUSING RESISTANCE TUBE 221 34121 94 MS FILTER Aged 221 48258 91 NOZZLE ASSY FID 221 41532 92 GRAPHITE POSITIONING JIG FID 221 45586 91 FTD COLLECTOR GC 2010 221 46520 92 FTD 2014 CONTROLLER 221 48457 92 FTD 2010 POWER CONTROLLER 221 47658 91 MAIN PART BASE ASSY FTD 221 70049 92 FLOW CONTROLLER H2 AIR FTD 221 47660 91 HEATER PT ASSY 120V DET FID 100V 221 47660 98 HEATER PT ASSY 240V DET FID 200 V FTD 2014 PACKED gt P N Part name Remarks 201 48386 3 WAY SPLIT TUBING M TYPE 221 18713 95 RESISTANCE TUBE ASSY H2 For FTD 221 18713 96 RESISTANCE TUBE ASSY AIR FTD 9 221 34121 94 MS FILTER Conditioned 221 70162 92 NOZZLE ASSY PACKED 221 18704 91 FTD COLLECTOR STANDARD For general use 221 42512 91 FTD COLLECTOR SPECIAL For pesticide analysis 221 46520 92 FID 2014 CONTROLLER 221 48457 92 CONTROLLER FTD 2014 221 70298 91 MAIN PART BASE ASSY FID 221 70049 92 FLOW CONTROLLER H2 AIR FTD 221 70610 91 FID 2014 HEATER ASSY 100 221 70610 34 FID 2014 HEATER ASSY 230 221 70662 FTD CABLE PTFE PACKING Collector cover packing lt ECD 2014 gt PIN Part name Remarks 221 70049 94 FLOW CONTROLLER AUX
73. l characters and the pf3 key is used to switch between upper and lower case Number Chr Lower Chr GC 2014 Service Manual 113 Chapter8 Service Window 8 6 2 Unit Serial Numbers Serial Number Main Body C11323800001 CPU Board 6626661 2 10 SA DET 1 6626903 12 30 SA DET 3 6626104 3 5 LP SLOT1 3452285 2 8 8 7 Maintenance Log Maintenance Log 1 50 Time changed P N name 98 08 12 08 00 ROM R S N Version 1 2500 98 08 12 07 55 2215555591 SPL UNIT A SIN 6626661 2 10 98 08 12 07 55 2215555591 SPL UNIT R S N 662690 12 30 SA 98 05 06 11 05 2214650991 FID 21 BOARD sss E 2014 Service Manual Note The display items vary with the unit This window can be used to check the serial numbers written in ROM for automatically recognized units There is no display for some units For example the serial number for a single injection unit SPL unit cannot be checked Information for DET 1 to DET 4 is displayed only for ports to which something is connected Information for SLOT 1 to SLOT 6 is displayed only for ports to which something is connected Records of board and flow controller replacement and ROM version upgrades are stored Up to 50 items can be recorded Note Once the number of items reaches 50 the oldest item is deleted in order to allow new information to be recorded The letter that appears before S N can be used to ascertain the attached removed
74. n where it touches the back of the oven if the motor shaft protrudes at least 5 mm in the front of the fan mount the fan with its outer face i e the back in alignment with the end of the shaft If the motor shaft protrudes less than 5 mm then the fan must be pulled forwards so that the outer face is an appropriate distance in front of the end of shaft It is secured this state using the screw provided with the fan The screw is on the motor side Back of oven elec Motor axis 5 to 5 5 mm Back of fan N Fan screw Rotate the fan to check N that it does not hit the tab Align the back of the fan with the end of the shaft Motor axis When securing the fan to the motor shaft orient it so that the screw makes contact with the flat side of the shaft GC 2014 Service Manual 25 Chapter2 Configuration of GC 2014 2 2 9 Structure of Oven Cooling Unit Attach the top end of spring 17 to the outer surface of air supply exhaust pipe 11 with tape lt 42 In the fully open intermediate and fully TNT closed positions the shaft must drop After assembly it must be far as it will go under its own weight when lifted possible to turn this gear smoothly with your fingers Insert gear 18 as GC 2014 Service Manual 26 Chapter 2 Configuration of GC 2014 2 3 Electric Circuits 2 3 1 Block Diagram
75. oration The unauthorized reproduction or copying of all or any part of this document is not permitted 2 In the interests of product improvement the contents of this document may be changed without notice 3 Although every effort has been taken to ensure that the contents of this document are accurate if an error or omission is discovered it may not be possible to correct the relevant part immediately 4 The supply period for parts required to repair this product is the 7 year period following the termination of manufacture It may not be possible to respond to requests for repair parts after this period has elapsed The supply period for parts other than genuine Shimadzu parts however is as specified by the original manufacturer Copyright 2005 Shimadzu Corporation GC 2014 Service Manual Introduction Purpose of This Service Manual This service manual is intended for use by service engineers approved by Shimadzu Corporation and describes the maintenance methods used for the GC 2014 series gas chromatograph Maintenance may only be performed by service engineers who have received training for this instrument There may be cases where information on subjects also covered in the instruction manual has been omitted Refer to the instruction manual if necessary New information required for maintenance will be issued as Technical Information Insert this information inside this document so that it can be referred to easily Disclaime
76. ow mark as left fi and fix at right angle with 28188 77 de TT Ties cas POWER ASSY 221 4574 n BOARD POWER 221 457430 J 5 Em ce Ye 4 8 3 s EP 44177774 4 o 7 O SYMBOL ure CB Fig 2 3 7 Assembly Diagram for Power Unit GC 2014 Service Manual 33 Chapter2 Configuration of GC 2014 Primary circuits 5V JE 511 ACCOS Heater Primary circuits UNIT UNIT es i RE 5 5 00 3 AGNDd 1 ret Pi Secondary circuits lt UNT gt Urit J7 DET eon ACC28 ACE 2 5 Heater Primary cirouts DET S 7 8l _ BETIS DETIS 2 00 5 77144 M P Secondary circuits gt 2 um J6 2 Hester Primary circuits CHECK By me 6 CONES gt 2 00 3 amp 44 4 Pt Secondary circuits Uer 00 3 5 ua Ja copy ACB 8 Hester Pri circuits 2 1 GE a0 4 1 4 Pt crcuts ETE w En gt 1 pma 1 S26MDO n DES S four 10V Bero men fi w 2 5202301 270 J2 DC24V Switching BEER ASV ASV PC 1 elt a 1 DC24V Pet 1 3 FTD TCD14 E gt 2 CROSS 7 CROSS R35 IKS 1 Rzo 100K A
77. played contents correspond to the old version repeat the upgrade procedure from the beginning GC 2014 Service Manual 117 Chapter9 Appendix 9 After reconfirming the Installation Position and Installation Piping parameters that were recorded before the version upgrade or after resetting them if they have been deleted reset the unit s power supply This is because changes in condition settings such as the Installation Position and Installation Piping parameters are only enabled when the power supply is reset 10 Press the FUNC key and select 3 Transmission parameter settings from the 6 Configuration settings menu Set the transmission parameters After selecting the values be sure to press the ENTER key to confirm the selections After completing the settings be sure to press the pf2 key Apply When using GCsolution Protocol LEVEL3 Baud rate bps 115 200 bps Note When connecting to Chromatopac set the GC 2014 s transmission parameters to the same values set for Chromatopac 11 For units controlled from GCsolution download the device parameters from the PC to the GC For units not connected to GCsolution check the contents of the analysis file and return the parameters to the values taken before the upgrade Note With new installations even if GCsolution is not connected it is not necessary to re input the contents of the analysis file Thi
78. r Due to product improvement the parts described and the diagrams given in this document may differ from the actual equipment Also not all the parts referred to in this document are handled as repair parts Notation Used for Precautionary Information The precautionary information provided in this service manual is labeled in the following way to indicate the degree of danger potential damage and urgency DANGER Indicates a hazardous situation which if not avoided could result in death or in serious or moderate injury WARNING Indicates a hazardous situation which if not avoided could result in minor injury or property damage Here minor injury indicates an injury that would not require hospitalization or long term outpatient care Property damage indicates damage to the product itself and to objects around the product such as housing and household items CAUTION e Indicates a hazardous situation which if not avoided could result in damage to the product or other property damage NOTE e ndicates information provided to facilitate efficient operation of the equipment clarify the subject matter GC 2014 Service Manual blank page GC 2014 Service Manual Table of Contents Table of Contents Product Guarantee usunn u kann asss II BEL EN T Notation U
79. r the temperature control port for the detector control unit to be used under Function Service Maintenance Installation piping 4 The baseline fluctuates when ready status is entered after sample injection Cause Countermeasure Zero at Ready is ON Either set Zero at Ready to OFF in the configuration settings or program so that ready status is not entered during analysis GC 2014 Service Manual 108 Chapter 8 Service Window Chapter8 Service Window This chapter describes the service window that is displayed by pressing the FUNC key selecting Z Service Maintenance 5 Service and inputting the correct password in the password input window that is displayed Service Flow Adjust CAR Flow Adjust DetAPC Flow Adjust AUX APC Temp Sensor Use Time Mode Serial Number Maintenance Log Fan and LCD Use Time Init for Shipment 1 2 3 4 5 6 7 8 9 Pf2 ID Window PARAMETER ID 0 Rem eee ____ pf2 Displays the ID window This single window can be used to check all the parameters Inputting a PARAMETER ID makes it possible to check the value of the corresponding parameter When the cause of a fault is unknown this function can be used to respond to requests such as Check the value set for No XXXX with the ID window issued from our Quality Assurance Department It is planned that this window will be used for remote maintenance in the future GC 20
80. s completes the upgrade procedure Note If a communications error occurs with the baud rate set to 115 200 bps lower the baud rate before repeating the upgrade procedure GC 2014 Service Manual 118
81. sed for Precautionary Information CHAPTER 1 INSTALLATION 5 1 tilnstallation cuts noo eins 5 12151 Rear Spaces ts ste uma RM 5 121 2 5146 5 a e Gere d or LRG 5 1 2 Installation Environment 5 1 2 1 Ambient Temperature and Humidity 5 1 2 2 Installation eee tite e ee HERE 6 1 2 3 Corrosive Gas and 6 1 2 4 Influence of Electromagnetic Waves and Power Supply Noise 6 1 2 5 Other Precautionary lItems uu aku eme 6 1 2 Power Supplyza Su u bun 7 1 3 1 Power Supply 7 1 3 2 Power Supply Capacity nennen 7 V SAS LEE 8 PUNY t a a eter 8 1 4 2 Supply Pressure 145 eser eee 8 CHAPTER 2 CONFIGURATION OF GC 2014 9 2 1 Configuration Diagrams for GC 2014 9 2 1 1 86 2014A te ee acter nt 9 2 1 2 6C 20 TAAE inert nnt n eR eb aet een vette 10 2 1 39 GC 2014 AF e e e eee 11 2 1 4 GC 2014AESPL vente e e et AS yau
82. soH I LNSA Lids I I I I ANSA 43H89 Jo xoeg c GC 2014 Service Manual jo yoeg 73 Chapter3 Gas Flow Controller blank page GC 2014 Service Manual 74 Chapter 4 Sample Injection Unit Chapter 4 Sample Injection Unit 4 1 Configuration Sample Injection Unit SPL 2014 Assembly Configuration Chart 221 70035 91 221 70082 91 221 47221 91 SPL 2014 SPL 2014 UNIT INJECTION PORT A ASSY 100 100 120 221 70166 91 221 70035 34 BASE INJECTION UNIT A ASSY 220 240V 221 70082 98 221 70602 91 221 70599 91 SPL 2014 SPL 2014 UNIT HEATER PT ASSY SPL 100 HEATER 120V 150W ASSY 230 220 240 221 70599 34 221 70602 34 HEATER 240V 124W ASSY HEATER PT ASSY SPL 230 221 70596 91 HEAT SENSITIVE MATERIAL INJ 221 47735 93 AFC 2014 D PURGE SPL 221 48440 93 221 42559 92 PIPING ASSY FILTER ASSY WITH BLIND AFC SPL ADDITION 221 48441 91 BUFFER ASSY 221 34121 94 MS FILTER CONDITIONING 221 48619 93 ACCESSORY ASSY SPL 2014 WBI 2014 Assembly Configuration Chart 221 70048 91 221 70082 91 221 47221 91 WBI 2014 SPL 2014 UNIT INJECTION PORT A ASSY 100 100 120 221 70166 91 221 70048 34 BASE INJECTION UNIT ASSY WBI 2014 230 221 70082 98 221 70602 91 221 70599 91 SPL 2014 UNIT HEATER PT ASSY SPL 100 HEATER 120V 150W ASSY 220 240 221 70599 34 221 70602 34 HEATER 240V 124W ASSY HEATER PT ASSY SPL 230 221 10596
83. status of the corresponding part A Attached R Removed If all the information cannot be displayed together the window can be scrolled The pf3 key is enabled when Chromatopac is connected 114 8 8 Fan amp LCD Use Time Fan amp LCD Use Time FanUseTime 1111 Acceptable value h Use time 57 5 LED Use Time 1 111111 Acceptable value h Use time 57 5 8 9 Init for Shipment Init for Shipment If you press pf2 some parameter initialized Caution Do not use this exept for manufacturing at factory Instability may occur 61320 0 46380 0 Chapter 8 Service Window This window is used to reset the operation times of the column oven fan and the LCD unit Note The settings for the acceptable values cannot be changed Fan 61320 0 hours approx 7 years LCD 46380 0 hours approx 5 years Operation beyond the period indicated by these acceptable values is possible but a result of Not Good will appear in self diagnostic reports After replacing the column oven fan or the LCD unit reset the corresponding operation time pf2 Pressing Reset clears the counter at the cursor position This window is used only when being shipped from the factory CAUTION Do not use this window GC 2014 Service Manual 115 Chapter8 Service Window blank page GC 2014 Service Manual 116 Chapter 9 Appendix Chapter9 Appendix Upgrade Procedure
84. the upper stream of the filter If the pressure decreases the filter is clogged Prepare a new filter Next remove the joint on the upper stream of the buffer If the pressure decreases the buffer is clogged If the pressure does not decrease the cause originates in the INJ Check the glass insert and the split line inside the INJ Check that there is no clogging in the purge line flow line The inlet pressure sensor in the AFC is inside the purge line If there is resistance in the purge line the pressure may fluctuate 5 The inlet pressure is lower than the setting in split mode Check for leaks using for example Snoop Check whether or not the total flow rate is controlled in accordance with the setting If it is not perform the checks described previously in items 1 to 3 Check that the source pressure i e the primary pressure has attained a sufficient level The source pressure can be ascertained by viewing the Actual value for the primary pressure in the Flow Adjust window It is not GC 2014 Service Manual 100 Chapter 7 Troubleshooting necessary to remove any piping Check that the set pressure is sufficiently higher than the primary pressure As a rough guide it should be at least 200 kPa but this value depends on the column Check whether or not the setting is within the range of settable pressures flow rates for AFCs A graph is given in the section on AFCs in the GC 2014 instruction manual
85. w It is not necessary to remove any piping Check that the set pressure is sufficiently higher than the primary pressure As a rough guide it should be at least 200 kPa but this value depends on the column Check that P mode time 10 P mode P term 50 and P mode term 100 If the values are different from the above values input these values and press the pf4 key to write them in the ROM If the AFC for WBI is used the above values are as follows P mode time 10 P mode P term 12 P mode I term 10 102 Chapter 7 Troubleshooting Check the offset and gain values The offset value is normally in the range 32 000 to 33 500 and the gain value is normally in the range 3 000 to 6 000 If the offset value is well outside this range perform offset calibration The method is described in the GC 2014 instruction manual If the gain value is well outside this range obtain the correct value from Shimadzu Corporation s Quality Assurance Department At this time provide notification of the serial number and lot number displayed on the side of the AFC Check that the status is not Flow off or System off If 0 is displayed as the valve voltage this indicates that there is no voltage being supplied from the control system to the valve TFC Total Flow Controller that is attempting to supply carrier gas to INJ 3 The pressure or the linear velocity is higher than the setting Check that P mode time 10 P mod

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