The miVac
Contents
1. OR ONLY DRY NON CONDUCTIVE POLLUTION ANY MAINTENANCE OR REPAIR OF THIS PRODUCT SHALL BE CARRIED OUT BY GENEVAC PERSONNEL OR APPROVED REPRESENTATIVES OF GENEVAC USING ONLY APPROVED SPARE PARTS 12 Accessories Part Number Description General STJ 10000 000 1 litre jar for miVac SpeedTrap 1 STJ 20000 000 2 litre jar for miVac SpeedTrap 1 System Connection kit for connection of pump and or cold trap to MCK 00000 Y00 concentrator complete with 2 5m 1 2 tube tube cutter power lead to control 1 pump amp catch pot for pump CRT 10000 200 Cart with two shelves suitable for all systems 1 Vapour Traps Vapour trap for neutralisation of ammonia or acid vapours complete with all 4 VAP TRAPO 100 connections Requires neutralising solution NH3 REFOO 100 Ammonia neutralising solution 4x 500ml 1 ACD REFO0 100 Acid neutralising solution 4 x 500ml 1 04 5057 Issue 1 15 June 2008 Page 19 of 22 miVac Series Part Number Description Rotors for miVac Duo and DNA DRC 15EPP 048 DRC 15EPP 084 DRC 05EPP 120 DRC MIXEP 048 DRC 50CCT 008 DRC 15CCT 012 DRC 18150 006 DRC 16100 028 DRC 13100 032 DRC 01275 040 DRC 01075 068 DRC 15V45 048 DRC 12V40 078 DRC 28V60 014 DRS 00000 200 BRS STKO0 004 48 x 1 5ml Eppendorf tube rotor Supplied as std with DNA system 84 x 1 5ml Eppendorf tube rotor 120 x 0 5ml Eppendorf tube rotor 24 x 0 5ml amp 24 x 1 5ml amp 24 x 2 0m2. 23050 x00 SpeedTrap models MST 23050 x00 Duo Pump models DUP 23050 x00 Quattro Pump models QUP 23050 x00 Super Vacuum Pump model SVP 23050 x00 Control Valve model UOP 00000 Y00 Serial Numbers from to Individual declarations are available on request Conform to the Essential Health and e Machinery Directive 98 37 EEC Safety requirements of European e EMC Directive 2004 108 EEC and Directives e Low Voltage Directive 73 23 EEC as amended Conformity is demonstrated by compliance to the following standards BS EN ISO 12100 pts 1 amp 2 2003 EN 60204 1 1998 EN 294 1992 Not Pump or SpeedTrap EN1088 1996 Not Pump or SpeedTrap IEC 61326 1997 and BS EN 61010 1 2001 Signed i um Position Director of Technology and Business Development Name Bob Evans Date 5 May 2005 Being the person appointed on behalf of Genevac Ltd to sign on their behalf Where x A B D E or F and denotes power lead code appropriate to destination EC country Page 18 of 22 04 5057 Issue 1 15 June 2008 miVac Series 11 Safety WARNING THIS SYSTEM MUST BE EARTHED THIS SYSTEM IS A SAFETY CLASS 1 PRODUCT ACCORDING TO IEC CLASSIFICATION IT MUST NEVER BE USED WITH ANY INTERRUPTION TO THE SAFETY EARTH CONDUCTOR IT IS AN INSTALLATION CATEGORY II PRODUCT AND IS INTENDED TO OPERATE FROM A NORMAL SINGLE PHASE SUPPLY THIS SYSTEM HAS BEEN DESIGNED TO BE USED IN A POLLUTION DEGREE 1 ENVIRONMENT NO POLLUTION
3. it remains the responsibility of the user to consider any solvents being evaporated within the context of the ATEX directive The presence of solvents on the list above indicates only that they will not damage the system If further information is required please contact your Sales Representative or visit http www miVac co uk Page 6 of 22 04 5057 Issue 1 15 June 2008 miVac Series DNA DUO QUATTRO CONCENTRATOR 4 Getting Started 10 11 12 13 Refer to Safety and Maintenance Notes and Installation Instructions Open Lid For Quattro Concentrator ensure that the latch engages Fit rotor by carefully sliding it on to shaft Load the rotor with your samples ensure evenly balanced Close Lid For Quattro Concentrator lift lid to disengage latch Set Chamber Temperature refer to Para 5 1 if no temperature is selected the unit will run at the current chamber temperature Set Run Type refer to Para 5 2 if no type is set the unit will use the current settings Set Total Run Time refer to Para 5 3 if no time is set the unit will use the current settings Set Heat Time refer to Para 5 4 if no time is set the unit will use the current settings Press MANUAL or AUTO button to start the run If the MANUAL button was pressed the STOP button will need to be pressed to stop the run If the AUTO button was pressed the run will stop after the TOTAL time has passed The end of run is confirmed
4. provides easy access to all run settings and also provides you with the current status of the concentrator details are provided on page 7 CONCENTRATOR CONTROL PANEL The LCD display is also used to advise you of any problems that may occur either with the run settings or the concentrator These messages are defined later on in this manual Page 13 Page 2 of 22 04 5057 Issue 1 15 June 2008 miVac Series 2 Safety and Maintenance Notes 2 1 Symbols The following safety symbols are used throughout this manual and can be found on the equipment The definitions and scope of each symbol is as described below THIS SYMBOL INDICATES HAZARDS THAT CAN LEAD TO SERIOUS MATERIAL DAMAGE OR POTENTIAL SERIOUS INJURY THIS SYMBOL MEANS THAT YOU SHOULD NOT TOUCH SURFACES IN THESE AREAS THESE SURFACES CAN BE VERY HOT AND MAY LEAD TO BURNS This symbol indicates that you should refer to the relevant part of the User Manual for additional information SERIOUS MATERIAL DAMAGE OR POTENTIAL SERIOUS INJURY AND THAT YOU SHOULD READ THE RELEVANT PART OF THE USER MANUAL ED THESE 2 SYMBOLS COMBINED INDICATES HAZARDS THAT CAN LEAD TO 2 2 Safety BEFORE OPERATING THE SYSTEM IT IS IMPORTANT THAT THE FOLLOWING NOTES ARE READ TO ENSURE THAT THE IMPLICATIONS TO THE SAFETY OF PERSONNEL OPERATING THE SYSTEM AND FOR THE PROTECTION OF SAMPLE INTEGRITY ARE UNDERSTOOD Samples in the concentrator chamber are subjected to accelerations of
5. 4 5057 Issue 1 15 June 2008 miVac Series NOTES 04 5057 Issue 1 15 June 2008 Page 21 of 22 miVac Series j Genevac Limited The Sovereign Centre Farthing Road Ipswich IP1 5AP United Kingdom Sales and Service Hotlines Service Hotline 44 0 1473 243000 Sales Hotline 44 0 1473 240000 Fax 44 0 1473 461176 Email salesinfo genevac co uk Web site www miVac co uk Genevac Inc 707 Executive Boulevard Suite D Valley Cottage New York 10989 United States of America Sales and Service Hotline 1 845 267 2211 Fax 1 845 267 2212 Email salesinfo genevacusa com For main Distributor listing visit www mivac co uk 13 Warranty Statement This product is guaranteed for period of 12 months from the date of delivery to site In the unlikely event of any defect arising due to faulty materials or construction resulting in system failure the unit will be repaired free of charge This to include all labour and component costs incurred This warranty is subject to the following provisions 1 System must be sited installed and operated in accordance with User Manual Unit only used for the purpose it was sold and in accordance with Genevac published compatible solvent list Regular cleaning and preventative maintenance schedule to be adhered to as detailed in User Manual See item 3 5 Routine Checks on Page 6 Warranty does not cover accidental damage misuse modifications or inappropriate
6. TOTAL TOTAL es Chen 0AN arc Mm im ec M i UV HO f E FMI C J ML Select Parameter Adjust Value After Accepting Value 5 2 Setting Run Type Choose H20 for water only OH for alcohols and alcohol mixes and for all other solvents C snI Las TOTAL L Het sois HeD TOTAL ni paes c M ig a Cm iw DUC nn tr C1 ee ee pT Parameter Adjust Value After Accepting Value The run types are designed to vent air through the concentrator at a rate optimised for the solvent group selected No venting H2O Low vent rate and OH High vent rate 5 3 Setting Total Run Time Allows you to set the duration of the run He F TOTAL d Heg g TOTAL 1 L 20 TOTAL m ec M L C Uc DC MN SU FU CU Ue CH es pos Parameter Adjust Va Value After Accepting Value 5 4 Setting Heat Time Allows you to control the amount of time that chamber heating is applied this is only available if Chamber Temperature is set to 30 C or above HCU Heat neu j HeD PREA mj C MU pe DETE sec ANIN IL _ LS L q 110 Select Parameter Adjust Value After Accepting Value 5 5 Display mode in AUTO run The display is factory set to show TOTAL TIME but it can be changed to display HEAT TIME when using the AUTO run function To change the factory setting whilst in the Heat Time setting hold down the selector for 5 seconds until a single beep is heard The display will now indicate HEAT TIME until it has counted down to 00 00 it will then revert t
7. User Manual RATORS SPEEDTRAP amp DUO QUATTRO PUMPS Issue 1 15 June 2008 Part Number 04 5057 miVac Series Contents G N R a E E ee ee 2 1 MOUCHO EP ea ee ee eee 2 B 2 ANS SRE ES 2 2 Safety and Maintenance Notes iii ieesereeereeeeereeeseeeeennes 3 2 1 OR E E N 3 2 2 SES CN A E E E E E E E T A E EE A E ee A E ee 3 3 System Description and OPONS sspe aE Enee aE AE EE EAER EEEE ai 4 3 1 Scope of delivery and installation ss 4 3 2 CRC ME El Ne on dc ie 4 3 3 IS AUS SV SCO E ot de te ae 4 EN S 4 DUO QUATTRO SPEEDTRAP and PUMP cccccccecceceeeeceeeeceeeeceeeeeeaeeceaeesseeesaeessaeeeseeeeneeesseseens 4 HO cen sco sec ncaa ese pene etter so wei ig eo meee ls cents ood een ae ete eeatiee Seceasoene eee oeeeanenedacss 5 CABLE ee E 5 3 4 Good procedural practice ss c5c 2c2asscncacncnchsacidevendasncidnosdndesebbadecdandacidedancaensiaedadsnadadedencadhosdneniehedsaccbandedoses 6 3 9 ROIS eee 2 ee ee eee eee eee 6 3 6 List of acceptable solvents cccccccsecceececececeeeceeceueecseeceeeseueseeeseeecaueesueeseeesseessueeseeesueesseessueeseeesanees 6 miVac Systems and Combustible Solvents ss 6 Genevac and the ATEX Directive ii iiiiiiiiiiiieesseeeeeeereeensnes 6 DNA DUO QUAT TRO CONCENTRATOR 5 2 6 anaana aaa aaa Naa aaa Aaaa 7 4 CS UNG S OR E A E seesecosnaceanses T 5 COR E E A 8 5 1 Setting Chamber TEMPS AWS sce 2 ds cenaree tecusesceetesa ten eesmoessc t
8. ap and Duo Pump as positioned on a bench If you have purchased the Cart from your Distributor and are using the Concentrator SpeedTrap and Pump then the Pump should be positioned on the lower shelf with the hose from the SpeedTrap to the Pump routed accordingly Page 4 of 22 04 5057 Issue 1 15 June 2008 miVac Series NOTE The system is to be positioned so that there is a 50mm air gap between each unit and the next object wall fume hood etc After installation leave the SpeedTrap in the upright position for 24hrs before connecting power HOSES HOSE CLIPS EXTRACTION SYSTEM L k a gt 7 Ce CATCH POT PUMP SPEEDTRAP CONCENTRATOR NOTE Ensure that the Catchpot is fitted to the upper row of vent holes on the Pump Follow the diagram above to connect the units together using 72 Vac hose cut to length using the hose cutter Secure hose with hose clips as indicated The hose hose clips and the hose cutter are available in the miVac Connection Kit Part Number MCK 00000 Y00 Extra lengths of hose are available separately Vacuum hose Part Number 04 4783 Exhaust hose Part Number 04 5016 specify length when ordering If you do not have the SpeedTrap just connect the hose between the concentrator and the pump The arrows on the diagram indicate the direction of vapour flow CABLES Once you have fitted the hoses you then need to connect the electrical supply cables There are only 3 cables re
9. arranty 3 5 Routine Checks 3 6 Check all hose joints on a regular basis to ensure that they are secure Always ensure that the condenser jar is emptied before every run Clean the condenser jar at regular intervals Check the catch pot connected to the pump exhaust on a regular basis and drain as necessary Clean the lid lid seal exterior paintwork and inside of the chamber with a soft lint free cloth using one of the following Detergent solution e g fairy liquid Bleach solution if using biological agents Methanol Ethanol List of acceptable solvents Acetic Acid 1 2 Dichloroethane Methyl Tertiary Butyl Ether Acetonitrile ACN Dioxane Methylene Chloride DCM Acetone Ethanol EtOH Propan 1 ol or Propanol Ammonium Hydroxide NH3OH Ethyl Acetate Propan 2 ol or isopropyl Butan 1 ol Formic Acid alcohol IPA Butan 2 ol Heptane THF Butyl Acetate Hexane Hex Toluene Chloroform TCM Methanol MeOH Water SOLVENTS IN RED CAN ONLY BE USED IN COMPLETE SYSTEMS WHERE ALL UNITS CONCENTRATOR SPEEDTRAP AND PUMP HAVE A DATE OF APRIL 2007 OR LATER ON THE SERIAL PLATE miVac Systems and Combustible Solvents Please note it remains the responsibility of the user to consider safety when evaporating any combustible solvents and ensure the system is placed in a well ventilated environment Genevac and the ATEX Directive This Statement is applicable only to Member Countries of the EU Please note that
10. been optimised for aluminium rotors Always use this function when you have more than a few tubes of water However you might find full vacuum faster with just a few tubes Always use the H20 function on DNA system when evaporating water or solvents with similar boiling points Note for existing users e Existing systems will still benefit from the new aluminium rotors even without the new software you ll still get 80 90 of the improvement shown on the graphs Page 10 of 22 04 5057 Issue 1 15 June 2008 miVac Series SPEEDTRAP 6 Introduction The miVac SpeedTrap offers you the following features Unique frost free cold trap No defrosting required all solvents including water collect as liquids Easy to empty collection jar is removed by quarter turn Ideal for use on all concentrators except freeze driers 6 1 Safety NOTE After installation leave the SpeedTrap in the upright position for 24hrs before connecting power Please be assured that sudden boiling of solvent within the jar is normal and it will re condense You may also see ice forming in the jar this is normal under certain conditions The collection jar is only to be emptied at the end of a run when the Concentrator has stopped If ice forms in the Condenser jar allow it to thaw naturally Do not use implements to try and break the ice as this may damage the jar Cold water may be added to the jar to accelerate the thawing proc
11. by the system emitting 4 long beeps and unlocking the lid NOTE The rotor may continue to spin slowly after the run has ended WHEN REMOVING YOUR SAMPLES CARE SHOULD BE TAKEN AS THE CHAMBER AND SAMPLE HOLDERS WILL BE AT THE SAME TEMPERATURE THAT WAS SET FOR THE RUN 04 5057 Issue 1 15 June 2008 Page 7 of 22 miVac Series 5 Controls Let s take a closer look at the controls and what they do Switch the unit on and the LCD screen will temporarily illuminate to display 888 TOTAL HEAT L 68 9588 J U This is a test to ensure that all LCD segments are functioning correctly it will then revert to the ready mode The display will indicate the current run settings For example with a current chamber temperature of 24 C and a TOTAL run time of 1 hour the display will indicate There are 4 buttons and a rotary selector PRE HEAT When pressed this allows you to pre heat the chamber to 40 C prior to starting the run when selected the LED is illuminated Pre heat is cancelled when you press either of the start buttons the STOP button or the PRE HEAT button again MANUAL Runs until you push STOP When pressed this emits a single beep and starts the run and will continue to run until the STOP button is pressed When this mode is selected the LED is illuminated and the time counts UP to indicate the time accumulated AUTO Runs for the time set and then stops When pressed this emits a single beep and start
12. ed Max Force Drive system Duo Max rotor speed Max Force Drive system Quattro Max rotor speed Max Force Drive system SpeedTrap Condenser temperature Minimum Maximum defrost Jar capacity Rapid defrost Condenser jar Refrigerant Vacuum pump Duo Pump Flow rate Quattro Pump Flow rate Dimensions Including pipework at back DNA Concentrator W x D x H Weight Duo Concentrator W x D x H Weight Quattro Concentrator W x D x H Weight SpeedTrap W x D x H Weight Duo Pump W x D x H Weight Quattro Pump W x D x H Weight Page 16 of 22 1465 RPM 250G Permanent magnet electronic drive 1465 RPM 250G Permanent magnet electronic drive 1130 RPM 250G Permanent magnet electronic drive 50 C 60 C 1 litres 2 0 litres Optional Yes Borosilicate Glass R404a 10 0 mbar nominal 7 5 torr 38 l min 1 34 cf m lt 2 0 mbar nominal 1 5 torr 33 I min 1 16 cf m 360 501 with Catchpot x 602 x 300 mm 37 Kg 360 x 424 x 300 mm 20 Kg 480 x 594 x 300 mm 32 5 Kg 212 x 563 x 450 mm 25 8 Kg 215 x 389 x 315 mm 17 Kg 215 x 389 x 315 mm 17 5 Kg 04 5057 Issue 1 15 June 2008 miVac Series Electrical Volts V 120V 410 60Hz USA 230V 10 50Hz UK Europe 100V 10 50 60Hz Japan 220V 10 60Hz Saudi Arabia Korea Power Consumption Amps A 230V 50Hz 220V 60Hz 120V 60Hz 100V 50 60Hz DNA Concentrator 2 6 2 6 4 7 4 5 Du
13. ess THE DRIP TRAY IS TO BE EMPTIED REGULARLY TO AVOID THE RISK OF SPLASHING CARE IS TO BE TAKEN WHEN REMOVING THE COLLECTION JAR AS IT IS HEAVY ESPECIALLY WHEN FULL OF SOLVENT INSPECT THE COLLECTION JAR BEFORE EVERY USE FOR DAMAGE CRACKS ETC DO NOT ALLOW TO FILL ABOVE MAX LINE AS IT MAY CAUSE DAMAGE TO THE PUMP AND STOP CONCENTRATION EMPTY THE COLLECTION JAR AFTER EVERY RUN REFER TO LIST OF ACCEPTABLE SOLVENTS BEFORE USE 6 2 Cleaning Exterior surfaces can be cleaned using a lint free cloth the following also apply Do not use abrasives Collection jar is Dishwasher safe Collection jar is not suitable for an Autoclave 04 5057 Issue 1 15 June 2008 Page 11 of 22 miVac Series 6 3 Setting up If you are using the SpeedTrap as part of a miVac system refer to Pages 3 to 6 inclusive If you are using the SpeedTrap as a Stand Alone miVac unit in conjunction with other equipment please refer to Safety and Maintenance notes on Page 3 of this manual Connect the SpeedTrap to your existing equipment as detailed below FOR USE IN JAPAN BEFORE CONNECTING TO MAINS POWER SUPPLY ENSURE THAT THE FREQUENCY ADJUSTER ON THE REAR OF THE SPEEDTRAP IS SET TO THE CORRECT POSITION FOR YOUR MAINS SUPPLY REFER TO DIAGRAM BELOW 50Hz 60Hz EXTERNAL 7 A WW A VACUUM 7 So SOURCE bed Ts Connect Mains Power Cable A supplied with the SpeedTrap to the connector
14. iled to unlock The following tables list some possible symptoms and their corrective actions Concentrator Pump SYMPTOM CAUSE _ CORRECTIVE ACTION Display blank Check power supply lead Lid will not open difficult to open Dirty lid seal Clean lid and seal External control valve if fitted wrong way round Rotor will not spin double beep Lid not fully closed Excessive vibration noise Chamber fails to reach Heat time not set or insufficient Adjust programmed temperature Solvent splashes condensation SpeedTrap not operating correctly See SpeedTrap See Vacuum problem Overfull plates See loading limits Page 14 of 22 04 5057 Issue 1 15 June 2008 miVac Series Concentrator Pump continued SYMPTOM CORRECTIVE ACTION Vacuum problems Pump not running Check connections mains power supply Check for damage dirt Clean if required Check for leaks Check for blockages Check connections Control valve Check connected to concentrator if fitted not opening pump outlet Check vapour flow direction Condenser jar not sealed Remove jar and check seal for damage debris Replace Pump inefficient Run system without samples for 5 minutes Repeat 3 times then reload samples Replace exhaust silencer muffler See Speed Trap Lid seal leaks Hoses Exhaust silencer muffler blocked SpeedTrap Condenser jar full Empty jar Pump needs servicing Contact your distributor Excessive concentration
15. l Eppendorf tube rotor 8 x 50ml Conical Based Centrifuge tubes 28mm x 115mm 12 x 15ml Conical Based Centrifuge tubes 17mm x 120mm 6 x 18mm by 150mm tall glass tubes rotor 28 x 16 x 100mm tubes 32 x 13 x 100ml tubes 40 x 12mm by 75mm tall glass tubes rotor 68 x 10 x 75ml tubes 48 x 15 x 45mm vials 78 x 12 x 40mm vials 14 x 28 x 60mm scintillation vials 20ml Swing rotor to accept 2 microtitre plates deep or shallow well Qty 4 Stackers for swing rotor to allow stacking of up to 3 shallow well plates per swing increasing rotor capacity to 6 Can be double stacked if using 1 5ml tubes Rotors for miVac Quattro QRC 15EPP 200 QRC 50CCT 036 QRC 15CCT 072 QRC 18150 040 QRC 16100 100 QRC 01275 200 QRS 00000 400 BRS STKOO0 016 BRS STKO0 004 200 x 1 5ml Eppendorf tube rotor 36 x 50ml Conical Based Centrifuge tubes 28mm x 115mm 72 x 15ml Conical Based Centrifuge tubes 17mm x 120mm 40 x 18mm by 150mm tall glass tubes rotor 100 x 16mm by 100mm tall glass tubes rotor 200 x 12mm by 75mm tall glass tubes rotor Swing rotor to accept 4 microtitre plates deep or shallow well Qty 16 Stackers for swing rotor to allow stacking of up to 5 shallow well plates per swing increasing rotor capacity to 20 Qty 4 Stackers for swing rotor to allow stacking of up to 2 deep or shallow well plates per swing increasing rotor capacity to 8 Contact your Distributor for pricing and availability Page 20 of 22 0
16. o Concentrator 1 6 1 6 2 8 25 Quattro Concentrator 3 9 3 9 7 2 6 2 Duo Pump 1 1 1 1 2 1 2 5 Quattro Pump 0 60 0 60 1 2 1 5 Speed Trap 1 8 2 3 4 1 4 8 Volt Amperes VA 230V 50Hz 220V 60Hz 120V 60Hz 100V 50 60Hz DNA Concentrator 650 650 650 500 Duo Concentrator 400 400 400 250 Quattro Concentrator 950 950 720 720 Duo Pump 250 250 250 250 Quattro Pump 150 150 150 150 SpeedTrap 550 550 550 550 NOTE The systems may momentarily take current in excess of the figures quoted above Genevac therefore recommends the use of appropriately rated type C or D circuit breakers on the main supply Always assume that all power is dissipated as heat Environment The following figures apply Operating Storage Ambient Temperature 0 C to 30 C 10 C to 55 C Relative Humidity 0 95 0 95 Altitude Sea Level to 1 600m Sea Level to 12 000m Emissions Noise levels do not exceed 7OdBA at one metre from the concentrator 04 5057 Issue 1 15 June 2008 Page 17 of 22 miVac Series 10 EC Declaration of Conformity EC Declaration of Conformity miVac Products Manufacturers Name Genevac Ltd Manufacturer s Address Farthing Road Ipswich Suffolk IP1 5AP UK Type of Equipment Laboratory Equipment This is to certify that the following miVac products DNA Concentrator models DNA 23050 x00 Duo Concentrator models DBP 23050 x00 DUC 23050 x00 DPP 23050 x00 Quattro Concentrator models QLP 23050 x00 QUC 23050 x00 QHP
17. o display the remaining TOTAL TIME To revert back carry out the same but for TOTAL TIME 04 5057 Issue 1 15 June 2008 Page 9 of 22 miVac Series 5 6 Getting the best from miVac solid aluminium rotors Aluminium rotors are fast because compared to your tubes they re better at collecting heat from the concentrator This heat is then transferred to your tubes so speeding evaporation If you can start a run with the system pre heated it will be faster still Have a look at the graph to see typical differences depending on how the system is used Typical miVac Duo Evaporation Times Water in centrifuge tubes hh mm Duo with a pre Duo starting from wi warmed chamber AND cold warmed c If you really care about getting the fastest speed then try to get into the habit of leaving your empty rotor in the concentrator with the lid shut and pre heat enabled Short runs particularly benefit from this The software has also been modified to optimise the benefits from the new rotors V1 09 on See below DO NOT PRE HEAT WITH YOUR SAMPLES LOADED e Rather than the pre heat function being fixed at 40 C pre heat now heats to your control temperature e You can choose to latch on pre heat by holding down the pre heat button for 5 seconds The system then automatically remains warm between runs You can cancel this as usual with a short press of the pre heat button e The H20 function for Duo and Quattro concentrators has
18. on the SpeedTrap and your Mains Supply Connect existing equipment s Mains Power Cable B to your Mains Supply Switch the SpeedTrap ON 6 4 Collection jar fitting and removing To fit the jar position so that the handle is to the front lift the jar and rotate to the right a quarter turn until resistance is felt The collection jar is removed by rotating the jar to the left a quarter turn refer to Paragraph 6 1 Safety before attempting 6 5 LED indication of condition The blue LED on the front of the SpeedTrap indicates the current condition CONDITION FAST FLASH DEFROSTING SLOW FLASH CHILLING STEADY CONDENSING The system will defrost for 3 minutes every hour this is perfectly normal and requires no user intervention Page 12 of 22 04 5057 Issue 1 15 June 2008 miVac Series DUO QUATTRO PUMP UPPER VENT HOLES SAME BOTH SIDES 7 Introduction The miVac Duo and Quattro pumps offer you the following features Oil free operation Low maintenance Low vacuum DuoPump High Vacuum QuattroPump 7 1 Safety Refer to Page 3 Safety and Maintenance Notes 7 2 Cleaning Exterior surfaces can be cleaned using a lint free cloth e Do not use abrasives Catch Pot is Dishwasher safe Catch Pot is not suitable for an Autoclave 7 3 Setting up If you are using the pump as part of a miVac system refer to Pages 3 to 6 of this manual inclusive If you are u
19. quired Just follow the diagram below gg e le 0 0 A L a O ia B i ii C gt PUMP SPEEDTRAP CONCENTRATOR Connect the interconnecting cable A supplied in Connection Kit between the connector on the Concentrator and the connector on the Pump Do not use the Mains Power Cable supplied with the pump this is supplied for standalone use of the pump only Connect Mains Power Cable B supplied with the SpeedTrap to the connector on the SpeedTrap and your Mains Supply Connect Mains Power Cable C supplied with the Concentrator to the connector on the Concentrator and your Mains Supply NOTE The interconnecting cable is only to be used between the Concentrator and the Pump 04 5057 Issue 1 15 June 2008 Page 5 of 22 miVac Series 3 4 Good procedural practice few general rules for safe operation of a system Ensure only users familiar with all the issues outlined in this document are permitted to operate the equipment e Only load rotors that have been approved by Genevac or your Distributor The System should be loaded and started by the same person Never leave system unevenly loaded with the lid closed Someone may start it Never start or restart a system without checking it is evenly loaded and all swings swing freely Do not place any objects on top of any of the system components during a run Misloading may result in damage to samples and the machine and could void the w
20. repair by untrained personnel 5 Warranty does not cover consumable items Failure to adhere to the above would invalidate the warranty and result in the costs of repairs being charged 14 Contact information See opposite please ensure that you have the serial numbers at hand for the components of your system 15 Disposal and Recycling AN The miVac product should not be discarded in your regular disposal stream Contact your Distributor or Genevac for proper disposal instructions Within the EU it is Genevac s responsibility under the WEEE directive to provide for the recycling of their products 04 5057 Issue 1 15 June 2008 Page 22 of 22
21. s the run The system will shut down when the TOTAL time set has elapsed When this mode is selected the LED is illuminated and the time counts DOWN to indicate the time remaining STOP When pressed this emits a single beep and stops the run The STOP button can be pressed at any time and the system will safely shutdown If the STOP button is pressed again when the system is idle it will cause the system to enter standby Pressing any button will bring the system out of standby SELECT This is a rotary selector and switch unit that is used to set and adjust the various run parameters to suit your needs These are Maximum Temperature Run Type Run Time and Heat Time Page 8 of 22 04 5057 Issue 1 15 June 2008 miVac Series To adjust and set the required parameters rotate the knob to move to the desired position the display changes with appearing at each position in turn To adjust the value press the knob to select it the will flash then turn the knob to increase or decrease the value Once the correct value is attained press the knob to accept it NOTE The selected value will be accepted automatically after 30 seconds if you do not press the knob Repeat the procedure for all parameters 5 1 Setting Chamber Temperature Note Once you press the selector to accept the new value the display reverts back to displaying the current chamber temperature We have used 24 C as the current temperature for all examples TOTAL
22. sing the pump as a Stand Alone miVac unit in conjunction with other equipment please refer to Safety and Maintenance notes on Page 3 of this manual Irrespective of what model miVac pump you have the connections and function are the same When used with the miVac series of concentrators the electrical power is controlled and supplied by the concentrator using the interconnecting lead When used with non miVac concentrators the power lead is connected to your mains power supply Connect the pump to your existing equipment as detailed below If using a Catch Pot ensure that the Catch Pot is fitted to the lower row of opening of the upper vent and empty after every run If you are not using a Catch Pot connect a length of suitable hose from the pump exhaust to a waste container 04 5057 Issue 1 15 June 2008 Page 13 of 22 miVac Series 8 Error messages amp Troubleshooting Errors may be displayed on the LCD display when problems are detected by the internal self check routine see example below a Error codes will not be displayed during a run NOTE If you experience any of the Errors listed below always switch the system power OFF wait 5 seconds and then switch the power back ON and try again If the problem is still apparent contact your Distributor or Genevac Service Er CODE CAUSE OF ERROR RECTIFICATION 03 Lid not locked during run Rotor failed to reach speed 07 Rotor stops unexpectedly Lid fa
23. t notice No part of these instructions may be reproduced in any form or be processed duplicated or distributed by electronic or optical means without the written permission of Genevac Limited All rights reserved Genevac Limited These operating instructions should be read fully before you use the miVac system Keep them near the system for easy reference Your attention is drawn in particular to Safety and Maintenance Notes 04 5057 Issue 1 15 June 2008 Page 1 of 22 miVac Series GENERAL 1 Introduction Drawing on extensive experience in the drug discovery field the miVac Series is designed to provide very high performance coupled with ease of use occupying the minimum of laboratory space Simple to use controls enable the run type run time and temperatures to be set in an instant This manual will guide you through the start up requirements set up needs and operation of the system to facilitate the most efficient procedure to protect your product s integrity and to ensure optimum performance at all times Details The miVac Series is supplied as three modular units that can be combined to suit your needs and requirements examples below CONCENTRATOR SPEEDTRAP PUMP Models available are DNA Concentrator Combined Concentrator and Pump Duo Concentrator Concentrator Quatro Concentrator Concentrator SpeedTrap Condenser Duo Pump Low Vacuum Pump Quatro Pump High Vacuum Pump The simple control panel
24. times Poor vacuum See Vacuum problem SpeedTrap not operating correctly See SpeedTrap Insufficient Chamber heat Adjust Heat time Excessive solvent in pump SpeedTrap not operating correct See SpeedTrap Incorrect run settings Select run settings suitable for your solvent miVac pump runs continuously Connected directly to mains Connect to concentrator using power interconnecting lead Excessive sample odour Solvent vapour exhausting in to Check connections lab Check pump system exhaust ducted to suitable fume extraction point SpeedTrap SYMPTOM CAUSE CORRECTIVE ACTION No mains supply Check SpeedTrap mains power supply lead Excessive boiling of solvent in jar Warm solvent Stop run and empty jar Restart run Check vacuum appropriate to application Incorrect run type Select suitable run type Poor cooling Allow SpeedTrap to cool for 30 minutes with no concentration then Restart run Check LED status Check air flow ensure vents are clear from obstruction Check vacuum appropriate to application Incorrect run type Select suitable run type Poor cooling Allow SpeedTrap to cool for 30 minutes with no concentration then restart run Check LED status Check air flow ensure vents are clear from obstruction No solvent in jar Excessive vacuum Poor recovery rate Excessive vacuum 04 5057 Issue 1 15 June 2008 Page 15 of 22 miVac Series TECHNICAL DATA 9 General Concentrator DNA Max rotor spe
25. unes 9 5 2 SOA RUN et the 9 5 3 Seting Total RUN TIME csiis aa aE AEA Eiaa iR 9 5 4 PUNT CAE i seas E E E E E E 9 do Display mode in AUTO run ses seeesereeeeeneeeeneeeeeeeeeneeeeeeeeeeseeeeenes 9 5 6 Getting the best from miVac solid aluminium rotors ccecccseeecseeeeceeeeeeeeceeeeceeeeaeueesaeeseeeeeseeesaeeeess 10 SPEEDIRAP Semaines ANR EAER aai A a Ea a en ban an annees n manne c ep ON tance 11 6 MOU CUO e a ee E bb 11 DUC QUATTRO PME a a EEE sa cas ae da a sale ti ta in 13 T MOGUCU a E E E E E eo 13 8 Error messages amp Troubleshooting ssssssssssssnnnsnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnn nnnm 14 TECHNICAL 7 4 pen aa Aaaa aaa a a aaa 16 9 EE e E A EA E E EE E N ye E E E E E OEE E EE E ETT 16 ONG TN OV neers secrets E E CD On 2 D ue 16 DOC AD eee os eee anne encor ie te A a den 16 NU AG IAN OUI os sae acceso acts E E E E seasneseaadann aes caeeict aeseanche esate eaceescenat 16 DIMENSIONS D seers saseueacesoas 16 POSE Ol NIM OA a te reece eae a uae ee D a 17 BPA FOUN AS ING ea 17 SO dear EEE 17 10 EC Declaration OF CONTOFMITV 55 EEA AEE mens ane tanem sise AAA aAa 18 11 DS EE LES EY onda seus EE E D DE E RE 19 12 ACC SS OCS ee een es nee ae ne de anse S 19 13 Warranty SAONE anse ete dass ese mn sise ere names ec tns be nue nsc a en De desc tas seeds eue 22 14 COR ACC OA te eee ee eee 22 15 DISDOSAal ANC RECY CMING eninin AR a AEA aa aaia 22 These instructions are subject to change withou
26. up to 250G The following precautions should therefore always be observed 2 3 Safe loading of concentrator Always balance the rotor within 10g for the DNA Duo and Quattro Only use miVac rotors with your system Only load tubes or vials into the rotors that are specified on the rotor Always locate tubes vials correctly in the rotor Only use a maximum of THREE Shallow Well Microplates with Stackers or ONE Deepwell microplate per location on the Duo 2 Position Swing Rotor Only use a maximum of FIVE Shallow Well Microplates with Stackers or TWO Deepwell microplates per location on the Quattro 4 Position Swing Rotor Only fill wells of Microplates to 66 of their maximum fill level Always load opposite swings with the same or similar type of plates Always rotate a swing rotor by hand after loading to check that all plates are correctly located before starting a run and before re starting an interrupted run 04 5057 Issue 1 15 June 2008 Page 3 of 22 miVac Series 2 4 Limitations of use Your concentrator system is unsuitable for use under the following circumstances With strong acids such as HCI TFA and HBr at all concentrations See page 6 for approved list For use as a pressure vessel Rotary vane oil vacuum pumps are not recommended for use with miVac systems because vapours from the system may cause damage to the pump However for users wishing to use their miVac system with rotary
27. vane oil pumps we recommend that the pump is run with the gas ballast set to position 1 to help prevent vapour damage to the pump Oil pumps should then be run for 1 hour after the end of the concentration process with ballast still engaged to ensure that there is no condensed vapour in the pump Ultimately it is the responsibility of the user to check with the pump manufacturer as to how the pump should be operated 3 System Description and Options 3 1 Scope of delivery and installation On delivery it is advisable to unpack your system at the point of receipt to ease the movement of the component parts to the point of use It would be advisable to retain the packaging as Genevac and its Distributors will only accept returns in the original packaging 3 2 Checking the delivery Check the contents of the delivery as soon as possible against the delivery note and notify your Distributor immediately of any missing or damaged parts Refer to our web site for up to date contact details 3 3 Installing the system DNA The DNA Concentrator with its built in Pump can be easily positioned on most benches Fit the Catchpot to the upper vent holes on the Concentrator connect the short tube between the exhaust connector on the pump and the Catchpot Fit the mains power cable that was supplied EXHAUST CONNECTOR UPPER VENT HOLES MAINS POWER DUO QUATTRO CONCENTRATOR SPEEDTRAP and PUMP Below is an example of the Duo Concentrator SpeedTr
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