User guide for RIGAKU powder diffractometer
Contents
1. User guide for RIGAKU powder diffractometer September 2013 by Dr Rie Fredrickson e X ray set 1 Open XG Control window and click SET kV mA to set X ray tube at__kVand mA forthe operation standby setting is 20kV 2mA 3XG o x Fie Edit Instrument Tools Tasks Window Help XG Control XG Control XG State XG TYPE f XG STATUS SealedTube Mo LongFine kv min 20 max 54 step 2 m min 2 max 54 step 2 NOT READY READY GRAY ON ALARM kw max 2 70 POWER l FUNCTION Abort XG Task ON Reset Alarms OFF Alarms Shutters 2 CW Cooling Water R PF Power Failure ae 7 SHUTTER amp CLOSED e HY High Voltage e L Low Voltage N 5 TC Tube Current FC Flament Current aeni a Yos e OL Overload eS LC Line Current Messages k changed to 50 mA changed to 50 2 50 kW k changed to 50 mA changed to 30 1 50 kW k changed to 40 mA changed to 20 0 80 kw k changed to 30 mA changed to 10 0 30 kw k changed to 20 mA changed to 2 0 04 kw k changed to 24 mA changed to 2 0 05 kW k changed to 28 mA changed to 2 0 06 kw SSS oA R e Sample set on the machine 1 Open the RINT RAPID control software and Goniometer control Manual gt Goniometer control Select Phi position as Init 2 Set your sample on the holder Open2. ad range Wide Goniometer Pixel size 4700x2560 Attachment stage Manual x y stage Change Dee ES Sample holder Reflectionismall Change Image file list Omega axis Oscillation Position deg 0 lt gt 40 Speed deg sec 1 Mode H Phi axis Oscillation Position deg 180 0 Speed deg sec 3 i Drive test heasurefExecute Process PID Gonio server 348 XG server 548 Video 0 Xg control 0 Display 0 i 9 12 2013 10 19 AM A 2 Change the folder and file name Go to Project gt data folder and choose your folder Then give the new file name sample and operator name 3 Set exposure time 10 15 min stage sample holder conditions and axis motions See Table 1 RIGAKU user manual UW Madison Geology 2 Table1 Appropriate stage sample holder axis motions and speed for different samples Sample holder fea Omega l 1 degree min O lt omega lt 40 or tubes Phi 3 degree min 180 lt phi lt 0O 3 degree min 180 lt phi lt 0O aaa 35 lt omega lt 60 Omega i surfaces Phi 3 degree min 180 lt phi lt 0 3 degree min 180 lt phi lt 0 e Run test measurement Click the Drive test button to see there is no collision e Press the measure Execute button Now your raw data X ray image file is saved under c raxwish image Group_name your_name img on RIGAKU instrument computer RIGAKU user manual UW Madison Geology 3 e 2DP Pattern Integration softwar
3. e to integrate the X ray pattern 1 Load gt double click the file Fie Edt Tasks Process Options Tools Help Tak ComerinegioPae 3 8 82 2 ita S mam jjcece jo ja JV ece ree ieee e ie Se xj Directory C Vaxvash mage D anvel_Frednckson Fie a Sename FIFI gt C Vaxwash enage D areel_Frednckson Aie R TF 104 1 mg 1D Profile Set 1DConv_BG_Goe_Cr 1DConv_BG_Goe_C12 1DConv_BG_Goe_Al 1DConv_BG_Goe_2we 1D Conv_BG_Gline_Aug22_ph6 eae Ke 4 2 Convert to profile Select the region you want to analyze ain x File Edt Tasks Process Options Tools Help Genera 26 vs intensity C p vsintenity Step 0 0200 Min Max a from e B fra 4563 faze 445 B Smp a BG_Goe_Cr 10Conv_8G_Goe_Cr BG_Goe_Ci2 10Comv_8G_Goe_Ci2 BG_Goe_AI 1DConv_8G_Goe_Al BG_Goe_2wk 10Conv_BG_Goe_2wk BG_Gine_Aug22 ph 10Conv_8G_6line_Aug22_ph RIGAKU user manual UW Madison Geology 3 Click Run Tasic Conven imagetoProfie SS 17 a we 1DConyv_RTFI041 1 CEEE x BG_Goe_Cr 1DConv_BG_Goe_Cr Goe_Cr2 BG_Goe_Cr2 1DConv_BG_Goe_Cr2 Goe_Al BG_Goe_Al 10Conv_BG_Goe_Al Goe_2wk BG_Goe_2wk 1DConv_BG_Goe_2wk BG_Sline_Aug22_ph6 1DConv_BG_6line_Aug22_ph6 For Help press F1 NM 4 Now your integrated data RINT ASCII file is saved under z Group_name your_name asc on RIGAKU instrument computer e Data analysis For the data analysis using JADE program the data you sa
4. the door press the door button before opening machine 3 Mount goniostad on the manual XYZ stage RIGAKU user manual UW Madison Geology e Centering 1 Rotate Phi to 0 2 Select Omega window toggle move and enter a value of _ Center and focus the area for x ray measurement on the cross o section using X Y and Z screws Rotate Omega to __ and adjust the area of interest using only Z screw 3 Rotate Phi to 360 to check your sample is centered properly e Measurement 1 Open the RINT RAPID control software ISSRINT RAPID control software Ioj x File F Project P Manual M Optional measurement S Programs G Adjust 4 Help H L G S OB S Quit Device check Sample set Shutter CCD camera XG control Display Stop Shutter System u o ANTRA PID Project Data folder C raxwishimageiGroup_name Available disk 38 09GB Device status Standard Measurement Omega axis 0 000 eae r X ray conditions Phi axis 360 000 Fil ile name Target Mo m sample X rayMeasureme 50 H w boH ma IP position Read Operator name after Meas hold mini off Eraserlamp Off Memo RINT RAPID l Exposure time Cho 3 min Shutter Close Resolution 100x100 Micrometer Collimator 0 1 fmm IP read conditions Read line 0 2Teata l Auto Conversion C Execute Conversion Don t Execute Conversion Conditions Re
5. ved on z drive is also shared under c Document and Settings All Users Documents data Group_name your_name on the JADE computer e Finishing session 1 Set the X ray standby mode If no one is booked after your measurement is done right away turn down the X ray to the standby setting at __kV and __ mA Keep the X ray ON Turn off the light for specimen illumination and the monitor Record your activities data your name PI s name the number of your sample patterns on the log book RIGAKU user manual UW Madison Geology 5
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