Analytical Circle No.77
Contents
1. siyaku com http www siyaku com 540 8605 1 2 TEL 06 6203 1788 103 0023 42. Analytical Circls Wako Bio Window Wako Organic Square http www wako chem cojp siyaku journal index htm KN B Q amp A
3. A ILSSG2227a20 ci002
4. Rf 3 70FM 250 400nm Rf
5. 1 1 Ssample Nstd mestd Msample Psample XX XX Sstd Wsample msample Mstd x std S V m M HH NMR NMR SI 2 NMR NMR
6. CAS 10mg 51 800 ASB 00011065 010 Atranorin 479 20 9 C H O P 100mg 315 000 5mg 23 800 _ _ oe 10mg 31 800 ASB 00003024 005 Caffeic Acid AHP Verified 31 39 5 C H O 25mg 47 600 100mg 76 200 10mg 31 400 ASB 00003021 010 F Caffeic Acid Phenethyl Ester CAPE 104594 70 9 CH O4 P 25mg 61 900 _ al 5mg 61 900 ASB 00003028 005 Rg Caftaric Acid AHP Verified 6 78 79 58 CHi O 10mg 91 000 mg 18 200 10mg 27 900 ASB 00003198 005 F Carnosic Acid 3650 09 7 CzoHzaO4 5Ome 110 600 1g 826 000 5mg 46 200 ASB 00003199 005 F Carmosol 5957 80 2 C H 0 P 10mg 54 600 50mg 203 000 5mg 9 500 10mg 15 800 ASB 00003450 005 Chlorogenic Acid 327 97 9 CsHi O P 25mg 31 600 50mg 47 300 _ a 100mg 25 100 ASB 00003623 100 Chromium III Picolinate 14639 25 9 CaH N O Cr P 250mg 50 300 Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 17 ANALYTICAL CIRCLE 2015 6 No ZZ i JJ
7. FASTKIT VvVer et 9 Y a Circle E mail analytt wako chem coJp E DKK DKK DKK NPW 400 1 7 5 1L 2w v9 6 3 5L Noc NPW 1 7 5 DKK 145 07665 Ref NPW 1 15w v 6 L
8. 13mm HPLC 50ppb PSF 1 24 GHP PVDF PTFE 25mm 3 9cm lt
9. a M M kikkoman 15 9 1 Methoxy PMIS 1 Methoxy PMS
10. x x O SilTite SilTite SGE GC SilTite 1 5 70 400C Air Water 2 SilTite 5 70 400 Air Water Graphite Vespel ferrule SilTite Finger Tite ferrule Relative Abundances 28 69 0 97 Nitrogen 96 32 69 0 39 Oxygen 9 100 Relative Abundances 28 69 9 08 Nitrogen 96
11. Yamazaki T et al Bunseki Kagaku 63 323 2014 Study of Sample Preparation Method Using Internal Standard F a Solution to Accurate dua le Analysis with H NMR SG 5 No 041 33641 Rf DSS d 500me NMR 1mLx 5A 18 000 085 10161 Rer 500mg L d NMR 1mLx 5A K S Ref 2 10 F 20 80 80C T I T HI T 1 2 1 2
12. CD GTK OQO amp A yhttp www wako chem co jp siyaku pickup chromato index htm 7 ANALYTICAL CIRCLE 2015 6 No ZZ ED AL BHA HPLC GHP HPLC 3 13 25
13. LED IIP65 B 470nm G 525nm R 660nm 4 3 0 01 1 56 5 4 3 1 5mL 1 1 L13 x W23 x H25mm L165x W110 x H65mm 20mm 330g 20C lt 25C 60 000 NGo 384 07331 ABS B470 B 1 60 000 381 07341 ABS G525 G 1 60 000 388 07351 ABS R660 R 1 60 000 NGo 380 03151 WAK CC10 10 600
14. SilTite FingerTite No Description Column ID Ferrule ID 073610 Split Splitless amp FID 0 1 0 2mm 0 4mm 1 33 100 073612 Split Splitless amp MS 0 1 0 25mm 0 4mm 1 34 400 SilTite FingerTite Split a 0 _ 0 No Description Column ID Ferrule ID 073620 GC2010 Split Splitless amp FID 0 1 0 25mm 0 4mm 1 28 300 073621 QP2010 Split Splitless amp MS 0 1 0 25mm 0 4mm 1 31 200 073628 GC17A Split Splitless amp FID 0 1 0 25mm 0 4mm 1 28 300 073629 QP5050 Split Splitless amp MS 0 1 0 25mm 0 4mm 1 31 200 No Description Column ID Ferrule ID 073614 Split Splitless amp FID 0 1 0 25mm 0 4 0 5mm 1 31 700 073615
15. 1 No 024 17031 50 30 000 Ref 1 4 BTMSB d TraceSure 020 17033 50mg Xx 4 75 000 044 31671 _ 6 50mg 30 000 Ref DSS d T Sure 040 31673 RY 50mg x 4 75 000 048 33271 Ref TraceSure 100mg 15 000 135 17951 Ref TraceSure 100mg 15 000 Ref NMR 4 093 06731 1 4 BTMSB d 50mg x 1 DSS d 50mg x 1 NMR 1 55 000 100mg x 1 100mg x 1 NMIJ CRM No 634 29181 NMR HF 3 5 NMIU CRM 4601 a 200mg 18 750 No 045 32061 10096 99 9596 NMR 5g 6 000 048 32051 qd 1009 6 99 959 6 NMR 5g 15 000 136 17121 d 10096 99 959 NMR 5g 16 000 NMR No
16. A C18 C8 NN CN Diol 1 2 3 NH
17. 470nm i 6 19 WH 6 Ee i a a 470nm a 20 No 308 16121 60441 Rer 60 30 000 M M 14 yhttp Wwww siyaku com 2015 6 No Z7Z ANALYTICAL CIRCLE Spark 10M
18. 4 9 TLC TLC 1 3 1 254nm 254nm
19. APLAC MRA G J 22 yhttp www siyaku com 2015 6 No ZZ ANALYTICAL CIRCLE DMSO0 d CIL Cambridge Isotope Laboratories Inc NMR qNMR DMSO d 5mM 15mM 2 NMR Other NMR fill volumes and tubes are available Please inquire a NIST Qoo o DF NAO RD ooop vw EN BRUKER a We Y NIST SRM350 ClL DMSO qd JO NMR 9 DMSO d Figure 1
20. a 1 lt lt Fusion Optics amp Gas Control Module a amp Nano Quant OO o 0 o olol o oO ol oO O O O M M GFP
21. 16 16 2011 2004 R2A R2A MPN 16 No 396 01611 R2A 300g 11 700 393 00381 300g 8 800 395 01681 R2A 300g 11
22. H NMR 1 2 3 4 5 NMR SI NMR qNMR 1 H NMR H NMR
23. Buy5 Get1 Free 2015 2 2 7 31 5 1 PTFE GHP PVDF PSF E mail analyti wako chem co jp 8 yhttp www siyaku com 2015 6 No ZZ ANALYTICAL CIRCLE No mm um 362 00691 E031 3 3 0 45 100 12 000 a 363 06081 E134 13 13 0 2 100 17 000 a A 369 00721 E131
24. EU 405 1 16 R a HE No 555 03861 251185 Ref BD BBL 20 3 800 252292 Ref BD BBL SCD 100 11 000 514 99581 252028 Ref BD BBL LP SCD 100 15 750 BD BBL r SCD 553 01101 252369 90mm RT 120 30 000 BD BBL y SCDLP 550 01111 252370 90mm RT 120 30 000 557 70471 251949 Ref BD BBL 7 SCD 20 4 200 251877 Ref BD BBL 7 SCD 150mm 24 10 080 NH 554 70481 251950 Ref BD BBL y SCDLP 20 4 200 BD BBL
25. 30mL 22 No 553 01101 252369 BD BBL 3 SCD 90mm RT 120 30 000 550 01111 252370 BD BBL 7 3 SCDLP 90mm RT 120 30 000 BD a BD BBL G K yhttp www siyaku com 2015 6 No Z7Z ANALYTICAL CIRCLE R2A E P 7 0 2011
26. 4 5um SunShell 946 um 3 m _ 46 m Sunniest C18 6 9 2 6 m SunShell 06m HPLC gt SunShellC18 5 nm nD 8 MPa S 10mL mn 24000 40C Ne 20 000 SunShellC1 8 2 6 hm 3 2 5 BOD 4 21 MPa 4 6 6 5 9 o 6 7 SunniestC18 5 um 7 HPLC Hitachi LaChrom ELITE Ns 14 000 0 25mm 20 Retention time rnin 1 2 3 4 5 o 6 7
27. HPLC 3 13 HT 25 1 2 3CR 13CR 25CR PTFE 13 25 PTFE HPLC GHP PVDF GHP HPLC PVDF
28. SCDLP SCDLP 80 4 BD 3 2 25 6 BD BBL LL 554 24691 252424 7 3 SCDLP RT 100 25 000 G K Q amp A http www wako chem co jp siy
29. 2 CO SFC 1 Ak KN 2 CO0 3 0mm 3 m SFC 3 o Hesperetin ET oe Chlorbufam flavonoid qc herbieids Chlofenprop methyl herbicide Column CHIRALPAKY IA 3 Column CHIRALPAKY IE 3 Column CHIRALPAKY IF 3 3 0 x 100mmL 3 0 x 100mmL 3 0 x 100mmL Mobile phase CO CH OH 90 10 v Y Mobile phase CO CH OH 65 35 v Y Mobile phase CO CH OH 98 2 v Y Flow rate 1 0mL min Flow rate 1 0mL min Flow rate 1 0mL min Temperature 40C Temper
30. Ethy 2 Chloro 3 2 chloro 5 1 2 cyclohex 1 enedicarboximido phenyllacrylate C H CLNO4 394 25 142891 20 1 97 096 qNMR 2 4 Chloropheny 3 ethy 2 5 dihydro 5 oxopyridazine 4 carboxylic Acid C sH CIN 0 278 69 129025 54 3 97 096 qNMR lt Dially 2 2 dichloroacetamide CaH ClNO 208 09 37764 25 3 98 096 HPLC 3 5 Dichloro 4 hydroxy 2 methoxy 6 methylbenzoic Acid C H CLO 251 06 4101 80 8 2 98 096 cGC S Ethyl Hexahydro 2 oxo 1 azepine 1 carbothioate C H NO S 201 29 24928 89 0 98 096 qNMR lt 1 2 Anilino 6 methylpyrimidine 4 y 2 propano
31. 297 47951 0 10 4 000 NMR HG 4 951 4 965 x 7 NMR 293 47953 100 38 000 295 48351 10 4 400 NMR HG 4 951 4 965 8 NMR 291 48353 2 92 A 100 41 800 295 35161 10 13 000 NMR SHG 4 951 4 965 x 7 NMR 291 35163 2 A ME 100 110 000 Q amp A yhttp www wako chem co jp siyaku pickup chromato index htm 23 ANALYTICAL CIRCLE 2015 6 No ZZ me NMR Wako NMR NMR NMR D gt NMR Delta for qNMR JEOL RESONANCE URL http www resonance com products nmr delta T1
32. 254nm 7nm 70A H 7 6 0 8mL g 230 gt 250 m HG EE 254nm 70F TLC A DD a 1 2 3 op a 95 5 b 90 10 c 85 15 gd 80 20 v v UV254nm 10cm 70F TLC A a 8 2 1 v v v 4 105C 5 10cm Lu 16
33. No Description Column ID Ferrule ID 073630 SilTite FingerTite 0 4mm 0 1 0 25mm 0 4mm 10 8 800 073631 SilTite Fingerlite 0 5mm 0 32mm 0 5mm 10 8 800 073633 SilTite FingerTite Blanking 2 3 500 073636 SilTite FingerTite 5 10 600 P N 073610 P N 073620 Split Splitless amp FID GC2010 Split Splitless amp FID Q amp A yhttp www wako chem co jp siyaku pickup chromato index htm O Y Ak KN ANALYTICAL CIRCLE 2015 6 No ZZ TLC 5 70F TLC 7nm 70A 5 15 gm
34. SC1 SIC Q amp A 57 B G R gae DMSO de NMR BD BBB y 3 SCDLP RT BD BBLTWM y 3 SCD SCDLP BD SparkTW10M NH 0157 DNC ONCE CO COCCO 2 65 10 2 4 0 AEEG 3 70Fzs4TLC 6 HPLC 2 PPPPE DKK RA ANE IRCLE 9 2 a gt SunShell C18 5m
35. 2990 10 13 500 9 500mL 9 7 a 2 251180 Ref BD BBL 20 4 410 405 IL 16 Se gt No RF BD BBL VM 292627 10 12 000 90mD 215177 Ref BD BBL 10 13 000 251172 Ref BD BBL 20 3 150 251270 Ref BD BBL II 100 15 750 a a e TM 215199 Ref BD BBL RVS 10mL 10
36. lt GC SilTite SilTite GC SilTiter FingerTite 10096 SilTite FingerTite 450 C 350 C 450 C GC MS x O O
37. 4 GxF a Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm a ANALYTICAL CIRCLE 2015 6 No ZZ BD BD Eee BD JP USP EP Certificate of 2 Analysis COA WEB gt WEB http www bdj co jp micro support coa pub gt BD Made in Japan BD 1987 i gs
38. 2 No mm 199 17813 10 5cm Xx 10cm 2 900 193 17811 25 20cm x 20cm 16 800 197 17814 NT TP To TE 100 5cm x 20cm 22 500 193 17816 200 5cm x 10cm 25 500 TLC TLC No mm 193 08381 10 5cm x 10cm 2 700 197 08384 NN 100 5cm x 20cm 22 500 199 08383 5 25 20cm x 20cm 17 500 190 08391 9 10 5cm x 10cm 3 000 194 08394 i 1 a 100 5cm x 20cm 24 500 196 083931 Ma 25 20cm x 20cm 19 500 195 12871 70 PF TLC 0 75 10 20cm x 20cm 15 000 NH TLC No mm 146 08631 25 20cm x20cm 39 000 143 08641 i 100 2 5cm x 6 6cm 20 000 149 08621 I CG DOO OP 0 5 10 20cm x20cm 35 000 145 08721 0 75 10 20cm x20cm 58 000 K TN 6 yhttp www siyaku com 2015 6 No 77
39. 98 0 qNMR R 215 25 CAS 81261 84 9 N N CH 2 4 Hydroxyanilino 4 6 dimethylpyrimidine RT i 0 2 CsH aN O HO CHs Ref Trifloxystrobin Metabolite B Standard B 208 20061 100mg 30 000 98 0 qNMR 6 E o Methoxyimino 2 1 3 trifluoromethyl phenyll N ethylidenejaminoloxymethyllbenzeneacetic Acid O O a HsC N OH Ci Hi7FaN 04 394 34 CAS 252913 85 2 KM Wako _ No Ref Buquinolate Standard 021 18761 100mg 45 000 CH 98 09 6 HPLC lt CH3 Ethyl 4 Hydroxy 6 7 bis 2 methylpropoxy
40. 13 547 000 MO Q amp A http www wako chem co jp siyaku pickup chromato index htm 15 ANALYTICAL CIRCLE 2015 6 No ZZ AO0AC PTM NH O157 a NH O157 AOAC PTM AOAC NH 7 1 AOAC 3 2 PTM Performance Tested Methods USDA FSIS ML
41. 25 25 0 2 50 22 000 361 00281 4560T GHP 25 25 0 45 50 22 000 365 01921 4559T GHP 25 GF 25 0 45 50 27 000 369 01321 4450T PVDF 13 13 0 2 100 24 000 365 00201 4455T PVDF 13 13 0 2 100 24 000 PVDF 365 00181 4452T PVDF 13 13 0 45 100 24 000 362 00211 4457T PVDF 13 13 0 45 100 24 000 366 00111 4406T PVDF 25 25 0 2 50 24 000 363 00121 4408T PVDF 25 25 0 45 50 24 000 366 00231 4483T 13 13 0 2 100 25 000 369 01441 4485T 13 13 0 45 100 25 000 360 01971 4583T 25 25 0 2 50 25 000 367 01981 4585T 25 25 0 45 50 25 000 367 01861 4550T 13 13 0 2 100 22 500 367 00261 4551T 13
42. M F TR FRET TR FRET DFusion Optics F M F M F F 30 Gas Control Module 02 CO
43. P NMR MS HPLC GC ChromaDex yhttp www siyaku com U TN 2015 6 No 7Z ANALYTICAL CIRCLE 5 Wako 2 AF FAX E mail FAX Mail 10 3 0
44. V Em ti ig FEh E Fs 6 a met wpe os HE Rh _ ll IN TT a aa LF i G K Q amp A rhttp www wako chem co jp siyaku pickup chromato index htm 13 ANALYTICAL CIRCLE 2015 6 No ZZ B G R NY KYORITSU HEh4IAL HEHK r LED B
45. DKK 500mL 2 500 148 07655 Ref H NPDW DKK 500mL 3 500 f NPW 2w v96 DKK 149 07685 HT NPW 8w v9 DKK 500mL 3 500 208 15811 Ref L TNP 201 DKK 4L 15 500 208 15791 Ref TNP 201 1 DKK 4L 11 000 201 15801 T TNP 201 2 DKK 1L 3 500 205 15821 Rf TNP 201 DKK 6L 9 200 3 KM CE ChromaDeX ChromaDex
46. amp 5 200 1000nm OD Humidity Cassette 38 CO O DNA amp FRET TR FRET BRET 1 2 3 Nco a 2 442 500 TM a I Spark 10M
47. 0 254nm Mel 250 400nm a 2 2 NR a
48. 2 10 SunShell C18 5 m 5096 5 m 3 m SunShell C18 5 m No 383 04861 CB3371 SunShell C18 5 m 150mm x 3 0mmID 84 999 42 000 380 04871 CB3381 SunShell C18 5 m 250mm x 3 0mmID H9 999 55 000 387 04881 CB3471 SunShell C18 5 m 150mm x 4 6mmID 84 999 42 000 384 04891 CB3481 SunShell C18 5 m 250mm Xx 4 6mmID HH49 899 55 000 C18 ODS C18 ODS SunShell 2 6 m O Y 2 yhttp www siyaku com 2015 6 No ZZ ANALYTICAL CIRCLE SFC SFC
49. 13 13 0 45 100 17 000 368 00791 E254 25 25 0 2 50 13 000 360 00751 E251 25 25 0 45 75 18 000 365 00701 E032 3CR 3 0 45 100 15 000 360 06091 E135 13CR 13 0 2 100 23 500 CT 363 00741 E132 13CR 13 0 45 100 23 500 361 00801 E255 25CR 25 0 2 50 25 500 364 00771 E252 25CR 25 0 45 50 25 500 367 00141 4423T PTFE 13 13 0 2 100 35 000 361 01881 4552T PTFE 13 13 0 2 100 35 000 365 01281 4422T PTFE 13 13 0 45 100 35 000 1 368 01891 4553T PTFE 13 13 0 45 100 35 000 360 01091 4225T PTFE 25 25 0 2 50 32 500 369 00081 4219T PTFE 25 25 0 45 50 32 500 366 00091 4226T PTFE 25 25 1 0 50 32 500 361 01901 4554T GHP 13 13 0 2 100 21 000 TG 364 00271 4556T GHP 13 13 0 45 100 21 000 366 01951 4564T GHP
50. NMR 2 NMR Nuclear Magnetic Resonance NMR NMR NMR NMR H C NMR NMR
51. rhttp www wako chem co jp siyaku pickup chromato index htm 19 ANALYTICAL CIRCLE 2015 6 No ZZ lt Wako CAS CAS Ref CAS Ref CAS F 2 K AS Ref AS Ref CAS 20 Ref Cinidon ethyl Standard Ref Clofencet Standard Dichlormid Standard Ref Dichloroisoeverninic Acid Standard Ketomolinate Standard C Ref Mepanipyrim Propanol Standard C Rsf Methazole Standard 98 096 qNMR
52. 1 700 XLD 252020 Ref BD BBL XLD 20 3 150 297882 Ref BD BBL Pseudosel 10 1 690 a i 251173 Ref BD BBL 20 4 620 Ref BD BBL 100mL i 1 Ref wm gt 215191 Ref BD BBL 20 4 000 a nM 0 TM __ a 251180 BD BBL 20 4410 1 1 10 yhttp www siyaku com 2015 6 No Z7Z ANALY
53. 2015 6 no 77 Fingerlite RR 7 70F2s4 TLC 9 70Fzs4TLC 7nm 70A 254nm FV 1 2 3 p 4 p a 95 5 b 90 10 c 85 15 d 80 20 VvV V UV254nm 10cm ANALYTICAL CIRCLE 2015 6 No ZZ SunShell 8 SunShell C1 8 5 um NY SunShell C18 5 ux m ODS 3 u m HPLC SunShel 2 6 m
54. 13 0 45 100 22 500 365 01301 4427T 13 13 0 2 100 22 500 a 362 01291 4426T 13 13 0 45 100 22 500 362 01311 4436T 25 25 0 2 50 23 000 368 00171 4438 25 25 0 45 50 23 000 360 01851 4549T 25 GF 25 0 45 50 27 500 365 05821 AP 4497T PSF 25 HT 25 0 45 50 22 000 PSF gt 367 05761 AP 4189T PSF 25 25 0 8 50 22 000 AP 4001T PSF 25 25 10 50 22 000 368 05791 AP 4225T PSF 25 PTFE 25 0 2 50 26 000 PSF 361 05781 AP 4219T PSF 25 PTFE 25 0 45 50 26 000 AP 4790T PSF 25 GxF PTFE 25 0 2 50 29 000 361 05801 AP 4303T PSF 25 GxF PTFE 25 0 45 50 29 000 AP 4796T PSF 25 PVDF 25 0 2 50 24 000 365 08501 AP 4408T PSF 25 PVDF 25 0 45 50 24 000 AP 4793T PSF 25 GxF PVDF 25 0 2 50 27 000 369 08521 AP 4310T PSF
55. Split Splitless amp MS ISQ 0 1 0 25mm 0 4 0 5mm 1 32 500 073616 Split Splitless amp MS 0 1 0 25mm 0 4 0 5mm 1 32 500 For TRACE 1300 073610 Split Splitless amp FID 0 1 0 25mm 0 4 0 5mm 1 33 100 073612 Split Splitless amp MS 0 1 0 25mm 0 4 0 5mm 1 34 400 No Description Column ID Ferrule ID 073619 Split Splitless amp MS 0 1 0 25mm 0 4mm 1 26 800 073618 Split Splitless amp FID 0 1 0 25mm 0 4mm 1 32 600 No Description Column ID Ferrule ID 073623 Split Splitless amp MS 0 1 0 25mm 0 4mm 1 26 800 073622 Split Splitless amp FID 0 1 0 25mm 0 4mm 1 26 800 SilTite FingerTite 0 4mm 10 2 SilTite FingerTite 1 SilTite FingerTite 0 4mm 10 SilTite FingerTite 1 SilTite FingerTite
56. 1 18 CAS 5mg 40 600 ASB 00003640 005 F Cichoric Acid AHP Verified 6537 80 0 CH P 10mg 74 200 50mg 235 200 25mg 16 700 ASB 00003720 025 Coniferaldehyde 458 36 6 EID P 100mg 41 900 100mg 19 000 ASB 00003881 100 RgP Cresyl Acetate M 122 46 3 C H 0 P 250mg 31 400 1g 47 300 o 5mg 61 900 ASB 00003969 005 Ref Cyclocurcumin 153127 42 5 LO P 10mg 93 500 Dicaffeoylquinic Acid 1 3 5mg 39 100 ASB 00003991 005 Ref AHP Verifieg 30964 13 EL 10mg 54 600 ASB 00004891 250 Dimethylcaffeic Acid 2316 26 9 CHO 250mg 28 600 5mg 18 900 ASB 00005020 005 F Echinacoside AHP Verified 82854 37 3 CMAO P 10mg 26 600 25mg 53 200 10mg 12 600 ASB 00005071 010 Ellagic Acid 476 66 4 CH O P 25mg 18 200 100mg 43 400 5mg 4 900 ASB 00006005 005 kf Ferulic Acid Trans 537 98 4 Ch P 10mg 9 500 100mg 15 800 10mg 9 500 ASB 00007040 010 Gallic Acid 149 91 7 C H O P 100mg 31 600 1g 61 900 5mg 41 900 ASB 00007164 005 F Gingerol 6 23513 14 6 CO P 10mg 60 200 25mg 120 400 5mg 37 900 ASB 00007163 005 F Gingerol 8 77398 92 6 CoH3004 P 10mg 60 200 25mg 120 400 5mg 3
57. 1 TEL 03 3270 8243 TEL 092 622 1005 TEL 082 285 6381 TEL 052 772 0788 TEL 0466 29 0351 TEL 029 858 2278 TEL 022 222 3072 TEL 011 27 1 0285 0120 052 099 0120 052 806 esWako Chemicals USA Inc Wako Chemicals GmbH Europe Office http www wakousa com http www wako chemicals de Head Office Richmond VA Tel 49 2131 311 0 Tel 1 804 714 1920 Boston Sales Office MA Tel 1 617 354 6772 DM E mail analyti wako chem co jp URL http www wako chem co jp 15612 4 o1DN
58. 3 quinolinecarboxylate 9 gt Cz HzNO HsC O 3 CH 361 43 Ne T O OH CH3 CAS 5486 03 3 Ref Orbifloxacin Standard 154 03351 100mg 15 000 CH3 98 096 qNMR a lt HN F Y 1 Cyclopropy 7 3S 5 3 5 dimethylpiperazin 1 yll NN N 5 6 8 trifluoro 4 oxoquinoline 3 carboxylic Acid HC Ci H FaN O 395 38 F COOH CAS 113617 63 3 F O 01 http www wako chem cojp siyaku info env article positivelist_1 htm KM QO amp A yhttp www wako chem co jp siyaku pickup chromato index htm 21 ANALYTICAL CIRCLE 2015 6 No ZZ 65 Wako a NMR
59. 32 69 2 56 Oxygen 9 6 0 10 15 20 25 30 35 40 45 50 55 60 65 70 75 m z 0 10 15 20 25 30 35 50 55 60 65 70 75 m Z 96 Response of Base Fragment 69 m z 96 Response of Base Fragment 69 m z 1 5 2 SilTite 5 MS MS 70 400C 400 MS 4 http www siyaku com 2015 6 No ZZ ANALYTICAL CIRCLE SilTite FingerTite GC GC MS SilTite FingerTite SilTite SilTite FingerTite
60. ANALYTICAL CIRCLE EE Q amp A 57 Wako TLC Thin Layer Chromatography TLC QO TLC Ak KN
61. ID 3 SFC IE 3 SFC IF 3 SFC 3 0 50 3 80S82 81S82 83S82 84S82 85S82 86S82 165 000 3 0 100 3 80S83 81S83 83S83 84S83 85S83 86S83 180 000 3 0 150 3 80S84 81S84 83S84 84S84 85S84 86S84 195 000 2 1 150 3 304 99981 382 01031 380 01071 384 01111 382 01151 384 01231 195 000 80S94 81S94 83S94 84S94 85S94 86S94 301 99991 389 01041 387 01081 381 01121 389 01161 381 01241 80S95 81S95 83S95 84S95 85S95 8es95 OO09 46 150 3 300 99961 388 01011 386 01051 384 01091 388 01131 380 01211 195 000 80S24 81S24 83S24 84S24 85S24 86S24 307 99971 385 01021 383 01061 387 01101 385 01141 38 7 01221 80S25 81S25 83S25 84S25 85S25 86s25 PO00 SFC SFC OY OQO amp A yhttp www wako chem co jp siyaku pickup chromato index htm ANALYTICAL CIRCLE 2015 6 No ZZ lt 9 spTRAIAN SGE SilTite FingerTite _ SilTite FingerTite GC GC MS
62. 00 27 7 31 No 76 54 10 103 0023 4 1 rE A MIE E mail analyti wako chem coJp 4 135
63. 141 Ref NH 20 14 000 EE NH NH 2 No 300 85671 Ref NH O157 25 8 000 307 85681 Ref NH O26 25 8 000 304 85691 Ref NH O111 25 8 000 GeneLine DNA No 386 02391 Ref GeneLine 48 32 000 389 02381 F GeneLine 48 12 000 307 99591 Rer GeneLine 48 32 000 300 99581 F GeneLine 48 16 000 G KN 16 yhttp www siyaku com 2015 6 No 77 ANALYTICAL CIRCLE FAST NEWS 1
64. 25 GxF PVDF 25 0 45 50 27 000 366 08151 AP 4564T PSF 25 GHP 25 0 2 50 24 000 PSF 368 05931 AP 4560T PSF 25 GHP 25 0 45 50 24 000 362 08251 AP 4307T PSF 25 GxF GHP 25 0 2 50 26 000 361 05921 AP 4559T PSF 25 GxF GHP 25 0 45 50 26 000 363 08161 AP 4436T PSF 25 25 0 2 50 23 000 360 08171 AP 4438T PSF 25 25 0 45 50 23 000 AP 4787T PSF 25 GxF 25 0 2 50 25000 367 05901 AP 4549T PSF 25 GxF 25 0 45 50 25 000 362 05951 AP 4585T PSF 25 IC 25 0 45 50 23 000 PSF ER 0 4 AP 4799T PSF 25 GxF IC 25 0 2 50 26 000 366 08271 AP 4425T PSF 25 GxF IC 25 0 45 50 26 000 PSF 63 08281 AP 4523T PSF 25 GxF 25 0 so 22000 3 GF
65. 7 900 ASB 00007162 005 F Gingerol 10 107257 18 1 C2 Hs404 P 10mg 60 200 25mg 120 400 a 100mg 19 000 ASB 00007418 100 Ref Guaiacol 90 05 1 C H O P 18 61 900 5mg 15 800 a 10mg 25 200 ASB 00008330 005 Rgr Honokiol 35354 7 4 6 CHL O P 25mg 47 300 100mg 156 800 100mg 14 300 ASB 00008356 100 Hydroxybenzoic Acid 4 99 96 CH O P 250mg 28 400 ASB 00008728 005 Rg Hydroxytyrosol 10597 60 OO P 5mg 37 800 25mg 19 000 ASB 00009251 025 Isoferulic Acid 537 73 5 CO P 100mg 31 400 ASB 00013461 025 F Methyl Caffeate 3843 74 1 OU P 25mg 28 600 ASB 00013585 100 Rg Methy 4 Hydroxybenzoate 99 76 3 CaH O P 400 ASB 00016306 100 Protocatechuic Acid 99 50 3 C H O P 100mg 25 200 5mg 22 300 ASB 00018370 005 Rg Rosmarinic Acid 20283 92 5 HO P 10mg 27 900 25mg 50 300 10mg 19 000 ASB 00019029 010 Salicin AHP Verified 138 52 3 OO P 25mg 31 600 100mg 61 900 a 50mg 25 200 ASB 00019034 050 Salicylic Acid 69 72 7 C H O P 100mg 31 400 5mg 41 900 ASB 00019211 005 F Shogaol 6 23513 13 5 CRO P 10mg 69 900 25mg 138 600 ASB 00020158 250 Tetrahydrocurcumin 36062 04 1 C HzO P 2 sO0 100mg 25 200 ASB 00022305 100 Vanillin 121 33 5 C H O P 200mg 28 400 1g 47 300 ASB 00022351 250 Veratric Acid 93 07 2 C H O 250mg 27 900 a i 5mg 41 900 ASB 00022390 005 F Verbascoside 61276 1 7 3 C H 0 10mg 54 600 ASB 00025010 005 F Yangonin 500 62 9 CaHO4 P i ChromaDex
66. 700 No 630 26241 14013220 Ref R2A 20 4 000 639 23031 15178720 R2A 200mL x 10 9 800 638 16531 41131 10 x 2 2 400 e gt 634 16533 41132 Rg KBM 10 x 10 10 000 http www nihon pharm cojp d CS i EDITION 16 I oti LT LV I IV
67. 850 MHz H NMR spectrum of benzoic acid in DMSO d Resonances from the aromatic protons of benzoic acid HOD and DMSQ d are assigned The acid proton resonance from benzoic acid 12 13 ppm is not shown Courtesy Joe Ray Baxter Healthcare Corporation Round Lake IL 1 850MHz H NMR NMR No 5 553 24661 DLM 9491A 1 7mm O D Bruker Part No Z106462 50uL 119 000 550 24671 DLM 9491B 5mM Benzoic acid in DMSO d 3mm O D Wilmad Part No 335 PP 9 160 L 119 000 557 24681 DLM 9491C 5mm O D Wilmad Part No 528 PP 8 150uL 119 000 552 24631 DLM 7061A 1 7mm O D Bruker Part No Z106462 50uL 119 000 559 24641 DLM 7061B 15mM Benzoic acid in DMSO d 3mm O D Wilmad Part No 335 PP 9 160uL 119 000 556 24651 DLM 7061C 5mm O D Wilmad Part No 528 PP 8 150uL 119 000 KW NMR FN lt a 2 LL JJ NMJ S HH
68. G 5 08 98 0157 65 33 EcoliO157 E coliO157 gt E coliO157 EcoiiO157 0157 1 2 15 500 700 1 NH No 304 31361 RF NH O157 AOAC 20 10 000 304 34421 Ref NH O26 20 10 000 301 34431 Rf NH O111 20 10 000 382 03971 Ref NH 0103 20 10 000 302 93321 Ref NH VT1 2 20 14 000 300 31581 Ref NH 20 14 000 303 31691 Ref NH 20 10 000 301 83
69. NMR TRM Traceable Reference Material NMIJ NMIJ SI NMIJ SI TraceSure JAJapan ASNITE ASNITE 1
70. TICAL CIRCLE BD BBL LL BD 3 SCDLP RT
71. aku pickup chromato index htm 11 ANALYTICAL CIRCLE 2015 6 No ZZ NY BH 2 12 AW BD BBL 7 3 SCD SCDLP 2BD BD Difco BBL 2 25C 2 25 C 7 3 1 000L 32 5 C 7 4
72. ature 40C Temperature 40C Pressure 150bar Pressure 150bar Pressure 150bar HJ Siduron Meo ww herbicide Tofisopam anxiolytic eR _ Minutes Column CHIRALPAKY IB 3 Column CHIRALPAKY IC 3 30x100mmL Mobile phase CO CH OH 70 30 v Y Additive 196 DEA in CH OH Flow rate 1 0mL min 40C 150bar 30x100mmL Mobile phase CO CH OH 94 6 v Y 1 0mL min 40C 150bar Flow rate Temperature Pressure Temperature Pressure SFC SFC SFC SFC SFC CHIRAL 6 3 m No 2 1 3 2 _ i CHIRALPAK CHIRALPAK CHIRALPAK CHIRALPAKY CHIRAPAKGT CHIRALPAK AN IA 3 SFC IB 3 SFC IC 3 SFC
73. l Ci4H N O 243 30 204571 52 8 98 096 qNMR 2 3 4 Dichloropheny 4 methy 1 2 4 oxadiazolidine 3 5 dione C H ClN O 261 06 20354 26 1 yhttp www siyaku com No 034 24041 100mg 18 000 O N CI CI O CH C oclkcs O 035 24451 100mg 20 000 Cl O C2Hs COOH 042 33791 100mg 15 000 H C CH CH QO N C HC CH CH gt CHCb 048 33771 50mg 30 000 OCH CI COOH HO CH CI 116 01031 100mg 40 000 ol N QO 138 18421 100mg 30 000 5 SE NN OH CHs HsC 131 18411 100mg 45 000 O CI 1 HsC N N CI 2015 6 No ZZ ANALYTICAL CIRCLE No Ref Prosulfuron Standard 160 27291 100mg 23 000 98 0 qNMR OCHs lt N 4 Methoxy 6 methy1 3 5 triazin 2 yUaminoJcarbonyl SO NHCONH 4 NN 2 3 3 3 trifluoropropybenzene Sulfonamide 0 5 CsHi F N O4S CAS 94125 34 5 Ref Pyrimethanil Metabolite B Standard B 166 27391 100mg 30 000
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