化学物質環境実態調査実施の手引き （平成 20 年度版）
Contents
1. 5 3 52. QO ul 3
3. 1 3 9 11 8 9
4. 3 2 o 119 GO MDL MDL
5. 5
6. 10 GPS 60 11 12 JIS Z 8721 18
7. v 54 A D W 2 29
8. 89 N WY o 3
9. 1 EE 1
10. 1 2 4 A B C D
11. 4 24 2 1
12. 10 1 3 2 4 11 GO
13. 2 3 H
14. 34 Ed B A B C 2 13 HV MV 9 2 kk 417 lt A RY 200 X254mm 84mm 200mm
15. cu
16. 3 5 3 5 1
17. 3 1 1 5 ul 3 x y 5 1 20
18. 55 2 3 4 3 4 1
19. 25 3 3 2 3 5 3 POPs 1 000g 10 4 1
20. 3 E 4 E NE 8 MV 1
21. 2 MDL 5 MDL 5 125 A 5 4 5 4 1 pH
22. 2 23
23. OO 3 C OO 1 13 Pa 0 1 mmHg 3 OO
24. 4 4 2 O z ISO IEC Guid
25. 270 1145 115 TEL 04 7182 1107 EAX 04 7182 4342 E mail BMRC yamashina or jp http www yamashina or jp hp ashiwa ashiwa_index html
26. 3 4 2 4 4 6 2
27. f 24 EGO Ls 24 par 2 81 3mm
28. 150 cm RIL UT TD NE Y 10
29. 5 4 E 1 E
30. IDL 5 n 5 n 1 X
31. 3 O E 102
32. 2 pH DO SS LT 67 68
33. LAS
34. 5 4 2 pH 4 4 o 1 VOC pH 5 7 9 ngmL MDL 10 100
35. 47 2 b J i i 50g 4C 2 JIS K 0557 A3 JIS K 8953 5 g 500 mL JISK8576 6g 300 mL JISK 8960 70 g 1L 100 g L JIS K 8356 12g 100mL
36. H 2 HH 2 1 2 2
37. 2 55 GC 68 2 1 2 2 2 2
38. WS bu 3 E 1
39. Cs Crs Xx As Ars b a Cs Crs As Ars a b y 71 E H PC 106
40. 1 2 1 r uk 2 6 11 E
41. 4 4 1 1 400 600 0 5 20 50 2 a 2 b
42. _ 51 58 3 1
43. MDL E 3 3 2 2
44. RRFss RRFss 50 120 Rss Ass Ars XX Qrs RREss X 100 Qss Co Rss Ass Ars Qss Qrs RRFss RRFss Cilrs Ci ss
45. DVD 18 9 1 HV MV HV MV 2 13 2 14 HV MV 2 15 20X25 cm 0 3 nm 99
46. 2 4 13 2 4 2 2 2 2 2 SK
47. 80 kPa 80 6L 24 8 8 mL min 10 2 29 6L 100 pL 25 50 3
48. x y 3 1 3 2 x 3
49. 1 2 7 S 2 2 5 Ns 6 1 1 kk 6 2 lt SESSA lt i lo 6 2 6 1 0 2 7 ROSS 8 1 10 He HH HO ed de a nd a de 11 9 wk EE Ee ee a 11 DE Ni 12 e SR nd te 12 12 12 Re 12 2 12 2 ed 13 9rd RE Ne Nb 13 OE a 14 14 14 2 2 14 000 14 2 15 057975 15 2 Dd RR ee en cd 15 2 3 DD 15 2 16 202 17 SR ki EE 19 3 3 19 21 3
50. 2 500 rpm 10 3 mL 2 500 rpm 10 2 3 100 105 19 1 11 5mL 2 21 TOC 13 3
51. 4 4 1 TDL MDL 4 2 4 2 1 1 8S N 8 5
52. 69 3 1 3 2 5 97
53. es i emi RS 25 2006 2 2 kg 1 1 5 10 12 10 1 100 g 1 4 kg 2 2 1 5 10 10 1 kg 5 ee Ss ep 3 1 5 10 11 200 1000 g 5 10 4 1 5 9 11 11 12 20 50 cm 1 9 2 9 1 9 lt 8 BA a Bay 5
54. 2 1 70 65 N S 10 2 N 5 2 5 N
55. E 5 3 2 O IDL H MDL MDL MDL
56. 20 VOC E 0r S EE on 8 B 27 28 k
57. PTTFE 16 2 3 2
58. 2 3 O 4 2 1 20 2 1 cm m C m
59. 15 2 2 5 1 10 1 5 ED gt 4 EEED 2 1 4 1 h ET EE 2 5
60. 80 2 GC MS GC MS LC MS 32 O 1 lt x
61. MDL MQL MDL MQL MQL 100 mL 1000 mL 5 10g 144 1440 L 0 1 L min 1 L min 24 5 20g
62. 2 MDL 30 n 5 n 1 3 MDL 30 2 MDL 5 1 5 1 10 n 5 n 1 MDL 30
63. 61 5 2 4 1 20 C 5 3 5 3 1 1
64. n 3 1 2 1 2 33 40 5 3 5 3 1 35 40 70 70
65. 1 3 3 GO 1 4 1 4 1 1 4 2 2 B 12
66. 80 1 j ly 5 5 2 4 5 4 7 E
67. OO OO OOC OOC O OO OO 1 1 A4 gt TI 63 6 1
68. 2 3 2 k Ea H j 1
69. IDL 5 5 3 3 IDL 5 IDL 5 IDL 5 HT 77 118 4 ID
70. 5 5 E Qc ba 52 53 54
71. 500 m 3 1 2 2 500 m 8 500 m 2 3 500 m 3 bb 1 ii QPS 2 2 2
72. LV 2 17 HV ON Vv gt 2 16 LV 19 9 2
73. 5 1 0 m3 min 0 05 m3 min E HV MV E MV 0 10 m3 min HV 0 50 0 70 1 0 m3 min 10 24 2 LV LV
74. I A juvenile full grown 2 29 9 2
75. 2 2 Ed E Rr b 2 4 POFs
76. 2 24 5 3 2 20 62 5 4
77. E lt lt i lt 3 E HH Pi 21 3 Cs
78. k k 3 kk RE 1 1 1 2 3 1 3 9 11
79. 122 1 2 3 5 3 5 3 3 1 10 3
80. 5 1 5 1 2 3 4
81. 20 1 MORE 2 OD ed ee tod en ed a 2 1 i 2 3 2 4 3 2 1 1 1 1 2 i 2 a a dn a ed ed en 2 25 ES Ee ee ee NT T2235 ne ee td a ed a dh 10 390 a dd 11 E39 ki ELIE SLR AN 11 320 12 12 1 4 12 KW SRI CS 12 Dd SA CS A ed SRR 12 2 12 2 000 MANSK6e00NNR0e0NAMD0NR2002 Se 13 2 13 14 Dr lt et dt 14 2 ed ot 14 2 2 D nn 14 DD 14 HE ad dn 15 2 2 gt 15 Re eas ot ea lt 15 2 3 15 ph ES A DEI EIR i sR 16 205
82. Ne E ER j
83. Rss Ass Ars X Qrs RRFss X 100 Qss Ress Ass Ars Qss CD Qrs RRFss RRFss H RRFss
84. 3 2 3 ES 20 x 1 250 mL
85. IDL Currie 1997 3 4 1 Currie IDL Currie IDL BE 61 j 5
86. H 29 1 2 E 24
87. 124 5 3 6 MDL MDL MDL 7 1 MDL 5 1 2
88. Cs Css Xx As Ass b a eC Css As Ass b a y
89. Octa Decyl Silyl Ea E j H EF x a
90. 2 2 2 2 1 2 2 28 are sonido 24 24 2 OO OO Sg
91. Kaiser Currie 16 Kaiser 1 TIDL IDL Currie 5 IDL 8 Kaiser Currie Kaiser 1 Currie 5
92. 4 1 k ul Wr re 5 5 1 MDL MQL 5 1 1 MDL MQL MDL MQL
93. 3 1 1 1 2 1 2 2 3 4
94. 9 GC MS 2H 13C E 5 E RRF 103 LC MS yy 9
95. PF 85 3 1 70 120 50 120 1 MDL
96. 3 6 63 MDL MDL 3 3 MDL MDL MDL MDL MDL 83 1 2 gt ge gt
97. VOC 4 1 GC GC MS GC MS
98. MDL MQL gt HI 4 1 1 1 1 1 2 WebKis Plus ll 1 http 7 db out3 nies go jp kis plus
99. 2 2 2 2 2 3 2 2 4 1 1 1
100. 1 1 2 2 1 2 3 O MDL 7 1 IDL 5 MDL MDL QDL IDL 5
101. 101 SRC PhysProp Database http www syrres com what we do databaseforms aspx id 386 ChemBiofinder com http chembiofinderbeta cambridgesoft com Default aspx smiles Onhine SMILES Translator and Structure File Generator http cactus nci nih gov7services translate LogKow Interactive LogKow KowWin Demo http www srcinc com what we do databaseforms aspx 2id 385 NIST Chemistry WebBook http webbook nist gov chemistry EnvMed http db out3 nies go jp emdb 1 3 9
102. on 1 M MDL orm m 10 MQL n 2 n 7 MDL MDL MDL t n 1 0 05 x on 1MX2 MQL 10 x oi mw MDL Method Detection Limit MQL Method Quantification Limit t n 1 0 05 5 n 7 1 On 1 M HH MDL H HH 9432 n 1 t
103. 4 2 1 5 42 1 2 19 2mm ooopm 20 3 000 20 YY vy A H 2 19 9 VOC
104. 8 90 4 2 2 1 1 20 2 5 3 15 25 4 2 3
105. E j PS2 ODS Cs 2 3 2 2 2 12 4 6 mm 20 mm Eh 100 mm 1H 33 j mp 2 12 3 HV MV LV
106. MDL MDL MDL n 7 MDL 3 5 88 3 5 5 1 GC
107. CD Ne 31 _ 100kPa 300 kPa 2 2 LC 2 10 2 11
108. 3 VOC ul 4 IDL n 2
109. 5 3 4 MDL 2 2 E 2 3 2 3 1
110. H 1 E ER 4 Bp 2 4 E 4
111. 1 2 3 1 O 2 2
112. MDL MDL 1 MDL IDL IDL TDL IDL IDL 3 5 S N 5 81 IDL TDL
113. 2 6 2mm 2 SA MT 500 1 000g 2 mm 2 mm Ne a 2 mm 2 6 21
114. 1 2 2 1 2 8 GPS m GPS 4 5 9 0 m
115. V 4 PUF ACF PUF 16 24 ACEF 2 3 16 24
116. 58 POP s 59 H 13C 72 ul I
117. 14 15 21 POPs PUF
118. 2 1 mm 2 25 51 2 O 1 O O 2 QO 1 20 20 0 1 g 2 26 1 mm
119. DVD a k 7 9 _ E i 3 2 1
120. Eh 96 3 4 O O O DO 5 6 _ 7
121. 3 2 RRP J As Ais m Z m z Cis Cs As Ais 50 0 75 2 54 0 295 1 18 50 0 74 2 50 0 296 1 18 50 0 76 2 53 0 300 1 20 100 1 34 2 55 0 525 1 05 100 1 33 2 58 0 516 1 03 100 1 32 2 51 0 526 1 05 300 3 84 2 56 1 500 1 00 300 3 86 2 57 1 502 1 00 300 3 88 2 58 1 504 1 00 600 7 76 2 51 3 092 1 03 600 7 80 2 53 3 083 1 03 600 7 85 2 50 3 140 1 05 1000 13 0 2 52 5 143 1 03 1000 6 5 059 1 01 1000 5 280 1 06 gt 200ng mL Cis 3 1 5 3 3 0 10 20 80 40
122. O 5 X 4 1 4 3 x
123. 18 2 2 1
124. GC MS LC MS 123 2 1 3 3 LC MS LC
125. X 3 4 2 0 ng g dry B B r tr 3 5 84 3 4 X X ng g dry ng g dry ng g dry A 50 2 0 3 0 lt 2 0 B 25 1 3 2 0 1 6 C 30 1 4 2 1 3 2 3 5 X n
126. 0 5 GO LI 69 J H R2 R2 0 990 0 995 56
127. 3 1 3 3 POFs 1 000g 4 1 3 2 3 C C m cm C m 3 3 3 3 1 1
128. R2 5 0 5 R2 R2 0 990 0 995 1 5 x
129. 1 87 3 5 1 2 3 2 3 5 3 1 10
130. 1 Wl be
131. 70 7 4 6 1 3 1 128 MDL MDL 10 1 14 100 90 80 9 0 50 70 0 759 1 0 99 1 5 he 50 2 5 40
132. IDL 3 5 2 5 1 5 1 10 200 kPa 1500 mmHg 5 n 5 n 1 2 5 2 70 120
133. 2 59 4 3 5 4 2 4 2 2 4 3 6 5g 20 mL 40 mL 20 mL 2 1 1 80 mL 60 mL 4 4
134. 7 2 MDL 10 2 7 3 MDL 10 7 2 1710 MDL 10 14 70
135. lt E 1 E
136. 10 2 31 1 20 20 20 80 2 31 2 1 3
137. E B a 73 2H 13C 107
138. 1 10 dwell time Lb 3 3 1 S N 10 DL 5 R2 5
139. 4 MDL MDL 30 n 3 n 1 MDL 64
140. F VY 1 ul 93 10 3
141. 3 Hy E 4 E 5
142. 3 4 3 3 gt 1
143. MDL MQL 2 3 1 1
144. 3 Ds E lt be
145. 20 E lt 1H 57 2 mm 20 cm 10 1 1 25 FE
146. Ais As RRFis 5 15 RRF 10 5 RRF 20 60 RRF RRF 3 74 3 2 3 50 lt 120
147. 5 1 O E A 1 4 PCB SS
148. 10 mmol L JIS K 8920 1 27 g JIS K 8918 5g 50 mL 1L 0 1 mo1 JIS K 8637 26 g JIS K 8625 0 2 g 1L 2 JIS K 8005 130 C 2 0 72 g 0 001 g 200 mL 20 mL 300 mL JIS K 8913 2g 1 5 5mL 5 100 mL
149. Cs As b a Cs As 8 b y 56 70 3 1 2 5
150. Kaiser Currie 16 IDL Currie 5 TIDL Kaiser Currie 1 t Kaiser 1 MURA IDL Currie 5 76 LEE
151. 10gL 1 mL 2 mL 0 1mol1 L ff f a x b 100 x 20 200 x 1 x x 0 003567 x 0 1 mo1 mL 0 003567 0 1 mo1 1 mL 10 mmo1 L 0 1 mo1 L 20 mL 48 200 mL 12 0 1 mo1 L
152. 27 3 4 3 4 1 1 VOC 13 Pa 0 1 mmHg 200 kPa 1500 mmHg 2 7 a el b
153. Tenax GC 300 3 17 300 C 2
154. 6 S
155. ul Cs Crs x As Ars b a Cs Crs As Ars a b y En 57 H PC 71 3 1
156. 7 80 80 2 200 kPa 1500 mmHg Swagelok 2 9 VOC 20 1
157. H ul j Cs Css Xx As Ass b y a os Ass y NE NE oe
158. Kaiser 3 3 opt 95 1 596 S N 10 959 1 596 t n 1 0 05 x oi 1 9432 x on 3 2 2 IDL 1QL 7 7 7 Pd P gt t n 1 0 05 x 2 x 1 9432 x 2X on 2 EN HI NN Sy M Nl dh fr TT su 3 ai F 596 59 6 IDL 3 4 Currie IDL IDL IQL
159. Ml er ra HE o o 2 10 20 10 2 11 20 10
160. 1 2 3 4 JIS K0094 JIS K0101 JIS KO102 3 E 3 4 2 4 5 6 JIS A1204 7 PN 8 2 9 2000
161. 9 50 120 Ai ss RRFss Cilrs Ci ss XAi ss Ai rs Ai rs Ci ss Cis 108 3 2 4 RRF RRF Relative Response Factor 3
162. MDL 30 1 12 70 50 MDL MDL 30 mn 5 n 1 MDL
163. 5 1 40 825C 46 2 80 0 1 6 0 mg 0 001 mg
164. 86 a Bal 7 n 1 5 10 mn 3 MDL 30 bb n 3 1 5
165. 3 1 3 7 4 3 1 1 1 RRE 20 20 5 2 91
166. E 4 5 2 20 80cm 10 3 1 E 2
167. 80 3 3 MDL MQL 81 3 3 1 MDL MQL kkk 81 3 3 2 MDL kk 81 3 3 3 MDL MQL kk 82 3 3 4 MDL 82 3994 MM 2 85 93954 nn 1S kh 85 OA DR ee A OC NN Rt En TE RNN 85 85 87 DSU R00 de ad od dn dn i 87 3902 EE 88 NSE 7 ee de 88 3 5 4 D 9 WW 88 3 5 5 kk 89 4 nD eon a 90 ne 90 111 1 1 9 9 23 90 20 AA 90 4 2 2 91 4 2 3 91 90 a a 91 43 ed nd 91 4 3 2 93 4 3 3 Ci lt 93 3 94 0 005CK AIAMASUADS2S00CReROON0 id 94 0 94 94 A422 Sk NN 95 96 0
168. 10 gL JISK8659 1 g 10 mL 100 mL 1 3 2 22 J A 1L _ B 800mL 1L P 500mL C 300 500 mL D RE 200mL 200 mL LI spe 4 2 23 2 22 13 3 1 um
169. b a 2 O lt 60 4 1 30 2 3 4 5 6 7 8 9 5 E
170. E MDL 6 MDL HH HH 1 a ER 3 MDL HH MDL 117 K B C 5
171. S N lt 5 S N 10 SN 10 5 3 1 3 2 7 os m1 os 1 on1 S N gt 5
172. 20 21 3 H 1 H 18 49 Ea
173. 0 01 g 300 500 mL 45 4 2 2 300 500 mL 20 30 mL 100 g L 20 mL 1 5 5 mL 100 mL 7 30 mL Se 42 48 2 5g 44
174. IDL IQL IDL IQL S N 10 7 17 S N 5 15 S N 15 E S N 10 X 1 8S N 5 112
175. 125 5 4 Li 126 2 Ek kk kf EE lt lt 126 0 M2 Sit Dn a a 126 5 5 kk 127 127 GO Re oe er 127 5 6 ort 129 A 129 4 4 4 1 GC LC MS IDL IQL
176. 3 2 3 IDL 1 GC LC MS 2 0 1 ng mL 5 10 S N lt 5
177. C m s 1L min ST m re 39 4 4 1 pH BOD COD DO gt al MYY O 4 1 1 pH 4 6 4 1 2 pH JIS K0102 2008 4 1 3 BOD
178. MDL MDL MQL MDL MQL 116 MQL 5 1 2 MDL MQL 7 MDL
179. RRE 4 RRE RRF 4 2 y 0 RRF 4 2 RRF RRF RRFis Cis Cs RRFis x As Ais GiGs Ci s k AiGs Ai s
180. lt 2 1 2 1 1
181. Cs As Ais x Cis RREHis Cs ul Cis As Ais RRFis 15 D RRF 10 RRF RRF 20 74 RRF 3 109 3 2
182. 95 5 7 W MDL 5 30 70 120 50 120 6 2 1
183. 5 10 n 5 n 2 h MDL 120 1 MDL 30 n 5 MDL 1
184. n 1 2 MDL 5 10 n 5 n 2 1 E 1 MDL 30
185. n 3 1 200 kPa 1500 mmHg 3 121
186. MDL 30 n 3 2 MDL n 1 5 10 n 3 n 1 2
187. NE 10 a b X10 x W2 W1 1 g 4 2 6 1 1 g DIO 41 G 6 L 5 DB 300mL 4 2 6 1 2
188. 3 2 y 0 RRF 3 2 RRF RRF RRFis Ois Cs x As Ais GiGs Ci s AiGs Ai s S ul Cs As Ais x Cis RRFis Y Ois Cs
189. I 3 1 3 1 1 _ 0 50 cm 0 2 cm
190. 0 1 mg g _ 4 1 2 20 100 105 100 105 C 250 nm 250 pm 250um 45 2 2 21 ee a 0 01 mg 10 mL O 100 105 1 11 5 mL
191. 2000 15 9 2 16 VOC 20 2 17 20 10 18 20 3 19 UNESCO 1962 Report of the Joint Panel on the equation of state of seawater NS 9 114B Pars 4th December 20 Svensson Lars 1992 Identification Guide to European Passerines Sweden 21 1991 135 22 1986 I 78 23 1984 399 24 1997 25 1978a I 65
192. 2 8 18 2 4 pH
193. 90mm 50mm 2 Co 575 2 14 HV MV 18 20 3 35 DA 2 15 9 2
194. MDL 5 bt MDL 5 bt bt MQL bt bt 3 7 4 3 4 1 2 2 2 lt 10 1 10 1
195. y E E MDL Cs As b a KSC EL As 20 5 1 E C a b y 105 X
196. H ul E H
197. 05 OOOO 1 00025 g L 1L d7 05 IDL 0 72 ng mL a 1 IDL C 0 72 ng L oooo MDL 107 ng 2 H18 15 MQL 2 75 ng L GC MS SIM H18 1 8 BL 1 1L BL 1 L 1 3 9ng mL EE 1 PE BL 2 6ng mL 1 1 2 L 1 GC MS SIM GC MS SIM 7 5 O 1 2 3 4 5 6 7 8 5 500 ng mL 0 4ng mL 5 10 25 50 100 250 500 7 O O O O O O O
198. 2 PRD S 1 3 QFF 600 6
199. PUF 1 2L HCB HCH PCB 50L 250 L 1
200. 8 33 38 3 4 3 24 POPs HV MV 1 l 1 000 m3 HV 700 L min x3 MV 100 L min 7 1 C 24 2 i kPa
201. 2 1 20 5 2 Rs 509 gt Rs 1209 lt Rs 3 50 gt Rs 1 120 lt Rs 50 lt Rs 120 0 ERE FE I d bo gt d gt MDLx5 SN bo MDL 1 bo MDLx5 1 bt gt d gt MDLx5 9 bt d bt MQL bt bo
202. 2 7 9 2 2 2 8 28 2 8 BE 8Swagelok
203. 4 1 ng mL 1 00 0 80 0 60 0 40 0 20 0 00 0 0 1 200 As Ars m2 m z As Ars y 0 1588x 0 0011 R 0 9999 2 3 4 5 6 400 600 800 1000 ng mU 200ng mU 4 3 3 2 3 UH E 5 as 72 POP s E 1H
204. 53 5 6 ul fF ff
205. 7 ab ml o nt opn1 oi i 4 DL n IDL pg pg nL IDL t n 1 o xon1x2 o 5 tm 1 a n 1 a 0 05 t 4 3 t on 1 4 A IDL 7 2 2 pg n 7 6 t 6 0 05 1 9432 IDL 1 9432 x 2 2 x 2 8 6pg 114 3 3 4 IDL IDL 3 3 3 IDL 1 IDL pg IDL ng
206. ka 1 IDL IQL IDL IDL IDL S N 10 7 62 17 E S N 5 15 3 S8S N 15 17 S N 10 S N 5 77 S N gt 5
207. 13 Pa 0 1 mmHg 300 kPa 2200 mmHg 13 Pa 0 1 mmHg 7 nm 2 nm
208. 17 JIS Z 8721 18 JIS KO0101 2 19 JIS K0102 20 9 22 3 2 3 2 O 1 10 cm A AH 10 1 3
209. 2 18 15 9 2 5 10 L min 0 5 L min 10 24 3 4 2 3
210. 7 IDL 1QL IQL I IDL 2 95 IDL IQL 10 IDL t n 1 0 IQL 10 X on IDL Instrument Detection Limit IQL Instrument Quantification Limit t n 1 0 05 5 On 1 I 5 t 3 3 3 3 St
211. E E 14 2 4 5 n 7 14 1 2 O O 2 O O 2 O A O A 2 O 1 1 MDL 10
212. S N gt 5 7 IDL 1QL IDL IQL 2 95 IDL 1QL 10 IDL t n 1 0 05 x orx 2 IQL 10 x on 1 1 TIDL Instrument Detection Limit IQL Instrument Quantification Limit t n 1 0 05 5 n 1 Dt n 7 1 9432 on IDL 5 t 4 3 4
213. S N 10 SN 10 5 3 1 3 1 2 7 o o on S N gt 5 7 ob n1 n 1 Ob n 1 On 1 4 DL n IDL pg pgnL 79 Os IDL t n 1 o x oix 2 na 5 t n 1 o nm 1 q 0 05
214. 1 105 C 3 400 2 7
215. 110 mm 47 mm 0 3 nm 99
216. 45 46 2 5 3 mL min 47 1 49 5 4 10 mmo1 L 25 mL 1 1 2mL 10 mmo1 L 1 mL oo 4 4 2 2
217. 1 O 1 O 1 2 2 MDL MDL 30 MDL
218. OOC OO OO 1 100 ul 2 1 24 GC MS 13 Pa 0 1 mmHg E 50 mL
219. 1g mgS g 8 b a x f x 0 1603 x 1 W S mg S g a 10 mmo1 L mL b 10 mmo1 L mL f 10mmo1 L W 4 1 8 0 1603 10 mmo1 L mL mg 25g 0 019 300 500mL 300mL 10mmol L A gt OO lt 1 1 2mL WV 1 5 5mL 5 4C 54 200mL vy 100g L 20mL 2 5 3mL min 10mmol L
220. 8 111 3 3 2 S N 10 os a 596 MM MD 596 1 1 t n 1 0 05 x on i 1 9432 x oni 1 2 959 J ud OLSESE t n 1 0 05 x 2 x 0 1 1 9432 x 2X on 1 OO r 59 596 IDL 4 5 Currie IDL 1 IDL 1IQL 76 17 IDL IQL
221. MQL OMQL MQI MDL WMQL MDLS x MQL MDL ND 2 2 MQL
222. Sr VOC E 3 4 3 4 1 1 F HV 1 T 14 E
223. x Ai ss Ai Ys Ass Ars Ci ss Girs 73 3 1 4 RRF RRF Relative Response Factor 3 RRF RREF RRF
224. 3 3 1 IDL IQL IDL IDL Currie 1997 5 4 5 2 Currie IDL Currie IDL 75
225. 10 amp VOC v H 2 1 1 pH A 2 7 3 pH B 3 C CE 79 20 5 VOC pH7 7 0 5 C
226. 2 26 3 Svensson2 0 0 O 1 O QO g 3 Maximum Wing Length 2 27 0 mm 2 28 9 24 25 cm 12 14 cm 75 90 g 23 29 mm 121 135 mm 28 32 mm 60 70
227. 3 3 1 4 2 Le S 3 2 GC MS El Cl Positive PCI Negative NCI MS LC MS ESI APCI Positive Negative pH
228. GC MS GC MS GC MS LC MS LC MS LC
229. bt d d bt gt MQL d bt lt MQL d bo d bo MQL d bo MQL 2 2 d bo d d bt d bt 3 7 92 4 3 2 4 3 1 2 QO MDL 5 H n 2 HH 10 1 1 10
230. 3 6 3 3 2 MDL 70 120 MDL x 1
231. RONSSSIRSKRSRA2AS20A0RSAD 62 Badr FARA Ne ee ee ee ha mp 63 6 63 CN ER CN Gi 64 2 64 508 64 6 3 1 kk 64 6 3 2 D 65 034 A ed el a Nh 65 7 2 De on om ne dn Codd od ea 65 2 2 20
232. kk 88 3 5 5 20 89 Ds 90 90 2 MNEE AKG 90 0 DD RE RE A 90 4 2 2 91 4 2 3 kk 91 490 63 ee SN 91 de39s Si 91 4 3 2 93 Re EC 2D Dy 7 2 0 lt E 93 94 4 950 dn 94 dd ee ee 94 4 Ds et 8 94 242 lt e a ea 95 OD ET et 96 ns Di RE EE NSPeS2 Ape 96 97 3 3 IDL
233. 3 4 2 10 100 mg 0 001 mg 3 3 o 2EN 20 3 4 4 2 2 lg mg g mg g b W1 3
234. 64 6 3 2 6 4 4 3 Oo 7 E 20 2 2
235. 3 8 MDL MDL MDL 1 2 MDL MQL
236. HV LV HV Lv 2 17 LV 10 2 5 10 2 SN 37 2 18
237. MJ vy 1um 100mL x 5 vy Y vy mgS g 9 2 23 18 3 5 48 49 5 0 1 mo1 L 0 1 mo1 L 50 50 2 2 24 1 5mL
238. 70 1 14 X 100 80 5 127 E
239. 30 30 1 MQL 4 3 5 50 120 4 4 4 4 1 94
240. f 1 O AN EY ff 2 1 3 QO
241. 22 23 5 3 2 2
242. 3 5 MDL MDL MDL 3 5 DL IDL a IDL b gt 3 5 IDL MDL 2 EX LT
243. H JIS Z8721 1994 1998 2008 1999 2001 2000 2001 1993 10 j 11 f 12 30 46 9 30 13 JIS K0312 65 1985 1982 1971 PC B 2005 14
244. POPs HV MV LV QFEF PUF MV 7 100 L min QFF 70 LV 10 L min
245. qd ff ul I 3 LC MS 3 1 2 hi POPs 1 1 IDL MDL MQL
246. 9 30 m 60 m 7 10 2 4 3 500 m 3 50 m D 8 2 2 500 m NII 3 A
247. et a 21 301 2 ER nd Ne 22 3 1 3 22 G2 EC ed NN CG 23 Re Oe 23 2 24 kk 1 E41 24 3 2 3 kk 24 i Gr OE eC IP 24 3 901 1 ee td a a 24 0922 ee he a ed 26 3 3 3 26 ANRC i NG 28 3 5 dd ed 28 3 4 2 38 3 4 3 39 40 2221 7 40 VER0 40 4 12 pH se od 40 4 1 3 BOD 40 4 1 4 C0D LL 40 4 1 5 D0 nn 40 A RS mR S20 40 ee 42 1 RB ed 42 4 2 2 42 412 3 0 43 4 2 4 44 452 5 3 44 4 2 6 i 47 de Oe A a NN NO Ns 51 4 3 1 ian 51 4 3 2 9 53 4 9 0 EI Ls nd 55 1 OE OO TO OO ET 56 4 3 5 60 4 3 6 0 60 OR OE N ae 60 NH Ee 60 ES 61 br OE en od a 61 5 62 0703 62 5 3 1 62 5 3 2
248. 3 C 71 09 N 10 86 4 C 52 17 Ni 20 28 5 C 41 6 N 8 1 89 44 6 7 8 99 999 9 99 999 10 99 999 3 1 2 3 4 5 6 7 8 0 001 mg 9 10
249. 4 6 3 6 3 1 5
250. 69 3 s SE 1S4 ki 69 0080 2002000S8 70 NAO UN OE We ee 71 72 3 1 4 RRF 74 3 1 5 75 3 2 IDL QLD Li 76 3 2 1 IDL IQL 76 3 2 2 IDL IQL 0 7 7 3 2 3 IDL kk 79 3 2 4 IDL 80 3 3 MDL MQL 81 3 3 1 MDL MQL kk 81 3 3 2 MDL 81 3 3 3 MDL MQL 82 3 3 4 MDL kk 82 3 4 85 84 0 ne EE 85 92402 1 5 DO de 85 93959 7 2 De 87 tN a ee he 87 3 542 de 88 5 2 88 3 5 4
251. d 3 2 40 0 001 g 100 a b a a g b g 100 a b b 4 2 3 1 1 600 25 2 600 25 2 40 0 001 g 2 1 4 2 2 2 2 5g 0 001 g E 2 600 C 25 2 g 3 0 001 100 b c b b g
252. m s 24 1 Ea H j E k 6 SA 8 mu kPa
253. ao 0 0080 al 0 1692 5 a2 25 3851 as 14 0941 Zai 35 0000 i 0 a4 7 0261 as 2 7081 C 1 KC1 Rt S ao ai Rt12 as Rt as Rta2 a4 Rt2 as Rt52 AS t 15 bo bi Rt12 bs Rt bs Rta2 b Rt2 bs Rt572 1 k t 15 bo 0 0005 bi 0 0056 5 bs 0 0066 bs 0 0375 bi 0 0000 1 ba 0 0636 bs 0 0144 k 0 0162 2 JIS K 0102 2008 mgL 8 o 1 80655 Xx Cl o 6 19 1 80655 XCl mg L 1000 8 Cl 34 35 pH 7 9
254. ul 2 1 2 LAS 3
255. 1 2 100 g POPs 1000 g 100 g 100 g 1 2 30 20
256. 20 2 30 56 composite sample 3 1 1 1 1 S 1 10 E 2
257. 5 E E EI Cp gt E 9 17 lt E DVD 17
258. NA AA22 000320 2 252oees 96 7 97 4 ee 101 eT eC 101 1 1 gt 101 is 101 EN eT EI ee 102 2 103 2 1 kk 103 2 2 i 103 ASA 103 2 3 1 103 2 3 2 104 3 i 104 9 i DN eb te a de 104 Gernot 104 9 2 1 302d 105 3 Sk le A ll 106 9 29 CN dn 107 3 2 4 RRF 109 3 5 nn 110 3 3 DL IQL i 111 3 3 1 IDL IQL DO OD 111 3 3 2 IDL 1IQL OO 112 3 3 3 IDL kk 113 3 3 4 IDL 115 3 3 5wIDE i SN EN 116 4 116 5 kN NE 116 5 1 MDL
259. bn SB 50 m 3 1 2 3 a b lt ES 2 1 1 50m D 3 c 500m 2 3 a 2 3 500 m 3 2 3 0
260. 5 10 11 _ 12 11 10 11 1 kg 8k 6 4 1 5 1 2 8 100 500 g 7 20 80 1 5 3 4 4 11 1 p 5 11 9 8 3 kg 1 2 10 9 20 900 g 9 10 50 1 a 10 5 5 6 iD 30 50 1 2 i Sa 11 5 7 25 100 g 500 g 26 2006
261. 3 20 32 33 gt 38 39 33 40 lt gt 4 42 43 7 44 43 45 44 35 47 47 46 45 35 27 SN tn SN 1 2 28 4 3 2 34 35 36 37 NN 3 53 1
262. n 7 MDL se 78 n 2
263. 1 000 g 100 g 1 10 1 1 2 2 3 3 3 1 GQm 2 26 2 2
264. S N 84 84 160 470 930 2300 5700 12000 R2 1 ae OA 00216 1 19 6 00007 0 20 1 2 3 4 5 6 7 8 13ng L 45 ng L 275ng L X MoL Bl 3 9 ng mL S N 50 8 BL 26 ng mL 50 120 45ng L 5 1 2 3 4 5 6 7 8 75 ng L 32ng L 1 0 0 0 0 0 ng L S N 2000 RSD 70 120 50 120 BL gt 0 1 7 6 7 O 1 2 3 4 5 6 7 8 1 ng mL 1ng mL 091 091 106 101 102 101 100 ES nmL
265. 110 5 4 0 075 mm 200 100 a b a a g b 0 075 mm 200 g 5 2 mm 0 075 mm 200 100 b a 0 075 mm 200 0 005mm 0 005 mm 4 2 5 1 1 11 CHN 2 1 JIS K 0557 A3 2 1 11 JIS K 8180
266. IDL ng m3 IDL x Va x 1 1000 x 1 Vg Vg 20 101 8 kPa m3 Va mL 3 IDL pg IDL ng m3 IDL X1000 Vg 80 IDL pg hL IDL ng m3 IDL x Vi x 1000 Vg Vi CD Vg 20 101 3 kPa m3 4 IDL pg IDL ng m3 IDL 1000 x 1 Va Va 20 101 3 kPa m3 IDL pg L IDL ng m3 IDL 20 101 8 kPa 3 3 MDL MQL
267. ng m3 IDL 1000 x 1 Va Va 20 101 3 kPa m3 IDL pg L IDL ng m3 IDL 20 101 8 kPa 3 3 5 IDL IDL dwell time IDL 4
268. 11 12 3 1 3 1 3
269. As Ars ng mL Cs m z R 0 9999 0 1 2 3 4 0 200 400 600 800 y 0 1588x 0 0011 5 6 1000 ng mL 200ng mU 3 2 3 1 3 9 5
270. 2 bh 3 1 3 POPs 40 3 5 LL 12 3 79 8 2 pH 9 DO 9 cm 93 m 2 6 SOO 16 PUF 1 000 L
271. IDL MDL 100 pL GO 3 3 3 MDL MQL MDL 7 on M MDL oxi w 10 MQL MDL t n 1 0 05 x oiMx 2 MQL 10 x onl Mm MDL Method Detction Limit MQL Method Quantification Limit tn 1 0 05 5
272. 2 16 LV LV 3L 24 El DD 32 3 L min 36
273. 3 50m 3 H 3 p D
274. MQL kk 116 5 1 1 MDL MQL 116 5 1 2 MDL MQL 117 532 do dd ee 119 5 Ek Nk k 119 2 SE RS 119 53535 122 92 122 55952 122 5 lt 9209 123 5 3 4 kk 123 Ds8D ZA a 124 5 3 6 MDL 125 5 4 kk 126 5541 SS NG 126 EE EI 126 5 5 RRS lS 127 DD tN DE a nd a a dn 127 5 5 2 kk 127 536 RSS GE GG 129 DN eed DN 129 1 1 SE EE EE Zn SS SEER 1 i 2 sonnet 9 0 Se 4 3 SS AS nb 1 1
275. SJR de he dn 17 2 WDE ed 19 3 RS asepn 19 RN EE NN CN 21 3E 2 21 2 28002 22 3 1 3 NB NR 22 23 92 1 ed NR 23 ed 24 3 2 3 24 OO 24 SS 2 24 10 a ed ed add 26 3 3 3 DD 26 9 SR ed NE 28 5 EPR 28 3 4 2 38 3 4 3 kk 39 4 nh 40 4 BE AP EE NO RE SOAP EE EO ER A 40 lt 40 22K 0 200 ASMLMG0R SE DGG 40 4 1 3 BOD kk 40 4 1 4 C0D AA 40 4 1 5 D0 nn 40 4 16 De 40 A CC CR CE 42 4210 NN NO NIR 42 4 2 2 42 4 2 3 kk 43 4 2 4 44 4 2 5 00 nc 44 4 2 6 nel Dron ee 47 We 2 5 RO TE NN 51 3 0a 51 4 3 2 D 53 4 3 3 kk 55 AI NE CR RE CN 56 4 335 0 SE DD db 60 4 3 6
276. n 1 Ot n 7 1 9432 oni M MDL ou rrx3 MDL MDL 4 5 1 3 MDL 3 3 4 MDL 3 3 2 MDL 70 120 MDL 3 5 MDL 82 MDL
277. 1 10 n 3 1 H n 1 E J 3 MDL 30 n 3 2 2 MDL 30 n 1 MDL 5 MDL 30 200 kPa 1500 mmHg
278. 4 2 GC MS LC MS IDL 10 2 70 1 IDL 10 104 S N 10 DL 5
279. JIS KO0102 2008 4 1 4 COD JIS K0102 2008 4 1 5 DO JIS K0102 2008 4 1 6 1 0 50 o 7 40 8 2 S 42 S ao al Kis12 az Kis as Kis32 a4 Kis2 as Kis52 Kis 15 1 KC1 1kg 32 435 g KC1
280. c g 38 E 600 25 2 40 0 001 g 43 4 2 4 9 3 1 E 2 mm 50 g 110 5 2 E 0 075 mm 200 3
281. pH 126 3 pH B Ax 100 C Ax 100 4 4 1 7 pH GU 7T 5 2 7 2 9 2 5 5 5 5 1
282. 1 2 3 1 ay E E 2 5 E
283. 1 2 1 GPS 9 19
284. 2 3 4 9 molL 2 mL 5 lt 6 2 24 http www gastec co jp reference frame php place c11 htm 4 3 4 3 1 1 Qs 0 1 0 1 g 100 g 1 g 1 20 20 2 25
285. 3 3 1 gt MQL MDL MDL MDL MQL MDL BE TDL MDL E E Ei MDL 3 3 2 MDL E
286. 49 54 POPs
287. 2 6 3H 3 Cl 5 mg 36 UNESCO 962 41 4 2 4 C 2 mm 500 mL 4 2 1 B 37 5 B
288. 3 140 5 143 5 059 5 280 E 9 Als 5 m z RRF 1 18 1 18 1 20 1 05 1 03 1 05 1 00 1 00 1 00 1 03 1 03 1 05 1 03 1 01 1 06 Cs As Ais Px yr y 110 10 20 30 40 50 ng mL 10 400 350 300 250 200 y 4 9393x 49 357 R 0 9996 7 O 10ng mL 30 ng mL 40 50 60 4 4 3 3 IDL IQL
289. 3 2 3 50 120 1000 1000 1000 4 2 As m zZ 0 75 0 74 0 76 1 34 1 33 1 32 3 84 3 86 3 88 7 76 7 80 7 85 13 0 12 8 13 2 2 54 2 50 2 53 2 55 2 58 2 51 2 56 2 57 2 58 2 51 2 53 2 50 2 52 2 53 50 9 5 200ng mL Cis GO 4 4 0 ngmL Cs bll a Cs a b 0 0 295 0 296 0 300 0 525 0 516 0 526 1 500 1 502 1 504 3 092 3 083
290. 50 ng mL 0 10 ng mL gt Cs bly a Cs a b y EE 75 400 10ng mL 20 10 0 10 ng mL 3 3 20 30 40 50 60 3 2 IDL IQL 3 2 1 IDL IQL IDL E
291. mm 74 102g 2 27 2 52 2 46 5 cm 120 cm 37 cm 36 cm 680 g 530 g29 88 5 cm 87 0 cm 400 44 56 mm 340 890 mm 50 61mm 129 155 mm 500 642 g 480 630 g28 gt 9 21 1 t0 22 CY 2 23 3 3 42 24 lt 4 3 25 lt 10 5 14 26 6 15 lt gt 8 73B9 le 271 UI 12 8 17 28 ST lt gt 29 ES 18 30 Ra 14 19 31
292. t 3 3 t on 1 4 IDL 7 2 2 pg n 7 6 t 6 0 05 1 9432 1DL 1 9432 x 2 2x2 8 6 pg 3 2 4 IDL 3 2 3 IDL 1 IDL pg IDL ngm3 IDL x VI Vi 1 Vg IDL pg nL IDL ng m3 IDL x Vl x 1 Vg VIl mL Vi nL Vg 20 101 3 kPa m3 2 IDL pg IDL ng m3 IDL 1000 x 1 Vg IDL pg mL
293. 0 200 kPa 1500 mmHg 6L 24 8 3 mL min 10 UN 3 3L 15L 300 kPa 2200 mmHg 13 Pa 0 1 mmHg 2 50 mL min 20 kPa 150 mmHg 10 300 kPa 2200 mmHg
294. 13 3 4 2 2 1 87 E 105 110 C 2 42 1 105 110 2 105 110 40 0 001 g 2 1 4 2 1 EE 5 g 1 cm 0 001 g 2 105 110
295. 2 26 1996 I 27 1985 26 55 28 1978b 654 29 9 17 7 pl 66 3 3 2 gt EGR 67 GN GO 68 1 1 68 2 68 1 3 DK2S 68 68 VN 0 D5 1 RE oe eR a ee 69 2 2 DD 69 2 3 D 69
296. 3 Student 56 n n 1 t n 1 0 05 5 4 2 1818 6 5 2 0150 7 6 1 9432 8 7 1 8946 9 8 1 8595 10 EE 9 1 8331 2 IDL ng L IDL pg x mL nL 3 3 3 IDL 1 113 GC LC MS 4 2 0 1 ng mL 5 10
297. 5 0 10 30 20 249 4 30 10 40 0 50 4 6 1 5 6 MDL 7 6 129
298. L 5 IDL 5 ED IDL IDL 6 5 2 5 2 1 5 2 2 O x 50 120 a O
299. L S N 11 10 0 22 lt a RSD 58 Rg 5 8 IDL 0 223 ng mL 0 72 0 2233 7 IDL 0 223 ng L 0 72 0 2233 7 7 1 2 3 4 5 6 7 8 ng L 1 1 BL M S N LT sp Ni IMDL 1 07 ng L 1 07 MQL 2 75 ng L 2 75 7 50 120 2 5 ng L BL gt 0 1 3 4 3 1 1 7 5 11 O 170 4 5 1 1 2 5 3 1 1 O 90 4 5 1 1 3 7 3 11 O 200 4 5 ng L 5 3 ne 75 SAN 90 200 3 3 8 98 L A Currie 1997 Detection International update and some emerging di lemmas involving calibration the blank and multiple detection decisions Chemometrics and Intelhgent Laboratory Systems 37 151 181 U S EPA 2003 Guidelines Establishing Test Procedures for the Analysis of Pollutants Procedu
300. NA i Sil1 104 3 i 104 SI DE Ne 104 3 2 Db oe 104 93 2 1 dd 105 3 2352 nm i 106 IIE RN Nk 107 3 2 4 RRF nn 109 9 2 110 3 3 DL IQL i 111 3 3 1 IDL IQL kk 111 3 3 2 IDL IQL kk 112 3 3 3 IDL kk 113 3 3 4 IDL 115 3070 DD OO 116 IA 116 6 SSRN El 116 5 1 MDL MQL kk 116 5 1 1 MDL MQL kk 116 5 1 2 MDL MQL kik 117 119 2 AA 119 D2 2 2 119 8 dd 122 5 122 513 2 dd 122 90 TT TN Ni i 123 5 3 4 kk 123 905 NT LD NR 124 5 3 6 MDL
301. e43 1 JIS Q0043 1 9 z 2 gzg z x X NIQR X NIQR Normalized Interquartile Range NIQR IQR x 0 7418 IQR Inter Quartile Range IQR 3 1 O ISO IEC Guide43 1 z 2 2 lt z lt 3 z 3 66 ISO IEC Guide43 1 JIS QO043 1 Proficiency testing by interlaboratory comparisons Part 1 Development and operation of proficiency testing schemes 1
302. g g dry A lt 2 0 B tr 1 6 1 3 C 3 2 3 4 3 4 1 HCB 10 ng g 20 ng g HCB 28 ng g 90 3 4 2 3 MDL 70 120
303. i 60 RS 60 4 56 SCO02oo0s 60 OSA ee 61 Ba SE A 61 62 EE ee ee ee 62 Dt OA et te Nn Aoi 62 5 3 1 kk 62 5 3 2 kk 62 DS Sa er te 63 ON ee A ed 64 02 64 O00 EM SN de Cn 64 6 3 1 D 64 6 3 D 65 0 SR Rt ed ee NR 65 7 65 3 SRN NR 67 1 68 1 1 kkk 68 2 68 3 38 SE 68 2 68 2 1 kk 69 2 2 69 2 3 ee 69 9 De Oa he SS 4 69 9 kk ks 69 8 11 RR Rk li 70 eh Dy RD gt OE 71 3 a 72 3 1 4 RRF nn 74 GD sh ME DI en ee 75 3 2 DL QLD ee 76 3 2 1 IDL IQL 76 3 2 2 IDL IQL OO kk 77 3 2 3 1IDL kkk 79 3 2 4 IDL
304. m3 IDL x VI Vi Xx1 Vg IDL pg hL IDL ng m3 IDL x VI x 1 Vg VI mL Vi nD Vg 20 101 3 kPa m3 2 IDL pg IDL ng m3 1DL 1000 x 1 Vg IDL pg mL IDL ng m3 IDL x Va x 1 1000 x 1 Vg Veg 20 101 3 kPa m3 Va mL 3 IDL pg IDL ng m3 IDL X1000 Vg IDL pg nL IDL ng m3 IDL x Vi x 1000 Vg Vi pL Vg 20 101 3 kPa m3 4 IDL pg 115 IDL
305. res for Detection and Quantitation Federal Register Vol 68 No 48 pp 11770 11790 Wed Mar 12 2003 Proposed Rules U S EPA 2003 Technical Support Document for the Assessment of Detection and Quantitatnon Concepts Federal Register Vol 68 No 48 pp 11791 11793 Wed Mar 12 2003 Proposed Rules U S EPA 2003 Technical Support Document for the Assessment of Detection and Quantitatnon Approaches EEPA 821 R 03 005 Feb 2003 Engineering and Analysis Division Office of Science and Technology U S Environmental Protection Agency Washington DC 20460 ISO IEC Guide43 1 JIS Q0043 1 Proficiency testing by interlaboratory comparisons Part 1 Development and operation of proficiency testing schemes 1 99 100 4 101 ey 101 1 1 kk 101 2 NN a 101 M02 BN SE hE dd dd de de 102 2 103 2 1 i 103 2 2 103 2 0 ANSU20RN22SSRRSSRRRGSE 2280 8802800828222GRNRE 103 2 3 Sk RE Ns 103 8 2 SEERNN
306. udent t 5 t 05 X On 1 1 X 2 I n 7 n 1 t 1 9482 IDL n n 1 t n 1 0 05 5 4 2 1818 6 5 2 0150 7 6 1 9432 8 7 1 8946 9 8 1 8595 10 9 1 8331 2 IDL DL IDL ng L IDL pg x mL nl 78 TIDL MDL MDL
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