FEB 2003 - PF photon factory
Contents
1. X 3 Uu bur er a 1 PF2. PF PF
3. 3 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 HOM Higher Order Mode X 10 40Amin S30Amin 50mA 60mA 60mA
4. BenchArt Z rich 2001 9 1075 Street Parade Z rich Fest 10 I1 W 2 IN
5. 2 KEK PF AR NW2 PF AR NW2
6. 84 Fig 2 Figure 2
7. 1 PF http www nims so jp xray pf7 FAX 2 28 E mail
8. ve PF Fig 4 References 1 J rg Osterwalder
9. BL 9A XAFS XAFS BL 9A XAFS SSD He X 4 X BL 9A S P K edge XAFS XANES
10. KEK PF Energy Recovery Linac ERL 2 ERL
11. He 3 3 3 BL 9A X Li Ze GRIA mmud E LiICoO LiNiO LiMn O Li Li
12. Fig 9 Network MRO Fe O OH Network
13. 7 4 X a 3 20 al FT gt K Be
14. S2 100um 50um 4 IH BL 7A BL 7A Fig 2 BL 7A BL 7A CK edge 290eV C 1s xx BL 7A Clim 2060 KO C 1s
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16. 1 1998 1999 PE BL 7B BL 7B 2 Prof J rg Osterwalder 2000 2001 1 1833 1 2 7 2
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18. http wwwmspf pfcs pf kek jp mishina PFCS entry html PF 3 1 15 HCE PF 15 90
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20. Energy Recovery Linac ERL 1 ERL PF 1 PF 2 3 3 PF
21. PF PF PF Eier st KEK PF KEK PF 2003 1 29 30
22. ERL KEK 285 KEK BL 1A BL 1A i D KEK CERC
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26. nm TERNI 32 Network 6 8 Fe 6 0 OH Network Fe O OH Network Fig 7 6 Fe O OH Network WS Fe 0 28Cu 0 5SCr 0 1SNi 0 49Mn 0 081P 0 51Si in mass Fig 4 FIB Focused Ion Beam TEM Fig 4 a a
27. 2 ERL KEK 5 http pfwww kek jp pf seminar pf_future2
28. 2 9 10 BT LER KEKB 2 2 Positron 020905 021031 m C cc EJ 52 i c O LI CC ce c 9 5 9 14 9 21 9 28 10 6 10 13 10 20 10 27 Date PF PF AR KEKB C KEKB R amp D
29. Fe C C ron steel PPK pig iron CERA 2 1 Fig 1 1 en RR pa BH Figure 1 Variety of steel products Control of their properties for specialized application Revised figure from Ref 26 Targets of research EE Properties Corrosion Electro chemical Reaction High Tee Gas Maistra
30. 1 tf WM Vol 41 2 J R Levine et al J Appl Cryst 22 528 1989 3 A Naudon in Modern Aspects of Small angle scattering ed H Brumberger p 181 Kluwer Dordrecht 1995 4 XV Holy U Pietsch and T Baumbach High Resolution X ray Scattering from Thin Films and Multilayers p 121 Springer 1999 5 KEK proceedings 2001 25 52 2002 6 H Okuda S Ochiai K Ito and Y Amemiya Appl Phys Letters 81 2358 2002 7 S K Sinha et al Phys Rev B38 2297 1988 8 M Rauscher et al J Appl Phys 86 6763 1999 9 J Stangl et al Pys Rev B62 7229 2000 10 M Rauscher T Saldit and H Spohn Phys Rev B52 16855 1995 Hiroshi OKUDA T 606 8501 TEL 075 753 5193 FAX 075 753 4841 e mail Okuda ilc Kkyoto u ac D 1988 2002
31. 0 5mm x 2mm emm 20 30 mm Xt 10mm 2 3cm 1cm ICF114
32. BL 7A C 1s gt BL 7A PC98 N88BASIC OS OS Windows LabVIEW OJE BL 7A GUI a 90 m a 20 cyanuric acid cj Ba Ee new BL 7A 10 Q A P E 0 280 290 300 310 320 PhotonEnergy eV Figure 2 C K edge NEXAFS spectra of cyanuric acid on Si The measurement was conducted at new solid and old dotted BL 7A In old BL 7A some ghost peaks are observed near C 1s n transition peak 290eV
33. Fig 2 I UT LCA Life Cycle Assessment 2 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 b Anodic reaction Cathodic reaction Performance SO Corrosion resistance
34. 3 18 19 HIC PF 3 17 PF RR S PF da ex deu QUEM RN d C HH iie PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 ASSI SAT VN CASTA RN Ax D S 9 1 9 24 PF
35. 2002 total performance total performance
36. 29 1 m 8mm ZD CCD 4o b Specular Beamstop Mirror Bent Monochro Ge 111 detector Beam Path Figure 1 Experimental setup for GI SAXS measurements at BL 15A NA G SAXS dz GI SAXS Figure 2 Relationship between GI SAXS reflectivity and diffuse scattering measurements Fig 1b GI SAXS X 2
37. KEK PF 97G311 99G180 2000G282 2002G288 1 H Namba H Daimon Y Idei N Kosugi H Kuroda M Taniguchi S Suga Y Murata K Ueyama and T Miyahara Rev Sci Instrum 60 1909 1989 2 K Amemiya Y Kitajima T Ohta and K Ito J Synchrotron Rad 3 282 1996 3 K Amemiya H Kondoh A Nambu M Iwasaki I Nakai T Yokoyama and T Ohta Jpn J Appl Phys 40 L718 2001 4 23 345 2002 5 K Amemiya H Kondoh T Yokoyama and T Ohta J Electro Spectrosc Relat Phenom 124 151 2002 6 http pfwww kek jp users_info users_guide_e stations_spe c_e bl7a pdf 7 A Fujimori T Araki H Nakamura E Ito M Hara H Ishii Y Ouchi and K Seki Langmuir 18 1437 2002 8 N Matsuie Y Ouchi H Oji E Ito H Ishii K Seki M Hasegawa and M Zharnikov Jpn J Appl Phys 42 L67 2003 Noritaka MATSUIE T 464 8602
38. 1 1 C PF 30 1970 XPS XAS XES Kotani Toyozawa KT DO W X RXES d fF Example of Analysis Kauno Schoe j TE Gupnarsson and oenhammer CeNa pf sil i A s d UN AN N J j KATERA HRONA TEMER KT
39. PF PF 1C o 3 10 17 10 1 48 41 2A 4 2 4 1 0 0 53 11 2B 19 14 3 2 0 0 104 38 2C 2 2 1 6 3 3 18 17 3A 1 18 11 19 13 10 91 72 3B 11 9 15 8 2 4 90 49 3C 1 1 2 0 2 1 14 7 4A 15 20 18 11 6 1 229 71 4B 13 11 10 4 13 3 118 54 4C 6 7 di di 4 6 169 45 6A 40 37 62 35 33 1 319 218 6B 29 19 38 17 6 4 296 113 6C 4 6 1 3 1 0 64 15 7A 1 3 1 2 6 3 32 16 7C 68 48 57 40 35 1
40. PF AR 2 5GeV PF 6 Adqdvanced Light Source c Alan Jackson International Machine Advisory Committee
41. 2a 2g Aa 4 X 3 Fig 2 GI SAXS
42. Nature 415 937 941 2002 Nature Structural Biology 9 527 531 2002 1 DNA 2 3 X 4 1 2
43. 12 31 10 XeF Si 111 1 15 da PF
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47. BL 5 BL 1SA 3 18 19 PF 2003 9 12 20 2004 1 3 2002 2003 2004 PF AR NE3 10 PE 12H 20 PE AR 14 1
48. PF 14 11 14 13 KEK4 X X 1980 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 X 1990 X X PP Energy Recovery Linac ERL ERL 0 01 nmrad
49. 2 UG PF VUV lt 50 eV BL 7B SX 50 2000 eV BL 7A XAFS XMCD XPD BU av BL 8A BL 11A XAFS XPS XMCD BL 13C XPD BL 16B D WEREVATOCRR T 7326 SX X 1800 5000 eV BL 2A 5321 WEHEV o ET 2726 XPEEM BL 11B XAFS BL 27A m 3 PF 2001 3 PF
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51. PRIMEPOWER400 9 24 000SPECfp2000 6 2 RAD 8 5 5TB 28TB 2003 3 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 4
52. 3 2003 6 18 CIO 6 H20H 2 4 5 4 e vs 1F 10 5 8
53. pH CI Br XAES 0 Imm xl0mm XAFS Type304 Fe 18 Cr 12 Ni 2 Mo 0 1mm 1M LiBr 0 8V vs Ag AgCl a b Ar gas bubbling Ref Elect Counter Elect A Lid iSol WA X 0 1 1 0 mm Lg Figure 10 Schematic illustration of a newly designed electrochemical c
54. Shojiro OCHIAI T 606 8501 TEL 075 753 4834 FAX 075 753 4841 e mail ochiai Q iic kyoto u ac p 1992 1997 2002 BL 7A NEXAFS RCMS NEXAFS measurement using BL 7A Noritaka MATSUIE Yukio OUCHI Kazuhiko SEKP IDepartment of Chemistry Graduate School of Science Nagoya Univ Research Center for Materials Science Nagoya Univ 1 BL 7A PGM VLSG 2000 BL 7A 1999 10 2001 6
55. 2 X Fig 1 BL 9A X He He X X Figure 1 XAFS measurement system for soft X ray region at BL 9A 20mm
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57. 1 Data Acquisitton PF SLS EPICS 8
58. 1 6 1 29 14 11 8 13 30 1 D 2 G S2 G
59. PAC PF web Daresbury SRS web http srs dl ac uk bob cernik station_plan_3 htm PF PF PF PF
60. PF 7 PF Advanced Photon Source Dr G Shenoy GUAE
61. Figure4 Farewell 2001 8 Han Woong Yeom 2 For exmaples I Matsuda H W Yeom T Tanikawa K Tono T Nagao S Hasegawa and T Ohta Phys Rev B 63 125325 2001 I Matsuda T Ohta and H W Yeom Phys Rev B 65 085327 2002 3 http www unizh ch 4 http www physik unizh ch groups grouposterwalder 5 For examples I Matsuda M Hengsberger F Baumberger T Greber H W Yeom and J Osterwalder Phys Rev B submitted H J Neff I Matsuda T Greber and J Osterwalder Phys Rev B 64 235415 2001 6 http www elettra trieste it 7 http ipawww epfl ch Ipme SLS UsersMain htm 8 Experimental Physics and Industrial Control System http www aps anl gov epics
62. 2 5SGeV 6 5GeV PF20 PE PF WG SSRL 2003 4 2 PF PF RRRA ARE 1 9 PF PF 1 PF
63. B NW12 2003G119 18 X NW12 6A 2003G120 Streptomyces griseus C XX NWI2 6A Center for Cellular Switch Seong Eon 2003G121 Structural studies of novel phosphatases and redox proteins Protein Structure KRIBB R 18B yu 2003G122 SMP30 X TH 6A 2003G123 CTP X NWI2 6A 2003G124 Carbazole 1 9a dioxygenase system 6A 18B HA Haloarcula marismortui KatG dis T Ag 2003G125 DES RAAEN WE 6A 18B 2003G126 6A NW12 2003G127 AzoR Azo Reductase HLA NW12 6A 2003G128 EIAETR CONI Pyrococcus horikoshii SAICAR synthase Od nf d NWI2 18B 6A uw TN NW12 18B 2003G129 DszC
64. KEK PF KEK PP KEK PE PF 14 12 20 21 KEK 3 20 30 15 3 14 2002 PE 1082 3 H 00 20
65. 3 0GeV 5 CC QF PF AR KEK B AR KEK B PF 2
66. RO A E B4 B5 B4 2003 1 7 K KEK B Factory PE 1 14 CA
67. Sn 1 PF PAC PF RREH PF 0 PF
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69. FF PF http pfwww kek jp unten titlej html VXESSN 4A rA VA P JN EAS OHxALU ICI ODN IANA E ATRI N NS NAAN 3 EASQUE What happens when iron gets wet Observation of reactions at liquid metal surfaces Masao KIMURA Advanced Technology Research Laboratories Nippon Steel Corporation 1 Photon Factory I
70. d multi pass ERL 2002 3 PF ERL single pass ERL single pass ERL 20 KEK ERL 7m TBA Triple Bend Achromat 35m
71. PF PF 3 6 CO x 12 H PF AR PF AR 9 26 2 GeV 3 0GeV 50mA
72. PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 BL 9A S P K edge XAFS S P K edge XAFS measurements with BL 9A Toshio AKAI Yokohama Laboratory Center for Analytical Chemistry and Science CACS Inc 1 BL 9A XAFS 12 BL 7C BL 12C 3 BL 9A He 2keV RO XAFS XAFS He Zr Df
73. Fresne GI SAXS Si Ge GrI SAXS WAZ a DWBA 3 2 Al Al As Al GI SAXS
74. Fig 4 Fig 4 Al ELU PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003
75. 15A 2003G142 2 15A m i i 2003G143 X 15A X ISARENMZUVAIVERBUKSSBEREXSOO EA E E p 2003G144 fk RZ 10C 2003G145 10C Ni z amp HU db OBS XS P etoi a BHH Aa Ot ERAT 4B1 Y 7 Y 2003P002 MR TTF CLTCNOQ DME DCNQD Li 18C m 2003P003 7518 4B2 gt LH lt lt Tar 2003P005 Re iic THRI S uae 6A 10A 2003S2 001 X 15B2 2003S2 002 3000
76. 8 ERL X X X X
77. sh JT T 305 0801 KIEO lt IAS 1 1 PF TEL 029 864 5196 FAX 029 864 2801 E mail pf news pfiqst kek jp URL http pfwww kek jp publications pfnews 2 PF PF Tb OK PF
78. 4 BL 15A GrI SAXS
79. X Alexei Souvorov X 1 X 0 2 OZ X X
80. en il 2003G107 MAD data collection on recR and shikimate dehydrogenase E 9 ai RS Se Won Suh 18B National Univ 2003G108 ATP CodWX X Pwani tutea 200 HYUN casn Science and Technology Eom 2003G109 Crystal structures of disulfide bond protein DsbE and its mutants and of Shanghai Institute of Zongxiang 6A 18B some novel proteins involved in structural genomics program Organic Chemistry Xia T H HAE ISERE E 2003G110 NY globiformis 6A 18B YR 227 RE E m E 2003G112 KEH sies 00 X RE E ENT 6A 2003G113 DNA X 6A 2003G114 X XR NW12 m T pe a e NEN 6A 18B 2003G115 X EME RR PAS0nor OO DX RB GEARS 2 2003G116 Xenobiotics CumA1A2 X ER 6A NWI2 2003G117 cupim XX WER 18B 6A 2003GI18
81. 20 PF International Machine Advisory Committee International Science Advisory Committee ISAC Advisory Committee MELOS is PF PF PF
82. 5 6 3 SK edge XAFS XANES 3 1 NaSO S K edge XANES a 5 a D B c D 2460 2480 2500 2520 2540 2560 Photon Energy eV b s Intensity arbit unit 2460 2480 2500 2520 2540 2560 Photon Energy eV Figure 2 S K edge XANES spectra of Na SO a measured with Conversion Electron Yield and b measured with Fluorescence Yield Fig 2 a b 1 1 15 S SN 2 a b b D
83. PF 4 1 3 4 BL 2 3 4 13 4 24 BL 18 27 28
84. 1 2 X Cor O 1s XES PF BE2E1 1 3 SPring 8 X Ce CeB
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86. Figure 7 The structure of Ge islands determined by the present measurement Fig 7 7 13nm 3 75nm 6x10 em US tes 7
87. OH d z in situ RM eun d EN lt Cr O CrCl sol 0 5M o Cr OH powder FT i y k 0 05 0 10 0 15 0 20 0 25 0 30 R nm Br Cr CrBr powder Bro LiBr sol 1 0M b 1 5 FT Y k 0 15 020 0 25 030 0 35 0 40 R nm Figure 12 Fourier transforms of XAFS spectra obtained by in situ measurement at a Cr K edge for d z 0 3 0 8 and 1 3 mm and b Br K edge obtained by in situ measurement for d z 0 2 0 5 and 3 5 mm Far iis the interface Cr OHD H O Br H O Liquid E Near the iene Salt iM Eeee Cr OH _ Br Zi Q A Stainless Steel CrBr FeBr NiBr Fe 17Cr 12Ni 2Mo Figure 13 Schematic illustration of change of ion complex structures inside the artificial crevice suggested by thi
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92. 2 M BL 15A Al ex situ 1998
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97. PF uu 15 3 19 OK 11 30 12 00 PF 2 1 PE PF KEK PF 15 1 9 R 15 00 16 00 A 16 PE PF PE 1
98. PF 500 Hj 4000 1 E PF PF PE PF PF ORAR ORBIZSBEO 20 PF 3 18 9 00 9 30 PE 9 45 12 00 _ PF AR 12 00 13 00 13 00 14 15 PF PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 14 15 14 30 14 30 16 30 ER 16 30 18 00 S U
99. CRISY cw FeOOH Fe O OHD Network y FeOOH a FeOOH Network Network MRO 6 12 Fe 2 0Cr Fe 1 6Cu in mass 15 Fe E Fe K edge 2SeV 300eV DZA XX 10 X Y gy r Fig Oo gz 7 gzx Fe 2 0Cr MRO Fe 2 0Cr 2 CR2W dry 31 ACA SR VC K V ii e ES ER U 7c O WS31
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101. 12 27 KEKB 11 11 1 10 2 PF PF AR 8 BPM Beam Position Monitor
102. Nice ZEE 38 ITE Ez AE E 4872 2003s1 00 BL WHERE Sm qm T HX PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 14 2 10 17 10 20 Date TUE WED THU FRI SAT SUN MON TuE WED THU MON TUE THU Tme 9 i1 21 ls Bi j Ri ls n ls Ja 9 Tl2 ls 21 9 lat p e 21 le 2 I jn j 21 9 lat le 21 lo 21 Operation T M lxi USER RUN IMIEI B USER RUN M UR B USER RUN N O 02G177 01G070 02G074 02G180 026205 C2 02G172 01G188 B2 01S2 002 H P Oo o Setup N A o N m 01G013 gt J 02G127 N Oo H 02G137 OO 02G230 C2 Oo 01G324 d 01G217 W 01G379 02G171 y 02P017 01G034 10A 02G269 01G363 10 7 23 02G182 10B 10C Ra hr 11A 11B 11C 11D 12A 12B o yl EN S aH e LET 1 a9 Imi E M A H B 3t g e g amp 02G041 02G174 02G215
103. 2 rr Ir Tr 800Amin Belin AH 9 rr 1200Amin 2003 2 28 3 4 3 PF PF 2 PF 4
104. Fig 5 a b S s SIN Wn ES Diphenylsulfide Di n propyldisulfide Fig 5 a ES ES Fig 5 a MOD 2478eV 2480eV Na SO nCHis SOANa LiSO R SO Li 2482eV LiSO a O S o o deci Ethylenesulfite ES Intensity arbit unit PC ES5 anode PC ES5 cathode
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109. Cr Cr 5 10 mass GR Fe Cr Cr Fig 4 b ZRE Br fE 2 10nm Network D a Inm SRO Short Range b Figure 4 TEM observation of rusts formed on WS after exposure in a rural area for 31 years a a bright field image b scattering patterns at spots a in a XAFS Fourier Transform a u Distance from Fe nm Figure 5 Radial distribution functions obtained by XAFS from top crystalline a FeOOH CR15Y CR2W dry and CR2W wet where they are measured at Fe K edge and symbols such as Fe O show identification of peak Order b 1 10nm MRO Middle Range Order
110. PR 20B Monash 2007 Boomerans20 1 29 1 31 International Advisory Committee 3 GeV 200mA 216m 7 16nmrad 14 11 9 17 350
111. Pt 3 L4 XLD BEKK XMCD E PF Mu OK NFX Longitudinal XMCD Mn L Transverse E XMCD 2 4 XAFS XMCD XPD XMCD XMCD WEBER ON X
112. SAXS f 10C RER Xr E EANAN dz ES yh i 7J i 2003G057 a M 2 M XA 9A 9C 12C ub A sAN JR gt AN A M 2003G058 MIR 3 LHR ORA 15A 9C 2003G060 15A 2003G061 InmP ErP XAFS E 12C SAXS 5 9 1 009G062 iid M ULIS AO SES 2003G063 dd 10C FR W gt SX ES SEE 2003G064 2 Mg Y Nd AAT EM XE 15A XE BS EEA 73 JENE FE E EUR XAFS BAAI 10B 2003G066 Cr Mn XAFS
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115. 65 1267 1996 7 H Sekiyama N Kosugi H Kuroda and T Ohta Bull Chem Soc Jpn 59 575 1986 8 H Ota T Akai H Namita S Yamaguchi and M Nomura Extend abstract no 243 in Proceedings of the 11 International Meeting on Lithum Batteries Monterey California 2002 H Ota T Akai H Namita S Yamaguchi and M Nomura J Power Sources to be published Toshio AKAI T 227 0033 1000 TEL 045 963 3155 FAX 045 963 4261 e mail 1102382 Q cc m kagaku co p 1985 2000 XAFS ET 20 PF PF 20 PF
116. 1 Windows Net server RTC Super Sinet TV PC PC 10 1 23MB IP TV PC PC CCD
117. 16 ee T What Happens When Iron Gets Wet Observation of Reactions at Liquid Metal Surfaces AE ee 24 GL SAXS Experiments of Inorganic Materials at BL 15A BL 7A 48H L 7 NEXAFS ti WU PM RBE ee 29 NEXAFS Measurement Using BL 7A BL 9A S P K edge DXAFS HE e MH eee 32 5 P K edge XAFS Measurements with BL 9A 20 PF EE 37 38 PF 2 et PH 38 PF 3 ee 39 PF WAERED EE ORE t JEE OSRERpSeS ses MM
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148. 2470 2480 2490 2500 2510 Photon Energy eV b Diphenylsulfide Ph S Ph Dimethylsulfide H C S CH Diphenyldisulfide Ph S S Ph Intensity arbit unit Di n propyldisulfide H C S S C H PC ES5 anode PC ES5 cathode 2470 2480 2490 2500 2510 Photon Energy eV Figure 5 S K edge XANES spectra of graphite anode and LiCoO cathode compared with standard sulfur reagent a nC H SO Na Ethylenesulfite ES Na SO Li SO b Na S S sulfur Diphenylsulfide Ph S Ph Dimethylsulfide H C S CH Diphenyldisulfide Ph S S Ph Di n propyldisu Ifide H C S S C H 2482eV 2478eV 2480eV LiSO R SO Li LiSO Fig 5 b S 2472 2473eV C S C C S S C
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159. ERL 200m tentative ERL 5m 6 30m 2 1 single pass ERL K o ERL 1250m 600m 200m PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 17 BERL ERL 2 5 5 0 GeV Circumference 1253m 1 1 Beam Current 100 mA p eeu Normalized Emittance 0 l mmrad Horizontal emittance 10 0 pmrad at 5 0 GeV Vertical emittance 10 0 pmrad at 5 0 GeV Energy Spread _ 5x10 0 1 ps 100 fs RF Frequency I13GHz ACC Gradient 20 MVim Lo
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176. 1 M Tanino and S Suzuki Science of Steel UCHIDA ROKAKUHO Pub Co LTD Tokyo 2001 2 H H Uhlig and R W Revie in Corrosion and Corrosion Control 3rd ed John Wiley amp Sons Inc New York 1984 3 I Matsushima Low Alloy Corrosion Resistant Steel Chijin Shokan 1995 4 H Okada Y Hosoi K Yukawa and N H J Iron Steel Inst Japan TETSU TO HAGANE 55 355 365 1969 5 H Okada Y Hosoi K Yukawa and N H J Iron Steel Inst Japan TETSU TO HAGANED 56 277 284 1970 6 M Kimura T Suzuki G Sigesato M Saito S Suzuki H Kihira K Tanabe and Y Waseda J Japan Inst Metals 66 166 175 2002 7 M Kimura T Suzuki G Shigesato H Kihira and S Suzuki ISIJ International 42 1534 1540 2002 8 M Kimura T Suzuki H Shigesato H Kihira and S Suzuki Surface and Interface Analysis 35 in print 2003 9 Y Udagawa X ray absorption fine structure GAKKAI SHUPPAN CENTER 1995 10 Y Waseda Novel Application of Anomalous X ray Scattering for Structural Characterization of Disordered Materials Springer Verlag Heidelberg 1984 11 R L McGreevy and L Pusztai Mol Simulation 1 359 367 1988 12 M Kimura M Saito S Suzuki T Suzuki and Y Waseda JIM submitted 2002 13 M Yamashita H Sachi H Nagano and T Misawa Tetsu to Hagane ISIJ 83 448 453 1997 I4 H H Uhlig and R W
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204. 9 Walter Baumann BenchArt Z rich 2001 Naptun Verlag Kreuzlingen S witzerland 2001 10 Z rich Fest 4 1 Limmat Jazz Classic Western Techno 2 11 P I Tchaikovsky Swan Lake Op 20 12 J Strauss Die Fledermaus Overture Op 367 13 Walter Moore A LIFE OF ERWIN SCHR DINGER Cambridge Press 1994 14 E Shr dinger Ann Phys 79 361 1926 ibid 79 489 1926 ibid 80 437 ibid 81 109 1926 RE SC Gm 1 UG 35
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215. o E TA without surface treatments SB Eg EE 9 8 8 E E Reaction Time of corrosion o SE D Metal surfaces II Reactions III Nano structures of at Liq Metal interfaces reaction products rusts a Schematic illustration of corrosion and b fundamental phenomena necessary for understanding corrosion Figure 3 anodic reaction OH cathodic reaction 1 Fig 3 2 Fe OH Fig 3 pH
216. unit ES OO 2460 2480 2500 2520 2540 2560 Photon Energy eV Figure 3 S K edge XANES spectra of Li SO measured with Conversion Electron Yield e O e O1 Intensity arbit unit O o 2460 2480 2500 2520 2540 2560 Photon Energy eV Figure 4 S K edge XANES spectra of Na SO measured with Conversion Electron Yield 3 2 He gig 3 LiSO S K edge XANES He He He i Fig 2 a
217. 30 5 E 20 c D 2140 2150 2160 2170 2180 2190 2200 Photon Energy eV Figure 6 P K edge XANES spectra of H PO a measured with Conversion Electron Yield and b measured with Fluorescence Yield Fig 2 1 1 S S N XANES P 5 BL 9A X S K edge P K edge XAFS XANES X PF XAFS
218. 3nm fF q DACO EO d 2 7x SS UISOD A HU 73 Ge X Si q AWHA Fig 5 FRig 6 0 2 GI SAXS 2a q q lt 0 15nm
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220. Bs 2 00S2 02 C3 Li B1 B1 01G244 02G228 02G156 02G145 02G151 01G167 RA Bow 02G288 01G298 02G249 01G120 3 S 3 t B 02G230 C2 01G296 02P010 01G117 01G254 02G066 11 4 23 02G091 02G260 01G034 D 02G166 e Lo UA n TUE WED THU FRI SAT n2 9 n 9 on lo J je H21 21 j fai USER RUN 10 22 10 23 10 24 10 25 10 26 10 27 10 28 10 29 10 30 10 31 11 8 11 9 01G230 02G215 l m 0292 002 02G010 01G242 rH H 02G201 01G015 d z B 0052 02 C3 02S2 003 o Q w e PL VER TEE B2 B2 02G062 02G059 01G347 B8 01G145 02G140 01G163 02G149 ARL AN 01S2 003 02P011 02G233 02G274 01G139 02G230 C2 01G141 02G252 01G217 01G049 PH 11 4 23 X 01G009 gt 01G034 x 02G185 02G033 02G301 01G316 01G078 01G330 TUE WED THU FR
221. CrBr 1M LiBr 0 55M IM Na HDCI 1 08M 2021 2 lt 100 10 3 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 1M LiBr 10M CrBr SM CrCl SM 20 21 FeCl 5 08M FeBr 5 08M 22 C
222. PF AR 0 000000 2 5797 13 5797 NW20 ID IHHnXAFsSHHHHHH BL NE5 PF AR 0 0 0 0 HHHHHHUHHHHHHHHH NW12HID 7t 3846 n BL NE9 HHHHHHHUHHH e IDHHHHHHH gt Hu pm HH N 0200 HHHHH O O PHS 4209 LB UL E 3800 029 864 5778 Ud Ii I BLx x 38x x BL6 3806 HHHHHHHHHHHHHH 029 864 5200 HHHHHHHHHHHHU4XX H 3xxx HHHHHHHHHL C O 10C 1 t Ii HHHHHHH Uu POW C D Ce LU B LU D LU HHHHHHHH uu pul uml Lu LT LL L3 r3 XI Uu B 1 U LI ie ESI LU Bu Und Daum UU HH 13 3874 000006 LL UUU0D01 HHHHHH 113858 000002 000003 LU uuu LL 13 3873 000004 115650 71 5708 12 DUOODO0ODODO COTTI 000000020 RT TE EHE i i E E ROOD LE E ODDO
223. Vladimir G Stankevich 2002 12 3 13 30 14 30 KERR 2002 12 4 16 00 17 00 X BB ER 2002 12 13 H 15 00 16 00 Ultra fast photo induced phase transformation in TTF CA by time resolved X ray diffraction Doctress Marie Helene Lemee Cailleau 2002 12 16 H 14 00 16 00 X 2002 4E 12 19 CR 14 00 15 30 2003 2 H 14 00 15 00 http pfwww kek jp pf seminar PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 15
224. 03G089 AE 7C PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 2x i ES 2000090 XAFS a XAFS TN 10B 9A 2003G091 Bf 1 gt iid cm OH vC 2003G092 XAFS Re RO De TS in situ XAFS 2003G093 0 i E 9A _ E ERE nu 2003GO94 fup d iia Zn HKI TEES 12C 9A xe SERIE OD EE RAE pk h Tg Jak HE ZI FS NIRE A 2003G095 SETUR OAA ERREFU XARA o gg ug DN sc e m 2003G096 9A 2003G097 MgO Ga
225. 1 588 259 8A 0 2 0 0 0 0 20 2 8B 0 0 2 1 1 0 16 4 8C 1 3 2 1 0 0 49 7 9A 0 0 2 9 22 5 46 38 9C 1 1 2 3 7 2 49 16 10A 6 10 6 9 6 2 91 39 10B 74 43 56 45 38 24 856 280 10C 15 25 24 16 17 9 320 106 11A 5 7 9 7 7 4 39 11B 22 11 17 6 5 2 63 11C 1 6 7 4 2 4 24 11D 2 6 7 1 0 5 21 12A 3 2 4 1 1 6 83 17 12C 11 15 30 19 25 9 143 109 13A 0 1 0 0 0 1 2 2 13C 8 3 5 4 3 0 36 23 14A 7 12 7 11 7 1 135 45 14B 7 8 9 10 7 4 78 45 14C 12 14 7 10 7 6 156 56 15A 26 24 28 17 18 11 342 124 15B 2 8 10 6 6 3 98 35 15C 8 13 7 8 14 2 129 52 16A 3 7 a 4 43 26 16B 2 3 4 6 4 6 33 25 17A 4 1 2 2 3 0 19 12 17B 0 0 EE 0 11 0 17C 1 2 3 0 0 0 15 6 18A 9 9 9 3 3 11 82 44 18B 23 18 a 14 195 148 18C 10 12 10 8 13 6 60 59 19A 5 7 4 1 8 7 52 32 19B 9 10 2 6 7 1 48 35 20A 5 4 7 1 1 2 47 20 20B 0 0 0 3 1 27A 8 7 EE 4 82 48 27B 3 5 10 5 6 4 43 33 28A 2 6 i 0 40 18 28B 5 3 4 5 3 1 29 21 NE1A 6 7 7 4 5 0 71 29 NE1B 3 3 0 32 12 NE3 1 4 0 3 0 o0 29 8 NE5A 10 8 0 60 29 NE5C 5 9 1 2 5 1 111 23 495 488 542 226 7077 2616 ib 3A1 3A2 3A3 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 TX UTC Die SR ET HRS es OO Ee E
226. 5A Si Ge 2 2 1 GI SAXS a 2 3 D BL 15A CuK 0 0722 5 0 35 09 FHig la OD CCD QGI SAXS
227. 60 7700 10 972 S HUHHHHHHHHHHHLH zn TEIL 029H851 2255 5 5000 1 1 0 1 0 HHHHHHHH http www yama nami co jp TEIL 0290 851 0003 5 8000 0000 HHHHHHHHLH HH TEIL 0290 852 3939 6 0000 20 Lll D UUUDUUUD TEIL 029 856 Pr 1 HHHHHUHHL TEIL 0290 856 221 ufum HHHHHHHH http www yama nami co jp TEIL 029 851 0008 6 0000 HHHHHHH http www gakuen hotel co jp 130 E 9 TEIL 029 851 3011 6 3500 00000 T HHHHHHUHHL TEL 029 852 5811 5 000 HOODOO 2000000 UU TEL 029 852 8603 4 700 21 000 L 0000 00000 eov rio UU TEIL 029 836 4011 6 825 00000 6 090 0000000 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 KEK 2003 1 28 800m KEK 1 IlHHHHHHHHHHHH T nn HHH Pp TY 9 00 12 00 15 00 19 00 1 2 HHH di 864 0051 Dung Y 7 8 00 11 00 13 30 16 45 Cun n 000000 864 0303 mM AHHHHHMH N 864 0188 UD 190 864 7501 e HHHH 19 00 20 00 UUUUUUUUUD 11 30 14 30 17 30 100r 1 D L1 D D D D 10 00 22 00 kagetsu 877 4717 appo nouo 060200 UM Quam QQ0000 9 00 12 00 15 00 18 00 HHHHHHHHHH HN OO OOD W OEE OE amp O00000000 HHHHHHHHHHHHHHHHH W HHHHHHHHHHHHHHHH Hnnn HHHHHHHHH
228. 8 oo hs z gt 02G230 C2 02G289 02PF17 02G251 02G282 02PF17 02G212 um 02G191 10A RU 01G327 01G080 N x 10B 02G277 01G359 10C H e di u52 E 11A 11B 11C 01G034 11D 12A N N w H 028133 01G332 Kolobov 2 O 5 N ER Data 10 22 10 23 10 24 10 25 10 26 10 27 MON TUE WED THU FRI SAT SUN Time 9 la 9 Ja n j Pi e 2 9 21 Operation M B USER RUN 13A HS 4 3t 02G050 02G072 02G110 B1 13C 01G314 14A 02G042 02G223 C2 C2 As 00S2 003 B2 02G053 02G298 19G Fons D 0182 002 16A G A2 EN G 18A E HH 02G138 01G146 02G321 01G150 19A 01G027 02G175 a n 20A 01G198 01G334 02G264 aTa Ts 01G381 02G334 um we OSR 02G003 28A 28B 10 22 10 25 10 26 10 27 MON WED THU FR SAT SUN 9 21 l9 USER RUN 02G025 Time 9 21 21 9 M Operation NE1A1 NE1A2 NE3A c Ri RJ li x B 01G030 NE5A 02G168 NE5C 02G049 m x FSS NW2A 10 28 MON z 10 28 21 02G067 02G041 02S2 002 01G312 E x 01G244 02G221 02G201
229. 9 TUE WED THU FRI SAT SUN MON TUE WED THU FRI M B 3GeV USER RUN 3GeV B 3GeV USER RUN 3GeV STOP 12 19 12 20 MON TUE WED SUN MON Operation M UR 13A E E A Qo 14C 15A 15B 15C gt 6 sk N N 17C 18A 18B 18C 19A 19B M 0 27B 28A 28B Time Operation NE1A1 NE1A2 NE1B NE3A NE5A NE5C NW2A C1 E p E Timchenko A25 Mohan 00S2 003 B2 02G070 01G022 B1 02S2 003 G A1 01G250 G A2 01G202 Lanblanquie G Ferd n 01G149 i Td 01G149 EOM EOM 02G203 M 01G004 02G105 E e D e e 02G007 mi il WED THU FRI SAT SUN MON USER RUN 02G188 02G188 as 01G240 01G360 02G208 M i Mi NN MEQUE OEE BEBON SESA EM NM LN DRE UNT M B 3GeV USER RUN 3GeV USER RUN 3GeV G B Vanpeteghem 02G076 02G280 aeos C2 C2 C2 Semistnov Semistnov ipalsi B1 G A2 A2 G A2 BENSL orana o O N 02G309 OI BL i Liaw 0 Co E ER Ra 02G334 02G334 ro Mn 197 Zum e op gt gt WW WI DR THU
230. B C 5A B 5C 6A B A B C A B c A B A 7A B 8A 8B 2 1711 MON Time 9 21 Operation M NE1A1 NE1A2 NE1B NE3A NE5A NE5C H NW2A MON TUE WED THU FRI SAT SUN MON Time 9 21 9 21 l9 21 le 21 9 21 9 Operation M B SB USER RUN Single Bunch M M B 01G008 02PF 010 02S2 003 e 02G273 2 H 02G108 01G126 bk 02G253 02G104 01G139 01G321 HH i 01G270 01G311 WG 02G100 01G195 B 11 12 11 13 11 14 E c Bh c n 2 c z B LSB USER RUN Single Bunc 02G103 e J 02G071 zi 02S2 001 02P013 C1 01G031 01G007 Harries G 01G191 n n 01G329 XR mm 11 12 11 17 TUE WED THU FRI SAT 9 21 9 21 j 21 j 21 jo 21 Bl usERRUN 02G025 02G195 01G215 WE c 01G380 01G069 Dn TU WED THU FRI SAT SUN MON M UsERRUN USER RUN 01G058 01G263 02S2 002 02G021 01G048 01G015 00S2 02 C3 02G091 02G343 02G074 B2 01S2 002 01G355 02G312 02G141 02G306 02G316 RF m NW z i T m 01G070 CB2 01G052
231. Colloids Reaction Corrosion resistance Surface layers Color Texture and layer metal interfaces Magnetic properties Environment OFunctional m Eam Y Surface region Layer Bulk grains Mechanical Microstructures Materia phase morphology Strength gt Grain growth ve de X Dislocation and defects SM EDU Strain and st T EN OAffordability Effects of additional elements Workability Weldability Life time design Figure 2 Targets in research of steel 1680 1200 3000
232. E1A1 BH 3 amp co o c bi Wom oH o SW aE NE1A2 028006 NE1B i E 02PF 15 NE3A 3 01G360 NE5A Em NE5C 01G057 NW2A 10 4 10 5 10 6 10 7 10 10 10 11 THU FRI SAT SUN MON M 02G134 02G291 3x Jb 3t is 3 01G054 J Hester 0 02S2 001 C1 01G062 02G070 01S2 00 G A2 N 02S2 003 GCA1 01G021 G 01G023 02G149 01G353 01G162 02G219 zu 2 042 01G020 b 01G201 E 02G157 028334 01G334 REAN 01G180 02G080 02G250 muy 02G191 01G232 10 13 TUE THU USER RUN 02G006 0268136 02G163 02G208 P ne 02S2 002 01G260 01G210 02G179 g 02G206 C2 02G099 02G303 il t8 B ME 02PF16 B1 02PF15 B1 02G202 02G150 02G307 XH PKRKuma 02G207 RN gt t H i z 01G339 01G157 02G317 a a 0152 003 02G235 17 12 00 01G273 Lei 02G230 E C2 02G089 01G309 E 02G199 ml PH Ma 02G182 02G019
233. HHHHHHHLH 17 0023 0 0 Piazza http www tsukuba corri d C Y qu 8642421 HHHHHHHHHHH IC KEK DUBIE En PORREN GU NG ummupDtutleltlc K HH f Q gun 7 CA W000 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 KEK 4 CHR Sv OEE 1 3029 00 17 00 12 28 1 4 gSERGURH DD URL http www lib kek jp riyou index html Q 5000 GS E 1 8 30 17 00 OS 2986 t dS
234. ISSN 0916 0604 PHOTON FACTORY NEWS http pfwww kek jp publications pfnews Vol 20 No 4 FEB 2003 HHHHHHHHHHHHHHIHIL 2 munpnnmnaonm nmnmnmnnnnnnnnn BEHBEEUBE IET ELS e EHI ELTE B BL 7A1 000 NEXAFS 0 B BL 9AI OOOD S P K edge NEXAFS O PFILI HEU D D OS 137 D Cathodic reaction m Performance b 2 Corrosion resistance o Ei Without surface treatments ge IN P E iL TEN 5 2 I O 8 3 Reaction Time of corrosion co o E O D Metal surfaces ID Reactions III Nano structures of at Liq Metal interfaces reaction products rusts c Fe 2Cr 2w Ws G1y ideal x FeOOH ideal t FeOOH R srersresrerresessrseresesseesesseseresrerresessessresrerrosesseserssresrosessererseresroseeseseesererreseoseseeses IE es eeeeeee n Hee emen eene esee sess esses ess esse esses eene nn a 2 PE eee 3 eee e e e memnmememmememeemememe eme eesememe sese nennen 4 eee 6 ID oceeeeeeeeee 33 nennen hehehe enne 7
235. K X JRELBRHAIX LaFeCoPd O X X dq 2p MBE La Sr MnO in situ 2 1 RA X PF
236. R dz 0 2mm R2022nm R2025nm Br Br O Br AR Br Cr 0 2mm Br c MEE I ME OH CrBr 0 55M 10M
237. Revie in Corrosion and Corrosion Control 3rd ed John Wiley amp Sons Inc New York 1984 15 H H Uhlig Z Elektrochem 62 700 1958 16 S Quian R C Newman and R A Cottis J Electrochem Soc 137 435 439 1990 17 M P Ryan N J Laycock R C Newman and H S Isaacs J Electrochem Soc 137 435 439 1990 18 M Kimura M Kaneko and T Suzuki J Synchrotron Rad 8 487 489 2001 19 M Kimura M Kaneko and N Ohta ISIJ International 42 1398 1402 2002 20 H S Isaacs J H Cho M L Rivers and S R Sutton J Electrochem Soc 142 1111 1995 21 H S Isaacs and M Kaneko in Pitting u XAFS Montreal 1997 ECS p 341 22 R C West in CRC Handbook of Chemistry and Physics 70th ed edited by R C West CRC Press Inc Boca Raton FL 1989 p B 103 23 M Kimura J Mater Sci Soc Jpn 38 43 48 2001 24 M Kimura Transactions of the Materials Research Society of Japan 26 775 778 2001 25 M Kimura Materials Science Research International Special Technical Publication 1 394 397 2001 26 21 1999 Masao KIMURA ES ow T 293 8511 20 1 TEL 0439 80 3130 FAX 0439 80 2746 e
238. ar reflectivity of the sample used for GI SAXS measurements PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 3 c 2 C b 1 N 0 Figure 5 GI SAXS pattern with w 0 28 degree Holy 4 ELSE e v Jed C y JE OD 2 41nm 19m 5 6 Fig 5 amp a 0 28 GI SAXS BL 15A 0 15nm Si Ge q q 0
239. eal a FeOOH Figure 7 Evolution of Fe O OH network structure in the process of corrosion Each octahedron is composed of one iron atom at the center and six oxygen atoms surrounding it PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 Fourier Transform a u Distance from Absorbing Atom nm Figure 8 Radial distribution functions obtained by XAFS from top Cr foil WS bulk WSHY WS5Y WS15Y where they are measured at Cr K edge and symbols such as Cr O show identification of peak RDF for the crystalline a FeOOH around Fe K edge is also shown the bottom for comparison 5 13 Fe O OH Cr WS 0 5 5 15 Cr XAFS Fig 8 0 15 0 24 nm Cr O Cr O NN Cr Fe Cr Cr Fe NN Cr O Cr O2 NN Cr Fe NN Cr O 2 NN D cv FeOOH Cr Cr Fe Fe Fe
240. ell conducted for in situ XAFS and XANES measurements B e lt Gg 04 De Concentration CV 04 0A Distance from the interface imm b 10 Concentration LM Q 5 1 1 5 20 2D Distance from the interface imm Figure 11 Ion concentrations inside the artificial crevice of a chromium and b bromine 24 mm lt Fig 100 lt g lt XX Hig 11 d z CrCl
241. mail kimura re nsc co jp 1987 1993 1987 1993 Northwestern Univ Dept Mater Sci amp Eng E 1995 PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 GI SAXS experiments of inorganic materials at BL 15A Hiroshi OKUDA Shojiro OCHIAI International Innovation Center Kyoto University 1 PF
242. ngUnduatr 200m xl _ MiddleUndulator 30m x4 Short Undulator 5 m x12 9 ERL KEK ERL 70 m 100 MeV 200 300 MeV 100 mA kW ERL 10nm 10 H 11 3 PF
243. rClL CrBr CI Br XAFS zy Cr K Br K XAFS Fig 12 CrBr LiBr CrBr Cr OH XAFS Fig 12 Cr g lt 0 3 0 8 1 3mm Cr O Br d z 23 5mm 0 25nm
244. s study 5 Fig 2 2 1985 FAK V Photon Factory c 38V C jf in situ review 23 25 dE 3
245. spice getschtxt 02 4 1 6 5GeV PF AR Photon Factory Advanced Ring 1999 3 X 1 1 3 X X 15 2 28
246. tek pfweis kek jp TEL 029 864 5642 Email masahiko hiraki kek jp James HARRIES H14 11 30 H14 12 31 H15 1 15 1 14 12 9 2 4 5 15s O0 7 15 1 20 Queens University of Belfast Interaction of VUV radiation with light atoms You only live once Cycling guitar squash ex OO OO OO D Hi HE mE PHA 1 1 1 1 1 2
247. unction of the angle of incidence for Al Ag single crystal sample aged at 423K PHOTON FACTORY NEWS Vol 20 No 4 FEB 2003 GI SAXS Fig 8 Al Ag 423K GI SAXS X Al
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