CHIRALPAK IC カラム取扱説明書
Contents
1. 90 10 0 100 pH gt 9 0 pH7 0 25 0 5um HPLC2. gt s 1 0 ml min 30 2 48 e nh 2 90 10 v v 1 0 ml min 60 4 6 mm
3. 1 h 2 90 10 v v A a DEA pH 9 0 pH 2 0 AK 20mM NHHC0 60 40 DEA NHHC0 CH CN Me0H EtOH IPA 2 THF 7C002 037
4. 0 5ml min 2 4 6mm 60 40 v v CHIRALCEL CHIRALPAK CROWNPAK CPI 108 8230 2 18 1 TEL 03 6711 8222 _ FAX 03 6711 8228 530 0001 3 4 5 TEL 06 6342 6161 FAX 06 6342 6168 _4
5. 50 lt 100mM 100mM KPF NaPF CHIRALPAK IC pH 2 0 100mM KPF NaPF THF 2 L 0 5um 60 40 v v
6. 7C002 037 gt CHIRALPAK IC HPLC t MTBE CHIRALPAK IC THF 2
7. 5 40C pH 7 5 25C pH 7 HPLC pH 7 0 25C 4 5 0120 780 104 gt
8. DEA DEA TFA EDA EDA DEA EtNA 2 n BuA 0 1 0 5 0 5
9. A 1 2 MITBE THF 1 402 MTBE2 GHC 2 80 20 80 20 0 98 2 50 50 V V V 99 1 99 1 90 10 0 0 100 0 85 15 8 v v V 50 50 50 50 0 60 40 0 60 40 0 100 n is
10. 7C002 037 OJAICEL The Soflution for Ej Oe CHIRALPAKIC je Cellulose tris QG 5 dichloropheny carbamate a Cl n 2 90 10 v v V i OR b silica sel 5 0 MM 5 8 50 9 10 x 250 mm 20 x 250 mm x 4 30MPa 305 kgf cm 0 40C
11. 20 100 0 V V V 0 100 0 100 0 100 0 100 0 100 2 THF 2 THF UV RI ELSD UV B DEA EDA EtNA 0 1 7C002 037 i EDA EtNA
12. o n MTBE MTBE 2 1 lt 5 lt 20 2 a 1 I 70 30 50 50 70 30 100 0 100 0 vV V V 95 5 80 20 85 15 80
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